For more information please contact [email protected] or visit …processaids.in/pdf/Syntho-Sleeve...

For more information please contact [email protected] or visit www.processaids.in

NRI Contact Info iii TECHNICAL DATASHEETS

Syntho-Sleeve Technical Datasheet 1-2 Wrapid Bond Technical Datasheet 3-4

CASE STUDY HDD: Horizontal Directional Drilling 5

TESTING

Shell Wrapid Bond Testing 6-27 Shell Confirmation Letter 28 Water Absorption of Syntho-Glass by Pittsburgh Testing (12/12/85): ASTM D-570 29-30 Abrasion Resistance: ASTM-4060 31 Impact Resistance Tests: ASTM G-14 32 Impact Test (Drop Weight) 33-34 Test Results 35 Test of Fiberglass Material (3/25/84): Dielectric ASTM D-149 36 Chemical Compatibility: Shore D 37 DNV Impact Resistance Testing 38-46

SPECIFICATION AND APPLICATION GUIDE

Syntho-Sleeve Specification and Application Guide 47 ISO 9001 CERTIFICATE 48 MATERIAL SAFETY DATA SHEETS

Syntho-Sleeve 49 Wrapid Bond 50

TERMS & CONDITIONS 51-52


NRI CONTACT INFO Muhammad Farooq

Composite Materials Engineer | | 1346 S. Killian Dr. Lake Park, FL 33403 Tel: 561.683.6992 x115 | Fax: 561.683.8366 | [email protected] Tammy Bomia

Regional Sales Manager | | 1346 S. Killian Dr. Lake Park, FL 33403 Tel: 561.683.6992 x111 | Fax: 561.683.8366 | [email protected] Tina Beck

Sales Coordinator | | 1346 S. Killian Dr. Lake Park, FL 33403 Tel: 561.683.6992 x101 | Fax: 561.683.8366 | [email protected] Bart Davis

Regional Manager, NRI Texas | | 1346 S. Killian Dr. Lake Park, FL 33403 Tel: 713.492.4223 | Factory: 561-683-6992 | [email protected] Matt Green

International Sales Engineer | | 1346 S. Killian Dr. Lake Park, FL 33403 Tel: 561.683.6992 x106 | Fax: 561.683.8366 | [email protected] Jose Zapata

Gas Utility Sales Manger | | 1346 S. Killian Dr. Lake Park, FL 33403 Tel: 561.683.6992 x116 | Fax: 561.683.8366 | [email protected] Ryan Schwarz

Vice President Sales & Marketing | | 1346 S. Killian Dr. Lake Park, FL 33403 Tel: 561.683.6992 x112 | Fax: 561.683.8366 | [email protected] Christopher Lazzara

President | | 1346 S. Killian Dr. Lake Park, FL 33403 Tel: 561.683.6992 x110 | Fax: 561.683.8366 | [email protected]


kruss_neptuneresearc

Text Box

iii

©Neptune Research Inc. (NRI) 1996, 2009. Syntho-Sleeve™ is a trademark of NRI. Patent Pending. NRI utilizes a process of continuousproduct improvement for all of our products. While we do strictly adhere to our products’ specifications, we routinely implement productimprovements. Therefore, please contact your local NRI distributor or office for the most current product specifications. NRI warrantsthe quality of this product when used according to directions. User shall determine suitability of product for use and assumes all risk.The seller will not accept liability for more than product replacement. SYS0110

Syntho-Sleeve Outer Wrap providesincreased mechanical protection andstrength for field joints and directionaldrilling applications with its:

• Higher impact resistance• Higher abrasion resistance• Higher tensile and flexural strength• Pressure retention capabilities• Reduced damage during pull through;

90% smoother profile than shrink sleeves

Benefits• Quick setting• Simple, cost-effective installation• Nonhazardous • Drastically reduced installation

time and materials• Easy to apply• Consistency of application, joint

after joint• Pre-impregnated, no field mixing

or messy field wetting• Water activated, no UV light or

heating required

NEPTUNERESEARCH.COM

Innovative Composite Solutions

1346 S. KILLIAN DRIVE • LAKE PARK, FL 33403 USA • 561.683.6992

Description

Syntho-Sleeve™ Outer Wrap is designed to protect field-welded joints on pipelines from the abrasion stressesand scarring of directional drilling and boring on a wide range of pipe diameters. Syntho-Sleeve providesmechanical protection to the preapproved corrosion coating of your choice, such as Viscous Elastic Coatings,Epoxy Coatings, Shrink Sleeves, and Cold Applied Tapes. This unique product has a faster setting time, iseasier to apply, has a very low profile, is extremely conformable, and is highly impact resistant. The resultis cost-effective, long-term protection against corrosion with superior mechanical protection.

BURY, BORE, OR DRILL IN LESS THAN ONE HOUROUTER WRAP

Syntho-Sleeve Mechanical Properties

Tensile Strength ASTM D638 36,000 PSI (2482.7 BAR)

Flexural Strength ASTM D790 26,000 PSI (1793.1 BAR)

Compressive Strength ASTM D695 24,000 PSI (1655.1 BAR)

Impact Resistance ASTM G14/G62 123 ft. lb. (167 J)

Dielectric Strength ASTM D149 16 Kv

Hardness Shore D 80

Lap Shear ASTM D5379 900 PSI (62.1 BAR)

Gel Time Time 5 Min @ 75°F (167°C)


NEPTUNERESEARCH.COM

Innovative Composite Solutions

1346 S. KILLIAN DRIVE • LAKE PARK, FL 33403 USA • 561.683.6992

BURY, BORE, OR DRILL IN LESS THAN ONE HOURSYSTEM

Viscous Elastic Coating Mechanical Properties

Thickness Measured > .071" (> 1.8mm)

Density ASTM D792 0.04 - 0.1 lb/in3 (1.1-3 g/cm3)

Impact Resistance EN 12068 11 ft. lb. (15 J)

Indentation Resistance EN 12068 .02" remaining (pass) (0.60mm)

Peel Strength EN 12068 > 72.5 PSI Cohesive failure (> 0.5 N/mm2)

Lap Shear Strength EN 12068 2.9 PSI (0.02 N/mm2)

Glass Transition Temperature ASTM D3418 < -4°F (< -20°C)

Cathodic Disbondment Resistance ASTM G8/EN 12068 .08" @ 73°F (2mm @ 23°C)

Cathodic Disbondment Resistance ASTM G42/EN 12068 .04" @ 140°F (1mm @ 60°C)

Electrical Resistance EN 12068 > 9.3x106 ohm/ft2

(> 108 ohm/m2)

Unwinding Test @ -22°F (-30°C) EN 12068 No separation, tears, or cracks

Low Temperature Flexibility @ -22°F (-30°C) EN 12068 No separation, tears, or cracks

Water Absorption ASTM D570 < 0.05%

Drip Resistance EN 12068 Pass at 194°F (90°C)

The Syntho-Sleeve System consists of two components: the primary layer, a Viscous Elastic Coating,requires minimal surface preparation and provides guaranteed corrosion protection of the field joint; whilethe secondary composite layer, Syntho-Sleeve Outer Wrap, provides mechanical protection againstabrasion during pull through. This unique product has a faster setting time, is easier to apply, has a verylow profile, is extremely conformable, and is highly impact resistant. The result is cost-effective, long-termprotection against corrosion with superior mechanical protection.

The Syntho-Sleeve System provides areliable, more cost-effective solution by:

• Increasing speed of application; nowaiting for epoxy to set; no additionaltools required for application

• Extremely surface tolerant; no gritblasting, only wire brushing or hand tool cleaning required

• Eliminating the need for flame torch and preheating

• Reducing damage during pull throughdue to its strength and low profile; 90%reduction in thickness as compared to competition

• Self-healing capabilities; cold flowproviding permanent saturation into the finest pores of the substrate

• Outstanding impact resistance• Low surface tension; adheres on

all dry substrates at a molecular level

Benefits• Simple, cost-effective installation• Highly effective protection against corrosion• Nonhazardous • No osmosis or under creep• Product can self heal• No hot work, no torches, no cooling time• No sandblasting

Syntho-SleeveOuter Wrap

Viscous ElasticCoating


CANUSA-CPS

Wrapid Bond™A visco-elastic adhesive based system for pipeline corrosion protection

Full System Approach

Field Friendly

Complete Line of Wrapid™ Products

The Wrapid Bond™ product line includesfiller materials, weld bead and seam tapesand Wrapid Coat™ mechanical protection.Refer to the Wrapid Coat™ product datasheet for more information.

• Long shelf-life

• Various widths available with convenientroll lengths for ease of inventory

• Fast installation with excellent adhesionon steel and many other base surfaceswithout applying primer

• No drying or hardening time

• Self healing ability when slightlydamaged due to plastic-elasticproperties

• Impermeable to water and oxygen

Canusa-CPS products such as WrapidSleeve™, Wrapid Tape™ and WrapidSeal™have been oil, gas and civil infrastructureindustry standards for many years.

For more than 35 years, Canusa-CPS has

been a lead ing deve loper and

manufacturer of specialty pipeline

coatings for the sealing and corrosion

protection of pipeline joints and other

substrates. Canusa-CPS high performance

products are manufactured to the highest

quality standards and are available in a

number of configurations to accommodate

many specific project applications.

™ wraparound corrosionprotective

™provides effective corrosion protection byproviding a barrier to water and oxygen.

™

™

Wrapid Bond™ is ideally suited for adiverse range of pipeline applicationsincluding: coating repair on new pipelineconstruction; transition areas from aboveto below ground pipelines; specialsections such as bends, tees, flanges, etc.;rehabilitation of existing pipelines.

The thick layer of adhesive provides atough barrier to water and oxygen whichprovides effective corrosion protection.

Wrapid Bond is acoating consisting of a modified

and reinforced visco-elastic adhesiveapplied onto a polyethylene carrier film.Supplied in roll form, Wrapid Bond

Wrapid Bond is for use on abovegroundand underground pipelines.

The specially formulated adhesive bondstenaciously to even the most difficultsubstrates and provides good elevatedtemperature creep resistance and resis-tance to soil stresses. Improved soil stressresistance is achieved with the installationof WrapidCoat outer wrap.

Adhesion & Creep Resistance

Wide Range of Applications

Long Term Corrosion Protection

Product Description

Features & Benefits

CANUSA-CPS is registered to ISO 9001:2008.

Product Data SheetProduct Data Sheet

Applications

Configurations

Temperature Range

Pipe Sizes

Up to 75°C (167°F)

Applications

Oil & Gas

Onshore Pipelines

Wrapid Bond™

All Sizes

Wrapid Coat™

Girth-Weld Joints

Corrosion Coating

Repair & Rehab

Fittings & Bends


Canusa warrants that the product conforms to its chemical and physical description and is appropriate for the use stated on the installation guide when used in compliance with Canusa’s written instructions. Sincemany installation factors are beyond our control, the user shall determine the suitability of the products for the intended use and assume all risks and liabilities in connection therewith. Canusa’s liability is stated in thestandard terms and conditions of sale. Canusa makes no other warranty either expressed or implied. All information contained in this installation guide is to be used as a guide and is subject to change without notice.This installation guide supersedes all previous installation guides on this product. E&OE

The product selection chart shown here is intended as a guide for standard products.Consult your Canusa-CPS representative for specific projects or unique applications.Below are typical values based on ShawCor CR&D Testing. Wrapid Bond™

PDS-NA-WrapidBond-rev016

Celsius

110°

90°

70°

50°

30°

Fahrenheit

230°

194°

158°

122°

86°

PipelineOperatingTemperature

Sle

eve

Opera

ting

Chara

cteri

stic

s

Product Selection Guide

PE, PP, FBE, PU, Coal tar, Bitumen

Resistance to Circumferential Forces

Resistance to Soil Stress

Resistance to Axial Pipe Movement

Main Line Coating Compatibility

Maximum Pipeline Operating Temperature °C (°F)

Wrapid Bond with

Wrapid Coat™PVC

™

75 (167)

Very Good

Very Good

Very Good

Typical Product Properties

UnitTest MethodProperty

How to OrderProduct Name Contents Packaging Quantity/Carton

50mmx10m

100mmx10m

200mmx20m

100mmx30m

150mmx10m

150mmx30m

Various widths available

Carton

Carton

Carton

Carton

Carton

Carton

Carton

12

6

4

2

12

6

Various

Thickness

Density

Peel Strength*

Lap Shear Strength

Glass Transition Temperature

Cathodic Disbondment Resistance*

Electrical Resistance*

Unwinding Test @ -30°C

Water Absorption

Drip Resistance

Impact Resistance*

Indentation Resistance*

Cathodic Disbondment Resistance*

Low Temperature Flexibility @ -30°C

Measured

ASTM D792

EN 12068

EN 12068

EN 12068

EN 12068

ASTM G8/EN 12068

ASTM G42

EN 12068

EN 12068

ASTM D3418

/EN 12068

EN 12068

EN 12068

ASTM D570

>1.8mm

1.1-1.3 g/cm³

15J

0.60 mm remaining (pass)

>0.5 N/mm Cohesive failure

0.02 N/mm²

<-20°C

2 mm @ 23°C

1 mm @ 60°C

>10 ohm/m²

No separation, tears or cracks

No separation, tears or cracks

< 0.05%

Pass at 90°C

8

Wrapid Bond™

Wrapid Bond™

Wrapid Coat

Wrapid Bond™

Wrapid Bond™

™PVC

Wrapid Coat™PVC

Wrapid Coat™XL*

Designation

WRB-B 50-10 BL

WRB-B 100-10 BL

WRB-B 150-10 BL

WRB-B 200-20 BL

WRC-B 100-30 BK

WRC-B 150-30 BK

WRC-XL-B XXX-XX BK

* When used with Wrapid Coat™PVC. Refer to the Wrapid Coat™ data sheet for more information.

Printed on recycled paper. Recyclable.

www.canusacps.com

CANUSA-CPSSHAWCOR LTDa division of .

25 Bethridge RoadToronto, OntarioM9W 1M7,CanadaTel: +1 (416) 743-7111Fax: +1 (416) 743-5927

Canada U.S.A./Latin AmericaCANUSA-CPS

SHAWCOR INC.a division of2408 Timberloch PlaceBuilding C-8The Woodlands, Texas77380, U.S.A.Tel: +1 (281) 367-8866Fax: +1 (281) 367-4304

Europe/Middle East Asia/PacificCANUSA-CPSa division of Canusa Systems Ltd.Unit 3, Sterling ParkGatwick RoadCrawley, West SussexEngland RH10 9QTTel: +44 (1293) 541254Fax: +44 (1293) 541777

CANUSA-CPSSHAWCOR LTD.a division of

#05-31, Blk 52, FrontierUbi Avenue 3Singapore408867Tel: +65-6749-8918Fax: +65-6749-8919

* Contact your Canusa-CPS sales representative for more information.


HDD: HORIZONTAL DIRECTIONAL DRILLING

Problem A 64-year-old section of natural gas pipeline, attached to a street bridge on the outskirts of downtown Houston, must be replaced to improve the reliability and integrity of the system. Conditions Crews face numerous challenges, including boring a 1,200-foot channel for the new 12-inch gas line 85-feet under Buf-falo Bayou. The replacement line was placed beneath the bayou to avoid compromising the bridge structure. The bayou wraps around Houston’s downtown skyline district and forced workers to maneuver large equipment and materials in areas with limited space and a lot of traffic. Solution With the clock ticking, the crew didn’t have time for machine applied systems or slow curing field joint compounds. Syntho-Sleeve Outerwrap was applied as abrasion protection for the specified cold applied corrosion tape. Both the corrosion tape and Syntho-Sleeve Outerwrap were quickly hand applied and the fast cure of the Syntho-Sleeve resin system kept the job rolling. Result Integrity issues with the field joint coating in an inaccessible line such as this are unacceptable. Syntho-Sleeve provided the added protection to ensure a 100% protected pipe and a successful job. The Syntho-Sleeve System survived the pull-back fully intact.

1346 S. KILLIAN DRIVE ◊ LAKE PARK, FL 33403 USA ◊ 561.683.6992 NEPTUNERESEARCH.COM

Syntho-Sleeve Outerwrap is designed to protect field welded joints on pipelines from the abrasion stresses and scarring of Directional Drilling and boring. Syntho-Sleeve provides me-chanical protection to the preapproved coating of your choice. This unique product has a faster setting time, is easier to ap-ply, has a very low profile, is extremely conformable, and is highly impact resistant. The result is a cost effective; long term protection against corrosion with superior mechanical protection.


TYPICAL URETHANE CHEMICAL RESISTANCE

1346 S. KILLIAN DRIVE ◊ LAKE PARK, FL 33403 USA ◊ 561.683.6992 ◊ NEPTUNERESEARCH.COM

EXCELLENT RESITANCE

Ammonium hydroxide, 10% solution

Ammonium sulfate, 2% solution

Benzene

Benzene chloride Butyl acetate

Brine, saturate

Brine, 10% solution

Butarol

Carbon tetrachloride

Diesel fuel

DiiIsobutylene

Diisobutylketone

Gasoline

Hexane

Hydrochloric acid, 10% solution

Hydrogen sulphide, 100% wet

Isopropanol

JP-4 Fuel; JP-5 Fuel

Kerosene

Linseed oil

Mineral spirits

Motor oil Acetone

Orthodichlorobenzene

Potassium chlorate, 5% solution

Potassium hydroxide, concentrated

Styrene

Sulfuric acid, 10% solution

Toluene

Trichloromonoflouromethane

Turpentine

Water

Xylene

GOOD RESISTANCE

Acetic acid, 2% solution

Ammonium hydroxide, concentrated

Anylacetate

Butyl acetate

Chlorobenzene

Ethylene glycol, 100%

Formaldehyde

Hydrochloric acid, concentrated

Trichloroethylene

Varsol

FAIR RESISTANCE

Ethyl acetate

Methylene chloride

POOR RESISTANCE

Acetone

Ethyl Alcohol , Methal Alcahol

Methyl ethyl ketone

SEVERE SOLVENT ACTION

Sulfuric acid, concentrated

Nitric acid, concentrate


DRAFT REPORT

REPORT NO BRIUS915 091608 REVISION NO

DET NORSKE VERITAS

Neptune Research – Lake Park, FL.

Impact Testing of Composite Repair Systems for Pipelines


DET NORSKE VERITAS

Report No: BRIUS915 – 86080391 ,

DRAFT REPORT

Page i Reference to part of this report which may lead to misinterpretation is not permissible.

Error! Reference source not found.

Client: Neptune Research – Lake Park, FL

DNV COLUMBUS 5777 Frantz Road Dublin, Ohio 43017-1386 U.S.A. Tel: (614)761-1214 Fax: (614)761-1633 http://www.dnvcolumbus.com

Report No.: 86080391

BRIUS915 091608

Subject Group: DNVR & I

Indexing terms: Summary: Neptune Research has manufactured fiber composite repair systems for pipelines comprising layered fiber/resin

materials that combine to provide structural reinforcement, impact resistance, and protection of the pipe surface from the exterior environment. In order to test the suitability of the product for field service, the impact resistance of the composite repair system was investigated using a modified ASTM G14: Standard Test method for Impact Resistance of Pipeline Coatings (Falling Weight Test). The specimens were tested until penetration was achieved. The impact area was tested for penetration via ASTM G62: Standard Test Methods for Holiday Detection in Pipeline Coatings. Two products were tested: Syntho-Glass XT (4” pipe) and Syntho-Sleeve (2” pipe). Each product was subjected to impact testing.

The following conclusions were reached:

1. The impact resistance of the composite system is considerably higher than most pipeline coatings, which is to be expected.

2. Multiple impacts are required to achieve a conductive path to the metal surface underneath the composite repair. The tests here may be used to simulate the impact of hard objects dropped from a moderate height, such as rocks dropped from a backhoe in the field.

3. These tests were performed in the central region of the repair; behavior may vary near the edges of the repair.

Prepared by: Davion Hill Senior Engineer

Signature

Reviewed by: Name and position

Signature

Approved by: Narasi Sridhar Director of DNV Research and Innovation - USA

Signature

Date of issue: 09/16/2009 Project No: 86080391

No distribution without permission from the client or responsible organizational unit (however, free distribution for internal use within DNV after 3 years)

No distribution without permission from the client or responsible organizational unit

Strictly confidential

Unrestricted distribution

All copyrights reserved DNV Columbus. This publication or parts thereof may not be reproduced or transmitted in any form or by any means, including photocopying or recording, without the prior written consent of DNV Columbus.


DET NORSKE VERITAS


DRAFT REPORT

Page ii Reference to part of this report which may lead to misinterpretation is not permissible.


Contents

1.0 BACKGROUND .....................................................................................................................1

2.0 RESULTS ................................................................................................................................2

3.0 SUMMARY AND CONCLUSIONS ......................................................................................5 Figures

Figure 1 2” pipe A (Syntho-Sleeve) impact site. Impact is less than ½” in diameter. Impact energy: approximately 167 J repeated 4 times. ............................................. 3

Figure 2 2” pipe B (Syntho-Sleeve) impact site. Impact is less than ½” in diameter. Impact energy: approximately 167 J repeated 4 times. ............................................. 3

Figure 3 4” pipe A (Syntho-Glass XT) impact site. Impact is less than ½” in diameter. Impact energy: approximately 167 J repeated 4 times.. ............................ 4

Figure 4 4” pipe B (Syntho-Glass XT) impact site. Impact is less than ½” in diameter. Impact energy: approximately 167 J repeated 4 times. ............................. 4


DET NORSKE VERITAS


DRAFT REPORT

Page 1 Reference to part of this report which may lead to misinterpretation is not permissible.


1 BACKGROUND Neptune Research has manufactured composite repair systems to be applied on the external surfaces of pipelines to structurally reinforce areas that may have suffered from metal loss or external damage. The composite system is being tested for impact resistance, as third party damage of pipelines is often a concern.

Since the desired goal was to test the specimens for penetration, a weight of 5.51 kg (2.5 lbs) was dropped from 3.1 m (10.2 ft) to impact the specimen. This was repeated 4 times, and ASTM G62 was performed after each impact. For all specimens, conductivity was established after the fourth impact. It is calculated that the weight impacted the surface at approximately 7.8 m/s which corresponds to an impact energy of 167 J. The specimen names, dimensions, and impact parameters are described in Table 1.

Table 1 Specimen description and impact energy specifications. Description

Specimen Pipe Diameter (in.)

Syntho-Glass XT A 4.00

Syntho-Glass XT B 4.00

Syntho-Sleeve A 2.00 Syntho-Sleeve B 2.00

INPUTS

mass (kg) 5.51 g (m/s^2) 9.80 height (ft) 10.16 height (m) 3.10

OUTPUTS

v (m/s) 7.79 Energy (J) 167.35


DET NORSKE VERITAS


DRAFT REPORT



2 RESULTS

Two test methods were employed. First, the specimens were impacted per ASTM G14. After each impact, conductivity of the impact site was tested per ASTM G62 (commonly used to detect defects in pipeline coatings).

Since composite repair systems are a relatively new technology, the ASTM standards used for this evaluation were adapted slightly to accommodate the different properties of the composite repair systems. ASTM G14 is designed to impact pipeline coatings, but the impact energy required to penetrate a composite is significantly higher. Therefore, more weight, greater height, and repeated impacts are often required to achieve penetration for composite repair systems. In addition, the ASTM G62 holiday detection test normally requires a wet sponge to defect pipeline coating defects which are usually small and shallow; however the thickness of the composite system can make it difficult to detect conductivity with the sponge method. In this case, a metal pick like what is used for most commercial multi-meters was instead used to gently make contact with the interior of the impact site and test for conductivity with the bare pipe steel. Once conductivity was detected, the impact site was deemed to have reached full penetration.

The impacted specimens are shown in the figures below. In Figure 1, the Sytho-Sleeve A specimen is shown. In Figure 2, the Sytho-Sleeve B specimen is shown. The impact area is shown in both figures and represents an impact of less than ½” in diameter. In Figure 3 and Figure 4, the Sytho-Glass XT A and B specimens are shown, respectively.


DET NORSKE VERITAS


DRAFT REPORT



Figure 1 2” pipe A (Syntho-Sleeve) impact site. Impact is less than ½” in diameter. Impact energy: approximately 167 J repeated 4 times.

Figure 2 2” pipe B (Syntho-Sleeve) impact site. Impact is less than ½” in diameter. Impact energy: approximately 167 J repeated 4 times.

Syntho-Sleeve

B

Syntho-Sleeve

A


DET NORSKE VERITAS


DRAFT REPORT



Figure 3 4” pipe A (Syntho-Glass XT) impact site. Impact is less than ½” in diameter. Impact energy: approximately 167 J repeated 4 times..

Figure 4 4” pipe B (Syntho-Glass XT) impact site. Impact is less than ½” in diameter. Impact energy: approximately 167 J repeated 4 times.

Syntho-Glass XT

B

Syntho-Glass XT

A


DET NORSKE VERITAS


DRAFT REPORT



3 SUMMARY AND CONCLUSIONS These ASTM procedures (G14 and G62) were modified to accommodate the different properties of thick composite materials. As the ASTM procedures were originally intended to test coatings, some modifications were made as described in the beginning of this report. Compared to a pipeline coating, however, the composite repair system demonstrated superior impact resistance, but this is generally expected. The impacts were located near the center of the composite repair but impacts near the edge may perform differently.

These impact tests may approximate dropped rocks or hard objects from the bucket of a backhoe during excavation or burial. These dropping objects may threaten coating or repair systems on a pipeline. Impact from the backhoe itself is another consideration but is not adequately simulated by these tests because of differences in impulse (force magnitude and force duration). The aspect ratio of the rock edges and features, its weight, and its angle of impact will greatly influence its damage potential, but the tests performed here would generically simulate a 2.5 lb. rock with rounded corners dropping from 10 ft above a coated composite repair on a pipeline. Under those conditions, full penetration would not likely occur with just one impact.

In these tests, the impact was repeated at the same location four separate times. The chances of multiple rocks hitting the same impact site are extremely unlikely, but the purpose of the repetition is to determine the conditions required to fully penetrate the composite. Since penetration of the composite system will expose bare metal, the same concerns about exposed metal under a coating would apply to the composite system.

An impact on a thin coating would likely cause a pinhole-like defect, but the impact on a composite has a different effect. The impact may sever the fibers in the composite material, or simply displace them as the penetrating surface forces itself into the matrix. In addition, the impact creates cracks in the resin matrix. If the impacted area is exposed to water, the cracks in the matrix present pathways for the water to ingress into the impacted area. Unlike a coating, an impacted composite surface may present multiple water entry points via these cracks. The effect of the impact on the composite may not present an immediate issue, but the long term effect of the impact and the subsequent exposure to wet environments may be of interest. In addition, if fibers are severed and the matrix is weakened, this may have an effect on the overall strength of the system. This depends on how much load is expected to be borne by the composite at the impact site.


Det Norske Veritas DNV is a leading provider of technology in managing corrosion and materials risks. As one of the few firms to combine practical engineering solutions with state-of-the-art research and testing, we can offer our clients innovative, cost effective solutions. We specialize in engineering, research and testing for corrosion control and monitoring, fitness-for-service, pipeline/plant integrity analysis, materials evaluation and selection, failure analysis, litigation support, management systems approaches and instrumentation and software design and development.

- o0o -


©Neptune R esearch I nc. ( NRI) Syntho-Sleeve™ is a r egistered t rademark of N RI. P atent P ending. N RI ut ilizes a pr ocess o f c ontinuous product i mprovement f or al l of our products. While w e d o s trictly ad here t o o ur pr oducts’ s pecifications, w e r outinely i mplement pr oduct improvements. T herefore, please contact y our l ocal NRI distributor or of fice for t he m ost c urrent pr oduct s pecifications. N RI w arrants the quality of this product when used according to directions. User shall determine suitability of product for use and assumes al l r isk. The seller will not accept liability for more than product replacement.

1346 S. KILLIAN DRIVE ◊ LAKE PARK, FL 33403 USA ◊ 561.683.6992 ◊ NEPTUNERESEARCH.COM

1

2

3

4

5

6

7

Measure and mark the total application area. Clean and roughen surface using a wire brush to remove any loose materials and de-gloss. Be sure to abrade not only the metal surface, but also beyond onto the coated pipe, either side by a minimum distance of 6”. Remove any oils, greases or other foreign debris from surface by utilizing the enclosed solvent cleaning wipe. Dry pipe if wet. Remove the plastic release coating from the Wrapid BondTM and apply, overlapping the coating. Do not apply with tension, but be sure to avoid air enclosures. Apply the corrosion coating to a dry pipe surface.

Water is needed to activate the Syntho-SleeveTM Outer Wrap. Open foil pouch of Syntho-SleeveTM Outer Wrap and submerge in tepid water for 10 seconds. Note: water could also be poured into the pouch. Once opened, the Syntho-Sleeve cannot be repackaged.

Apply compression film in the same direction as the 2 previous layers, starting beyond the outer edge of the Syntho-SleeveTM Outer Wrap, pulling firmly during application. Apply 2 layers of compression film over the entire composite area.

Perforate the compression film using wire brush (or other perforating device) by tapping firmly on the tape with the metal bristles. Perforation allows the CO2 gas generated by the curing process to escape. Remove compression film after 10 minutes. Once the Syntho-Sleeve Outer Wrap has cured, during compression film stage @ 75°F (24°C), the pipe can then be pulled through at a hardness of 70d.

Massage the Wrapid BondTM tightly into the surface. Start by pressing fingers on either side of the weld and work outward.

The Syntho-SleeveTM Outer Wrap application should start on the side of the field joint that will be pulled into the hole first. Begin the application of Syntho-SleeveTM Outer Wrap at a minimum distance of 6” beyond the Wrapid BondTM and spiral wrap following the wrapping guideline. The Syntho-SleeveTM Outer Wrap should be applied in same direction as the Wrapid BondTM was applied. Apply pressure during application by pulling firmly on the roll as it is applied. Squeeze and mold firmly in the direction of the wrap until tacky.

NEPTUNERESEARCH.COM

PREPARATION AND APPLICATION READ ALL INSTRUCTIONS BEFORE OPENING PACKAGES


Section I Neptune Research 1346 South Killian Drive Lake Park, Florida 33403

Emergency Telephone Number – 800-535-5053 Telephone Number for Information – 800-328-0090 / 561-683-6992

Product Name – Syntho-Sleeve Date Prepared – 05-26-10 Section II—Hazardous Ingredients/Identity Information

Hazardous Components (Specific Chemical Identity, Common Name(s) CAS#)

OSHA PEL ACGIH TLV Other Limits Recommended

% (optional)

Homologues of methylene bisphenyl isocyanate* (9016-87-9) N/A N/A N/A 5-10 Methylene bisphenyl isocyanate* (101-68-8) N/A .005 ppm (TWA) N/A 1-5 .02ppmCeiling (STEL) N/A N/A .2mg/m3Ceiling(STEL) N/A N/A Polypropylene Polyol (25322-69-4) N/A N/A N/A 5-15 *This component is listed as a SARA section 313 Hazardous component Section III—Physical/Chemical Characteristics Vapor Pressure (mm Hg) – 0.0003 mm Hg Specific Gravity (H20 = 1) – 1.22 Vapor Density (AIR = 1) – 8.5 Evaporation Rate (Butyl Acetate = 1) , Ether =1 – N/A Boiling Point – N/A Melting Point – N/A Solubility in Water: Insoluble – reacts slowly with water to liberate carbon dioxide gas Appearance and Odor – Fiberglass cloth, coated with viscous resin, odorless Section IV—Fire and Explosion Hazard Data Flash Point - 370°F / Method Used – Pensky-Martens Closed Cup Flammable Limits - N/A LEL - N/A UEL - N/A Extinguishing Media: Carbon Dioxide, foam, dry chemical. Water spray for large fires Special Fire Fighting Procedures: Full emergency equipment with self-contained breathing apparatus and full protective clothing should be worn by firefighters. During a fire, MDI vapors and other irritating, highly toxic gases may be generated by thermal decomposition or combustion. At temperatures greater than 400° F, polymeric MDI can polymerize and decompose which can cause pressure build-up in closed containers. Explosive rupture is possible. Therefore, use cold water to cool fire-exposed containers. Unusual Fire & Explosion Hazards - None Section V—Reactivity Data

Stability: Stable Hazardous Decomposition or Byproducts: Carbon Monoxide, Oxides of nitrogen, traces of HCN, MDI vapors or aerosols Incompatibility (Materials to Avoid) Water, amines, strong bases, alcohols. Will cause some corrosion to copper alloys and aluminum Hazardous Polymerization: May Occur / Contact with moisture, other materials which can react with isocyanates or temperatures above 400°, may cause polymerization. Conditions to Avoid: Contamination with water

Section VI—Health Hazard Data Route(s) of Entry: Skin contact from liquid and aerosols (spray application). Inhalation. Although MDI is low volatility, an inhalation hazard can exist from MDI aerosols or vapors formed during heating, foaming or spraying. Can irritate mucous membranes, cause runny nose, sore throat, coughing, and other symptoms. Acute Skin Contact: Isocyanates react with skin protein and moisture and can cause irritation which may include the following symptoms: reddening, swelling, rash, scaling or blistering. Cured material is difficult to remove. Chronic Skin Contact: Prolonged contact can cause reddening, swelling, rash, scaling or blistering and in some cases, skin sensitization. Individuals who have skin sensitization can develop these symptoms from contact with liquid or vapor. Animal tests have indicated that respiratory sensitization can result from skin contact with MDI. These data reinforce the need to prevent direct skin contact with MDI. Acute Eye Contact: Liquid, aerosols or vapor are irritating and can cause tearing, reddening and swelling. If left untreated, corneal damage can occur and injury is slow to heal. Damage, however is usually reversible Acute Ingestion: Irritation and corrosive action can occur in the mouth, stomach tissue and digestive tract. Symptoms can include: sore throat, abdominal pain, nausea, vomiting and diarrhea. Carcinogenicity: In a chronic inhalation study, rats were exposed to an aerosol of polymeric MDI for six hours per day, five days per week, for a period of two years. The exposure concentrations were 0, 0.2, 1.0 and 6.0 mg/m3. The occurrence of pulmonary adenomas (benign tumors) and a single pulmonary adenocarcinoma (malignant tumor) was considered to be related to exposure. These tumors were observed only in the rats that were exposed to the high concentration of 6 mg/m3. NTP – No IARC Monographs – No OSHA Regulated – No Medical Conditions Generally Aggravated by Exposure – Asthma or other respiratory disorder (bronchitis, emphysema, bronchial hyper-reactivity), skin allergies & eczema Emergency and First Aid Procedures - Ingestion: Do not induce vomiting. Give one to two cups of milk or water to drink. Do not give anything by mouth to an unconscious person, consult a physician Inhalation: Move to an area free from risk of further exposure. Administer oxygen or artificial respiration as needed. Obtain medical attention. Asthmatic –type symptoms may develop and may be immediate or delayed up to several hours. Consult physician should this development occur. Skin contact: Remove contaminated clothing. Wash affected skin thoroughly with soap and water. Wash contaminated clothing thoroughly before reuse. For severe exposures, get under safety shower after removing clothing, then get medical attention. For lesser exposures, seek medical attention if irritation develops or persists after area is washed. Eye contact: Flush with copious amount of water. Preferably lukewarm, for at least 15 minutes, holding eyelids open at all times. Refer individual to a physician or ophthalmologist for immediate follow up. Notes to Physician – Eyes: stain for evidence of corneal injury. If cornea is burned, instill antibiotic steroid preparation frequently. Workplace vapors have produced reversible corneal epithelial edema impairing vision Skin: This compound is a known skin sensitizer. Treat symptomatically for contact dermatitis or thermal burns, if burned treat as a thermal burn. Ingestion: Treat symptomatically. There is no specific antidote. Inducing vomiting is contraindicated because of the irritating nature of this compound. Respiratory: This compound is a known pulmonary sensitizer. Treatment is essentially symptomatic. Remove exposed individual to any isocyanate. Section VII—Precautions for Safe Handling and Use Steps to Take if Material Is Released or Spilled – Resin is incorporated in cloth material, therefore non-flowable. Exposure to moisture results in resin becoming an inert solid. Waste Disposal Method – In accordance with federal, state and local regulations. Precautions to Be Taken in Handling and Storing – Store in a cool dry area. Transportation Information – DOT (49 CFR 172) - Unrestricted, IATA - Unrestricted Section VIII—Control Measures Respiratory – N/A Monitoring – N/A Medical Surveillance – N/A Skin protection – Permeation resistant gloves (butyl rubber, nitrile, and polyvinyl alcohol). However, please note that polyvinyl alcohol degrades in water. Cover as much of the exposed area as possible, with protective clothing. If skin creams are used, keep the area covered by the cream to a minimum. Eyes – Liquid, chemical goggles. Vapor resistant goggles should be worn when contact lenses are in use. In a splash hazard environment chemical goggles should be used in combination with a full face shield. Safety showers and eye wash stations should be available. Ventilation – Local exhaust sources regarding industrial ventilation (i.e. ACGIH Industrial Ventilation) should be consulted for guidance about adequate ventilation.

Section IX—Other Information The information contained herein is based on the data available to us and is believed to be accurate. The data is offered in good faith as typical values and not product specification. The information in this data sheet was compiled from the information supplied by the vendors of the components of this compound. Neptune Research, Inc. makes no warranty either expressed or implied regarding the accuracy of these data or the results to be obtained from the use thereof. The recommended industrial hygiene and safe handling procedures are believed to be genuinely applicable. However, each user should review these recommendations in the specific context of the intended use and determine whether they are appropriate. Neptune Research, Inc. assumes no responsibility for injury from the use of the product described herein. This information is intended only to assist in the safe handling of this material.


Section I Canusa-CPA, A division of Shawcor, Ltd Airport Road Huntsville, Ontario P0A 1K0

Emergency Telephone Number – (613) 996-666 (CANUTEC) Telephone Number for Information – (705) 789-1787 / 561-683-6992

Product Name – Wrapid Bond Date Prepared – 1/2008 Section II—Hazardous Ingredients/Identity Information

Hazardous Components (Specific Chemical Identity, Common Name(s) CAS#)

OSHA PEL

ACGIH TLV Other Limits Recommended

% (optional)

Mixture of Polyolefin mixture & lube oils containing polybutene (None) N/A N/A N/A Proprietary Section III—Physical/Chemical Characteristics Vapor Pressure (mm Hg) – ND Specific Gravity (H20 = 1) – ND Vapor Density (AIR = 1) – ND Evaporation Rate- ND Boiling Point – ND Melting Point – N/A Solubility in Water: NA Appearance and Odor – Solid with slight hydrocarbon odor Section IV—Fire and Explosion Hazard Data Flash Point – NA Flammable Limits -

N/A LEL – ND UEL - ND

Extinguishing Media: Water spray, foam, dry chemical Special Fire Fighting Procedures: Do not enter confined fire space without full bunker gear (helmet with face shield, bunker coats, gloves, and rubber boots) including a positive pressure NIOSH approved self-contained breathing apparatus. Section V—Reactivity Data Stability: Stable Hazardous Decomposition or Byproducts: Toxic gases liberated under fire condition Incompatibility (Materials to Avoid): Strong oxidizing agents Hazardous Polymerization: Will not occur Conditions to Avoid: Elevated temperatures

Section VI—Health Hazard Data Route(s) of Entry: Ingestion Acute Skin Contact: Contact with skin causes irritation and redness. Chronic Skin Contact: None anticipated Acute Eye Contact: Contact with eyes causes irritation. Acute Ingestion: No exposure effects anticipated under normal work conditions. May cause gastrointestinal irritation if swallowed. Inhalation: No exposure effects anticipated under normal work conditions. Carcinogenicity: Not listed NTP – No IARC Monographs – No OSHA Regulated – No Medical Conditions Generally Aggravated by Exposure – Not Determined Emergency and First Aid Procedures - Ingestion: Do not induce vomiting, consult a physician immediately Inhalation: Move to an area free from risk of further exposure. Administer oxygen or artificial respiration as needed. Obtain medical attention. Skin contact: Remove contaminated clothing. Wash affected skin thoroughly with soap and water. Wash contaminated clothing thoroughly before reuse. Seek medical attention if irritation develops or persists after area is washed. Eye contact: Flush with copious amount of water. Preferably lukewarm, for at least 15 minutes, holding eyelids open at all times.

Section VII—Precautions for Safe Handling and Use Steps to Take if Material Is Released or Spilled – Pick up material and dispose of according to the applicable Federal, State, or local regulations. Do not allow to enter sewers/surface or ground water. Waste Disposal Method – In accordance with federal, state and local regulations. Precautions to Be Taken in Handling and Storing – Avoid contact with skin or eyes. Wash thoroughly after use and before work breaks. Keep in cool, dry, ventilated storage and in closed containers. Transportation Information – Not regulated under TDG Section VIII—Control Measures Respiratory – N/A Monitoring – N/A Medical Surveillance – N/A Skin protection – Appropriate impervious gloves. Because a variety of protective gloves exist, consult glove manufacturer to determine the proper type for a specific operation. Eyes – Safety glasses or goggles. Ventilation – Local exhaust sources regarding industrial ventilation (i.e. ACGIH Industrial Ventilation) should be consulted for guidance about adequate ventilation.

Section IX—Other Information THIS INFORMATION IS ACCURATE AND RELIABLE TO THE BEST OF OUR KNOWLEDGE. IT IS FURNISHED WITHOUT WARRANTY, EXPRESSED OR IMPLIED. CANUSA-CPS, A DIVISION OF SHAWCOR LTD. ASSUMES NO LEGAL RESPONSIBILITY FOR THE USE OF, OR RELIANCE UPON, THIS DATA FOR HAZARDS WHICH MIGHT BE ASSOCIATED WITH THE USE OF THESE MATERIALS OR FOR RESULTS OBTAINED. IT IS THE RESPONSIBILITY OF THE USER TO COMPLY WITH ALL APPLICABLE LAWS AND REGULATIONS. THIS MSDS WAS CREATED IN COMPLIANCE WITH APPLICABLE HAZARDOUS MATERIAL REGULATIONS, AND IS NOT INTENDEDTO BE USED FOR ANY OTHER PURPOSE.


of 2 Rev 4: 5.11.10

1. Agreement. This order of sale (including ail attachments hereto and any amendments or m odifications m ade i n ac cordance with t he t erms h ereof, collectively the " Order") c onstitutes an e xpression o f i ntent b y N EPTUNE RESEARCH INC. ("Seller") t o sell the goods, machinery, eq uipment and services s pecified o n t he f ace hereof ( collectively t he " Goods") at t he price(s) and with the delivery date{s) so specified, upon the terms and conditions set forth herein and in accordance with any specifications on the face h ereof and i n an y attachments, s chedules, e xhibits, de signs or drawings at tached hereto (collectively the "Specifications"), This Order shall not constitute an a cceptance of any provisions in any purchase order or confirmation of Purchaser that add to or conflict with t he terms hereof. This O rder s hall c onstitute t he ent ire c ontract bet ween P urchaser a nd Seller, notwithstanding a ny s uch varying p rovisions o r a ny f orm o r electronic message sent by Purchaser after the date hereof. Any proposal to vary any of the terms hereof is hereby objected to and rejected, and shall not form a part of the contract. Technical documents, including b ut not limited t o any drawings, descriptions, illustrations or designs, whether supplied by Seller or Purchaser, and whether or not included as part of the Specifications, shall serve only to provide approximations and general guidance as t o the c haracteristics o f t he Goods an d s hall n ot bind ei ther party. T here ar e no o ral u nderstandings b etween P urchaser an d S eller, and no agreements other than those embodied herein. This Order may not be amended o r m odified e xcept i n w riting s igned by an authorized representative of Seller. 2. Cancellation. Purchaser may not cancel this Order, or any part, without Seller's w ritten c onsent. If P urchaser wrongfully c ancels t his O rder, Purchaser s hall b e l iable t o S eller f or a ny of t he f ollowing e xpenses incurred b y S eller: ( i) di rect c osts i n c onnection with t he ordering o r purchase of materials or parts in connection herewith; (H) engineering and labor costs in connection herewith; ( iii) administrative and overhead costs allocable to work already performed in connection herewith and (iv) costs and expenses to which Seller has been committed prior to cancellation of this order. The amount payable by Purchaser as set f orth above s hall be reduced by the amount of any payments made by Purchaser in respect of the G oods p rior t o t he d ate of c ancellation. In ad dition t o t he above, Purchaser agrees to pay Seller an amount equal to 15% of the total amount payable as s et forth above, to c ompensate S eller f or i ts anticipated profits lost as a result of Purchaser's cancellation. All sums owing pursuant to t his paragraph s hall b e pa yable i n f ull i mmediately upon P urchaser's receipt of written notice thereof from Seller. 3. Price. All prices are quoted F.O.B. Shipping Point and u nless otherwise agreed in writing, and except for Seller's internal costs with respect to inspection and compliance with governmental laws and regulations, do not include an y c osts of f reight, i nsurance, s pecial pac kaging o r i nstallation, any costs o f i nspection, permits o r o ther c ompliance with governmental laws and regulations, any sales, use, excise, customs or other taxes, duties or fees, or an y other charges, all of which must be paid by Purchaser. In the event Seller includes any such charges in any price herein, Seller may adjust s uch c harges at an y t ime pr ior t o p ayment t hereof b y S eller on Purchaser's behalf in respect of any applicable changes in governing laws or r egulations; a nd P urchaser agrees t o pay a ny a dditional c harges incurred as a result of any such adjustment. 4. Payment and Inspection. Unless otherwise agreed in writing, payment is due within t hirty days of i nvoice. P ayment t erms s hall b e pe r Seller's standard payment terms included in this order. If Purchaser delays delivery of any Goods, Seller shall submit, and Purchaser shall pay, invoices for such G oods as i f delivery h ad been m ade on the originally estimated delivery date; and i n addition, Purchaser s hall pay all reasonable storage a nd other expenses i ncurred by S eller a s a result of s uch delay. Purchaser m ay inspect G oods d elivered hereunder upon receipt at f inal destination. Within t en b usiness d ays t hereafter, P urchaser shall gi ve written not ice t o S eller of an y alleged defect i n t he c ondition or qu ality of such Goods, or of any alleged nonconformities with the Specifications, and s hall i ndicate t he basis o f i ts c laim i n detail. P urchaser's f ailure to furnish s uch no tice i n a timely, m anner s hall constitute i rrevocable acceptance of t he Goods. P urchaser agr ees t o pa y i nterest on a ny payment du e und er t his or der a t a r ate of 18% pe r an num, c omputed on the basis of a 360-day year and the actual days elapsed and to accrue from the date s uch p ayment i s d ue until paid i n f ull; p rovided, h owever, that i f such rate exceeds the maximum rate permitted under applicable law, then interest shall be charged at the maximum rate permitted under such law. In addition, Purchaser agrees to pay all costs, including reasonable attorneys' fees, incurred by Seller in the enforcement of any obligation of Purchaser hereunder.

5. Delivery. Goods are s old F.O.B. S hipping P oint. U nless ot herwise agreed i n writing, S eller m ay s elect t he m ethod of , an d ar range f or, transportation t o f inal d estination. T he del ivery da te s pecified o n t he f ace hereof represents Seller's estimate of the date of delivery of the Goods and is based, in part, on information supplied by Purchaser. Accordingly, Seller will attempt in good faith, but does not guarantee or covenant, to deliver the Goods by such estimated delivery date; and Seller shall not be obligated to take any extraordinary steps to meet such delivery date (including the use of ov ertime l abor) nor s hall S eller b e liable f or any damages s uffered b y Purchaser as a result of S eller's inability to meet the estimated delivery date. 6. Passage of Title and Security Agreement. Title t o G oods delivered hereunder shall pass to Purchaser at the time of F.O.B. delivery to carrier, and Purchaser agrees to assume all risk of loss of the Goods at that time. Purchaser hereby g rants to S eller a s ecurity interest in all s uch Goods t o secure payment of al l s ums d ue S eller hereunder. P urchaser a grees t o execute promptly an y financing s tatements o r f urther d ocuments S eller deems necessary to perfect i ts s ecurity i nterest, and t o p erform al l other acts necessary for the perfection and preservation of such security interest. 7. Limited Warranty. Subject t o t he l imitations and e xceptions below, al l Goods del ivered hereunder are warranted to be free from material defects in materials and workmanship for the Warranty Period (as defined below). This warranty shall apply only if (i) Purchaser notifies Seller in writing of the claimed def ect w ithin 20 da ys of discovery; ( ii) Purchaser discovers t he claimed defect within the Warranty Period; and (iii) Purchaser allows Seller to inspect the Goods claimed to be defective. This warranty shall not apply to Goods t hat have not been i nstalled and/or operated and maintained in accordance with i nstallation or operating i nstructions o r t hat h ave be en accidentally damaged, or to Goods with defects attributable in any way to installation, modification or repair made by any party other than Seller; nor shall this warranty apply if (i) Purchaser or a t hird party modifies or repairs the Goods without Seller's prior written approval; or (ii) after discovery of a defect, Purchaser fails to take prompt and reasonable steps to prevent the defect from becoming more serious. Further, this warranty shall not apply to the component parts of any Goods manufactured in whole or in part by a party other than Seller and resold by Seller except to the extent that any such third party has warranted such to Seller and is liable to Seller under such warranty. In t he e vent P urchaser c omplies i n f ull w ith al l o f i ts obligations under this Order, including but not limited to payment in full in respect of t he Goods, a nd t he c onditions of t his p aragraph are s atisfied, Seller shall correct any material defect either by (i) supplying F.O.B. S eller's pl ant replacement p arts or ( ii) r epairing an y defective p arts. If i n S eller's j udgment r epair or r eplacement would be commercially impracticable, Seller shall issue Purchaser a refund or credit in t he am ount of t he purchase price of t he defective Goods. A s u sed herein, t he " Warranty P eriod" i s 12 months. T he Warranty Period s hall commence on t he earlier of; ( i) t he dat e of s hipment ( or t he d ate of completion of installation if Seller has undertaken to install the Goods); or (ii) if delivery or installation is delayed for reasons beyond Seller's reasonable c ontrol, t he 30th day following the d ate u pon which s hipment would have been made (or if Seller has undertaken to install the Goods, the 30th da y f ollowing t he d ate upon which i nstallation would hav e b een completed) abs ent t he d elay. T he f oregoing w arranty i s e xclusive a nd made only to Pu rchaser. SEL LER MAKES N O O THER E XPRESS, IMPLIED O R ST ATUTORY WARRANTY, INCLUDING AN Y WARRANTY OF MERCHANTABILITY OR FITNESS FOR A PARTICULAR PURPOSE, AND ALL SUCH WARRANTIES ARE HEREBY EXPRESSLY EXCLUDED. Seller makes no warranty relative to damages caused by abrasion, chemicals, corrosion, wear or abnormal temperature. No person is authorized t o gi ve a ny a dditional warranties on S eller's b ehalf o r t o assume f or S eller a ny other l iability i n c onnection herewith, e xcept i n a writing s igned b y an a uthorized o fficer of S eller. For pu rposes o f t his paragraph, "Goods" shall specifically include any and all parts thereof. 8. Limitation of Remedies. Purchaser's s ole a nd exclusive r emedy against Seller arising out of or in connection with any claimed defect in any Goods sold he reunder, whether based upon contract, tort, warranty, s trict liability or negligence, and whether for personal injury, commercial loss or other monetary loss, shall be at Seller's option the repair or replacement of such Goods that Seller determines in its reasonable judgment and upon inspection to be defective, or if in Seller's judgment repair or replacement would be commercially impracticable, the issuance to Purchaser of a credit


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or r efund i n t he am ount of t he p urchase p rice of s uch G oods. S ELLER SHALL NOT BE LIABLE FOR ANY ADDITIONAL LOSS OR DAMAGE ARISING DIRECTLY OR I NDIRECTLY F ROM THE USE O F G OODS SOLD HE REUNDER O R FOR ANY S PECIAL, INCIDENTAL, O R CONSEQUENTIAL DAMAGES WHATSOEVER. Any action resulting from any breach, defect or failure of Seller to perform hereunder must be commenced w ithin one y ear af ter the cause o f ac tion has ac crued. F or purposes of this p aragraph, " Goods" s hall s pecifically i nclude any and al l parts thereof. 9. Engineering Services. Unless ot herwise a greed i n writing, P urchaser shall be responsible for the erection, installation and start-up of the Goods, and s hall p ay al l r elated expenses. S eller at i ts o ption m ay provide t he services of i ts personnel in connection with or subsequent to the erection, installation or start-up of the Goods if Purchaser so desires, and Purchaser shall pay all related expenses incurred by Seller, including but not limited to traveling an d l iving expenses of S eller's pe rsonnel, as well as a f ee f or labor performed by S eller's personnel in connection therewith, based on Seller's normal h ourly r ates. In t he e vent S eller f urnishes a ny i nstallation services, P urchaser s hall a t i ts e xpense f urnish t he required i nstallation space f or al l Goods, and s hall t imely c omply with al l applicable specifications f or i nstallation up t o a nd t hrough t he d ate of c ompletion o f installation. 10. Confidential Information. Purchaser ac knowledges t hat Seller has a proprietary interest in all information, technical data, designs, specifications and memoranda relating to the Goods and any processes and m ethods with respect to the operation thereof (collectively the "Information"), that the Information i s a uni que an d v aluable bus iness as set of S eller, and t hat Seller would be seriously and irreparably harmed by its wrongful disclosure or ot her m isuse. P urchaser therefore ag rees n ot t o use an y of the Information f or an y p urpose ot her t han t he i nstallation, s ervicing a nd operation of the Goods, not to copy any of the Information or disclose any part thereof to any person or entity other that its employees (and then only to the extent required in the performance of their work), and to return all of the Information i n i ts possession t o S eller up on request. P urchaser additionally agrees to use reasonable care to i nsure that its employees, subcontractors and suppliers do no t disclose any part of the Information to any other person or entity or appropriate any part of the Information to their own use. 11. Patents. Seller shall indemnify and hold Purchaser harmless from any liability or cost arising out of any suit, action or claim for the infringement of any patent or patent rights which are or may be asserted against Purchaser because of the design, nature or structure of any of Seller's standard-design Goods; provided, however, that (i) Purchaser notifies Seller in writing of the existence of any such suit, action or claim within 10 days after Purchaser's di scovery t hereof; ( ii) P urchaser gr ants t o S eller exclusive control over the defense and litigation of any such suit, action or claim, and over i ts ne gotiation, s ettlement or c ompromise; an d ( iii) i n t he e vent infringement oc curs, or S eller i n i ts r easonable j udgment determines t hat infringement i s l ikely t o occur, P urchaser p ermits S eller at S eller's o ption (A) to procure on P urchaser's behalf a license acceptable to Purchaser for the c ontinued use of t he G oods, (B) to m odify the G oods t o t he extent necessary to cure any problems of infringement, or (C) to issue Purchaser a refund o r c redit for the Goods in the amount of t he fair market value of the Goods at that time. Purchaser shall indemnify and hold Seller harmless from a ny l iability or c ost arising out of a ny s uit, ac tion or c laim f or the infringement o f an y pa tent o r pa tent rights t hat a re or m ay b e as serted against Seller because of the design, nature, structure or use of any Goods ordered h ereunder, t o t he e xtent s uch l iability o r c ost a rises f rom or i s caused by designs or specifications furnished by Purchaser or modified at Purchaser's request, and Purchaser shall indemnify and hold Seller harmless f rom any l iability for loss or damage, and from all court costs, attorneys' fees and other expenses, incurred by or imposed upon Seller, in connection with the defense of any action brought against Seller by reason of S eller's p erformance of t his Order. At S eller's request, P urchaser s hall promptly assume full responsibility for the defense of any such action which may be brought against Seller. 12. Force Majeure. Each party shall be e xcused f rom the dut y t o render timely performance of any obligation hereunder if such inability to perform is caused directly or indirectly by act of God, flood, war, riot, fire, accident, explosion, s trikes or l abor t rouble, act of g overnment, d elay or default by subcontractor or s upplier of m aterials or s ervices, t ransportation di fficulty, the e xistence of an y circumstance making per formance c ommercially impracticable or a ny ot her c ause b eyond t he p arty's r easonable c ontrol;

provided, however, that the obligation to make any payment due and owing under t his O rder shall n ot be e xcused f or a ny reason whatsoever. In t he event of a F orce Majeure ev ent S eller's s chedule s hall b e adj usted accordingly a nd the contract p rice shall b e a djusted to i nclude a ny additional costs, overhead and reasonable profit. 13. Wavier of Compliance; Severability. Waiver b y either p arty of a breach by the other of any provision of this Order shall not be deemed a full force a nd e ffect. Any part of this c ontract held t o be i nvalid or unenforceable s hall be de emed i neffective t o t he extent t hereof without affecting the validity or enforceability of any other part of this contact. 14. Governing Law. This Order shall be governed and construed under the laws of the State of Florida and of the United States of America. 15. Arbitration. Any controversy or claim arising ou t o f or relating to this Order or t he performance or breach hereof shall be s ettled in West Palm Beach, Florida by arbitration in accordance with the Rules of the American Arbitration A ssociation, and j udgment upo n t he a ward r endered b y t he Arbitrator(s) m ay b e entered i n any court h aving j urisdiction thereof. T he parties consent to the jurisdiction of the state and federal courts in Florida for all purposes in connection with such arbitration. The parties further consent that any process, notice of motion or other application to either of such courts or any judge thereof may be served by registered mail or personal s ervice outside t he S tate o f F lorida, pr ovided a reasonable t ime for a ppearance i s al lowed, o r i n s uch ot her m anner as m ay b e al lowed under the rules of such courts. 16. Assignment. Neither t his A greement n or an y associated O rder Acknowledgement m ay be a ssigned by t he P urchaser, o r i ts c ontents publicized by the Purchaser, without the written consent of Seller. Seller shall have the right to assign, transfer or sublicense all or any part of this Agreement or any associated Order Acknowledgement to another at any time and without the consent of Purchaser. 17. Miscellaneous. The v arious provisions of t his A greement an d a ny associated Order Acknowledgement are severable, and any determination of invalidity or unenforceability of any one provision hereof shall no bearing on the continuing force and ef fect of the remaining provisions hereof. This Agreement and any associated Order Acknowledgement and the terms and conditions c ontained h erein c onstitute t he en tire understanding of t he parties with respect to the purchase and sale of the Goods, and any prior agreements, with respect thereto, whether written or oral, are superseded hereby. This Agreement and any associated Order Acknowledgement shall be bi nding on t he pa rties an d t heir r espective s uccessors a nd a ny permitted assigns. 18. Electronic Data Interchange. The pa rties m ay e xecute a O rder Acknowledgement by t ransmitting and receiving the data contained i n the Order Acknowledgement el ectronically r ather than in paper f orm. T o provide t he legal validity and enforceability of such Order Acknowledgement, t he p arties f urther ag ree that t he dat a t ransmitted herein will be c onsidered " in w riting" and t o h ave b een " signed." T he parties ag ree not t o c ontest the v alidity or enforceability of a O rder Acknowledgement bec ause of t he e lectronic o rigination, t ransmission, storage or h andling of s uch O rder A cknowledgement. A ny computer printout of the d ata c ontained i n t he O rder Acknowledgement will b e considered an "original" when maintained in the ordinary course of business and will be admissible as between the parties to the same extent and under t he same conditions as other business records maintained in documentary f orm. T he p arties a gree t o p roperly use t hose s ecurity procedures which are reasonably sufficient to ensure that a transmission of the d ata c ontained i n a O rder A cknowledgement i s a uthorized and t o protect its business records and data from improper sources. 19. Export Restrictions. Buyer shall not export or re-export Goods in violation of any applicable laws o r regulations of the United States or the country in which Purchaser obtained them.


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