ENTERED - Welcome to NewMexico.gov Refinery - Gallup...2012/05/17 · SampType: MSD TestCode: EPA...
Transcript of ENTERED - Welcome to NewMexico.gov Refinery - Gallup...2012/05/17 · SampType: MSD TestCode: EPA...
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From: To: Cc: Subject: Date: Attachments:
Dear Kristen,
Larsen. Thurman VanHorn. Kristen. NMENV
Jc~ ENTERED
Chavez. Carl J. EMNRD; ~; Cobrajn. Dave. NMENV MPPE INmAL TEST RESULTS (5/8, 5/10, 5/11, 5/12, 5/13, 5/14) Thursday, May 17, 2012 11:46:38 AM Rot 1205459 vl.pdf Rot 1205563 vl.pdf Rpt 1205562 vl.pdf Rpt 1205591 vl.pdf Rpt 1205595 vl.pdf Rpt 1205592 vl.pdf
The MPPE began sending effluent wastewater to STP-1 at or about 1500 hrs on May 8, 2012. In
accordance with Comment 17 a, Western will be initially required to collect daily effluent samples to
submit to Hall Environmental Laboratories. The laboratory results and flow measurements will be
submitted via e-mail to both NMED and OCD as prescribed in accordance with Comment 17 f.
Effluent sample collection for MPPE wastewater going to STP-1 began on the evening of May 8. The
initial results of the analysis were recently received for May 8, 10, 11, 12, 13, and 14. The May 9
sample results will not be used because it was learned that the sample bottle was previously used
and contained a hydrochloric acid preservative. Western plans to collect one additional day of
samples in order to meet the 15 day sampling requirement.
Regards,
Beck Larsen
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May 17, 2012
Western Refining Southwest, GallupThurman B. Larsen
Dear Thurman B. Larsen:
RE: MPPE-1 OrderNo.: 1205459
FAX (505) 722-0210TEL: (505) 722-3833
Rt. 3 Box 7Gallup, NM 87301
Hall Environmental Analysis Laboratory4901 Hawkins NE
Albuquerque, NM 87109
Website: www.hallenvironmental.comTEL: 505-345-3975 FAX: 505-345-4107
Hall Environmental Analysis Laboratory received 1 sample(s) on 5/10/2012 for the analyses presented in the following report.
Andy Freeman
These were analyzed according to EPA procedures or equivalent. To access our accredited tests please go to www.hallenvironmental.com or the state specific web sites. See the sample checklist and/or the Chain of Custody for information regarding the sample receipt temperature and preservation. Data qualifiers or a narrative will be provided if the sample analysis or analytical quality control parameters require a flag. All samples are reported as received unless otherwise indicated.
Please don't hesitate to contact HEAL for any additional information or clarifications.
Sincerely,
Laboratory Manager4901 Hawkins NEAlbuquerque, NM 87109
http://www.hallenvironmental.comhttp://www.hallenvironmental.com
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Project: MPPE-1Client Sample ID: MPPE-1
Collection Date: 5/8/2012 5:00:00 PMMatrix: AQUEOUS
CLIENT: Western Refining Southwest, Gallup
Lab ID: 1205459-001
Date Reported: 5/17/2012
Analytical ReportLab Order 1205459
Analyses Result Qual Units Date AnalyzedDFRL
Hall Environmental Analysis Laboratory, Inc.
Received Date: 5/10/2012 8:00:00 AM
EPA METHOD 8015B: DIESEL RANGE Analyst: JMPDiesel Range Organics (DRO) 5/10/2012 4:22:31 PM1.0 mg/L 110Motor Oil Range Organics (MRO) 5/10/2012 4:22:31 PM5.0 mg/L 116 Surr: DNOP 5/10/2012 4:22:31 PM61.3-164 %REC 1120
EPA METHOD 8015B: GASOLINE RANGE Analyst: NSBGasoline Range Organics (GRO) 5/10/2012 11:43:43 AM0.25 mg/L 50.42 Surr: BFB 5/10/2012 11:43:43 AM69.3-120 %REC 5102
EPA METHOD 8021B: VOLATILES Analyst: NSBMethyl tert-butyl ether (MTBE) 5/10/2012 11:43:43 AM12 µg/L 5NDBenzene 5/10/2012 11:43:43 AM5.0 µg/L 5NDToluene 5/10/2012 11:43:43 AM5.0 µg/L 5NDEthylbenzene 5/10/2012 11:43:43 AM5.0 µg/L 5NDXylenes, Total 5/10/2012 11:43:43 AM10 µg/L 5ND Surr: 4-Bromofluorobenzene 5/10/2012 11:43:43 AM55-140 %REC 592.5
EPA METHOD 300.0: ANIONS Analyst: BRMFluoride * 5/11/2012 11:41:36 AM2.0 mg/L 2060Chloride 5/10/2012 10:40:46 PM25 mg/L 50430Nitrogen, Nitrite (As N) 5/10/2012 1:09:46 PM0.10 mg/L 1NDBromide 5/10/2012 1:09:46 PM0.10 mg/L 10.48Nitrogen, Nitrate (As N) 5/10/2012 1:09:46 PM0.10 mg/L 10.49Phosphorus, Orthophosphate (As P) 5/10/2012 1:09:46 PM0.50 mg/L 10.71Sulfate 5/10/2012 1:22:11 PM10 mg/L 20800
EPA METHOD 200.7: METALS Analyst: ELSCalcium 5/14/2012 8:20:36 AM1.0 mg/L 187Magnesium 5/14/2012 8:20:36 AM1.0 mg/L 121Potassium 5/14/2012 8:20:36 AM1.0 mg/L 162Sodium 5/14/2012 8:28:31 AM5.0 mg/L 5500
EPA 120.1: SPECIFIC CONDUCTANCE Analyst: DBDConductivity 5/10/2012 1:02:28 PM0.010 µmhos/cm 14,200
SM4500-H+B: PH Analyst: DBDpH H 5/10/2012 1:02:28 PM1.68 pH units 18.42
Qualifiers:
Page 1 of 9
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection LimitS Spike Recovery outside accepted recovery limits
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Project: MPPE-1Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205459WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID MB-1899
Batch ID: 1899
Analysis Date: 5/14/2012Prep Date: 5/11/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: PBW RunNo: 2742
SeqNo: 76144
MBLKSampType: TestCode: EPA Method 200.7: Metals
Calcium 1.0NDMagnesium 1.0NDPotassium 1.0NDSodium 1.0ND
Sample ID LCS-1899
Batch ID: 1899
Analysis Date: 5/14/2012Prep Date: 5/11/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: LCSW RunNo: 2742
SeqNo: 76145
LCSSampType: TestCode: EPA Method 200.7: Metals
Calcium 50.00 100 85 1151.0 050Magnesium 50.00 99.5 85 1151.0 050Potassium 50.00 95.4 85 1151.0 048Sodium 50.00 97.4 85 1151.0 049
Qualifiers:
Page 2 of 9
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
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Project: MPPE-1Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205459WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID MB
Batch ID: R2702
Analysis Date: 5/10/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: PBW RunNo: 2702
SeqNo: 75161
MBLKSampType: TestCode: EPA Method 300.0: Anions
Chloride 0.50NDNitrogen, Nitrite (As N) 0.10NDBromide 0.10NDNitrogen, Nitrate (As N) 0.10NDPhosphorus, Orthophosphate (As P 0.50NDSulfate 0.50ND
Sample ID LCS
Batch ID: R2702
Analysis Date: 5/10/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: LCSW RunNo: 2702
SeqNo: 75162
LCSSampType: TestCode: EPA Method 300.0: Anions
Chloride 5.000 94.1 90 1100.50 04.7Nitrogen, Nitrite (As N) 1.000 94.1 90 1100.10 00.94Bromide 2.500 95.9 90 1100.10 02.4Nitrogen, Nitrate (As N) 2.500 98.0 90 1100.10 02.5Phosphorus, Orthophosphate (As P 5.000 98.5 90 1100.50 04.9Sulfate 10.00 94.7 90 1100.50 09.5
Sample ID 1205476-001BMS
Batch ID: R2702
Analysis Date: 5/10/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2702
SeqNo: 75166
MSSampType: TestCode: EPA Method 300.0: Anions
Bromide 2.500 63.1 76 114 S0.10 01.6Sulfate 10.00 101 80.5 1190.50 27.2237
Sample ID 1205476-001BMSD
Batch ID: R2702
Analysis Date: 5/10/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2702
SeqNo: 75167
MSDSampType: TestCode: EPA Method 300.0: Anions
Bromide 2.500 65.3 76 114 20 S0.10 0 3.441.6Sulfate 10.00 103 80.5 119 200.50 27.22 0.61638
Sample ID MB
Batch ID: R2739
Analysis Date: 5/11/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: PBW RunNo: 2739
SeqNo: 76007
MBLKSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.10ND
Qualifiers:
Page 3 of 9
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
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Project: MPPE-1Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205459WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID LCS
Batch ID: R2739
Analysis Date: 5/11/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: LCSW RunNo: 2739
SeqNo: 76008
LCSSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.5000 97.8 90 1100.10 00.49
Sample ID 1205508-001BMS
Batch ID: R2739
Analysis Date: 5/11/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2739
SeqNo: 76012
MSSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.5000 105 72.9 1130.10 00.52
Sample ID 1205508-001BMSD
Batch ID: R2739
Analysis Date: 5/11/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2739
SeqNo: 76013
MSDSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.5000 102 72.9 113 200.10 0 2.820.51
Sample ID MB
Batch ID: R2739
Analysis Date: 5/11/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: PBW RunNo: 2739
SeqNo: 76061
MBLKSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.10ND
Sample ID LCS
Batch ID: R2739
Analysis Date: 5/11/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: LCSW RunNo: 2739
SeqNo: 76062
LCSSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.5000 104 90 1100.10 00.52
Sample ID 1205524-001AMS
Batch ID: R2739
Analysis Date: 5/11/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2739
SeqNo: 76068
MSSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.5000 95.0 72.9 1130.10 0.53671.0
Sample ID 1205524-001AMSD
Batch ID: R2739
Analysis Date: 5/12/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2739
SeqNo: 76069
MSDSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.5000 94.4 72.9 113 200.10 0.5367 0.3011.0
Qualifiers:
Page 4 of 9
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
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Project: MPPE-1Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205459WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID MB-1882
Batch ID: 1882
Analysis Date: 5/10/2012Prep Date: 5/10/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: PBW RunNo: 2674
SeqNo: 75054
MBLKSampType: TestCode: EPA Method 8015B: Diesel Range
Diesel Range Organics (DRO) 1.0NDMotor Oil Range Organics (MRO) 5.0ND Surr: DNOP 1.000 116 61.3 1641.2
Sample ID LCS-1882
Batch ID: 1882
Analysis Date: 5/10/2012Prep Date: 5/10/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: LCSW RunNo: 2674
SeqNo: 75055
LCSSampType: TestCode: EPA Method 8015B: Diesel Range
Diesel Range Organics (DRO) 5.000 93.5 74 1571.0 04.7 Surr: DNOP 0.5000 108 61.3 1640.54
Sample ID LCSD-1882
Batch ID: 1882
Analysis Date: 5/10/2012Prep Date: 5/10/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: LCSS02 RunNo: 2674
SeqNo: 75056
LCSDSampType: TestCode: EPA Method 8015B: Diesel Range
Diesel Range Organics (DRO) 5.000 96.9 74 157 231.0 0 3.584.8 Surr: DNOP 0.5000 113 61.3 164 000.57
Qualifiers:
Page 5 of 9
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
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Project: MPPE-1Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205459WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID 5ML RB
Batch ID: R2706
Analysis Date: 5/10/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: PBW RunNo: 2706
SeqNo: 75305
MBLKSampType: TestCode: EPA Method 8015B: Gasoline Range
Gasoline Range Organics (GRO) 0.050ND Surr: BFB 20.00 103 69.3 12021
Sample ID 2.5UG GRO LCS
Batch ID: R2706
Analysis Date: 5/10/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: LCSW RunNo: 2706
SeqNo: 75306
LCSSampType: TestCode: EPA Method 8015B: Gasoline Range
Gasoline Range Organics (GRO) 0.5000 95.2 101 123 S0.050 00.48 Surr: BFB 20.00 110 69.3 12022
Sample ID 1205459-001AMS
Batch ID: R2706
Analysis Date: 5/10/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: MPPE-1 RunNo: 2706
SeqNo: 75308
MSSampType: TestCode: EPA Method 8015B: Gasoline Range
Gasoline Range Organics (GRO) 2.500 103 75.4 1210.25 0.42003.0 Surr: BFB 100.0 112 69.3 120110
Sample ID 1205459-001AMSD
Batch ID: R2706
Analysis Date: 5/10/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: MPPE-1 RunNo: 2706
SeqNo: 75309
MSDSampType: TestCode: EPA Method 8015B: Gasoline Range
Gasoline Range Organics (GRO) 2.500 92.0 75.4 121 10.50.25 0.4200 9.522.7 Surr: BFB 100.0 111 69.3 120 00110
Qualifiers:
Page 6 of 9
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
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Project: MPPE-1Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205459WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID 5ML RB
Batch ID: R2706
Analysis Date: 5/10/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/L
PQL
Client ID: PBW RunNo: 2706
SeqNo: 75366
MBLKSampType: TestCode: EPA Method 8021B: Volatiles
Methyl tert-butyl ether (MTBE) 2.5NDBenzene 1.0NDToluene 1.0NDEthylbenzene 1.0NDXylenes, Total 2.0ND Surr: 4-Bromofluorobenzene 20.00 91.9 55 14018
Sample ID 100NG BTEX LCS
Batch ID: R2706
Analysis Date: 5/10/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/L
PQL
Client ID: LCSW RunNo: 2706
SeqNo: 75367
LCSSampType: TestCode: EPA Method 8021B: Volatiles
Methyl tert-butyl ether (MTBE) 20.00 94.3 50.5 1582.5 019Benzene 20.00 93.5 80 1201.0 019Toluene 20.00 96.2 80 1201.0 019Ethylbenzene 20.00 93.1 80 1201.0 019Xylenes, Total 60.00 92.3 80 1202.0 055 Surr: 4-Bromofluorobenzene 20.00 96.3 55 14019
Sample ID 1205459-001AMS
Batch ID: R2706
Analysis Date: 5/10/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/L
PQL
Client ID: MPPE-1 RunNo: 2706
SeqNo: 75369
MSSampType: TestCode: EPA Method 8021B: Volatiles
Methyl tert-butyl ether (MTBE) 100.0 102 58 13912 1.445100Benzene 100.0 95.9 70.1 1185.0 096Toluene 100.0 99.5 72.3 1175.0 0100Ethylbenzene 100.0 91.9 73.5 1175.0 0.597092Xylenes, Total 300.0 93.5 73.1 11910 3.165280 Surr: 4-Bromofluorobenzene 100.0 95.6 55 14096
Sample ID 1205459-001AMSD
Batch ID: R2706
Analysis Date: 5/10/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/L
PQL
Client ID: MPPE-1 RunNo: 2706
SeqNo: 75370
MSDSampType: TestCode: EPA Method 8021B: Volatiles
Methyl tert-butyl ether (MTBE) 100.0 99.3 58 139 15.212 1.445 2.35100Benzene 100.0 86.0 70.1 118 16.45.0 0 10.886Toluene 100.0 88.9 72.3 117 13.95.0 0 11.389Ethylbenzene 100.0 83.7 73.5 117 13.55.0 0.5970 9.2284Xylenes, Total 300.0 82.8 73.1 119 12.910 3.165 12.0250 Surr: 4-Bromofluorobenzene 100.0 97.1 55 140 0097
Qualifiers:
Page 7 of 9
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
Project: MPPE-1Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205459WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID 1205459-001BDUP
Batch ID: R2699
Analysis Date: 5/10/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: µmhos/cm
PQL
Client ID: MPPE-1 RunNo: 2699
SeqNo: 75151
DUPSampType: TestCode: EPA 120.1: Specific Conductance
Conductivity 200.010 0.3084,200
Qualifiers:
Page 8 of 9
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
Project: MPPE-1Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205459WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID 1205459-001BDUP
Batch ID: R2699
Analysis Date: 5/10/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: pH units
PQL
Client ID: MPPE-1 RunNo: 2699
SeqNo: 75108
DUPSampType: TestCode: SM4500-H+B: pH
pH H1.688.44
Qualifiers:
Page 9 of 9
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
May 17, 2012
Western Refining Southwest, GallupBeck Larsen
Dear Beck Larsen:
RE: MPPE-4 OrderNo.: 1205562
FAX (505) 722-0210TEL: (505) 722-0258
Rt. 3 Box 7Gallup, NM 87301
Hall Environmental Analysis Laboratory4901 Hawkins NE
Albuquerque, NM 87109
Website: www.hallenvironmental.comTEL: 505-345-3975 FAX: 505-345-4107
Hall Environmental Analysis Laboratory received 1 sample(s) on 5/12/2012 for the analyses presented in the following report.
Andy Freeman
These were analyzed according to EPA procedures or equivalent. To access our accredited tests please go to www.hallenvironmental.com or the state specific web sites. See the sample checklist and/or the Chain of Custody for information regarding the sample receipt temperature and preservation. Data qualifiers or a narrative will be provided if the sample analysis or analytical quality control parameters require a flag. All samples are reported as received unless otherwise indicated.
Please don't hesitate to contact HEAL for any additional information or clarifications.
Sincerely,
Laboratory Manager4901 Hawkins NEAlbuquerque, NM 87109
http://www.hallenvironmental.comhttp://www.hallenvironmental.com
-
Project: MPPE-4Client Sample ID: MPPE-4
Collection Date: 5/11/2012 3:55:00 PMMatrix: AQUEOUS
CLIENT: Western Refining Southwest, Gallup
Lab ID: 1205562-001
Date Reported: 5/17/2012
Analytical ReportLab Order 1205562
Analyses Result Qual Units Date AnalyzedDFRL
Hall Environmental Analysis Laboratory, Inc.
Received Date: 5/12/2012 11:30:00 AM
EPA METHOD 8015B: DIESEL RANGE Analyst: JMPDiesel Range Organics (DRO) 5/15/2012 9:44:42 AM1.0 mg/L 17.1 Surr: DNOP 5/15/2012 9:44:42 AM61.3-164 %REC 1125
EPA METHOD 8021B: VOLATILES Analyst: NSBMethyl tert-butyl ether (MTBE) 5/15/2012 12:35:23 AM12 µg/L 5NDBenzene 5/15/2012 1:42:28 PM5.0 µg/L 5NDToluene 5/15/2012 1:42:28 PM5.0 µg/L 5NDEthylbenzene 5/15/2012 1:42:28 PM5.0 µg/L 5NDXylenes, Total 5/15/2012 1:42:28 PM10 µg/L 5ND1,2,4-Trimethylbenzene 5/15/2012 1:42:28 PM5.0 µg/L 5ND1,3,5-Trimethylbenzene 5/15/2012 1:42:28 PM5.0 µg/L 5ND Surr: 4-Bromofluorobenzene 5/15/2012 1:42:28 PM55-140 %REC 597.3
EPA METHOD 300.0: ANIONS Analyst: SRMFluoride * 5/15/2012 2:19:31 PM5.0 mg/L 5080Chloride 5/16/2012 12:02:52 AM50 mg/L 100960Phosphorus, Orthophosphate (As P) H 5/14/2012 3:11:55 PM2.5 mg/L 5NDSulfate 5/15/2012 2:19:31 PM25 mg/L 50870Nitrate+Nitrite as N 5/14/2012 5:37:53 PM1.0 mg/L 5ND
EPA METHOD 200.7: METALS Analyst: ELSCalcium 5/16/2012 6:48:55 AM1.0 mg/L 190Magnesium 5/16/2012 6:48:55 AM1.0 mg/L 128Potassium 5/16/2012 6:48:55 AM1.0 mg/L 169Sodium 5/16/2012 7:29:16 AM10 mg/L 10890
EPA 120.1: SPECIFIC CONDUCTANCE Analyst: DBDConductivity 5/14/2012 9:25:14 PM0.010 µmhos/cm 15,900
SM4500-H+B: PH Analyst: DBDpH H 5/14/2012 9:25:14 PM1.68 pH units 18.40
Qualifiers:
Page 1 of 9
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection LimitS Spike Recovery outside accepted recovery limits
-
Project: MPPE-4Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205562WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID MB-1934
Batch ID: 1934
Analysis Date: 5/16/2012Prep Date: 5/15/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: PBW RunNo: 2797
SeqNo: 77728
MBLKSampType: TestCode: EPA Method 200.7: Metals
Calcium 1.0NDMagnesium 1.0NDPotassium 1.0NDSodium 1.0ND
Sample ID LCS-1934
Batch ID: 1934
Analysis Date: 5/16/2012Prep Date: 5/15/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: LCSW RunNo: 2797
SeqNo: 77729
LCSSampType: TestCode: EPA Method 200.7: Metals
Calcium 50.00 102 85 1151.0 051Magnesium 50.00 101 85 1151.0 050Potassium 50.00 98.1 85 1151.0 049Sodium 50.00 99.5 85 1151.0 050
Sample ID 1205563-001DMS
Batch ID: 1934
Analysis Date: 5/16/2012Prep Date: 5/15/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2797
SeqNo: 77734
MSSampType: TestCode: EPA Method 200.7: Metals
Calcium 50.00 82.9 70 1305.0 336.8380Magnesium 50.00 96.7 70 1305.0 77.99130Potassium 50.00 94.6 70 1305.0 51.0098
Sample ID 1205563-001DMSD
Batch ID: 1934
Analysis Date: 5/16/2012Prep Date: 5/15/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2797
SeqNo: 77735
MSDSampType: TestCode: EPA Method 200.7: Metals
Calcium 50.00 85.6 70 130 205.0 336.8 0.354380Magnesium 50.00 96.4 70 130 205.0 77.99 0.154130Potassium 50.00 93.8 70 130 205.0 51.00 0.43398
Qualifiers:
Page 2 of 9
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
Project: MPPE-4Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205562WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID MB
Batch ID: R2765
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: PBW RunNo: 2765
SeqNo: 76616
MBLKSampType: TestCode: EPA Method 300.0: Anions
Phosphorus, Orthophosphate (As P 0.50NDNitrate+Nitrite as N 0.20ND
Sample ID LCS
Batch ID: R2765
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: LCSW RunNo: 2765
SeqNo: 76617
LCSSampType: TestCode: EPA Method 300.0: Anions
Phosphorus, Orthophosphate (As P 5.000 97.0 90 1100.50 04.9Nitrate+Nitrite as N 3.500 95.7 90 1100.20 03.3
Sample ID 1205583-003AMS
Batch ID: R2765
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2765
SeqNo: 76623
MSSampType: TestCode: EPA Method 300.0: Anions
Nitrate+Nitrite as N 3.500 102 83.9 1120.20 03.6
Sample ID 1205583-003AMSD
Batch ID: R2765
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2765
SeqNo: 76624
MSDSampType: TestCode: EPA Method 300.0: Anions
Nitrate+Nitrite as N 3.500 90.6 83.9 112 200.20 0 11.43.2
Sample ID MB
Batch ID: R2795
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: PBW RunNo: 2795
SeqNo: 77644
MBLKSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.10NDChloride 0.50NDSulfate 0.50ND
Sample ID LCS
Batch ID: R2795
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: LCSW RunNo: 2795
SeqNo: 77645
LCSSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.5000 96.4 90 1100.10 00.48Chloride 5.000 98.5 90 1100.50 04.9Sulfate 10.00 99.1 90 1100.50 09.9
Qualifiers:
Page 3 of 9
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
Project: MPPE-4Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205562WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID 1205624-002AMS
Batch ID: R2795
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2795
SeqNo: 77649
MSSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.5000 85.4 72.9 1130.10 1.7192.1Sulfate 10.00 105 80.5 1190.50 37.4048
Sample ID 1205624-002AMSD
Batch ID: R2795
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2795
SeqNo: 77650
MSDSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.5000 84.7 72.9 113 200.10 1.719 0.1652.1Sulfate 10.00 102 80.5 119 200.50 37.40 0.53448
Sample ID 1205631-001AMS
Batch ID: R2795
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2795
SeqNo: 77681
MSSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.5000 85.3 72.9 1130.10 1.5622.0Sulfate 10.00 103 80.5 1190.50 30.1640
Sample ID 1205631-001AMSD
Batch ID: R2795
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2795
SeqNo: 77682
MSDSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.5000 87.6 72.9 113 200.10 1.562 0.5762.0Sulfate 10.00 103 80.5 119 200.50 30.16 0.16240
Qualifiers:
Page 4 of 9
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
Project: MPPE-4Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205562WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID MB-1936
Batch ID: 1936
Analysis Date: 5/15/2012Prep Date: 5/15/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: PBW RunNo: 2758
SeqNo: 76513
MBLKSampType: TestCode: EPA Method 8015B: Diesel Range
Diesel Range Organics (DRO) 1.0ND Surr: DNOP 1.000 116 61.3 1641.2
Sample ID LCS-1936
Batch ID: 1936
Analysis Date: 5/15/2012Prep Date: 5/15/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: LCSW RunNo: 2758
SeqNo: 76834
LCSSampType: TestCode: EPA Method 8015B: Diesel Range
Diesel Range Organics (DRO) 5.000 96.5 74 1571.0 04.8 Surr: DNOP 0.5000 97.7 61.3 1640.49
Sample ID LCSD-1936
Batch ID: 1936
Analysis Date: 5/15/2012Prep Date: 5/15/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: LCSS02 RunNo: 2758
SeqNo: 76835
LCSDSampType: TestCode: EPA Method 8015B: Diesel Range
Diesel Range Organics (DRO) 5.000 88.7 74 157 231.0 0 8.414.4 Surr: DNOP 0.5000 103 61.3 164 000.52
Qualifiers:
Page 5 of 9
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
Project: MPPE-4Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205562WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID 5ML-RB
Batch ID: R2774
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/L
PQL
Client ID: PBW RunNo: 2774
SeqNo: 77103
MBLKSampType: TestCode: EPA Method 8021B: Volatiles
Methyl tert-butyl ether (MTBE) 2.5ND Surr: 4-Bromofluorobenzene 20.00 90.0 55 14018
Sample ID 100NG BTEX LCS
Batch ID: R2774
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/L
PQL
Client ID: LCSW RunNo: 2774
SeqNo: 77104
LCSSampType: TestCode: EPA Method 8021B: Volatiles
Methyl tert-butyl ether (MTBE) 20.00 98.2 50.5 1582.5 020 Surr: 4-Bromofluorobenzene 20.00 92.3 55 14018
Sample ID 1205559-001A MS
Batch ID: R2774
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/L
PQL
Client ID: BatchQC RunNo: 2774
SeqNo: 77112
MSSampType: TestCode: EPA Method 8021B: Volatiles
Methyl tert-butyl ether (MTBE) 20.00 97.9 58 1392.5 0.176020 Surr: 4-Bromofluorobenzene 20.00 108 55 14022
Sample ID 1205559-001A MSD
Batch ID: R2774
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/L
PQL
Client ID: BatchQC RunNo: 2774
SeqNo: 77113
MSDSampType: TestCode: EPA Method 8021B: Volatiles
Methyl tert-butyl ether (MTBE) 20.00 97.3 58 139 15.22.5 0.1760 0.65020 Surr: 4-Bromofluorobenzene 20.00 100 55 140 0020
Sample ID 5ML RB
Batch ID: R2805
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/L
PQL
Client ID: PBW RunNo: 2805
SeqNo: 77914
MBLKSampType: TestCode: EPA Method 8021B: Volatiles
Benzene 1.0NDToluene 1.0NDEthylbenzene 1.0NDXylenes, Total 2.0ND1,2,4-Trimethylbenzene 1.0ND1,3,5-Trimethylbenzene 1.0ND Surr: 4-Bromofluorobenzene 20.00 93.2 55 14019
Qualifiers:
Page 6 of 9
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
Project: MPPE-4Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205562WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID 100NG BTEX LCS
Batch ID: R2805
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/L
PQL
Client ID: LCSW RunNo: 2805
SeqNo: 77915
LCSSampType: TestCode: EPA Method 8021B: Volatiles
Benzene 20.00 101 80 1201.0 020Toluene 20.00 104 80 1201.0 021Ethylbenzene 20.00 102 80 1201.0 020Xylenes, Total 60.00 103 80 1202.0 0621,2,4-Trimethylbenzene 20.00 93.6 80 1201.0 0191,3,5-Trimethylbenzene 20.00 98.6 80 1201.0 020 Surr: 4-Bromofluorobenzene 20.00 104 55 14021
Qualifiers:
Page 7 of 9
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
Project: MPPE-4Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205562WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID 1205508-001B
Batch ID: R2760
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: µmhos/cm
PQL
Client ID: BatchQC RunNo: 2760
SeqNo: 76802
DUPSampType: TestCode: EPA 120.1: Specific Conductance
Conductivity 200.010 0.1471,400
Sample ID 1205514-001B
Batch ID: R2760
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: µmhos/cm
PQL
Client ID: BatchQC RunNo: 2760
SeqNo: 76818
DUPSampType: TestCode: EPA 120.1: Specific Conductance
Conductivity 200.010 1.485,700
Qualifiers:
Page 8 of 9
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
Project: MPPE-4Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205562WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID 1205508-001B
Batch ID: R2760
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: pH units
PQL
Client ID: BatchQC RunNo: 2760
SeqNo: 76756
DUPSampType: TestCode: SM4500-H+B: pH
pH H1.68 0.1437.02
Sample ID 1205514-001B
Batch ID: R2760
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: pH units
PQL
Client ID: BatchQC RunNo: 2760
SeqNo: 76767
DUPSampType: TestCode: SM4500-H+B: pH
pH H1.68 0.6517.66
Qualifiers:
Page 9 of 9
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
May 17, 2012
Western Refining Southwest, GallupBeck Larsen
Dear Beck Larsen:
RE: MPPE-3 OrderNo.: 1205563
FAX (505) 722-0210TEL: (505) 722-0258
Rt. 3 Box 7Gallup, NM 87301
Hall Environmental Analysis Laboratory4901 Hawkins NE
Albuquerque, NM 87109
Website: www.hallenvironmental.comTEL: 505-345-3975 FAX: 505-345-4107
Hall Environmental Analysis Laboratory received 1 sample(s) on 5/12/2012 for the analyses presented in the following report.
Andy Freeman
These were analyzed according to EPA procedures or equivalent. To access our accredited tests please go to www.hallenvironmental.com or the state specific web sites. See the sample checklist and/or the Chain of Custody for information regarding the sample receipt temperature and preservation. Data qualifiers or a narrative will be provided if the sample analysis or analytical quality control parameters require a flag. All samples are reported as received unless otherwise indicated.
Please don't hesitate to contact HEAL for any additional information or clarifications.
Sincerely,
Laboratory Manager4901 Hawkins NEAlbuquerque, NM 87109
http://www.hallenvironmental.comhttp://www.hallenvironmental.com
-
Project: MPPE-3Client Sample ID: MPPE-3
Collection Date: 5/10/2012 8:00:00 PMMatrix: AQUEOUS
CLIENT: Western Refining Southwest, Gallup
Lab ID: 1205563-001
Date Reported: 5/17/2012
Analytical ReportLab Order 1205563
Analyses Result Qual Units Date AnalyzedDFRL
Hall Environmental Analysis Laboratory, Inc.
Received Date: 5/12/2012 11:30:00 AM
EPA METHOD 8015B: DIESEL RANGE Analyst: JMPDiesel Range Organics (DRO) 5/15/2012 10:06:08 AM1.0 mg/L 17.1 Surr: DNOP 5/15/2012 10:06:08 AM61.3-164 %REC 1127
EPA METHOD 8021B: VOLATILES Analyst: NSBMethyl tert-butyl ether (MTBE) 5/15/2012 1:06:11 AM12 µg/L 5NDBenzene 5/15/2012 1:06:11 AM5.0 µg/L 5NDToluene 5/15/2012 2:13:02 PM5.0 µg/L 511Ethylbenzene 5/15/2012 1:06:11 AM5.0 µg/L 5NDXylenes, Total 5/15/2012 1:06:11 AM10 µg/L 5ND1,2,4-Trimethylbenzene 5/15/2012 1:06:11 AM5.0 µg/L 5ND1,3,5-Trimethylbenzene 5/15/2012 1:06:11 AM5.0 µg/L 5ND Surr: 4-Bromofluorobenzene 5/15/2012 1:06:11 AM55-140 %REC 5100
EPA METHOD 300.0: ANIONS Analyst: SRMFluoride * 5/15/2012 2:56:45 PM2.0 mg/L 2025Chloride 5/15/2012 3:21:35 PM250 mg/L 5003,700Phosphorus, Orthophosphate (As P) H 5/14/2012 3:34:22 PM2.5 mg/L 5NDSulfate 5/15/2012 3:09:10 PM25 mg/L 501,100Nitrate+Nitrite as N 5/14/2012 5:49:07 PM1.0 mg/L 5ND
EPA METHOD 200.7: METALS Analyst: ELSCalcium 5/16/2012 6:37:16 AM5.0 mg/L 5340Magnesium 5/16/2012 6:37:16 AM5.0 mg/L 578Potassium 5/16/2012 6:37:16 AM5.0 mg/L 551Sodium 5/16/2012 7:26:01 AM20 mg/L 201,700
EPA 120.1: SPECIFIC CONDUCTANCE Analyst: DBDConductivity 5/15/2012 11:30:13 AM0.050 µmhos/cm 514,000
SM4500-H+B: PH Analyst: DBDpH H 5/14/2012 9:29:21 PM1.68 pH units 18.46
Qualifiers:
Page 1 of 9
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection LimitS Spike Recovery outside accepted recovery limits
-
Project: MPPE-3Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205563WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID MB-1934
Batch ID: 1934
Analysis Date: 5/16/2012Prep Date: 5/15/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: PBW RunNo: 2797
SeqNo: 77728
MBLKSampType: TestCode: EPA Method 200.7: Metals
Calcium 1.0NDMagnesium 1.0NDPotassium 1.0NDSodium 1.0ND
Sample ID LCS-1934
Batch ID: 1934
Analysis Date: 5/16/2012Prep Date: 5/15/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: LCSW RunNo: 2797
SeqNo: 77729
LCSSampType: TestCode: EPA Method 200.7: Metals
Calcium 50.00 102 85 1151.0 051Magnesium 50.00 101 85 1151.0 050Potassium 50.00 98.1 85 1151.0 049Sodium 50.00 99.5 85 1151.0 050
Sample ID 1205563-001DMS
Batch ID: 1934
Analysis Date: 5/16/2012Prep Date: 5/15/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: MPPE-3 RunNo: 2797
SeqNo: 77734
MSSampType: TestCode: EPA Method 200.7: Metals
Calcium 50.00 82.9 70 1305.0 336.8380Magnesium 50.00 96.7 70 1305.0 77.99130Potassium 50.00 94.6 70 1305.0 51.0098
Sample ID 1205563-001DMSD
Batch ID: 1934
Analysis Date: 5/16/2012Prep Date: 5/15/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: MPPE-3 RunNo: 2797
SeqNo: 77735
MSDSampType: TestCode: EPA Method 200.7: Metals
Calcium 50.00 85.6 70 130 205.0 336.8 0.354380Magnesium 50.00 96.4 70 130 205.0 77.99 0.154130Potassium 50.00 93.8 70 130 205.0 51.00 0.43398
Qualifiers:
Page 2 of 9
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
Project: MPPE-3Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205563WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID MB
Batch ID: R2765
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: PBW RunNo: 2765
SeqNo: 76616
MBLKSampType: TestCode: EPA Method 300.0: Anions
Phosphorus, Orthophosphate (As P 0.50NDNitrate+Nitrite as N 0.20ND
Sample ID LCS
Batch ID: R2765
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: LCSW RunNo: 2765
SeqNo: 76617
LCSSampType: TestCode: EPA Method 300.0: Anions
Phosphorus, Orthophosphate (As P 5.000 97.0 90 1100.50 04.9Nitrate+Nitrite as N 3.500 95.7 90 1100.20 03.3
Sample ID 1205583-003AMS
Batch ID: R2765
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2765
SeqNo: 76623
MSSampType: TestCode: EPA Method 300.0: Anions
Nitrate+Nitrite as N 3.500 102 83.9 1120.20 03.6
Sample ID 1205583-003AMSD
Batch ID: R2765
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2765
SeqNo: 76624
MSDSampType: TestCode: EPA Method 300.0: Anions
Nitrate+Nitrite as N 3.500 90.6 83.9 112 200.20 0 11.43.2
Sample ID MB
Batch ID: R2795
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: PBW RunNo: 2795
SeqNo: 77644
MBLKSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.10NDChloride 0.50NDSulfate 0.50ND
Sample ID LCS
Batch ID: R2795
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: LCSW RunNo: 2795
SeqNo: 77645
LCSSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.5000 96.4 90 1100.10 00.48Chloride 5.000 98.5 90 1100.50 04.9Sulfate 10.00 99.1 90 1100.50 09.9
Qualifiers:
Page 3 of 9
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
Project: MPPE-3Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205563WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID 1205624-002AMS
Batch ID: R2795
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2795
SeqNo: 77649
MSSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.5000 85.4 72.9 1130.10 1.7192.1Sulfate 10.00 105 80.5 1190.50 37.4048
Sample ID 1205624-002AMSD
Batch ID: R2795
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2795
SeqNo: 77650
MSDSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.5000 84.7 72.9 113 200.10 1.719 0.1652.1Sulfate 10.00 102 80.5 119 200.50 37.40 0.53448
Sample ID 1205631-001AMS
Batch ID: R2795
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2795
SeqNo: 77681
MSSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.5000 85.3 72.9 1130.10 1.5622.0Sulfate 10.00 103 80.5 1190.50 30.1640
Sample ID 1205631-001AMSD
Batch ID: R2795
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2795
SeqNo: 77682
MSDSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.5000 87.6 72.9 113 200.10 1.562 0.5762.0Sulfate 10.00 103 80.5 119 200.50 30.16 0.16240
Qualifiers:
Page 4 of 9
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
Project: MPPE-3Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205563WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID MB-1936
Batch ID: 1936
Analysis Date: 5/15/2012Prep Date: 5/15/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: PBW RunNo: 2758
SeqNo: 76513
MBLKSampType: TestCode: EPA Method 8015B: Diesel Range
Diesel Range Organics (DRO) 1.0ND Surr: DNOP 1.000 116 61.3 1641.2
Sample ID LCS-1936
Batch ID: 1936
Analysis Date: 5/15/2012Prep Date: 5/15/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: LCSW RunNo: 2758
SeqNo: 76834
LCSSampType: TestCode: EPA Method 8015B: Diesel Range
Diesel Range Organics (DRO) 5.000 96.5 74 1571.0 04.8 Surr: DNOP 0.5000 97.7 61.3 1640.49
Sample ID LCSD-1936
Batch ID: 1936
Analysis Date: 5/15/2012Prep Date: 5/15/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: LCSS02 RunNo: 2758
SeqNo: 76835
LCSDSampType: TestCode: EPA Method 8015B: Diesel Range
Diesel Range Organics (DRO) 5.000 88.7 74 157 231.0 0 8.414.4 Surr: DNOP 0.5000 103 61.3 164 000.52
Qualifiers:
Page 5 of 9
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
Project: MPPE-3Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205563WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID 5ML-RB
Batch ID: R2774
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/L
PQL
Client ID: PBW RunNo: 2774
SeqNo: 77103
MBLKSampType: TestCode: EPA Method 8021B: Volatiles
Methyl tert-butyl ether (MTBE) 2.5NDBenzene 1.0NDEthylbenzene 1.0NDXylenes, Total 2.0ND1,2,4-Trimethylbenzene 1.0ND1,3,5-Trimethylbenzene 1.0ND Surr: 4-Bromofluorobenzene 20.00 90.0 55 14018
Sample ID 100NG BTEX LCS
Batch ID: R2774
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/L
PQL
Client ID: LCSW RunNo: 2774
SeqNo: 77104
LCSSampType: TestCode: EPA Method 8021B: Volatiles
Methyl tert-butyl ether (MTBE) 20.00 98.2 50.5 1582.5 020Benzene 20.00 101 80 1201.0 020Ethylbenzene 20.00 100 80 1201.0 020Xylenes, Total 60.00 102 80 1202.0 0611,2,4-Trimethylbenzene 20.00 89.3 80 1201.0 0181,3,5-Trimethylbenzene 20.00 96.1 80 1201.0 019 Surr: 4-Bromofluorobenzene 20.00 92.3 55 14018
Sample ID 1205559-001A MS
Batch ID: R2774
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/L
PQL
Client ID: BatchQC RunNo: 2774
SeqNo: 77112
MSSampType: TestCode: EPA Method 8021B: Volatiles
Methyl tert-butyl ether (MTBE) 20.00 97.9 58 1392.5 0.176020Benzene 20.00 105 70.1 1181.0 021Ethylbenzene 20.00 104 73.5 1171.0 021Xylenes, Total 60.00 105 73.1 1192.0 0631,2,4-Trimethylbenzene 20.00 96.7 65.8 1211.0 0.4080201,3,5-Trimethylbenzene 20.00 104 71.1 1181.0 021 Surr: 4-Bromofluorobenzene 20.00 108 55 14022
Sample ID 1205559-001A MSD
Batch ID: R2774
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/L
PQL
Client ID: BatchQC RunNo: 2774
SeqNo: 77113
MSDSampType: TestCode: EPA Method 8021B: Volatiles
Methyl tert-butyl ether (MTBE) 20.00 97.3 58 139 15.22.5 0.1760 0.65020Benzene 20.00 101 70.1 118 16.41.0 0 4.4520Ethylbenzene 20.00 98.6 73.5 117 13.51.0 0 5.4420
Qualifiers:
Page 6 of 9
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
Project: MPPE-3Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205563WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID 1205559-001A MSD
Batch ID: R2774
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/L
PQL
Client ID: BatchQC RunNo: 2774
SeqNo: 77113
MSDSampType: TestCode: EPA Method 8021B: Volatiles
Xylenes, Total 60.00 99.9 73.1 119 12.92.0 0 5.23601,2,4-Trimethylbenzene 20.00 92.4 65.8 121 13.51.0 0.4080 4.42191,3,5-Trimethylbenzene 20.00 99.2 71.1 118 13.71.0 0 4.2620 Surr: 4-Bromofluorobenzene 20.00 100 55 140 0020
Sample ID 5ML RB
Batch ID: R2805
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/L
PQL
Client ID: PBW RunNo: 2805
SeqNo: 77914
MBLKSampType: TestCode: EPA Method 8021B: Volatiles
Toluene 1.0ND Surr: 4-Bromofluorobenzene 20.00 93.2 55 14019
Sample ID 100NG BTEX LCS
Batch ID: R2805
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/L
PQL
Client ID: LCSW RunNo: 2805
SeqNo: 77915
LCSSampType: TestCode: EPA Method 8021B: Volatiles
Toluene 20.00 104 80 1201.0 021 Surr: 4-Bromofluorobenzene 20.00 104 55 14021
Qualifiers:
Page 7 of 9
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
Project: MPPE-3Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205563WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID 1205591-001C
Batch ID: R2782
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: µmhos/cm
PQL
Client ID: BatchQC RunNo: 2782
SeqNo: 77366
DUPSampType: TestCode: EPA 120.1: Specific Conductance
Conductivity 200.010 0.8804,900
Qualifiers:
Page 8 of 9
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
Project: MPPE-3Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205563WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID 1205508-001B
Batch ID: R2760
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: pH units
PQL
Client ID: BatchQC RunNo: 2760
SeqNo: 76756
DUPSampType: TestCode: SM4500-H+B: pH
pH H1.68 0.1437.02
Sample ID 1205514-001B
Batch ID: R2760
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: pH units
PQL
Client ID: BatchQC RunNo: 2760
SeqNo: 76767
DUPSampType: TestCode: SM4500-H+B: pH
pH H1.68 0.6517.66
Qualifiers:
Page 9 of 9
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
May 17, 2012
Western Refining Southwest, GallupBeck Larsen
Dear Beck Larsen:
RE: MPPE-5 OrderNo.: 1205591
FAX (505) 722-0210TEL: (505) 722-0258
Rt. 3 Box 7Gallup, NM 87301
Hall Environmental Analysis Laboratory4901 Hawkins NE
Albuquerque, NM 87109
Website: www.hallenvironmental.comTEL: 505-345-3975 FAX: 505-345-4107
Hall Environmental Analysis Laboratory received 1 sample(s) on 5/14/2012 for the analyses presented in the following report.
Andy Freeman
These were analyzed according to EPA procedures or equivalent. To access our accredited tests please go to www.hallenvironmental.com or the state specific web sites. See the sample checklist and/or the Chain of Custody for information regarding the sample receipt temperature and preservation. Data qualifiers or a narrative will be provided if the sample analysis or analytical quality control parameters require a flag. All samples are reported as received unless otherwise indicated.
Please don't hesitate to contact HEAL for any additional information or clarifications.
Sincerely,
Laboratory Manager4901 Hawkins NEAlbuquerque, NM 87109
http://www.hallenvironmental.comhttp://www.hallenvironmental.com
-
Project: MPPE-5Client Sample ID: MPPE-5
Collection Date: 5/12/2012 8:00:00 AMMatrix: AQUEOUS
CLIENT: Western Refining Southwest, Gallup
Lab ID: 1205591-001
Date Reported: 5/17/2012
Analytical ReportLab Order 1205591
Analyses Result Qual Units Date AnalyzedDFRL
Hall Environmental Analysis Laboratory, Inc.
Received Date: 5/14/2012 1:39:00 PM
EPA METHOD 8015B: DIESEL RANGE Analyst: JMPDiesel Range Organics (DRO) 5/15/2012 10:27:49 AM1.0 mg/L 18.2Motor Oil Range Organics (MRO) 5/15/2012 10:27:49 AM5.0 mg/L 1ND Surr: DNOP 5/15/2012 10:27:49 AM61.3-164 %REC 1125
EPA METHOD 8015B: GASOLINE RANGE Analyst: NSBGasoline Range Organics (GRO) 5/14/2012 5:55:43 PM0.25 mg/L 50.97 Surr: BFB 5/14/2012 5:55:43 PM69.3-120 %REC 594.7
EPA METHOD 8021B: VOLATILES Analyst: NSBMethyl tert-butyl ether (MTBE) 5/14/2012 5:55:43 PM12 µg/L 5NDBenzene 5/14/2012 5:55:43 PM5.0 µg/L 5NDToluene 5/14/2012 5:55:43 PM5.0 µg/L 515Ethylbenzene 5/14/2012 5:55:43 PM5.0 µg/L 5NDXylenes, Total 5/14/2012 5:55:43 PM10 µg/L 5ND1,2,4-Trimethylbenzene 5/14/2012 5:55:43 PM5.0 µg/L 5ND1,3,5-Trimethylbenzene 5/14/2012 5:55:43 PM5.0 µg/L 5ND Surr: 4-Bromofluorobenzene 5/14/2012 5:55:43 PM55-140 %REC 597.3
EPA METHOD 300.0: ANIONS Analyst: SRMFluoride * 5/15/2012 7:54:37 PM10 mg/L 10015Chloride 5/14/2012 8:28:11 PM25 mg/L 50480Phosphorus, Orthophosphate (As P) H 5/14/2012 4:57:07 PM2.5 mg/L 5NDSulfate 5/14/2012 5:09:32 PM10 mg/L 20790Nitrate+Nitrite as N 5/15/2012 1:17:29 PM1.0 mg/L 5ND
EPA METHOD 200.7: METALS Analyst: ELSCalcium 5/16/2012 7:04:39 AM1.0 mg/L 182Magnesium 5/16/2012 7:04:39 AM1.0 mg/L 122Potassium 5/16/2012 7:04:39 AM1.0 mg/L 150Sodium 5/16/2012 7:32:33 AM10 mg/L 10580
EPA 120.1: SPECIFIC CONDUCTANCE Analyst: DBDConductivity 5/15/2012 11:34:20 AM0.010 µmhos/cm 14,900
SM4500-H+B: PH Analyst: DBDpH H 5/15/2012 11:34:20 AM1.68 pH units 18.01
Qualifiers:
Page 1 of 1
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection LimitS Spike Recovery outside accepted recovery limits
-
Project: MPPE-5Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205591WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID MB-1934
Batch ID: 1934
Analysis Date: 5/16/2012Prep Date: 5/15/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: PBW RunNo: 2797
SeqNo: 77728
MBLKSampType: TestCode: EPA Method 200.7: Metals
Calcium 1.0NDMagnesium 1.0NDPotassium 1.0NDSodium 1.0ND
Sample ID LCS-1934
Batch ID: 1934
Analysis Date: 5/16/2012Prep Date: 5/15/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: LCSW RunNo: 2797
SeqNo: 77729
LCSSampType: TestCode: EPA Method 200.7: Metals
Calcium 50.00 102 85 1151.0 051Magnesium 50.00 101 85 1151.0 050Potassium 50.00 98.1 85 1151.0 049Sodium 50.00 99.5 85 1151.0 050
Sample ID 1205563-001DMS
Batch ID: 1934
Analysis Date: 5/16/2012Prep Date: 5/15/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2797
SeqNo: 77734
MSSampType: TestCode: EPA Method 200.7: Metals
Calcium 50.00 82.9 70 1305.0 336.8380Magnesium 50.00 96.7 70 1305.0 77.99130Potassium 50.00 94.6 70 1305.0 51.0098
Sample ID 1205563-001DMSD
Batch ID: 1934
Analysis Date: 5/16/2012Prep Date: 5/15/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2797
SeqNo: 77735
MSDSampType: TestCode: EPA Method 200.7: Metals
Calcium 50.00 85.6 70 130 205.0 336.8 0.354380Magnesium 50.00 96.4 70 130 205.0 77.99 0.154130Potassium 50.00 93.8 70 130 205.0 51.00 0.43398
Qualifiers:
Page 2 of 1
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
Project: MPPE-5Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205591WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID MB
Batch ID: R2759
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: PBW RunNo: 2759
SeqNo: 76514
MBLKSampType: TestCode: EPA Method 300.0: Anions
Chloride 0.50NDPhosphorus, Orthophosphate (As P 0.50NDSulfate 0.50ND
Sample ID LCS
Batch ID: R2759
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: LCSW RunNo: 2759
SeqNo: 76515
LCSSampType: TestCode: EPA Method 300.0: Anions
Chloride 5.000 95.5 90 1100.50 04.8Phosphorus, Orthophosphate (As P 5.000 101 90 1100.50 05.0Sulfate 10.00 96.5 90 1100.50 09.6
Sample ID 1205594-001BMS
Batch ID: R2759
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2759
SeqNo: 76517
MSSampType: TestCode: EPA Method 300.0: Anions
Phosphorus, Orthophosphate (As P 5.000 99.0 79.3 1080.50 04.9
Sample ID 1205594-001BMSD
Batch ID: R2759
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2759
SeqNo: 76518
MSDSampType: TestCode: EPA Method 300.0: Anions
Phosphorus, Orthophosphate (As P 5.000 101 79.3 108 200.50 0 1.715.0
Sample ID MB
Batch ID: R2795
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: PBW RunNo: 2795
SeqNo: 77644
MBLKSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.10NDNitrate+Nitrite as N 0.20ND
Sample ID LCS
Batch ID: R2795
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: LCSW RunNo: 2795
SeqNo: 77645
LCSSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.5000 96.4 90 1100.10 00.48Nitrate+Nitrite as N 3.500 100 90 1100.20 03.5
Qualifiers:
Page 3 of 1
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
Project: MPPE-5Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205591WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID 1205624-002AMS
Batch ID: R2795
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2795
SeqNo: 77649
MSSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.5000 85.4 72.9 1130.10 1.7192.1Nitrate+Nitrite as N 3.500 98.9 83.9 1120.20 0.54934.0
Sample ID 1205624-002AMSD
Batch ID: R2795
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2795
SeqNo: 77650
MSDSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.5000 84.7 72.9 113 200.10 1.719 0.1652.1Nitrate+Nitrite as N 3.500 96.2 83.9 112 200.20 0.5493 2.403.9
Sample ID 1205631-001AMS
Batch ID: R2795
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2795
SeqNo: 77681
MSSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.5000 85.3 72.9 1130.10 1.5622.0Nitrate+Nitrite as N 3.500 98.5 83.9 1120.20 2.4075.9
Sample ID 1205631-001AMSD
Batch ID: R2795
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2795
SeqNo: 77682
MSDSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.5000 87.6 72.9 113 200.10 1.562 0.5762.0Nitrate+Nitrite as N 3.500 98.8 83.9 112 200.20 2.407 0.1975.9
Qualifiers:
Page 4 of 1
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
Project: MPPE-5Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205591WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID MB-1936
Batch ID: 1936
Analysis Date: 5/15/2012Prep Date: 5/15/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: PBW RunNo: 2758
SeqNo: 76513
MBLKSampType: TestCode: EPA Method 8015B: Diesel Range
Diesel Range Organics (DRO) 1.0NDMotor Oil Range Organics (MRO) 5.0ND Surr: DNOP 1.000 116 61.3 1641.2
Sample ID LCS-1936
Batch ID: 1936
Analysis Date: 5/15/2012Prep Date: 5/15/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: LCSW RunNo: 2758
SeqNo: 76834
LCSSampType: TestCode: EPA Method 8015B: Diesel Range
Diesel Range Organics (DRO) 5.000 96.5 74 1571.0 04.8 Surr: DNOP 0.5000 97.7 61.3 1640.49
Sample ID LCSD-1936
Batch ID: 1936
Analysis Date: 5/15/2012Prep Date: 5/15/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: LCSS02 RunNo: 2758
SeqNo: 76835
LCSDSampType: TestCode: EPA Method 8015B: Diesel Range
Diesel Range Organics (DRO) 5.000 88.7 74 157 231.0 0 8.414.4 Surr: DNOP 0.5000 103 61.3 164 000.52
Qualifiers:
Page 5 of 1
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
Project: MPPE-5Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205591WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID 5ML-RB
Batch ID: R2774
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: PBW RunNo: 2774
SeqNo: 77075
MBLKSampType: TestCode: EPA Method 8015B: Gasoline Range
Gasoline Range Organics (GRO) 0.050ND Surr: BFB 20.00 86.7 69.3 12017
Sample ID 2.5UG GRO LCS
Batch ID: R2774
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: LCSW RunNo: 2774
SeqNo: 77076
LCSSampType: TestCode: EPA Method 8015B: Gasoline Range
Gasoline Range Organics (GRO) 0.5000 112 101 1230.050 00.56 Surr: BFB 20.00 97.6 69.3 12020
Sample ID 1205591-001A MS
Batch ID: R2774
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: MPPE-5 RunNo: 2774
SeqNo: 77091
MSSampType: TestCode: EPA Method 8015B: Gasoline Range
Gasoline Range Organics (GRO) 2.500 116 75.4 1210.25 0.97403.9 Surr: BFB 100.0 98.5 69.3 12098
Sample ID 1205591-001A MSD
Batch ID: R2774
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: MPPE-5 RunNo: 2774
SeqNo: 77092
MSDSampType: TestCode: EPA Method 8015B: Gasoline Range
Gasoline Range Organics (GRO) 2.500 102 75.4 121 10.50.25 0.9740 9.083.5 Surr: BFB 100.0 104 69.3 120 00100
Qualifiers:
Page 6 of 1
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
Project: MPPE-5Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205591WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID 5ML-RB
Batch ID: R2774
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/L
PQL
Client ID: PBW RunNo: 2774
SeqNo: 77103
MBLKSampType: TestCode: EPA Method 8021B: Volatiles
Methyl tert-butyl ether (MTBE) 2.5NDBenzene 1.0NDToluene 1.0NDEthylbenzene 1.0NDXylenes, Total 2.0ND1,2,4-Trimethylbenzene 1.0ND1,3,5-Trimethylbenzene 1.0ND Surr: 4-Bromofluorobenzene 20.00 90.0 55 14018
Sample ID 100NG BTEX LCS
Batch ID: R2774
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/L
PQL
Client ID: LCSW RunNo: 2774
SeqNo: 77104
LCSSampType: TestCode: EPA Method 8021B: Volatiles
Methyl tert-butyl ether (MTBE) 20.00 98.2 50.5 1582.5 020Benzene 20.00 101 80 1201.0 020Toluene 20.00 103 80 1201.0 021Ethylbenzene 20.00 100 80 1201.0 020Xylenes, Total 60.00 102 80 1202.0 0611,2,4-Trimethylbenzene 20.00 89.3 80 1201.0 0181,3,5-Trimethylbenzene 20.00 96.1 80 1201.0 019 Surr: 4-Bromofluorobenzene 20.00 92.3 55 14018
Sample ID 1205559-001A MS
Batch ID: R2774
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/L
PQL
Client ID: BatchQC RunNo: 2774
SeqNo: 77112
MSSampType: TestCode: EPA Method 8021B: Volatiles
Methyl tert-butyl ether (MTBE) 20.00 97.9 58 1392.5 0.176020Benzene 20.00 105 70.1 1181.0 021Toluene 20.00 105 72.3 1171.0 0.386021Ethylbenzene 20.00 104 73.5 1171.0 021Xylenes, Total 60.00 105 73.1 1192.0 0631,2,4-Trimethylbenzene 20.00 96.7 65.8 1211.0 0.4080201,3,5-Trimethylbenzene 20.00 104 71.1 1181.0 021 Surr: 4-Bromofluorobenzene 20.00 108 55 14022
Sample ID 1205559-001A MSD
Batch ID: R2774
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/L
PQL
Client ID: BatchQC RunNo: 2774
SeqNo: 77113
MSDSampType: TestCode: EPA Method 8021B: Volatiles
Qualifiers:
Page 7 of 1
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
Project: MPPE-5Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205591WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID 1205559-001A MSD
Batch ID: R2774
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/L
PQL
Client ID: BatchQC RunNo: 2774
SeqNo: 77113
MSDSampType: TestCode: EPA Method 8021B: Volatiles
Methyl tert-butyl ether (MTBE) 20.00 97.3 58 139 15.22.5 0.1760 0.65020Benzene 20.00 101 70.1 118 16.41.0 0 4.4520Toluene 20.00 99.1 72.3 117 13.91.0 0.3860 5.8520Ethylbenzene 20.00 98.6 73.5 117 13.51.0 0 5.4420Xylenes, Total 60.00 99.9 73.1 119 12.92.0 0 5.23601,2,4-Trimethylbenzene 20.00 92.4 65.8 121 13.51.0 0.4080 4.42191,3,5-Trimethylbenzene 20.00 99.2 71.1 118 13.71.0 0 4.2620 Surr: 4-Bromofluorobenzene 20.00 100 55 140 0020
Qualifiers:
Page 8 of 1
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
Project: MPPE-5Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205591WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID 1205591-001C
Batch ID: R2782
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: µmhos/cm
PQL
Client ID: MPPE-5 RunNo: 2782
SeqNo: 77366
DUPSampType: TestCode: EPA 120.1: Specific Conductance
Conductivity 200.010 0.8804,900
Qualifiers:
Page 9 of 1
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
Project: MPPE-5Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205591WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID 1205591-001C
Batch ID: R2782
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: pH units
PQL
Client ID: MPPE-5 RunNo: 2782
SeqNo: 77348
DUPSampType: TestCode: SM4500-H+B: pH
pH H1.68 0.2498.03
Qualifiers:
Page 10 of 1
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
May 17, 2012
Western Refining Southwest, GallupBeck Larsen
Dear Beck Larsen:
RE: MPPE-7 OrderNo.: 1205592
FAX (505) 722-0210TEL: (505) 722-0258
Rt. 3 Box 7Gallup, NM 87301
Hall Environmental Analysis Laboratory4901 Hawkins NE
Albuquerque, NM 87109
Website: www.hallenvironmental.comTEL: 505-345-3975 FAX: 505-345-4107
Hall Environmental Analysis Laboratory received 1 sample(s) on 5/14/2012 for the analyses presented in the following report.
Andy Freeman
These were analyzed according to EPA procedures or equivalent. To access our accredited tests please go to www.hallenvironmental.com or the state specific web sites. See the sample checklist and/or the Chain of Custody for information regarding the sample receipt temperature and preservation. Data qualifiers or a narrative will be provided if the sample analysis or analytical quality control parameters require a flag. All samples are reported as received unless otherwise indicated.
Please don't hesitate to contact HEAL for any additional information or clarifications.
Sincerely,
Laboratory Manager4901 Hawkins NEAlbuquerque, NM 87109
http://www.hallenvironmental.comhttp://www.hallenvironmental.com
-
Project: MPPE-7Client Sample ID: MPPE-7
Collection Date: 5/14/2012 8:00:00 AMMatrix: AQUEOUS
CLIENT: Western Refining Southwest, Gallup
Lab ID: 1205592-001
Date Reported: 5/17/2012
Analytical ReportLab Order 1205592
Analyses Result Qual Units Date AnalyzedDFRL
Hall Environmental Analysis Laboratory, Inc.
Received Date: 5/14/2012 1:39:00 PM
EPA METHOD 8015B: DIESEL RANGE Analyst: JMPDiesel Range Organics (DRO) 5/15/2012 10:49:17 AM1.0 mg/L 19.9Motor Oil Range Organics (MRO) 5/15/2012 10:49:17 AM5.0 mg/L 1ND Surr: DNOP 5/15/2012 10:49:17 AM61.3-164 %REC 1125
EPA METHOD 8015B: GASOLINE RANGE Analyst: NSBGasoline Range Organics (GRO) 5/15/2012 1:36:57 AM0.25 mg/L 50.97 Surr: BFB 5/15/2012 1:36:57 AM69.3-120 %REC 5104
EPA METHOD 8021B: VOLATILES Analyst: NSBMethyl tert-butyl ether (MTBE) 5/15/2012 1:36:57 AM12 µg/L 5NDBenzene 5/15/2012 1:36:57 AM5.0 µg/L 5NDToluene 5/15/2012 1:36:57 AM5.0 µg/L 5NDEthylbenzene 5/15/2012 1:36:57 AM5.0 µg/L 5NDXylenes, Total 5/15/2012 1:36:57 AM10 µg/L 5ND1,2,4-Trimethylbenzene 5/15/2012 1:36:57 AM5.0 µg/L 5ND1,3,5-Trimethylbenzene 5/15/2012 1:36:57 AM5.0 µg/L 5ND Surr: 4-Bromofluorobenzene 5/15/2012 1:36:57 AM55-140 %REC 5103
EPA METHOD 300.0: ANIONS Analyst: SRMFluoride * 5/15/2012 12:52:40 PM5.0 mg/L 50120Chloride 5/14/2012 8:15:46 PM25 mg/L 50460Phosphorus, Orthophosphate (As P) 5/14/2012 5:46:47 PM2.5 mg/L 5NDSulfate 5/14/2012 5:59:12 PM10 mg/L 20530Nitrate+Nitrite as N 5/15/2012 1:29:53 PM1.0 mg/L 5ND
EPA METHOD 200.7: METALS Analyst: ELSCalcium 5/16/2012 7:11:13 AM1.0 mg/L 157Magnesium 5/16/2012 7:11:13 AM1.0 mg/L 117Potassium 5/16/2012 7:11:13 AM1.0 mg/L 190Sodium 5/16/2012 7:35:40 AM10 mg/L 10730
EPA 120.1: SPECIFIC CONDUCTANCE Analyst: DBDConductivity 5/15/2012 11:42:39 AM0.010 µmhos/cm 14,900
SM4500-H+B: PH Analyst: DBDpH *H 5/15/2012 11:42:39 AM1.68 pH units 19.09
Qualifiers:
Page 1 of 10
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection LimitS Spike Recovery outside accepted recovery limits
-
Project: MPPE-7Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205592WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID MB-1934
Batch ID: 1934
Analysis Date: 5/16/2012Prep Date: 5/15/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: PBW RunNo: 2797
SeqNo: 77728
MBLKSampType: TestCode: EPA Method 200.7: Metals
Calcium 1.0NDMagnesium 1.0NDPotassium 1.0NDSodium 1.0ND
Sample ID LCS-1934
Batch ID: 1934
Analysis Date: 5/16/2012Prep Date: 5/15/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: LCSW RunNo: 2797
SeqNo: 77729
LCSSampType: TestCode: EPA Method 200.7: Metals
Calcium 50.00 102 85 1151.0 051Magnesium 50.00 101 85 1151.0 050Potassium 50.00 98.1 85 1151.0 049Sodium 50.00 99.5 85 1151.0 050
Sample ID 1205563-001DMS
Batch ID: 1934
Analysis Date: 5/16/2012Prep Date: 5/15/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2797
SeqNo: 77734
MSSampType: TestCode: EPA Method 200.7: Metals
Calcium 50.00 82.9 70 1305.0 336.8380Magnesium 50.00 96.7 70 1305.0 77.99130Potassium 50.00 94.6 70 1305.0 51.0098
Sample ID 1205563-001DMSD
Batch ID: 1934
Analysis Date: 5/16/2012Prep Date: 5/15/2012
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2797
SeqNo: 77735
MSDSampType: TestCode: EPA Method 200.7: Metals
Calcium 50.00 85.6 70 130 205.0 336.8 0.354380Magnesium 50.00 96.4 70 130 205.0 77.99 0.154130Potassium 50.00 93.8 70 130 205.0 51.00 0.43398
Qualifiers:
Page 2 of 10
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
Project: MPPE-7Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205592WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID MB
Batch ID: R2759
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: PBW RunNo: 2759
SeqNo: 76514
MBLKSampType: TestCode: EPA Method 300.0: Anions
Chloride 0.50NDPhosphorus, Orthophosphate (As P 0.50NDSulfate 0.50ND
Sample ID LCS
Batch ID: R2759
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: LCSW RunNo: 2759
SeqNo: 76515
LCSSampType: TestCode: EPA Method 300.0: Anions
Chloride 5.000 95.5 90 1100.50 04.8Phosphorus, Orthophosphate (As P 5.000 101 90 1100.50 05.0Sulfate 10.00 96.5 90 1100.50 09.6
Sample ID 1205594-001BMS
Batch ID: R2759
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2759
SeqNo: 76517
MSSampType: TestCode: EPA Method 300.0: Anions
Phosphorus, Orthophosphate (As P 5.000 99.0 79.3 1080.50 04.9
Sample ID 1205594-001BMSD
Batch ID: R2759
Analysis Date: 5/14/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2759
SeqNo: 76518
MSDSampType: TestCode: EPA Method 300.0: Anions
Phosphorus, Orthophosphate (As P 5.000 101 79.3 108 200.50 0 1.715.0
Sample ID MB
Batch ID: R2795
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: PBW RunNo: 2795
SeqNo: 77644
MBLKSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.10NDNitrate+Nitrite as N 0.20ND
Sample ID LCS
Batch ID: R2795
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: LCSW RunNo: 2795
SeqNo: 77645
LCSSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.5000 96.4 90 1100.10 00.48Nitrate+Nitrite as N 3.500 100 90 1100.20 03.5
Qualifiers:
Page 3 of 10
*/X Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method BlankE Value above quantitation range H Holding times for preparation or analysis exceededJ Analyte detected below quantitation limits ND Not Detected at the Reporting LimitR RPD outside accepted recovery limits RL Reporting Detection Limit
-
Project: MPPE-7Client: Western Refining Southwest, Gallup
17-May-12
QC SUMMARY REPORT 1205592WO#:Hall Environmental Analysis Laboratory, Inc.
Sample ID 1205624-002AMS
Batch ID: R2795
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref Val %REC %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/L
PQL
Client ID: BatchQC RunNo: 2795
SeqNo: 77649
MSSampType: TestCode: EPA Method 300.0: Anions
Fluoride 0.5000 85.4 72.9 1130.10 1.7192.1Nitrate+Nitrite as N 3.500 98.9 83.9 1120.20 0.54934.0
Sample ID 1205624-002AMSD
Batch ID: R2795
Analysis Date: 5/15/2012Prep Date:
Analyte Result SPK value SPK Ref