GC/MS - chem-agilent.com · (GC) (GC/MS) (SHS) (DHS) (Extractables & Leachables) 2. A (1mL) B4 /...
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GC/MS E&L GC/MS GC/MS / / Extractables & Leachables E&L TOTM ( (2- )) Key word / Extractables & Leachables E&L GC/MS TDU2 7697A Author 5977B GC/MSD
Transcript of GC/MS - chem-agilent.com · (GC) (GC/MS) (SHS) (DHS) (Extractables & Leachables) 2. A (1mL) B4 /...
GC/MS
E&L
GC/MS
GC/MS
/ /
Extractables & Leachables E&L
TOTM ( (2- ))
Key word / Extractables & Leachables E&L
GC/MS
TDU2 7697A
Author
5977B GC/MSD
2
1.
1
(GC) (GC/MS)
(SHS) (DHS)
(Extractables & Leachables)
2.
(1mL) 4
/ (20 1mL) 4 /1
1mL 2 10mL
20mL
/ PVC( )
10mL
20mL
10cm 20mL
20 (TDU)
50%
40 3 50%
2
SHS ,
DHS
Agilent 7890B GC / 5977B MSD
Agilent 7697A
GERSTEL MPS2/TDU2/CIS4
GC
, , /
, VF-5MS (30m, 0.25mm, 1 m)
, VF-5MS (30m, 0.25mm, 0.5 m)
MS
SCAN m/z 29~550
280 150
HSS SHS
/ 60 /30min 120 /60min
TDU DHS
/ / 120 /20min/50mL/min
3.
3-1
3-1-1 (SHS)
( ) SHS
(EIC)
A
B ETBE (tert- )
SHS EIC
m/z 58, 78, 91
3
3-1-2 (SHS)
SHS
100
3
(TICC)
A B
3. SHS TICC
4 B
4. SHS
3-2 /
3-2-1 (SHS)
SHS
-
TOTM DEHP( (2- ))
-
( 5) C
1,2-
D4 D5 D6
5. SHS / TICC
3-2-2 (SHS)
PVC SHS
BHT
( 6)
6. SHS / TICC
3-2-3 (DHS)
DHS SHS
7 SHS
DHS
DHS SHS
DEHP
7. SHS DHS
4
3-2-4
1 L
50%
8 DHS
DHS
TOTM 40
TOTM 4
8. / TICC
4.
GC/MS
LC/MS
E&L
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Printed in Japan, October 30, 2018
GC-MS-201810OT-001
