DEVELOPMENT OF INSTRUMENTED OEDOMETER …

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DEVELOPMENT OF INSTRUMENTED OEDOMETER INCORPORATED WITH BENDER ELEMENT AND ELECTRICAL CONDUCTIVITY MOHAMMED MANSOOR MOFREH GUBRAN A thesis submitted in fulfillment of requirement for the award of Doctor of Philosophy Faculty of Engineering Technology Universiti Tun Hussein Onn Malaysia April 2018

Transcript of DEVELOPMENT OF INSTRUMENTED OEDOMETER …

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DEVELOPMENT OF INSTRUMENTED OEDOMETER INCORPORATED WITH

BENDER ELEMENT AND ELECTRICAL CONDUCTIVITY

MOHAMMED MANSOOR MOFREH GUBRAN

A thesis submitted in

fulfillment of requirement for the award of

Doctor of Philosophy

Faculty of Engineering Technology

Universiti Tun Hussein Onn Malaysia

April 2018

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Praised to Allah. Sincerely dedicated to my beloved parents, brothers and wife…

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ACKNOWLEDGEMENT

Deep and humble gratitude to ALLAH Almighty for providing the opportunity and

giving me the strength to complete this work. I would like to express heartiest thanks

to my supervisor Assoc. Prof. Dr. Chan Chee Ming whose encouragement, guidance

and continuous support enabled me to carry out this research work. My appreciation

goes to technicians from Research Center for Soft Soil (RECESS) for their assistance.

I would like to extend my thanks to my family and colleagues for their support and

encouragement throughout my study.

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ABSTRACT

Soft soils are normally associated with high moisture content and fine-grained particles

possessing poor geotechnical properties such as low shear strength and high

compressibility. Solidification, using hydraulic binders could be adopted to improve

these poor properties. The compressibility of soil is quantified by the settlement

reduction due to the application of vertical load. Usually, the compressibility test is

conducted on undisturbed saturated soils using standardised oedometer. In this study,

an instrumented oedometer was developed by incorporating bender element

transducers and electrical conductivity probe to investigate and correlate the

compressibility, shear wave velocity (Vs) and electrical conductivity (EC)

characteristics of solidified dredged marine clay and refined kaolin. Ordinary Portland

cement was used at 5 %, 10 % and 15 % by dry weight of soil as a solidification agent.

All specimens were mixed at twice the liquid limit. Prior to testing, all solidified

specimens were cured for 7 days. It was found that Vs increased continuously with

further curing time whereas EC increased during the first day and decreased with

further curing. The compressibility was reduced and yield stress was developed as the

cement content increased. Vs and EC showed good correlation with applied stress

during the loading stage as the strain increased. For all loading stages, Vs increased

when the strain increased while EC decreased as the strain increased. Similarly, Vs,

EC and e showed good relationship as the vertical stress increased. These results

showed good relationship and strong correlations between the compressibility

parameters and Vs and EC measurements which give some insights on the

solidification mechanism and improvement of stiffness. These results also confirmed

that the instrumented oedometer incorporated with bender element and electrical

conductivity probes can be applied on soft soils to monitor the compressibility

behaviour at micro level. Moreover, the obtained relationships could be adopted in

numerical modelling as well design analysis of similar soils in situ.

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ABSTRAK

Tanah lembut lazim dikaitkan dengan kandungan lembapan yang tinggi dan zarah-

zarah tanah yang halus dengan sifat geoteknik yang lemah, yakni kekuatan ricih yang

rendah dan kebolehmampatan yang tinggi. Solidifikasi tanah dengan menggunakan

bahan tambah hidraulik boleh diaplikasikan untuk menambahbaik sifat tanah yang

lemah ini. Kebolehmampatan tanah dianggarkan melalui pengurangan enapan akibat

aplikasi beban tegak. Lazimnya, ujian pengukuhan dijalankan ke atas sampel tanah tak

terusik dengan alat oedometer piawai. Dalam kajian ini, sebuah oedometer yang

diubahsuai dengan menambah alat ‘bender elements’ dan proba kebolehaliran elektrik

telah dibangunkan untuk mengkaji hubungan di antara parameter kebolehenapan,

halaju gelombang ricih (Vs) serta kebolehaliran elektrik (EC) bagi tanah liat kerukan

marin dan kaolin yang disolidifikasikan. Simen Portland biasa ditambah sebagai bahan

pengikat pada kadar 5%, 10% dan 15% daripada jisim kering tanah. Semua spesimen

telah disediakan pada kandungan lembapan 2 kali ganda had cecair tanah. Sebelum

ujian dijalankan, spesimen dibiarkan untuk mengawet selama 7 hari. Adalah didapati

bahawa Vs meningkat secara berterusan dengan tempoh pengawetan, manakala EC

hanya meningkat pada hari pertama dan disusuli penurunan dengan pengawetan.

Kebolehenapan didapati menurun dan tegasan alah meningkat dengan penambahan

kandungan simen. Vs dan EC menunjukkan korelasi yang baik dengan tegasan yang

dikenakan semasa pembebanan dan peningkatan terikan. Untuk kesemua peringkat

pembebanan, Vs meningkat dan EC menurun dengan peningkatan terikan. Juga, Vs,

EC dan e menunjukkan korelasi yang baik dengan peningkatan tegasan tegak.

Keputusan yang diperolehi menggambarkan korelasi yang baik di antara parameter

kebolehenapan serta Vs dan EC, yang mencerminkan mekanisme solidifikasi dan

penambahbaikan sifat kekukuhan tanah tersebut. Keputusan ini juga mengesahkan

korelasi ini boleh juga digunapakai dalam menyediakan model numerikal serta reka

bentuk analisis tanah lembut serupa di tapak. Juga bahawa Oedometer yang diubahsuai

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dengan menambah alat “bender elements” dan proba keboleh aliran elektrik boleh

digunrakan ke atas tanah lembut untuk memantau kebolehenapan pada tahap mikro.

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CONTENTS

ACKNOWLEDGEMENT iv

ABSTRACT v

ABSTRAK vi

CONTENTS viii

LIST OF TABLES xi

LIST OF FIGURES i

1CHAPTER 1 INTRODUCTION 1

1.1 Problem statement 2

1.2 Objectives of the research 3

1.3 Scope of Research 4

1.4 Significance of Study 4

1.5 Thesis Layout 5

2CHAPTER 2 LITERATURE REVIEW 6

2.1 Oedometer Test 6

2.1.1 Overview 6

2.1.2 Principle of Consolidation 7

2.1.3 Historical Development 8

2.1.4 Standard Oedometer Test 9

2.1.5 Modified Oedometer cells 10

2.2 Bender Element (BE) 16

2.2.1 BE System Design 16

2.2.2 Arrival Time Determination 18

2.2.3 Shear wave velocity (Vs) Mechanism (Propagation) 23

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2.2.4 Relationship Between Vs and Compressibility 26

2.3 Electrical Conductivity 28

2.4 One-Dimensional Consolidation Test 30

2.4.1 Effects of High Moisture Content 30

2.4.2 Coefficient of Consolidation (Cv) 32

2.5 Treatment Effects on Compressibility 35

2.6 Mechanism of Cement Solidification 41

2.7 Curing Time Effects 44

2.8 Yield Stress 46

3CHAPTER 3 RESEARCH METHODOLOGY 50

3.1 Introduction 50

3.2 Instrumented Oedometer Test 52

3.2.1 Bender Element 55

3.2.2 Electrical Conductivity 64

3.3 1-D Consolidation Test Preparation 66

3.4 Materials 67

3.4.1 Dredged Marine Soil 68

3.4.2 Kaolin 71

3.4.3 Cement 71

3.5 Characterisation Tests 72

3.5.1 Moisture Content (MC) 72

3.5.2 Particle Density 72

3.5.3 Particle Size Distribution (PSD) 73

3.5.4 Atterberg Limit (AL) 74

3.5.5 Loss of Ignition (LOI) 74

3.5.6 X-Ray Fluorescence (XRF) 74

4CHAPTER 4 RESULTS AND DISCUSSION 75

4.1 Calibration of Instrumented Oedometer Cell 76

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4.1.1 Consolidation 76

4.1.2 Bender Element 78

4.1.3 Electrical Conductivity 78

4.2 Cement Effects on Curing Time 80

4.2.1 Moisture Content (MC) 80

4.2.2 Shear Wave Velocity (Vs) 82

4.2.3 Electrical Conductivity (EC) 85

4.3 Compressibility Behavior 87

4.3.1 Void ratio 87

4.3.2 Coefficient of Consolidation (Cv) 90

4.3.3 Coefficient of Volume Compressibility (Mv) 93

4.3.4 Compression Index 95

4.4 Yield Stress 96

4.5 Shear Wave Velocity 99

4.5.1 Relationship between ε and Vs with Time 99

4.5.2 Void Ratio (e) and S-Wave Velocity (Vs) 111

4.6 Electrical Conductivity 120

4.7 Correlation Parameters 127

4.7.1 Vs and EC during Curing 127

4.7.2 Vs and EC with ε-log t 129

4.7.3 Vs and EC with e-log σ’ 130

5CHAPTER 5 CONCLUSION AND RECOMMENDATIONS 132

5.1 Summary 132

5.2 Recommendations for Further Studies 135

REFERENCES 136

6 APPENDIX 145

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LIST OF TABLES

Table 2.1: Modified oedometers in previous studies 15

Table 2.2: Dynamic properties of tested organoclays 27

Table 2.3: Typical Cv of different soil clay 34

Table 2.4: Cv values of different soils using different methods 34

Table 2.5: Curing time for some previous studies for DMS 44

Table 2.6: Curing effects on initial water, Cs, Cc and yield stress of treated

DMS 45

Table 2.7: Yield stress of dredged soil from Chinese lake (L), marine (M) and

river sediment (R) 49

Table 3.1: Instrumented oedometer components 55

Table 3.2: GDSBEAT analysis parameters summary 63

Table 3.3: Specifications of EC probe 65

Table 3.4: Loading-unloading scheme 67

Table 3.5: Kaolin and DMS specimens 67

Table 3.6: Physical properties of Kuala Perlis DMS 69

Table 3.7: Mineral concentration in Kuala Perlis DMS 70

Table 3.8: Physical and chemical properties of Kaolin clay 71

Table 3.9: Typical chemical composition of the OPC 72

Table 4.1: Summary of the Vs in curing, yielding and post yield stages for all

specimens 117

Table 4.2: Coefficient of correlation (R) between the void ratio e, Vs, EC and

σ’ for kaolin 131

Table 4.3: Coefficient of correlation between the void ratio e, Vs and σ’ for

DMS 131

Table 5.1: Summarised relationships of the parameters 134

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LIST OF FIGURES

Figure 2.1: Spring and piston analogy illustrating the principle of

consolidation 7

Figure 2.2: Standard oedometer cell 10

Figure 2.3 (a, b, c, d, e, f): Schematic diagrams for modified oedometers from

previous studies 12

Figure 2.4: (a) Typical components of BE (b) Series and (c) Parallel type

connection 17

Figure 2.5: Conventional BE setup 18

Figure 2.6: (a) Crosstalk (b) Vp interference (c) Peripheral electronics 20

Figure 2.7: Typical transmitted and received sinusoidal Vs wave. (1) first

deflection (2) first maximum (3) zero crossing (4) major peak 21

Figure 2.8: Vs second arrival time 22

Figure 2.9: Relationship between the Vs and resonant frequency 23

Figure 2.10: Source and receiver polarization 25

Figure 2.11: Primary and secondary wave propagation 25

Figure 2.12: Relationship between the Vs and solidified granular soil with

respect to effective stress 27

Figure 2.13: Relationship between void ratio (e), vertical effective stress σ’

(kPa) and electrical conductivity σ (mS/cm) on Ticino sand 30

Figure 2.14: Effects of initial moisture content on secondary clay 31

Figure 2.15: Effects of initial moisture content on natural clay 32

Figure 2.16: Relationship between MC and cement during curing time 35

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Figure 2.17: Compression curves of Ariake clay for 7 days curing at different

water content, initial w= 130% LL=120%, PL=57%, G= 2.61 36

Figure 2.18: Compression curves for Ennore (India) solidified DMS (LL=54

PL=30 ps=2.69 clay 57% sand 10% 37

Figure 2.19: Compression curves for Ouistreham (France) solidified DMS

(MC=120, LL=104, PL=38, LOI=7, Sand=25, clay=25) 38

Figure 2.20: e-log σ’ compression curve of solidified Port Taranto (Italy)

LOI=2.2-1, LL=55, PL=26 39

Figure 2.21: e-log σ’ curves for solidified clay at different MC (a) 5% (b)

10% and (c) 15%, LL=103 Pl=43 clay=69 sand= 3% 40

Figure 2.22: Cement-clay-water interrelated phases during stabilisation

process 42

Figure 2.23: Relationship between Vs and curing time of fresh cement mix 46

Figure 2.24: Yield stress determination following Casagrande graphical

method 47

Figure 2.25: Effects of the cement content and curing time on solidified DM 48

Figure 2.26: Preconsoildation stress of Busan specimen determined by (a)

Casagrande(b) Janbu (c) Becker (d) Sridharan (e) Ontisuka (f) Vs 48

Figure 3.1: Experimental program flowchart 51

Figure 3.2: Instrumented oedometer setup 53

Figure 3.3: Instrumented oedometer components 54

Figure 3.4: Source and receiver bender element transducers 56

Figure 3.5: BE system set up 56

Figure 3.6: Hardware option (interface 1) 57

Figure 3.7: Acquisition option wizard (interface 2) 58

Figure 3.8: Waveform, wave frequency and amplitude wizard (interface 3) 59

Figure 3.9: Time Domain Stacking and Trigger Type (interface 4) 59

Figure 3.10: Test display screen example 60

Figure 3.11: Data sheet format 61

Figure 3.12: Arrival time for different loading stages (15DMS) 62

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Figure 3.13: Interactive and batch travel time analysis 63

Figure 3.14: Frequency domain analysis 64

Figure 3.15: EC probe 65

Figure 3.16: Sampling locations of dredged marine sediments 68

Figure 3.17: Clamshell dredger 68

Figure 3.18: Stored DMS in RECESS laboratory 69

Figure 3.19: Kuala Perlis DMS particle size distribution (PSD) 70

Figure 4.1: e-log σ' of standard and IOC (calibration) 77

Figure 4.2 Mv- log σ' of standard and IOC (calibration) 77

Figure 4.3: Cv- log σ' of standard and IOC (calibration) 77

Figure 4.4: BE calibration 78

Figure 4.5: EC vs NaCl concentration 79

Figure 4.6: EC for DMS diluted with distilled water to reduce the salt

concentration 79

Figure 4.7: Moisture content reduction after mixing and curing against

cement content (a) kaolin (b) DMS 81

Figure 4.8: Relationship between Vs and elapsed curing time for solidified

Kaolin specimens 83

Figure 4.9: Relationship between Vs and elapsed curing time for solidified

DMS specimens 84

Figure 4.10: Effects of (a) cement content on the final Vs and (b) final MC on

the final Vs at the end of curing time 85

Figure 4.11: Curing effects on EC for solidified kaolin specimens 86

Figure 4.12: Initial void ratio for kaolin and DMS 88

Figure 4.13: Compression curves (e-log σ’) of kaolin specimens 89

Figure 4.14: Compression curves (e-log σ’) of DMS specimens 90

Figure 4.15: Coefficient of consolidation (Cv) of kaolin specimens 91

Figure 4.16: Coefficient of consolidation (Cv) of DMS specimens 92

Figure 4.17: Coefficient of volume compressibility (Mv) of kaolin specimen 93

Figure 4.18: Coefficient of volume compressibility (Mv) of DMS specimens 94

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Figure 4.19: Compression index of the kaolin and DMS specimens 95

Figure 4.20: Relationship between yield stress and cement content for kaolin

and DMS 97

Figure 4.21: Relationship between yield stress and Vs with cement content for

kaolin specimens 98

Figure 4.22: Relationship between yield stress and Vs with cement content for

DMS specimens 98

Figure 4.23: Relationship between ε-log t and Vs-log t for each loading stage

in 0DMS 103

Figure 4.24: Relationship between ε-log t and Vs-log t for loading stage in

5DMS 104

Figure 4.25: Relationship between ε-log t and Vs-log t for loading stages in

10DMS 105

Figure 4.26: Relationship between ε-log t and Vs-log t for loading stages in

15DMS 106

Figure 4.27: Relationship between ε-log t and Vs-log t for each loading stage

in 0K 107

Figure 4.28: Relationship between ε-log t and Vs-log t for each loading stage

in 5K 108

Figure 4.29: Relationship between ε-log t and Vs-log t for each loading stage

in 10K 109

Figure 4.30: Relationship between ε-log t and Vs-log t for each loading stage

in 15K 110

Figure 4.31: Relationship between e-log σ' and Vs-log σ' curves for kaolin 112

Figure 4.32: Maximum Vs at the end of the last stage (800 kPa) for kaolin

specimens 113

Figure 4.33: Vs-log σ' curves for 5K and 15K 114

Figure 4.34: e-log σ' curves for 5K and 15K 114

Figure 4.35: Relationship between e-log σ' and Vs-log σ' curves for DMS 117

Figure 4.36: Vs-log σ' curves for DMS 118

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Figure 4.37: Maximum Vs at the end of the last stage (800 kPa) for DMS

specimens 119

Figure 4.38: Comparison between the Vs in kaolin and DMS 119

Figure 4.39: Relationship between ε-log t and EC-log t for each loading stage

in 5K 122

Figure 4.40: Relationship between ε-log t and EC-log t for loading stages in

10K 123

Figure 4.41: Relationship between ε-log t and EC-log t for each loading stage

in 15K 124

Figure 4.42: Relationship between the e-log σ' and EC-log σ' for solidified

kaolin specimens 126

Figure 4.43: Relationship between the EC peak time and cement content 126

Figure 4.44: Relationship between the Vs and EC for solidified kaolin

specimens 128

Figure 4.45: Relationship between the ε, and EC during the loading stage 129

Figure 4.46: Relationship between the ε, and EC during the loading stage 130

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LIST OF SYMBOLS AND ABBREVIATION

A - Al2 O3

AL - Atterberg limit

BE - Bender Element

C - Ca

CAH - Calcium Aluminate Hydrate

CASH - Calcium Silicate Hydrate

Cc - Compression Index

R - Correlation Coefficient

Cv - Coefficient of Consolidation

C3A - Tricalcium Aluminate

C4AF - Tetracalcium Aluminoferrite

CSH - Calcium Silicate Hydrate

C2S - Dicalcium Silicate

C3S - Tricalcium Silicate

DMS - Dredged Marine Soil

e - Void Ratio

EC - Electrical Conductivity

F - Fe2O3

GDS - Global Digital Systems Ltd

IOC - Instrumented Oedometer Test

Kg - Kilogram

KPa - Kilopascal

LL - Liquid Limit

LOI - Loss of Ignition

MC - Moisture Content

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Mv - Coefficient of Volume Compressibility

OMC - Organic Matter Content

PI - Plasticity Index

PL - Plastic Limit

PSD - Particle Size Distribution

S - SiO2

T50 - Time Corresponding to 50 % Settlement

Vs - Shear Wave Velocity

XRD - X-Ray Diffraction

XRF - X-Ray Fluorescence

σ' - Vertical Effective Stress

ε - Vertical Strain

ρ - Particle Density

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1 CHAPTER 1

INTRODUCTION

Marine dredging is a process of excavating sediments from the bottom of waterbodies

by mechanical or hydraulic machineries. The common purposes of marine dredging

are to make waterways for marine vessels navigation, coastal development projects,

and removal of contaminated sediments. There are two methods for disposal; open

water dumping and inland disposal. However, there are harmful environmental

consequences associated with each method. For instance, coral reefs, flora-fauna and

benthic organism could be affected directly by burial or indirectly by smothering

(Katsiaras et al., 2015). Moreover, finding a place inland is a challenge and there is

always a concern of contamination leaching to the groundwater table.

The normal practice in Malaysia is open water dumping which is restricted in

more advanced countries. Instead of dumping, these countries started utilising these

materials for beneficial purposes in civil engineering construction i.e. land

reclamation. However, the challenge for fine grained dredged marine soil is the high

moisture content and the presence of a considerable amount of organic matters making

direct use impossible due to the high compressibility and low shear strength.

Therefore, appropriate treatment must be adopted to reduce DMS compressibility.

Solidification technique could be adopted to reduce the compressibility. Past research

on soft soil have found that hydraulic binders (i.e. cement) and other pozzolanic by-

products (i.e. coal ash, steel slag) could successfully solidify and stabilise soft soils.

Usually 1-D consolidation test is conducted to evaluate the compressibility.

Conventional oedometer has been used to test compressibility primarily for

undisturbed saturated fine-grained soils in laboratory. Although, the outcomes of the

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test are useful in drawing the relationship between the applied vertical stress and the

associated 1-D consolidation deformation, but it didn’t give information about the

mechanism of consolidation.

Bender elements are piezoelectric transducers that can produce compression

waves and shear waves. Shear waves propagate through the solid medium while the

compression wave propagates through both solid and liquid. Thus, shear wave is

commonly used for soil stiffness assessment. It has the advantage of giving some

insights about small strain stiffness in the range of 10-6 and hence the interparticle state

of the soil. Since its first introduction to the soil testing by Shirley & Anderson (1975),

it has been showing promising indications of the inner state of soil particularly small

strain stiffness. Even though there is an agreement of its usefulness in determining the

small strain stiffness, it is worth mentioning that some obstacles have been faced

related to the results interpretation which hindered global standardisation, (such as

arrival time interpretation, near field effects).

Other non-destructive measurements are useful in quantifying the state of soil

without disturbing. In geophysics, however, there were attempts of utilising these

techniques to evaluate the soil. Yet, it couldn’t replace the conventional destructive

measurements due to the particulate nature of the soil. Nevertheless, it can give useful

insights on the soil behaviour in micro level. Electromagnetic and electrical

conductivity / resistivity deal with the pore fluid and surface charges of the soil. Hence,

it complements the shear wave velocity paralleled with the 1D consolidation especially

in evaluating the compressibility of the solidified soft soil.

1.1 Problem statement

Soft soils are normally associated with high moisture content and fine-grained particles

resulting in poor geotechnical properties such as high compressibility and low shear

strength. DMS is a truly example of such soil which requires proper treatment to be

useable for beneficial purposes (i.e. reclamation works as fill materials).

Solidification/stabilisation of these soils using hydraulic binders (i.e. cement) is

usually conducted to improve these poor properties. The conventional oedometer test

is designed to test the compressibility of undisturbed saturated fine-grained soil.

However, the specimen’s preparation of soils in slurry form using the conventional

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setup is impractical with inadequate travel distance for the expected large settlement.

Furthermore, the solidification mechanism and consolidation of the soil is still not

well-understood which requires more investigations. Therefore, modification for the

conventional oedometer is required with additional tools to monitor the solidification

and consolidation processes. Invasive and minimally invasive testing techniques for

geotechnical engineering purposes, nowadays, are developing progressively.

Nonetheless, due to the particulate nature of soil, there exists a transitional zone where

the conventional testing (macro-level), which is the compressibility in this study, is

studied simultaneously in micro-level using these techniques. For this purpose, an

instrumented oedometer test was developed with incorporation of bender element (BE)

transducers and electrical conductivity probe to investigate and correlate the

compressibility, shear wave velocity (Vs) and electrical conductivity (EC)

characteristics of solidified dredged marine clay and refined kaolin. The advantage of

using BE is that it can measure the small strain stiffness for less than 10-6 which can

evaluate the inter-particle condition of cementation process whereas EC measurements

can give an indication of the chemical reactions and water availability within cement-

water-soil mixture.

1.2 Objectives of the research

The aim of this research is to investigate and correlate the compressibility, shear wave

velocity and electrical conductivity characteristics of solidified fine-grained soils

using an instrumented oedometer. The following objectives are to be achieved in the

present study:

1. To develop an instrumented oedometer cell incorporated with electrical

conductivity and bender elements measurements.

2. To investigate the one-dimensional compressibility of solidified DMS and

kaolin in relation to the electrical conductivity and shear wave velocity

measurements.

3. To establish the correlations between the electrical conductivity and shear

wave velocity measurements with the improved compressibility of the tested

soils.

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1.3 Scope of Research

Based on the objectives of this study, the scope of study can be classified into two

phases. The first phase is about the development of the instrumented oedometer.

Modifications on the conventional oedometer were made considering enough travel

distance for slurry soil to settle and providing enough space for the additional probes

to be installed. One pair of BE was installed in the top cap and bottom platen, while

the EC probe was installed on the top cap. GDS master box was used to operate the

BE via computerised system.

The second phase is the implementation of the work. In this study two types of

soils were used; dredged marine soil collected from Kuala Perlis and refined

Malaysian kaolin clay. Ordinary Portland cement was used as solidification agents

with 5 %, 10 % and 15 % by dry weight. Characterisations of the DMS and kaolin

were conducted on the moisture content, plastic limit, liquid limit, particle density,

LOI and XRF. After specimen preparation, the treated specimens were cured for

7 days prior to testing. The shear wave velocity was determined using bender

element transducers and EC were taken during the curing time. Loading the soil

incrementally and taking the BE and EC simultaneously with the settlement.

Then, the relationship among these three parameters were investigated and the

relationship between these parameters was established.

1.4 Significance of Study

The oedometer was modified to incorporate additional instrumentation which can help

in understanding the mechanism of the compressibility of the solidified soil to assess

the quality control. Moreover, the non-destructive testing is more desirable in

geotechnical engineering. Instead of dumping the DMS into the open water, it could

be used for beneficial purposes after proper treatment. Hence, two things can be

achieved: (1) to avoid bad environmental consequences caused by dumping and (2)

utilise DMS instead of natural resources by adopting the solidification technique to

improve the compressibility of this soils to be used for reclamation hence providing

more areas/land especially at places where more space is needed such as recreational

spots (i.e. Dubai) and creating new infrastructures (i.e. airports in Japan).

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1.5 Thesis Layout

Chapter one presents the background of study, problem statement, research objectives,

scope of study, significance of study and theses layout.

Chapter two covers the literature review and results obtained by the previous related

works. Review on previous studies on modified oedometers incorporating bender

element and electrical conductivity measurements was providing in beginning of this

chapter followed by bender element and electrical conductivity. One-dimensional

consolidation test, treatments effects on compressibility, mechanism of solidification,

curing time effects, yield stress, physicochemical, solidification agent and DMS were

also reviewed in this chapter.

Chapter three describes the methodology, materials and experimental approach

adopted to achieve the objectives of this study. The first part describes the

instrumented oedometer and calibration. The second part describes the one-

dimensional consolidation test and samples preparations. The third part describes the

material used in this study followed by soils characterisation tests.

Chapter four presents the results and discussion in six subsections. The first part is

about the cement effects on the moisture, Vs and EC during the specified curing period.

The second part presents the compressibility parameters namely, void ratio, coefficient

of consolidation, coefficient of volume compressibility and compression index. The

third part is about the yield stress. The fourth and fifth part presents the relationship

between the compressibility and Vs and EC respectively. The last section compares

the correlation between the compressibility, Vs and EC parameters.

Chapter five concludes the results of the study and the recommendations for future

research.

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2 CHAPTER 2

LITERATURE REVIEW

This chapter evaluates critically on oedometer test including standard, modified

oedometers, bender element, electrical conductivity, soft soil treatment,

physicochemical properties of soft soil and dredged marine soil are presented. In

addition, a discussion of advanced analysis techniques of solidification is also

presented.

2.1 Oedometer Test

The oedometer test is commonly used in soil mechanics to determine parameters for

calculation of consolidation, settlement and for assessing stress history of soils.

2.1.1 Overview

As mentioned above, the oedometer consolidation test is used for the determination of

the compressibility characteristics of soils with low permeability. There are two

parameters required for this test: (1) The soil compressibility which is a measure of the

amount by which the soil will compress when loaded and allowed to consolidate which

can be expressed of the settlement or void ratio reduction. (2) The time related

parameter which indicates the rate of compression and hence the time-period over

which consolidation settlement will take place.

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The test is conducted by applying a sequence of specified incremental vertical

loads to a laterally confined specimen. The vertical compression under each load is

observed until the primary consolidation is achieved. Since no lateral deformation is

allowed, it is considered a one-dimensional test. The consolidation cell consists

essentially of a consolidometer and a supporting frame as detailed in section 2.1.4.

2.1.2 Principle of Consolidation

The theory of consolidation states that the compressibility of solid particles and water

can be negligible compared to the compressibility caused by the escaping of water.

Consolidation is rapid in low permeable soils such as sand and slow in high permeable

soils like clays hence requires longer time. Analogical illustration of the consolidation

was introduced by Terzaghi & Peck (1948) and Taylor (1948). The process of

consolidation is often explained with an idealized system composed of a spring in a

container, filled with water, with a hole in its top cap as shown in Figure 2.1.

Figure 2.1: Spring and piston analogy illustrating the principle of consolidation

(Taylor, 1948)

The spring represents the solid structure of the soil and the water represents the pore

water in the soil. When applying a load on the top cap, while the hole is closed, the

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