11th GCxGC Symposium

K. 12 Characterization Of Sebum Lipids Using Comprehensive Two-Dimensional Gas Chroma-tography Combined With Rapid-Scanning Quadrupole Mass Spectrometry

Laurent Boisaubert1, Valeria Manzin1, Peter Tranchida2, Luigi Mondello2

1 Advanced Research, L‘OREAL R&I, Aulnay sous bois, France

2 University of Messina, Italy

K. 66Characterization of Organic Sulfur Compounds in Fossil Fuels Using Flow-Modulated Compre-hensive Two-Dimensional Gas Chromatography and Tandem Mass Spectrometry

Maria E. Machado1, Flavio A. Franchina2, Claudia Zini1, Elina B. Caramao1,3, Peter Q. Tranchida2, Luigi Mondello2,4

1 Instituto de Quimica, Universitade Federal do Rio Grande do Sul, Porto Alegre, Brazil

2 Dipartimento di Scienze del Farmaco e Prodotti per la Salute, University of Messina, Italy

3 Instituto Nacional de Ciencia e Tecnologia em Energia e Ambiente, INCT E&A, Campus Universitário de Ondina, Salvador, Brazil

4 Centro Integrato di Ricerca (C.I.R.), University Campus Bio-Medico of Rome, Italy

K. 71 The Off-Line Combination of High Performance Liquid Chromatography and Comprehensive Two-Dimensional Gas Chromatography-Mass Spectrometry: a New Powerful Approach for Highly-Detailed Essential Oil Analysis

Mariosimone Zoccali1, Peter Q. Tranchida1, Paola Dugo1,2, Giovanni Dugo1, Luigi Mondello1,2

1 Dipartimento di Scienze del Farmaco e Prodotti per la Salute, University of Messina, Italy

2 Centro Integrato di Ricerca (C.I.R.), University Campus Bio-Medico of Rome, Italy

K. 87 Monodimensional (GC-FID And GC-MS) and Comprehensive Two-Dimensional (GC×GC) Gas Chromatography for the Assessment of Volatiles and Fatty Acids from Ruta Chalepensis L. Plants

Selenia De Grazia1, Rosaria Costa1, Laura Tedone1, Salvatore Ragusa2, Luigi Mondello1,3

1 Dipartimento di Scienze del Farmaco e Prodotti per la Salute, University of Messina, Italy

2 Dipartimento di Scienze della Salute, University of Catanzaro, Italy

3 Centro Integrato

K*. 01 Comprehensive HPLC Analysis of Alkaloids and Permitted Additives in Dark Chocolate Products

Gesa Schad, Björn T. Erxleben, Robert Ludwig, Brigitte Richrath

Shimadzu Europa GmbH, Duisburg, Germany

Poster Presentations

K*. 04 Continuous vs. Segmented Second Dimension System Gradients for Comprehensive Two-Dimensional Liquid Chromatography of Sugar-cane (Saccharum SPP.)

Francesco Cacciola1,2, Gabriel Mazzi Leme1, Paola Donato3,4, Alberto Jose Cavalheiro5, Paola Dugo3,4, Luigi Mondello3,4

1 Dipartimento di Scienze dell‘Ambiente, della Sicurezza, del Territorio, degli Alimenti e della Salute, University of Messina, Italy

2 Chromaleont s.r.l. A start-up of the University of Messina, Italy

3 Centro Integrato di Ricerca (C.I.R.), University Campus Bio-Medico of Rome, Italy

4 Dipartimento di Scienze del Farmaco e dei Prodotti per la Salute, University of Messina, Messina, Italy

5 Institute of Chemistry, São Paulo State University, Araraquara, Brazil

K*. 05Increase the Separation Power of Two-Dimen-sional Liquid Chromatography Through the Use of Shifted Gradients for Polyphenol Deter-mination in Red Wine

Francesco Cacciola1,2, Paola Donato3,4, Francesca Rigano4, Paola Dugo3,4, Luigi Mondello3,4

1 Dipartimento di Scienze dell‘Ambiente, della Sicurezza, del Territorio, degli Alimenti e della Salute, University of Messina, Italy

2 Chromaleont s.r.l. A start-up of the University of Messina, Italy

3 Centro Integrato di Ricerca, University Campus Bio-Medico of Rome, Italy

4 Dipartimento di Scienze

K*. 06 The On-Line Hyphenation of Comprehensive Liquid Chromatography to Triple Quadrupole Mass Spectrometry for the Elucidation of the Carotenoid Content in Foodstuffs with High Orthogonality and Sensitivity

Paola Donato1,2, Francesco Cacciola3,4, Francesca Rigano2, Daniele Giuffrida3, Paola Dugo1,2, Luigi Mondello1,2

1 Centro Integrato di Ricerca (C.I.R.), University Campus Bio-Medico of Rome, Italy

2 Dipartimento di Scienze del Farmaco e dei Prodotti per la Salute, University of Messina, Italy

3 Dipartimento di Scienze dell‘Ambiente, della Sicurezza, del Territorio, degli Alimenti e della Salute, University of Messina, Italy

4 Chromaleont s.r.l. A start-up of the University of Messina, Italy

K*. 07 Coupling of New Silver Thiolate and Mono-disperse Materials in Comprehensive Two-Dimensional Liquid Chromatography for Truly Orthogonal Lipid Separation

Giuseppe Sullini1, Paola Donato1,2, Marco Beccaria1, Francesco Cacciola3,4, Paola Dugo1,2, Luigi Mondello1,2

1 Dipartimento di Scienze del Farmaco e dei Prodotti per la Salute, University of Messina, Italy

2 Centro Integrato di Ricerca (C.I.R.), University Campus Bio-Medico of Rome, Italy

3 Dipartimento di Scienze dell‘Ambiente, della Sicurezza, del Territorio, degli Alimenti e della Salute, University of Messina, Italy

4 Chromaleont s.r.l. A start-up of the University of Messina, Italy

38th ISCC

E. 08 Analytical Comparison of the Determination of Bisphenol A in Paper for Food Packaging

Andrea Jurek, Erich Leitner

Institute of Analytical Chemistry and Food Chemistry, Graz University of Technology, Austria

I. 04Maximizing Efficiency in UHPLC-MS/MS Method Development for Multi Component Analysis

Anja Grüning, Julia Sander, Ute Potyka, Stéphane Moreau

Shimadzu Europa GmbH, Duisburg, Germany

J. 18 Isolation of Bioflavonoids from Citrus By-Products by Means of Multidimansional LC Preparative System Coupled with a Mass Spectrometer

Marina Russo1, Veronica Inferrera1, Paola Dugo1,2, Luigi Mondello1,2

1 Dipartimento di Scienze del Farmaco e dei Prodotti per la Salute, University of Messina, Italy

2 Centro Integrato di Ricerca (C.I.R.), University Campus Bio-Medico of Rome, Italy

J. 19 The On-Line Combination of Liquid Chromato-graphy-Large Volume Injection-Comprehensive Two-Dimensional Gas Chromatography-Triple Quad Mass Spectrometry: a Powerful Four-Dimensional Separation-Science Tool

Mariosimone Zoccali1, Peter Q. Tranchida1, Paola Dugo1,2, Luigi Mondello1,2

1 Dipartimento di Scienze del Farmaco e dei Prodotti per la Salute, University of Messina, Italy

2 Centro Integrato di Ricerca (C.I.R.), University Campus Bio-Medico of Rome, Italy

J. 22 Rapid Isolation of High Solute Amounts by Using an On-Line Fourdimensional Preparative System: Normal Phase-Liquid Chromatography Coupled to Methyl Siloxane-Ionic Liquid-Wax Phase Gas Chromatography

Sebastiano Pantò1, Danilo Sciarrone1, Mariarosa Maimone1, Peter Q. Trachida1, Paola Dugo1,2, Luigi Mondello1,2

1 Dipartimento di Scienze del Farmaco e dei Prodotti per la Salute, University of Messina, Italy

2 Centro Integrato di Ricerca (C.I.R.), University Campus Bio-Medico of Rome, Italy

J. 24Collection of Enantiomeric Pure Components by Using a Multidimensional Gas Chromatographic Preparative System

Danilo Sciarrone1, Sebastiano Pantò1, Paola Dugo1,2, Luigi Mondello1,2

1 Dipartimento di Scienze del Farmaco e dei Prodotti per la Salute, University of Messina, Italy

2 Centro Integrato di Ricerca (C.I.R.), University Campus Bio-Medico of Rome, Italy

L. 06 Multi-Component Quantitative Analysis of Pharmaceuticals in the Environment by UHPLC-MS/MS with Online Spe

Anja Grüning1, Julia Sander1, Ute Potyka1, Stéphane Moreau1, Mikael Levi2

1 Shimadzu Europa GmbH, Duisburg, Germany2 Shimadzu France, Marne-la-Vallée, France

Poster Presentations

L. 07 Analysis of Doping Agents Using UltrafastLC-MS/MS with Scheduled MRM

Anja Grüning1, Julia Sander1, Ute Potyka1, Stéphane Moreau1, Mikael Levi2

1 Shimadzu Europa GmbH, Duisburg, Germany2 Shimadzu France, Marne-la-Vallée, France

M. 05 Fast GC-MS/MS Analysis of 76 VOC Compounds Using Headspace-Trap Sampling

Hendrik J. Schulte, Hans-Ulrich Baier, Stéphane Moreau

Shimadzu Europa GmbH, Duisburg, Germany

O. 07 Comprehensive Analysis of Naphthoylindole-Type Synthetic Cannabinoids by GC-MS/MS Using Simultaneous EI-Scan, MRM and Precur-sor Ion Scan Mode

Hendrik J. Schulte1, Haruhiko Miyagawa2, Yuki Sakamoto2, Tooru Kamata3, Shuntaro Matsuta3, Hiroshi Nishioka3, Munehiro Katagi3, Kei Zaitsu4, Akira Ishii4, Kento Tsuboi5, Hitoshi Tsuchihashi5, Koichi Suzuki5

1 Shimadzu Europa GmbH, Duisburg, Germany2 Shimadzu Corporation, Kyoto, Japan3 Forensic Science Laboratory, Osaka Prefectural

Police Headquarters, Japan4 Department of Legal Medicine & Bioethics, Nagoya

University Graduate School of Medicine, Japan5 Department of Legal Medicine, Osaka Medical

College, Japan

O. 15 Throughout Investigation of Fused-Core Stationary Phases Coupled to Ion Trap-Time of Flight Mass Spectrometry Detection for a Comprehensive Elucidation of the Total Lipid Profile of Human Plasma

Nermeen Girgis1, Paola Donato1,2, Francesco Cacciola3, Paola Dugo1,2, Luigi Mondello1,2

1 Dipartimento di Scienze del Farmaco e dei Prodotti per la Salute, University of Messina, Italy

2 Centro Integrato di Ricerca (C.I.R.), University Campus Bio-Medico of Rome, Italy

3 Dipartimento di Scienze dell‘Ambiente, della Sicurezza, del Territorio, degli Alimenti e della Salute, University of Messina, Italy

P. 10 Fast GC-MS/MS Analysis of Multicomponent Pesticides Residue (>300) in Food Matrices Using of MS Technology

Hendrik J. Schulte, Hans-Ulrich Baier, Stéphane Moreau

Shimadzu Europa GmbH, Duisburg, Germany

P. 11 The Use of Linear Retention Indices in Pesticide Residue Analysis Using a Tandem GCMS with MRM Database

Hendrik J. Schulte, Hans-Ulrich Baier, Stéphane Moreau

Shimadzu Europa GmbH, Duisburg, Germany

38th ISCC

E. 08 Analytical Comparison of the Determination of Bisphenol A in Paper for Food Packaging

Andrea Jurek, Erich Leitner

Institute of Analytical Chemistry and Food Chemistry, Graz University of Technology, Austria

I. 04Maximizing Efficiency in UHPLC-MS/MS Method Development for Multi Component Analysis

Anja Grüning, Julia Sander, Ute Potyka, Stéphane Moreau

Shimadzu Europa GmbH, Duisburg, Germany

J. 18 Isolation of Bioflavonoids from Citrus By-Products by Means of Multidimansional LC Preparative System Coupled with a Mass Spectrometer

Marina Russo1, Veronica Inferrera1, Paola Dugo1,2, Luigi Mondello1,2

1 Dipartimento di Scienze del Farmaco e dei Prodotti per la Salute, University of Messina, Italy

2 Centro Integrato di Ricerca (C.I.R.), University Campus Bio-Medico of Rome, Italy

J. 19 The On-Line Combination of Liquid Chromato-graphy-Large Volume Injection-Comprehensive Two-Dimensional Gas Chromatography-Triple Quad Mass Spectrometry: a Powerful Four-Dimensional Separation-Science Tool

Mariosimone Zoccali1, Peter Q. Tranchida1, Paola Dugo1,2, Luigi Mondello1,2

1 Dipartimento di Scienze del Farmaco e dei Prodotti per la Salute, University of Messina, Italy

2 Centro Integrato di Ricerca (C.I.R.), University Campus Bio-Medico of Rome, Italy

J. 22 Rapid Isolation of High Solute Amounts by Using an On-Line Fourdimensional Preparative System: Normal Phase-Liquid Chromatography Coupled to Methyl Siloxane-Ionic Liquid-Wax Phase Gas Chromatography

Sebastiano Pantò1, Danilo Sciarrone1, Mariarosa Maimone1, Peter Q. Trachida1, Paola Dugo1,2, Luigi Mondello1,2

1 Dipartimento di Scienze del Farmaco e dei Prodotti per la Salute, University of Messina, Italy

2 Centro Integrato di Ricerca (C.I.R.), University Campus Bio-Medico of Rome, Italy

J. 24Collection of Enantiomeric Pure Components by Using a Multidimensional Gas Chromatographic Preparative System

Danilo Sciarrone1, Sebastiano Pantò1, Paola Dugo1,2, Luigi Mondello1,2

1 Dipartimento di Scienze del Farmaco e dei Prodotti per la Salute, University of Messina, Italy

2 Centro Integrato di Ricerca (C.I.R.), University Campus Bio-Medico of Rome, Italy

L. 06 Multi-Component Quantitative Analysis of Pharmaceuticals in the Environment by UHPLC-MS/MS with Online Spe

Anja Grüning1, Julia Sander1, Ute Potyka1, Stéphane Moreau1, Mikael Levi2

1 Shimadzu Europa GmbH, Duisburg, Germany2 Shimadzu France, Marne-la-Vallée, France

Poster Presentations

L. 07 Analysis of Doping Agents Using UltrafastLC-MS/MS with Scheduled MRM

Anja Grüning1, Julia Sander1, Ute Potyka1, Stéphane Moreau1, Mikael Levi2

1 Shimadzu Europa GmbH, Duisburg, Germany2 Shimadzu France, Marne-la-Vallée, France

M. 05 Fast GC-MS/MS Analysis of 76 VOC Compounds Using Headspace-Trap Sampling

Hendrik J. Schulte, Hans-Ulrich Baier, Stéphane Moreau

Shimadzu Europa GmbH, Duisburg, Germany

O. 07 Comprehensive Analysis of Naphthoylindole-Type Synthetic Cannabinoids by GC-MS/MS Using Simultaneous EI-Scan, MRM and Precur-sor Ion Scan Mode

Hendrik J. Schulte1, Haruhiko Miyagawa2, Yuki Sakamoto2, Tooru Kamata3, Shuntaro Matsuta3, Hiroshi Nishioka3, Munehiro Katagi3, Kei Zaitsu4, Akira Ishii4, Kento Tsuboi5, Hitoshi Tsuchihashi5, Koichi Suzuki5

1 Shimadzu Europa GmbH, Duisburg, Germany2 Shimadzu Corporation, Kyoto, Japan3 Forensic Science Laboratory, Osaka Prefectural

Police Headquarters, Japan4 Department of Legal Medicine & Bioethics, Nagoya

University Graduate School of Medicine, Japan5 Department of Legal Medicine, Osaka Medical

College, Japan

O. 15 Throughout Investigation of Fused-Core Stationary Phases Coupled to Ion Trap-Time of Flight Mass Spectrometry Detection for a Comprehensive Elucidation of the Total Lipid Profile of Human Plasma

Nermeen Girgis1, Paola Donato1,2, Francesco Cacciola3, Paola Dugo1,2, Luigi Mondello1,2

1 Dipartimento di Scienze del Farmaco e dei Prodotti per la Salute, University of Messina, Italy

2 Centro Integrato di Ricerca (C.I.R.), University Campus Bio-Medico of Rome, Italy

3 Dipartimento di Scienze dell‘Ambiente, della Sicurezza, del Territorio, degli Alimenti e della Salute, University of Messina, Italy

P. 10 Fast GC-MS/MS Analysis of Multicomponent Pesticides Residue (>300) in Food Matrices Using of MS Technology

Hendrik J. Schulte, Hans-Ulrich Baier, Stéphane Moreau

Shimadzu Europa GmbH, Duisburg, Germany

P. 11 The Use of Linear Retention Indices in Pesticide Residue Analysis Using a Tandem GCMS with MRM Database

Hendrik J. Schulte, Hans-Ulrich Baier, Stéphane Moreau

Shimadzu Europa GmbH, Duisburg, Germany

Shimadzu Europa GmbHAlbert-Hahn-Str. 6-10 · D-47269 DuisburgTel.: +49 - (0)203 - 76 87-0Fax: +49 - (0)203 - 76 66 25shimadzu@shimadzu.euwww.shimadzu.eu

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