GUIDELINES FOR CONCRETE DURABILITY TESTING.PDF
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GUIDELINES FOR CONCRETE DURABILITY TESTING IN
THE U.A.E.
Adil K. Al-Tamimi, Mufid Al-Samarai, Ali Elian, Nigel Harries,
and David Pocock
Synopsis: The construction industry in UAE in particular and theGCC in general, is witnessing a boom in constructing remarkable
infrastructure and buildings. The massive amounts of material be-
ing used have been produced either locally or imported from inter-national resources. However, the extensive use of materials has not
been accompanied by parallel research and development to vali-
date proper techniques, quality control standards and codes of practice. There exist numerous test methods related to concrete
durability, developed internationally and proved to varying extents
in practice. However, confusion exists on how these methods
should be applied, how to interpret the results on projects and whatare the criteria to be used in UAE by the industry, particularly
when using local materials in the harsh environment of the region.
Four international durability testing procedures have been eva-
luated in this study. It has been shown that durability performanceof existing structure is different than the performance of concrete prepared in test samples whether these samples are prepared at site
or at the lab due to the differences between the preparation proce-dure of samples and the actual concrete pouring, compacting and
curing methods in structures.
Keywords: Concrete durability, diffusion, macro-environment,
micro-environment, permeability, diffusion, absorption.
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Adil K. Al-Tamimi: Associate Professor of Civil Engineering at
the American University of Sharjah, UAE.
Mufid Al-Samarai, Professor of Civil Engineering at SharjahUniversity, UAE.
Ali Elian: Head of Engineering Materials Lab Section, Dubai Mu-nicipality, UAE.
Nigel Harries: General Manager, Icon Precast LLC, UAE.
D C Pocock : Market Sector Director , Halcrow.
DURABILITY PRINCIPLES
The durability of concrete structures is closely related to the nature
and severity of the environment in which they are located, as wellas the nature of the concrete construction. This section considers
the environments and associated mechanisms by which the envi-
ronment can penetrate into concrete. The influence of the concrete
itself in permitting or resisting environmental penetration is consi-dered in later sections.
The general environment is termed the “macro-environment”,e.g. coastal, inland.
The specific environments, more than one of which often oc-curs around a single structure, are termed “micro-
environments”, e.g. tidal zone, splash zone.
Both macro- and micro- environments may be natural, i.e. re-lated to geography and geometry, or may be man-made, whereoperational processes lead to exposure, e.g. in industrial plants
or watering for plant irrigation.
The macro- and micro- environments, in which a structure is lo-
cated, determine the transport mechanisms by which the environ-ment, i.e. water, chlorides, gases, can penetrate into concrete.
Therefore a definition of the various environmental conditions is
useful as a basis for discussing the transport mechanisms, and thetest methods themselves. This basic explanation of the environ-
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mental zones and the transport mechanisms should enable the re-
levance of each test to be considered when concrete durability testsare selected for specific projects.
These definitions are set out below, with reference to the followingdeterioration mechanisms:
Chloride-induced reinforcement corrosion: Parts of structureswhich are in contact with seawater, splash, spray, salty-dust, orother chloride sources (e.g. industrial process water, or irriga-
tion water), are at risk from chloride penetration leading to
reinforcement corrosion.
Carbonation-induced reinforcement corrosion: Parts of struc-tures which are not regularly wet, are subject to carbonation,
the rate of penetration of which is subject to humidity and con-crete mix. Good quality concretes which are durable against
chloride-induced corrosion are also unlikely to be vulnerable tocarbonation, subject to concrete mix details.
Sulphate attack: Severity of sulphate exposure should bechecked on a structure-by-structure basis, following systematic
methodology such as that provided by BRE Special Digest 1:2005 Concrete in Aggressive Ground.
Salt-scaling: Spalling of thin layers form concrete surfaces dueto splitting pressures arising from crystallization of salts in
concrete pores within the surfaces.
It is assumed that both alkali-silica reaction and the use of chlo-ride-containing concreting materials, are avoided by proper speci-
fications, and therefore are not relevant to a discussion on envi-
ronmental exposure and transport mechanisms.
Environmental conditions and zones
The following main macro-environments apply to concrete struc-tures in the UAE and most of the Gulf region and in each case
there are applicable micro-environments, as summarized in Table
1. This definition may not be comprehensive, and other situations
may occur outside the defined categories. Reference codes are
provided, to assist in illustrating the definition.
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Macro-environment Marine
Marine/coastal (M): Concrete structures which are close to orin contact with seawater, such as ports, harbors, jetty structures
or some bridge piers.
Micro-environments
Underwater (M-U): Parts of structures are exposed to constantimmersion in seawater.
Tidal zone (M-T): Parts of structures in the tidal range are sub- ject to alternating cycles of seawater immersion and drying.
Splash zone (M-S1): Parts of structures above high tide aresubject to splashing by sea-water wave action and drying by
wind and sun, all according to orientation and geometry.Spray zone (M-S2): Parts of structures above high tide andsplashing by waves are subject to wind-blown seawater spray,and drying according to wind and sun, all according to orienta-
tion and geometry, and are also exposed to carbonation.
Above the spray zone (M-S1), any other parts of marine/coastalstructures should be regarded as near-coastal (N-A).
Macro-environment NEAR-COASTAL
Near-coastal (N): Buildings or structures are typically locatedwithin 25- 250 m of the sea.
Micro-environments:o Above-ground (N-A): Parts of structures are exposed to
wind-blown spray/sand/dust, and are also exposed to car- bonation.
o Near-ground (N-N): Parts of structures are exposed to salts
rising from the ground water by capillary action and evapo-ration
o Below ground (N-B): Parts of structures are exposed to sa-
line ground-water, and probably sulphates.
Macro-environment INLAND
Inland (I): Typically buildings or structures beyond 25 – 250 mfrom the sea. Typically dry except for occasional rain, season-
al dewfall, and operational water sources.
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Micro-environments:o
Above-ground (I-A): Parts of structures are exposed towind-blown sand/dust, which may be salty, and are also
exposed to carbonation.
o Near-ground (I-N): Parts of structures may be exposed to
salts rising from the ground water by capillary action and
evaporation.
o Below ground (I-B): Parts of structures may be exposed to
saline ground-water, and possibly sulphates, depending
upon the height and salinity of the water-table.
Operational-micro-environments
In any of the above macro-environments (M, N, I), micro-environments may occur which result from operational
processes (-O-), as opposed to natural situations.
Underwater, tidal (i.e. wetting/drying), splash or spray condi-tions may also be created by process operations such as pump-
ing chambers or cooling water intakes/outfalls in industrial
plants, or irrigation watering at e.g. hotels or road interchanges.For example, a splash zone at a coastal outfall (M-O-S1), or
salt-water irrigation spray on inland concrete (I-O-A).
Internal Environment
The interior of buildings or structures is normally dry, and con-crete durability should be controlled by the combination of
good quality concrete so that carbonation is not excessive, and
proper building envelope detailing so that moisture is notavailable to support reinforcement corrosion in the event that
carbonation does penetrate to reinforcement; (N-I, I-I).
Measures other than concrete durability testing are required tocontrol non-typical situations such as leaking basements,excess moisture in kitchens, bathrooms, laundries, etc, or spe-
cial indoor structures such as swimming pools; (N-O-I, I-O-I).
TRANSPORT MECHANISMS
The section describes the principle mechanisms by which water,
ions; gases may be transported through concrete, to provide a basis
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for the following sections which describe durability test methods
and specifications.Transport is driven by pressure difference, for example water permeation through soil or concrete driven by hydrostatic pres-sure.
This typically applies to underwater zones of marine structures,or underground zones of structures built in the water-table such
as foundations, bridge piers, basements or tunnels.
The combination of ground-water permeation into concrete basements or tunnels, plus water evaporation on the inside of
these “hollow” structures, can result in more rapid transport of
water and salts into such concrete than by permeation alone.
Permeability measurement techniques and durability modelingare based on the Darcy equation for permeability based on
measurement of flow rate, and the Valetta equation for per-
meability based on measurement of penetration depth and time.
Transport is driven by concentration difference, for examplechloride ion diffusion through water, or carbon dioxide or wa-
ter vapor diffusion through air.
Diffusion is also used for representing the overall effect of wet-
ting and drying by salt-water which leads to chloride ingress,and is termed “effective diffusion”.
Measurement techniques and durability are based on Ficks
Laws of diffusion.Absorption
Transport is driven by capillary suction, for example waterabsorption into concrete or masonry.
This typically occurs in concrete structures around and justabove the ground-water table. Absorption is also the mechan-
ism by which a splashing wave penetrates into concrete, thecumulative effect of which is often termed effective diffusion,
as above.
The combination of absorption due to capillary suction, plusevaporation of the rising moisture, is often responsible for ver-
tical transport of salts from ground water leading to salt-scalingand/or reinforcement corrosion above the water-table.
Voltage-induced flow
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Some forms of durability test involve measuring voltage-
induced chloride ion flow through water, in which the voltageis provided in order to shorten the test duration.
Such conditions are artificial and do not normally exist in prac-tice, and do not provide a direct measure of permeability, diffu-sion or absorption.
TEST IN CURRENT PRACTICES
The problem of concrete durability in hot weather is very complex.
It can be seen that concrete structures in the hot, arid environments
tend to deteriorate more rapidly than those in temperate regions ofthe world, unless particular precautions are taken. Increases in
temperature also increase the risks of cracking, including plasticshrinkage cracking and drying shrinkage cracking, and facilitate
the ingress of salt-laden water and moisture, causing disintegration
of concrete due to reinforcement corrosion.
Core Testing
The examination and compression testing of cores cut from har-
dened concrete is a well-established approach, enabling visual in-spection of the interior regions of a member to be coupled with
strength estimation, and other physical properties which can be
measured include density, chloride diffusion, water absorption, or
water permeability. There are many factors that influence results,among which are the concrete characteristics and the testing va-
riables.
Compressive strength testing variables include factors as,Length/diameter ratio of core, Diameter of core, Direction of drill-
ing, Method of capping and reinforcement. The likely coefficient
of variation due to testing is about 6% for carefully cut and testedcore, which can be compared with a corresponding value of 3% for
cubes. The difference is largely caused by the effects of cutting.
It is claimed that the likely 95% confidence limits on actualstrength prediction for a single core are +-12% when the Concrete
Society calculation procedures are adopted. Uncertainties caused
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by reinforcement, compaction or curing may lead to an accuracy as
low as +-30%.
Ingress of moisture testsThe most important parameter that leads to premature deterioration
of reinforced concrete is the ingress of moisture, by absorption or
permeation, which can therefore. be used as an indicator of its
durability. Transport processes, which describe the movement ofaggressive substances through concrete, can be absorption, per-
meability or diffusion.
Absorption tests
In Absorption concrete takes in liquid by capillary suction to fillthe pore space available. Absorption tests should measure the
property mentioned and the sorptivity. However, due to the diffi-culty in achieving a unidirectional penetration of water and prob-
lems of determining the water penetration depth without actually
splitting open the concrete sample, the absorption characteristics ofconcrete are usually measured indirectly. The most common of
these tests are:
Standpipe tests
Initial Surface Absorption Test (ISAT) (Fig. 1)
Autoclam sorptivity test
Water-absorption test
Permeability tests
Permeability is where a fluid passes into concrete under the action
of pressure gradient. Experimental evidence of permeabili-
ty/durability correlation was well established from experimentscarried by Basheer. Permeability tests measure the transfer of a
liquid or gas into the concrete under the action of a pressure gra-
dient. They can be either steady state or non-steady state depend-ing on the condition of flow established within the pore system ofthe concrete. The most common of these tests are:
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Autoclam water and air permeability tests
Figg air permeability test
Schönlin air permeability test
Surface airflow test
Diffusion testsDiffusion is where a liquid, gas or ion migrates through concrete;
due to a concentration gradient. There is interest in ionic diffusion
tests because the rate at which chloride ions diffuse through con-
crete is closely related to the corrosion of reinforcement. There aretests which require cores to be extracted, while others can be car-
ried out in-situ. The most common of these tests are:
The rapid chloride permeability test
Steady state migration tests
In-situ chloride migration test
EVALUATION OF RESULTS AND REPORTING
Most tests have well-defined procedures and the methods used for
the calculation and assessment of different parameters from direct-ly measured values will depend to a large extent on the test method
used. Variation in properties of hardened concrete due to differ-
ences in materials, mixing, transportation, placing, finishing andcuring tend to be random and requires that the results be analyzed
using various statistical tools such as graphical and numerical me-
thods. The number of test types, test location and number of test
points used has a significant bearing on the ease with which thevariability of concrete within members and between members can
be assessed. For confidence, the variability of any tests employed
should be studied. Correlation differences between the laboratory
conditions under which results are obtained and site conditions canvary, and that this can affect the accuracy of our calibration. The
variability of the particular test method, the operator skill and the
variability of the concrete under test control the accuracy with
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which test results can be calibrated against a particular desired
concrete property.Reports should present all these variations and correlation and also
the limitations of the testing methods. Recommendations should beclear. Engineering judgment based on his experience and the avail-
able data should not be ambiguous or vague.
Durability tests – actual resultsConcrete, like any material, varies in its properties. The variations
arise from the raw materials, production methods and sampling
techniques. Table 2 shows the contributing factors on strength
variability at typical batch plants.
Statistical law and routine tests are used to measure the variation between concrete batches. Cube strengths plotted on a frequency
histogram will exhibit a normal distribution (Fig. 2).When designing mixes to meet a particular strength, a minimum is
stated below which a certain proportion of results, termed failures,
are found. This minimum is the specified strength and the mix isdesigned for a target mean strength, which incorporates an appro-
priate safety margin. A typical failure level allowed by specifica-
tions is 2.5%, in this instance, statistical tables indicate that therequired safety margin shall be 1.96 x standard deviation.
For example:Specified Strength = 40 MPa
Standard Deviation = 4 MPa
Target Mean Strength = 40 + (4.0 x 1.96) = 48 MPa
VARIABILITY OF THE TESTS
RCP Test
ASTM C1202 states the test method is suitable for evaluation of
materials and material proportions for design purpose and research
development. The numerical results (total charge passed in coloumbs) from this
test method must be used with caution, especially in applications
such as quality control and acceptance testing.
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Single Operator Precision--the single operator co-efficient of varia-
tion of a single test result has been found to be 12.3%. Thereforethe results of two properly conducted tests by the same operator on
concrete samples from the same batch and of the same diametershould not differ by more than 35%.
Multi – laboratory Precision--the multi-laboratory co-efficient ofvariation of a single test result has been found to be 18%. There-
fore results of two properly conducted tests in different laborato-
ries on the same material should not differ by more than 51%. The
average of three test results in two different laboratories should notdiffer by more than 29%.
DIN Water Penetration TestThe DIN standard does not address the issue of precision of the
test, Geiker et al reported data suggesting the maximum of three
results could deviate more than 100% from the mean with this test.The DIN test is based on the engineering principles relating to flow
of liquid subject to pressure. Research has proven that the test
method is highly susceptible to variations in specimen preparation,
curing and surface preparation. Furthermore measurement of theingress is a visual process prone to operator bias.
Water Absorption Test
The water absorption test gives a modification of total void spacein concrete. The variability of the test method is fairly low howev-er when applied to samples extracted from cubes during production
it gives little useful information. Whilst the absorption value is partially dependent on mix quality, it is also greatly affected by the
degree of compaction and effectiveness of initial curing. It is
therefore extremely difficult to determine whether „high results‟are caused by material or cube making / curing problems.
CONCLUSIONS
Over recent years an increasing amount of premature steel corro-
sion in concrete structures has created a big problem. In order to
ensure adequate durability and long-term performance of rein-
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forced concrete structures exposed to aggressive environments,
relevant quality parameters are needed, which can provide a better basis both for job specification and control of in situ quality.
The requirements set for these four tests differed among partiesand projects, the range is as follows:
Test UnitTest
duration
Maximum
Limits
specified
From to
Water absorption BS1881 Part 122
% 30 min <1 3
Initial Surface AbsorptionTest BS 1881 Part 208
ml/(m2.s) 10 min 0.02 0.3
Water penetration BS EN
12390 Part 8mm 28 d 8 20
Chloride Permeability
ASTM C-1202Coulomb -- 800 3800
Further investigations are required to study in depth the relation
between the four above-mentioned tests. This is required to arriveat a sound conclusion that will enable choosing the most suitable
test or combination of tests and to specify the performance levellimits for given project circumstances and Clients‟ expectations for
the service lives of their structures
REFERENCES
1. AASHTO Designation T 277-83, Standard method of test forrapid determination of the chloride permeability of concrete,
AASHT Washington D.C, 1983. 2. Andrade, C., Sanjuan, M.A., Alonson, M.C., 1993, Measure-
ment of chloride diffusion coefficient from migration tests,
NACE Corrosion ‟93.
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3. Andrews, R.J., Design and development of an in-situ chloride
migration test, PhD Thesis, Queen‟s University, Belfast, 1999,
4. ASTM: Standards test method for electrical indication of con-
crete‟s ability to resist chloride ion penetration, ASTM C 1202-94, American Society for Testing and Materials, 1994 Book of
ASTM Standards, Vol. 04.02, Concrete and Aggregates, Phila-
delphia, 1994. 5. Basheer, P.A.M., near – surface Testing for Strength and Dura-
bility of Concrete. Fifth CANMET/ACI International Confe-
rence on Durability of Concrete. Barcelona, Spain, 4-9 June
2000. 6. British Standards Institution, Testing Concrete – Recommenda-
tions for the assessment of concrete strength by near-to-surface
tests, BSI London, BS 1881, Part 207: 1992. 7. BSI (1981). BS 6089:Guide To the Assessment of Concrete
Strength in Existing Structures, BSI, London. 8. BSI (1986). BS 1881:Testing Concrete. Part 201:Guide To the
Use of Non- Destructive Tests for Hardened Concrete, BSI,
London. 9. Bungey, J.II. And Soutsos, M., Reliability of Partially-
Destructive Tests to Assess the Strength of Concrete on Site,Proceedings of the Fifth CANMET/ACI Conference on Dura-
bility of Concrete, Barcelona,2000 10. Whiting, D., Rapid measurement of the chloride permeability
of concrete, Public Roads, Vol.45, No. 3, pp. 101-112, 1981. 11. Nilsson, L.O., HETEK, Chloride penetration into concrete,
State-of-the-art, Transport processes, corrosion initiation, test
methods and prediction models, Report 53,Road Directorate,Copenhagen, 1996
12. RILEM – Committee “Nondestructive Testing Of Concrete
Materials and Structures “Vol. 2, No.10, July – Aug. (1969). 13. Specification for Roads and Bridge Works by Roads Depart-
ment, Dubai Municipality , 1992
ACKNOWLEDGMENT
This document has been prepared by a sub-committee of five se-
lected members of the steering committee. The members are the
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American University of Sharjah, RMCTOPMIX, University of
Sharjah, Halcrow, Dubai Central Laboratory. It has been also dis-cussed by the steering committee during general meeting which
comprised professionals in the concrete construction from manyUniversities, UAE Society of Engineers, Consultants, Dubai Cen-
tral Laboratory, Sharjah Municipality and Ministry of Public
Works & Housing.
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Table 1 - Macro- and Micro- Environment Summary
M a r i n e /
c o a s t a l
M a r i n e &
O p e r a t i o n a l
N e a r - C o a s t a l
N e a r - c o a s t a l &
O p e r a t i o n a l
I n l a n d
I n l a n d &
O p e r a t i o n a l
M M-O N N-O I I-O
Underwater (U) M-U M-O-U - - - -
Tidal (T) M-T M-O-T - - - -
Splash (S1) M-S1 M-O-S1 - - - -
Spray (S2) M-S2 M-O-S2 - - - -
Above-ground (A) - - N-A N-O-A I-A I-O-A
Near-ground (N) - - N-N N-O-N I-N I-O-N
Below-ground (B) - - N-B N-O-B I-B I-O-B
Internal (I) - - N-I N-O-I I-I I-O-I
Table 2 – Influence of various factors on standard deviation of
concrete strengths
Factors Plant A Plant B
Aggregates 1.2 1.5
Cement 2.0 2.5
Testing 1.0 1.5
Personnel and Plant 2.0 3.5
Total Standard Deviation 3.2 4.8
Note: The overall standard deviation is not calculated by simple
addition of individual figures, but on the square root of the sum of
the squared individual values.
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Fig. 1- Initial Surface Absorption Test
2
8
14
20
22
26
30
26
22
20
14
8
0
5
10
15
20
25
30
35
40 41 42 43 44 45 46 47 48 49 50 51
Compressive Strength (Mpa)
N u m b e r o f r e s u l t s
Fig. 2