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Determination of MetalsPart 7

Atomic Absorption Spectrometry

Flameless Atomization Techniques

Determination of Metals, Course # 55236, March 2016, Norbert MaierDetermination of Metals, Course # 55236, March 2017, Norbert Maier

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Determination of MetalsPart 8

Atomic Emisson Spectroscopy

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http://sites.cord.edu/chem-330-lab-manual/experiments/icp-aes

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ArgonSample

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http://cobblab.blogspot.fi/2012/09/enter-george-weve-spent-many-nights.html

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(for Sample containing High Amounts of Salts)

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The spray chamber consists oftwo concentric tubes sealed ateither end. The outer tube has anexit at the top that allows the gascontaining the particles to passto the torch. At the bottom of thetube there is a drain exit wherethe liquid caught on the walls ofthe inner and outer tubes collectand pass to waste. The gascarrying the sample particlesthen passes into the torch wherethe sample atoms are heated to avery high temperature.

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