DATA VALIDATION REVIEW REPORT EPA STAGE2Bnewtowncreek.info/docs2/2 Remedial Investigation/Phase...

305 West Grand Avenue, Suite 300 Montvale, New Jersey 07645

Phone 201.930.9890 Fax 201.930.9805

www.anchorqea.com

DATA VA L I DAT I O N RE V I E W R E P O R T – EPA STA G E2B Project: Newtown Creek

Project Number: 120782-01.01

Date: November 27, 2012

This validation report summarizes the review of analytical results for one rinse blank, four

trip blanks, two field duplicates and thirty-four sediment samples collected October 2-6,

2012. The samples were collected by Anchor QEA, LLC, and submitted to Alpha Analytical

(Alpha) in Mansfield, Massachusetts. Alpha sample delivery group (SDG) numbers L1217878

and L1218042 were reviewed in this report. Verification was performed electronically using

Automated Data Review (ADR) software followed by manual validation of the automated

qualifiers. Specific criteria that could not be automatically verified (i.e. tune criteria, select

calibration criteria, etc.) was also manually validated. Electronic and manual qualifications

made during the data validation process can be found in the attached reports referenced

throughout this document. Samples reviewed in this report can be found in the attached

EDD Summary Report. The samples were analyzed for the following parameters:

Total solids (TS) by SM 2540G

Ammonia (NH3), Kjeldahl nitrogen (KN), nitrate/nitrite, and total phosphorus by SM

4500

Soot carbon by Gustafsson 1997

Total metals by U.S. Environmental Protection Agency (USEPA) method 6020

Petroleum hydrocarbons by USEPA method 8015 modified

Volatile organic compounds (VOCs) by USEPA method 8260B

Semivolatile organic compounds (SVOCs) by USEPA method 8270C SIM modified

Total cyanide (CN) by USEPA method 9012A

Sulfide by method USEPA 9030B

pH by USEPA method 9045C

Total organic carbon (TOC) by USEPA method 9060

DATA VALIDATION AND QUALIFICATIONS

The following comments refer to the laboratory’s performance in meeting the quality

assurance/quality control (QA/QC) criteria outlined in Worksheet #36 (Validation Summary

Newtown Creek

November 27, 2012

Table) of the Quality Assurance Project Plan (QAPP, Anchor QEA, 2011). Laboratory results

were reviewed using the USEPA Contract Laboratory Program National Functional

Guidelines for Organic Data Review (USEPA 2008) and the USEPA Contract Laboratory

Program National Functional Guidelines for Inorganic Data Review (USEPA 2004).

FIELD DOCUMENTATION

Field documentation was checked for completeness and accuracy. The chain-of-custody

forms were signed by Alpha at the time of sample receipt; the samples were received cold

and in good condition.

HOLDING TIMES AND SAMPLE PRESERVATION

Samples were appropriately preserved and analyzed within holding times with the exception

of the soot carbon analyses in both SDGs. Several samples in SDG L1217878 were one or

three days outside of the project-specific fourteen day holding time, while all samples in SDG

L1218042 were analyzed four or five days outside of this holding time. The lab has indicated

that all samples were analyzed within their laboratory holding time of 28 days and that all

samples were stored frozen prior to analysis. Associated sample results have been qualified

“J” to denote this hold time anomaly.

LABORATORY METHOD BLANKS AND CALIBRATION BLANKS

Laboratory method and calibration blanks were analyzed at the required frequencies. Several

compounds were detected in method blanks at levels between the method detection limit

(MDL) and the project-required quantitation limit (QL). These detections occurred in the

phosphorus, ammonia, petroleum hydrocarbon, VOC, SVOC, and metals analyses. Some

metals were also detected in initial calibration blanks (ICB) and continuing calibration

blanks (CCB) at levels between the MDL and QL. Vanadium was detected in one of the

method blanks at a level above the QL. Associated detected sample results that were not

significantly greater than (>5x) the levels detected in these blanks were qualified “U” as non-

detects. Detected method blank results, associated samples, and qualified sample results can

be found in the attached Method Blank Outlier Report. Qualified sample results due to

concentrations found in the ICB/CCBs can be found in the attached Manual Changes History

Report.

Newtown Creek

November 27, 2012

FIELD QUALITY CONTROL

Rinse Blanks

One rinse blank (SG-RB-20121006) was collected and analyzed in association with these

sample sets. Detected results can be found in the attached Rinse Blank Summary Table. No

data were qualified based on rinse blank results.

Trip Blanks

Four trip blanks were analyzed in association with the VOC samples in these SDGs and were

mostly free of target analytes. Acetone was detected in three of these blanks at levels

between the MDL and QL. No data were qualified based on trip blank results.

Field Duplicates

Two field duplicates were collected in association with these sample sets. Results at or near

the QL (≤5x) may have exaggerated relative percent difference (RPD) values. Non-detected

values were treated as zero for the purposes of calculating RPD values. Detected results are

summarized in the attached Field Duplicate RPD Report. No data were qualified based on

field duplicate results.

INITIAL CALIBRATIONS AND CALIBRATION VERIFICATIONS

All initial calibrations (ICAL), initial calibration verifications (ICV), and continuing

calibration verifications (CCV) associated with reported results met method and validation

criteria with the exception of some VOC and phosphorus analyses. Associated sample results

have been qualified “J” or “UJ” to indicate that they are estimated. In instances of analyses

where the percent difference (%D) between the initial calibration and the continuing

calibration is above control limits, associated detected values would be qualified “J” to

indicate that they are estimates, while associated non-detect values would not be impacted

and no qualification is necessary. In instances of %D below control limits, associated sample

results have been qualified “J” or “UJ” to indicate a potential low bias. In instances of analyses

where the %R of a particular CCV is above control limits, all detected sample results

bracketed by this CCV are qualified “J” to indicate that they are estimated, while associated

non-detect values would not be impacted and no qualification is necessary. In instances

where the %R of a particular CCV is below control limits, all sample results bracketed by this

Newtown Creek

November 27, 2012

CCV are qualified “J” or “UJ” to indicate that they are estimated. Calibration values outside

of control limits and associated samples can be found in the attached Calibration Verification

Outliers reports. Qualified sample results due to calibration recoveries can be found in the

attached Manual Changes History and Qualification Summary Reports.

INTERNAL STANDARD/SURROGATE RECOVERIES

All internal standard and surrogate recoveries were within method or laboratory control

limits.

SERIAL DILUTION

Serial dilution analyses were performed and met method criteria with the exception of nickel

and silver in SDG L1217878. Associated sample results have been qualified “J” to indicate

that they are estimated.

INTERFERENCE CHECK

Interference check samples (ICS) were analyzed at the required frequency and met method

criteria.

LABORATORY CONTROL SAMPLES AND LABORATORY CONTROL SAMPLE DUPLICATES

Laboratory control samples (LCS) and laboratory control sample duplicates (LCSD) were

analyzed at the required frequencies and all LCS/LCSD analyses yielded %R and/or RPD

values within project-specific control limits with the following exceptions:

SDG L1217878:

o Phosphorus – The LCS analysis yielded a %R values above control limits. All

associated sample results have been qualified “J” to indicate that they are

estimated.

SDG L1218042:

o VOCs - The LCSD analysis yielded %R values above control limits for

dichlorodifluoromethane and methylene chloride; however, these compounds

were not detected in any of the associated samples, and no qualification is

necessary.

Newtown Creek

November 27, 2012

STANDARD REFERENCE MATERIAL

Standard reference materials (SRM) were analyzed in addition to or in lieu of LCSs for some

analyses and recovered within specified limits.

MATRIX SPIKE AND MATRIX SPIKE DUPLICATE

Matrix spike (MS) and matrix spike duplicate (MSD) samples were analyzed at the required

frequencies. When the parent sample concentration is greater than (>4x) the spike

concentration, the MS/MSD %R and/or RPD limits do not apply. All MS/MSD results were

within these criteria or within project-required control limits with the following exceptions:

SDG L1217878:

o VOCs – The MS/MSD analyses performed on sample SC001SG-000015-20121003

had zero percent recoveries for cyclohexane and methyl acetate. These

compounds were not detected in the associated sample and the results have been

qualified “R” and are rejected. The MS and/or MSD analyses on this sample also

recovered below control limits for twenty-five compounds. The associated sample

results have been qualified “J” or “UJ” to indicate that they are estimated.

o SVOCs – The MS analysis performed on SC001SG-000015-20121003 recovered

below control limits for n-nonane. The associated sample result has been

qualified “UJ” to indicate that it is estimated.

o Metals – The MS analysis performed on sample SC001SG-000015-20121003

recovered below control limits, and below 30% for antimony. This compound

was not detected in samples WE005SG-000015-20121004 and WE006SG-000015-

20121004 and the results have been qualified “R” and are rejected. All other

associated samples results were detected and have been qualified “J” to indicate

that they are estimated. The MS analysis performed on sample SC001SG-000015-

20121003 had a zero percent recovery for tin. This compound was detected in all

associated samples and results have been qualified “J” to indicate that they are

estimated.

SDG L1218042:

o Phosphorus – The MS analysis performed on sample HB001SG-000015-20121006

recovered below the control limits, and below 30% for phosphorus. This

compound was detected in all associated samples and results have been qualified

“J” to indicate that they are estimated.

Newtown Creek

November 27, 2012

o Metals – The MS analysis performed on sample TN005SG-000014-20121005

recovered below control limits and below 30% for antimony. This compound was

detected in all associated samples and results have been qualified “J” to indicate

that they are estimated.

These compounds, the %R values, and associated samples can be found in the attached

Matrix Spike/Matrix Spike Duplicate Outlier Reports. Edits to electronically applied

qualifiers can be found in the attached Manual Changes History Report.

LABORATORY DUPLICATES

Laboratory duplicates were analyzed at the required frequencies. If a sample or duplicate

result is less than 5x the QL, the RPD control limit does not apply and the sample and

duplicate result must be within ± 2x the QL of each other. All duplicate RPD values were

within these criteria or within project-required control limits with the exception of barium,

cadmium, calcium, lead, selenium, thallium, soot carbon and sulfide in SDG L1218042 which

all had RPD values above control limits. Associated sample results have been qualified “J” to

indicate that they are estimated.

SAMPLE ANALYSES

Some results for n-nonacosane, n-octadecane, n-pentacosane, phytane, and 2,6,10-

trimethyltridecane were indicated by the laboratory to have a potential high bias due to

matrix interference or co-elution with laboratory standards or non-target analytes. The

acetone concentration for sample WE008SG-000015-20121004 exceeded the level of

calibration. Results have been qualified “J” to indicate they are estimated. These

qualifications will be automatically applied during upload to the EQuIS database.

PROJECT REQUIRED QUANTIATION LIMITS

Quantitation limits were acceptable as reported. All values were reported using the

laboratory reporting limits. Values were reported as undiluted, or when reported as diluted,

the QL accurately reflects the dilution factor.

OVERALL ASSESSMENT

As was determined by this evaluation, the laboratory followed the specified analytical

methods and all requested sample analyses were completed. Accuracy was acceptable as

Newtown Creek

November 27, 2012

demonstrated by the LCS/LCSD, MS/MSD, SRM, internal standard, surrogate, and/or

interference check %R values with the exceptions noted above and in the validation reports.

Precision was also acceptable as demonstrated by the laboratory duplicates, LCS/LCSD and

MS/MSD RPD values with the exceptions noted above and in the validation reports. Most

data were acceptable as reported; other data are acceptable as qualified. One cyclohexane,

one methyl acetate and two antimony results have been rejected. Completeness was greater

than or equal to 90%; completeness goals were met. The qualifiers applied to samples

reviewed in this validation report can be found in the attached Qualifier Summary Report.

DATA QUALIFIER DEFINITIONS

U Indicates the compound or analyte was analyzed for but not detected at or above the

specified limit.

J Indicates an estimated value.

UJ Indicates the compound or analyte was analyzed for but not detected and the

specified limit reported is estimated

R Indicates data is rejected and unusable

ATTACHED VALIDATION REPORTS

EDD Summary Report by Analysis Method

Outlier Reports

Rinse Blank Summary Table

Field Duplicate RPD Report

History of Manual Changes to Automated Data Review Qualifiers

Data Qualifier Summary

Reason Code Legend (last page of summary)

REFERENCES

Anchor QEA, 2011. Quality Assurance Project Plan, Remedial Investigation/Feasibility

Study, Newton Creek. October.

USEPA, 1999. USEPA Contract Laboratory Program National Functional Guidelines for

Organic Data Review. U.S. Environmental Protection Agency, Office of Emergency

and Remedial Response (OERR). EPA 540-R-99-008. October 1999.

Newtown Creek

November 27, 2012

USEPA, 2004. USEPA Contract Laboratory Program National Functional Guidelines for

Inorganic Data Review. U.S. Environmental Protection Agency, Office of Superfund

Remediation and Technology Innovation (OSRTI). EPA 540-R-04-004. October

2004.

Data Review Sample Summary Report by Analysis MethodReviewed By: Approved By: Laboratory: AAL

PreparationMethod Validation CodeClient Sample ID Lab Sample ID Matrix Sample Type Collection Date

Lab Reporting Batch: L1217878

Method: SM2540GFC001SG-000015-20121002 L1217878-01 N METHOD 10/2/2012 10:54:00 AM S2BVEMSE

FC002SG-000015-20121002 L1217878-03 N METHOD 10/2/2012 12:20:00 PM S2BVEMSE




FC1004SG-000015-20121002 L1217878-11 FD METHOD 10/2/2012 3:21:00 PM S2BVEMSE

SC001SG-000015-20121003 L1217878-14 N METHOD 10/3/2012 9:16:00 AM S2BVEMSE

SC001SG-000015- WG565285-1 DUP METHOD 10/3/2012 9:16:00 AM S2BVEMSE



SC004SG-000015-20121003 L1217878-20 N METHOD 10/3/2012 12:36:00 PM S2BVEMSE




TN001SG-000015-20121004 L1217878-45 N METHOD 10/4/2012 4:08:00 PM S2BVEMSE

WE001SG-000015-20121004 L1217878-29 N METHOD 10/4/2012 8:28:00 AM S2BVEMSE

WE001SG-000015- WG565677-1 DUP METHOD 10/4/2012 8:28:00 AM S2BVEMSE

WE002SG-000015-20121004 L1217878-43 N METHOD 10/4/2012 3:12:00 PM S2BVEMSE





11/9/2012 3:46:03 PM ADR version 1.6.0.185 Page 1 of 17



Method: SM2540GWE007SG-000015-20121004 L1217878-39 N METHOD 10/4/2012 1:17:00 PM S2BVEMSE


Method: SM4500NH3HFC001SG-000015-20121002 L1217878-01 N METHOD 10/2/2012 10:54:00 AM S2BVEMSE








SC001SG-000015- WG567072-4 MS METHOD 10/3/2012 9:16:00 AM S2BVEMSE










WE001SG-000015- WG567121-4 MS METHOD 10/4/2012 8:28:00 AM S2BVEMSE






Method: SM4500NH3HWE004SG-000015-20121004 L1217878-33 N METHOD 10/4/2012 10:25:00 AM S2BVEMSE





Method: SM4500NO3FFC001SG-000015-20121002 L1217878-01 N METHOD 10/2/2012 10:54:00 AM S2BVEMSE





















Method: SM4500NO3FWE003SG-000010-20121004 L1217878-31 N METHOD 10/4/2012 9:39:00 AM S2BVEMSE






Method: SM4500NorgCFC001SG-000015-20121002 L1217878-01 N METHOD 10/2/2012 10:54:00 AM S2BVEMSE




















Method: SM4500NorgCWE001SG-000015- WG567215-3 DUP METHOD 10/4/2012 8:28:00 AM S2BVEMSE









Method: SM4500PEFC001SG-000015-20121002 L1217878-01 N METHOD 10/2/2012 10:54:00 AM S2BVEMSE

















Method: SM4500PESC007SG-000015-20121003 L1217878-24 N METHOD 10/3/2012 2:39:00 PM S2BVEMSE












Method: SOOTCFC001SG-000015-20121002 L1217878-01 N METHOD 10/2/2012 10:54:00 AM S2BVEMSE














Method: SOOTCSC004SG-000015-20121003 L1217878-20 N METHOD 10/3/2012 12:36:00 PM S2BVEMSE




SRM 1650B L1217878-50 N METHOD 10/4/2012 12:00:00 PM S2BVEMSE












Method: SW6020AFC001SG-000015-20121002 L1217878-01 N EPA 3050B 10/2/2012 10:54:00 AM S2BVEMSE

FC002SG-000015-20121002 L1217878-03 N EPA 3050B 10/2/2012 12:20:00 PM S2BVEMSE




FC1004SG-000015-20121002 L1217878-11 FD EPA 3050B 10/2/2012 3:21:00 PM S2BVEMSE

SC001SG-000015-20121003 L1217878-14 N EPA 3050B 10/3/2012 9:16:00 AM S2BVEMSE




Method: SW6020ASC001SG-000015- WG567867-3 DUP EPA 3050B 10/3/2012 9:16:00 AM S2BVEMSE

SC001SG-000015- WG567869-3 DUP EPA 3050B 10/3/2012 9:16:00 AM S2BVEMSE

SC001SG-000015- WG567867-4 MS EPA 3050B 10/3/2012 9:16:00 AM S2BVEMSE

SC001SG-000015- WG567869-4 MS EPA 3050B 10/3/2012 9:16:00 AM S2BVEMSE



SC004SG-000015-20121003 L1217878-20 N EPA 3050B 10/3/2012 12:36:00 PM S2BVEMSE




TN001SG-000015-20121004 L1217878-45 N EPA 3050B 10/4/2012 4:08:00 PM S2BVEMSE

WE001SG-000015-20121004 L1217878-29 N EPA 3050B 10/4/2012 8:28:00 AM S2BVEMSE

WE002SG-000015-20121004 L1217878-43 N EPA 3050B 10/4/2012 3:12:00 PM S2BVEMSE







Method: SW8015MFC001SG-000015-20121002 L1217878-01 N ALPHA OP-013 10/2/2012 10:54:00 AM S2BVEMSE

FC002SG-000015-20121002 L1217878-03 N ALPHA OP-013 10/2/2012 12:20:00 PM S2BVEMSE






Method: SW8015MFC005SG-000015-20121002 L1217878-07 N ALPHA OP-013 10/2/2012 2:35:00 PM S2BVEMSE

FC1004SG-000015-20121002 L1217878-11 FD ALPHA OP-013 10/2/2012 3:21:00 PM S2BVEMSE

SC001SG-000015-20121003 L1217878-14 N ALPHA OP-013 10/3/2012 9:16:00 AM S2BVEMSE

SC001SG-000015- WG566238-4 MS ALPHA OP-013 10/3/2012 9:16:00 AM S2BVEMSE

SC001SG-000015- WG566238-5 MSD ALPHA OP-013 10/3/2012 9:16:00 AM S2BVEMSE



SC004SG-000015-20121003 L1217878-20 N ALPHA OP-013 10/3/2012 12:36:00 PM S2BVEMSE




TN001SG-000015-20121004 L1217878-45 N ALPHA OP-013 10/4/2012 4:08:00 PM S2BVEMSE

WE001SG-000015-20121004 L1217878-29 N ALPHA OP-013 10/4/2012 8:28:00 AM S2BVEMSE

WE002SG-000015-20121004 L1217878-43 N ALPHA OP-013 10/4/2012 3:12:00 PM S2BVEMSE







Method: SW8260CFC001SG-000015-20121002 L1217878-01 N METHOD 10/2/2012 10:54:00 AM S2BVEMSE






Method: SW8260CFC004SG-000015-20121002 L1217878-09 N METHOD 10/2/2012 3:21:00 PM S2BVEMSE





SC001SG-000015- WG565979-7 MSD METHOD 10/3/2012 9:16:00 AM S2BVEMSE







SG-TB-20121002 L1217878-13 TB SW5030 10/2/2012 6:01:00 PM S2BVEMWS















Method: SW8270DSIMFC001SG-000015-20121002 L1217878-01 N ALPHA OP-013 10/2/2012 10:54:00 AM S2BVEMSE





FC1004SG-000015-20121002 L1217878-11 FD ALPHA OP-013 10/2/2012 3:21:00 PM S2BVEMSE


SC001SG-000015- WG566238-4 MS ALPHA OP-013 10/3/2012 9:16:00 AM S2BVEMSE

SC001SG-000015- WG566238-5 MSD ALPHA OP-013 10/3/2012 9:16:00 AM S2BVEMSE



















Method: SW9012AFC001SG-000015-20121002 L1217878-01 N SW9010B 10/2/2012 10:54:00 AM S2BVEMSE

FC002SG-000015-20121002 L1217878-03 N SW9010B 10/2/2012 12:20:00 PM S2BVEMSE




FC1004SG-000015-20121002 L1217878-11 FD SW9010B 10/2/2012 3:21:00 PM S2BVEMSE

SC001SG-000015-20121003 L1217878-14 N SW9010B 10/3/2012 9:16:00 AM S2BVEMSE

SC001SG-000015- WG566398-6 DUP SW9010B 10/3/2012 9:16:00 AM S2BVEMSE

SC001SG-000015- WG566398-4 MS SW9010B 10/3/2012 9:16:00 AM S2BVEMSE

SC001SG-000015- WG566398-5 MSD SW9010B 10/3/2012 9:16:00 AM S2BVEMSE



SC004SG-000015-20121003 L1217878-20 N SW9010B 10/3/2012 12:36:00 PM S2BVEMSE




TN001SG-000015-20121004 L1217878-45 N SW9010B 10/4/2012 4:08:00 PM S2BVEMSE

TN001SG-000015-20121004MS WG566440-4 MS SW9010B 10/4/2012 4:08:00 PM S2BVEMSE

TN001SG-000015- WG566440-5 MSD SW9010B 10/4/2012 4:08:00 PM S2BVEMSE

WE001SG-000015-20121004 L1217878-29 N SW9010B 10/4/2012 8:28:00 AM S2BVEMSE

WE002SG-000015-20121004 L1217878-43 N SW9010B 10/4/2012 3:12:00 PM S2BVEMSE







Method: SW9012AWE006SG-000015-20121004 L1217878-37 N SW9010B 10/4/2012 12:21:00 PM S2BVEMSE

WE006SG-000015- WG566400-4 MS SW9010B 10/4/2012 12:21:00 PM S2BVEMSE

WE006SG-000015- WG566400-5 MSD SW9010B 10/4/2012 12:21:00 PM S2BVEMSE



Method: SW9030BFC001SG-000015-20121002 L1217878-01 N METHOD 10/2/2012 10:54:00 AM S2BVEMSE





















Method: SW9030BWE002SG-000015-20121004 L1217878-43 N METHOD 10/4/2012 3:12:00 PM S2BVEMSE








Method: SW9045CFC001SG-000015-20121002 L1217878-01 N METHOD 10/2/2012 10:54:00 AM S2BVEMSE


















Method: SW9045CWE001SG-000015-20121004 L1217878-29 N METHOD 10/4/2012 8:28:00 AM S2BVEMSE









Method: SW9060FC001SG-000015-20121002 L1217878-01 N METHOD 10/2/2012 10:54:00 AM S2BVEMSE

















Method: SW9060SC007SG-000015-20121003 L1217878-24 N METHOD 10/3/2012 2:39:00 PM S2BVEMSE













Validation Label Legend

Label Code Label Decription EPA Level

N/ANV Not_Validated

N/AS1VE Stage_1_Validation_Electronic

N/AS1VEM Stage_1_Validation_Electronic_and_Manual

N/AS1VM Stage_1_Validation_Manual

Level 3 w/o calibrationS2AVE Stage_2A_Validation_Electronic

Level 3 w/o calibrationS2AVEM Stage_2A_Validation_Electronic_and_Manual

Level 3 w/o calibrationS2AVM Stage_2A_Validation_Manual

Level 3 with S2BVE Stage_2B_Validation_Electronic




Level 3 with S2BVEM Stage_2B_Validation_Electronic_and_Manual

Level 3 with S2BVM Stage_2B_Validation_Manual

Level 4S3VE Stage_3_Validation_Electronic

Level 4S3VEM Stage_3_Validation_Electronic_and_Manual

Level 4S3VM Stage_3_Validation_Manual







Lab Reporting Batch: L1218042

Method: SM2540GHB001SG-000015-20121006 L1218042-29 N METHOD 10/6/2012 3:54:00 PM S2BVEMSE

HB001SG-000015- WG565958-1 DUP METHOD 10/6/2012 3:54:00 PM S2BVEMSE

HB002SG-000015-20121006 L1218042-27 N METHOD 10/6/2012 3:05:00 PM S2BVEMSE




HB006SG-000015-20121006 L1218042-17 N METHOD 10/6/2012 11:30:00 AM S2BVEMSE



HB1005SG-000015-20121006 L1218042-21 FD METHOD 10/6/2012 12:19:00 PM S2BVEMSE

TN002SG-000011-20121005 L1218042-03 N METHOD 10/5/2012 10:41:00 AM S2BVEMSE





Method: SM4500NH3HHB001SG-000015-20121006 L1218042-29 N METHOD 10/6/2012 3:54:00 PM S2BVEMSE


HB001SG-000015- WG567349-4 MS METHOD 10/6/2012 3:54:00 PM S2BVEMSE





11/13/2012 8:57:12 AM ADR version 1.6.0.185 Page 1 of 11



Method: SM4500NH3HHB006SG-000015-20121006 L1218042-17 N METHOD 10/6/2012 11:30:00 AM S2BVEMSE









Method: SM4500NO3FHB001SG-000015-20121006 L1218042-29 N METHOD 10/6/2012 3:54:00 PM S2BVEMSE













TN005SG-000014- WG567243-3 DUP METHOD 10/5/2012 9:32:00 AM S2BVEMSE




Method: SM4500NO3FTN005SG-000014-20121005MS WG567243-4 MS METHOD 10/5/2012 9:32:00 AM S2BVEMSE


Method: SM4500NorgCHB001SG-000015-20121006 L1218042-29 N METHOD 10/6/2012 3:54:00 PM S2BVEMSE
















Method: SM4500PEHB001SG-000015-20121006 L1218042-29 N METHOD 10/6/2012 3:54:00 PM S2BVEMSE







Method: SM4500PEHB003SG-000015-20121006 L1218042-25 N METHOD 10/6/2012 2:21:00 PM S2BVEMSE












Method: SOOTCHB001SG-000015-20121006 L1218042-29 N METHOD 10/6/2012 3:54:00 PM S2BVEMSE














Method: SOOTCTN003SG-000015-20121005 L1218042-05 N METHOD 10/5/2012 11:24:00 AM S2BVEMSE




TN005SG-000014-20121005MS WG566732-4 MS METHOD 10/5/2012 9:32:00 AM S2BVEMSE


Method: SW6020AHB001SG-000015-20121006 L1218042-29 N EPA 3050B 10/6/2012 3:54:00 PM S2BVEMSE

HB002SG-000015-20121006 L1218042-27 N EPA 3050B 10/6/2012 3:05:00 PM S2BVEMSE




HB006SG-000015-20121006 L1218042-17 N EPA 3050B 10/6/2012 11:30:00 AM S2BVEMSE



HB1005SG-000015-20121006 L1218042-21 FD EPA 3050B 10/6/2012 12:19:00 PM S2BVEMSE

SG-RB-20121006 L1218042-11 EB SW3020A 10/6/2012 9:05:00 AM S2BVEMWS

TN002SG-000011-20121005 L1218042-03 N EPA 3050B 10/5/2012 10:41:00 AM S2BVEMSE




TN005SG-000014- WG568938-3 DUP EPA 3050B 10/5/2012 9:32:00 AM S2BVEMSE






Method: SW6020ATN005SG-000014-20121005MS WG568938-4 MS EPA 3050B 10/5/2012 9:32:00 AM S2BVEMSE

TN005SG-000014-20121005MS WG568940-4 MS EPA 3050B 10/5/2012 9:32:00 AM S2BVEMSE

TN005SG-000014-20121005MS WG570724-4 MS EPA 3050B 10/5/2012 9:32:00 AM S2BVEMSE

TN006SG-000015-20121005 L1218042-09 N EPA 3050B 10/5/2012 1:16:00 PM S2BVEMSE

Method: SW8015MHB001SG-000015-20121006 L1218042-29 N ALPHA OP-013 10/6/2012 3:54:00 PM S2BVEMSE

HB002SG-000015-20121006 L1218042-27 N ALPHA OP-013 10/6/2012 3:05:00 PM S2BVEMSE




HB006SG-000015-20121006 L1218042-17 N ALPHA OP-013 10/6/2012 11:30:00 AM S2BVEMSE



HB1005SG-000015-20121006 L1218042-21 FD ALPHA OP-013 10/6/2012 12:19:00 PM S2BVEMSE

SG-RB-20121006 L1218042-11 EB SW3510C 10/6/2012 9:05:00 AM S2BVEMWS

TN002SG-000011-20121005 L1218042-03 N ALPHA OP-013 10/5/2012 10:41:00 AM S2BVEMSE





Method: SW8260CHB001SG-000015-20121006 L1218042-29 N METHOD 10/6/2012 3:54:00 PM S2BVEMSE












SG-RB-20121006 L1218042-11 EB SW5030 10/6/2012 9:05:00 AM S2BVEMWS







Method: SW8270DSIMHB001SG-000015-20121006 L1218042-29 N ALPHA OP-013 10/6/2012 3:54:00 PM S2BVEMSE








HB1005SG-000015-20121006 L1218042-21 FD ALPHA OP-013 10/6/2012 12:19:00 PM S2BVEMSE

SG-RB-20121006 L1218042-11 EB SW3510C 10/6/2012 9:05:00 AM S2BVEMWS




Method: SW8270DSIMTN002SG-000011-20121005 L1218042-03 N ALPHA OP-013 10/5/2012 10:41:00 AM S2BVEMSE





Method: SW9012AHB001SG-000015-20121006 L1218042-29 N SW9010B 10/6/2012 3:54:00 PM S2BVEMSE

HB001SG-000015- WG567330-4 MS SW9010B 10/6/2012 3:54:00 PM S2BVEMSE

HB001SG-000015- WG567330-5 MSD SW9010B 10/6/2012 3:54:00 PM S2BVEMSE

HB002SG-000015-20121006 L1218042-27 N SW9010B 10/6/2012 3:05:00 PM S2BVEMSE




HB006SG-000015-20121006 L1218042-17 N SW9010B 10/6/2012 11:30:00 AM S2BVEMSE



HB1005SG-000015-20121006 L1218042-21 FD SW9010B 10/6/2012 12:19:00 PM S2BVEMSE

HB1005SG-000015- WG567329-4 MS SW9010B 10/6/2012 12:19:00 PM S2BVEMSE

HB1005SG-000015- WG567329-5 MSD SW9010B 10/6/2012 12:19:00 PM S2BVEMSE

TN002SG-000011-20121005 L1218042-03 N SW9010B 10/5/2012 10:41:00 AM S2BVEMSE




TN006SG-000015-20121005 L1218042-09 N SW9010B 10/5/2012 1:16:00 PM S2BVEMSE




Method: SW9030BHB001SG-000015-20121006 L1218042-29 N METHOD 10/6/2012 3:54:00 PM S2BVEMSE













TN004SG-000015-20121005MS WG566113-4 MS METHOD 10/5/2012 11:46:00 AM S2BVEMSE













Method: SW9045CHB008SG-000015-20121006 L1218042-13 N METHOD 10/6/2012 9:55:00 AM S2BVEMSE








Method: SW9060HB001SG-000015-20121006 L1218042-29 N METHOD 10/6/2012 3:54:00 PM S2BVEMSE


















Method: SW9060TN005SG-000014-20121005MS WG566725-4 MS METHOD 10/5/2012 9:32:00 AM S2BVEMSE


Validation Label Legend

Label Code Label Decription EPA Level

N/ANV Not_Validated

N/AS1VE Stage_1_Validation_Electronic

N/AS1VEM Stage_1_Validation_Electronic_and_Manual

N/AS1VM Stage_1_Validation_Manual

Level 3 w/o calibrationS2AVE Stage_2A_Validation_Electronic

Level 3 w/o calibrationS2AVEM Stage_2A_Validation_Electronic_and_Manual

Level 3 w/o calibrationS2AVM Stage_2A_Validation_Manual

Level 3 with S2BVE Stage_2B_Validation_Electronic

Level 3 with S2BVEM Stage_2B_Validation_Electronic_and_Manual

Level 3 with S2BVM Stage_2B_Validation_Manual








QC Outlier Report: HoldingTimes

Lab Reporting Batch ID: L1217878 Laboratory: AAL

EDD Filename: PrepL1217878 eQAPP Name: Newtown Creek - Alpha

Preparation Method: METHODMethod: SOOTC

Matrix: SE

Sample ID Type Actual Criteria Units Flag

FC001SG-000015-20121002 (RE/TFC001SG-000015-20121002 (RES/TFC002SG-000015-20121002 (RE/TFC002SG-000015-20121002 (RES/TFC003SG-000015-20121002 (RE/TFC003SG-000015-20121002 (RES/TFC004SG-000015-20121002 (RE/TFC004SG-000015-20121002 (RES/TFC005SG-000015-20121002 (RE/TFC005SG-000015-20121002 (RES/TFC1004SG-000015-20121002 (RE/TFC1004SG-000015-20121002 (RES/TN001SG-000015-20121004 (RE/TTN001SG-000015-20121004 (RES/TWE001SG-000015-20121004 (RE/TWE001SG-000015-20121004 (RES/WE001SG-000015-20121004DUP (WE001SG-000015-20121004DUP (WE001SG-000015-20121004MS (RWE001SG-000015-20121004MS (RWE002SG-000015-20121004 (RE/TWE002SG-000015-20121004 (RES/WE007SG-000015-20121004 (RE/TWE007SG-000015-20121004 (RES/WE008SG-000015-20121004 (RE/TWE008SG-000015-20121004 (RES/

Sampling To Analysis 17.0017.0015.0015.0017.0017.0017.0017.0015.0015.0017.0017.0015.0015.0015.0015.0015.0015.0015.0015.0015.0015.0015.0015.0015.0015.00

14.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.00

DAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYS

J (all detects)UJ (all non-detects)

Project Name and Number: 120782-01.01 - ADR version 1.6.0.18511/9/2012 3:44:10 PM Page 1 of 1

QC Outlier Report: HoldingTimes

Lab Reporting Batch ID: L1218042 Laboratory: AALEDD Filename: PrepL1218042 eQAPP Name: Newtown Creek - Alpha

Preparation Method: METHODMethod: SOOTC

Matrix: SE

Sample ID Type Actual Criteria Units Flag

HB001SG-000015-20121006 (RE/THB001SG-000015-20121006 (RES/HB002SG-000015-20121006 (RE/THB002SG-000015-20121006 (RES/HB003SG-000015-20121006 (RE/THB003SG-000015-20121006 (RES/HB004SG-000015-20121006 (RE/THB004SG-000015-20121006 (RES/HB005SG-000015-20121006 (RE/THB005SG-000015-20121006 (RES/HB006SG-000015-20121006 (RE/THB006SG-000015-20121006 (RES/HB007SG-000015-20121006 (RE/THB007SG-000015-20121006 (RES/HB008SG-000015-20121006 (RE/THB008SG-000015-20121006 (RES/HB1005SG-000015-20121006 (RE/THB1005SG-000015-20121006 (RES/SRM 1650B (RE/TOT)SRM 1650B (RES/TOT)TN002SG-000011-20121005 (RE/TTN002SG-000011-20121005 (RES/TTN003SG-000015-20121005 (RE/TTN003SG-000015-20121005 (RES/TTN004SG-000015-20121005 (RE/TTN004SG-000015-20121005 (RES/TTN005SG-000014-20121005 (RE/TTN005SG-000014-20121005 (RES/TTN005SG-000014-20121005DUP (RTN005SG-000014-20121005DUP (RTN005SG-000014-20121005MS (RETN005SG-000014-20121005MS (RETN006SG-000015-20121005 (RE/TTN006SG-000015-20121005 (RES/T

Sampling To Analysis 18.0018.0018.0018.0018.0018.0018.0018.0018.0018.0018.0018.0018.0018.0018.0018.0018.0018.0018.0018.0019.0019.0019.0019.0019.0019.0019.0019.0019.0019.0019.0019.0019.0019.00

14.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.0014.00

DAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYSDAYS


Project Name and Number: 120782-01.01 - ADR version 1.6.0.18511/13/2012 8:56:45 AM Page 1 of 1

Method Blank Outlier Report



Method: SM4500PE

Matrix: SE

Method Blank Sample ID Analysis Date Analyte Result

AssociatedSamples

WG567407-1 10/16/2012 12:00:00 PM PHOSPHORUS 2.8 mg/kg FC001SG-000015-20121002FC002SG-000015-20121002FC003SG-000015-20121002FC004SG-000015-20121002FC005SG-000015-20121002FC1004SG-000015-20121002SC001SG-000015-20121003SC002SG-000015-20121003SC003SG-000015-20121003SC004SG-000015-20121003SC005SG-000015-20121003SC006SG-000015-20121003SC007SG-000015-20121003

WG567408-1 10/16/2012 12:40:00 PM PHOSPHORUS 3.3 mg/kg TN001SG-000015-20121004WE001SG-000015-20121004WE002SG-000015-20121004WE003SG-000010-20121004WE004SG-000015-20121004WE005SG-000015-20121004WE006SG-000015-20121004WE007SG-000015-20121004WE008SG-000015-20121004

Method: SW6020A

Matrix: SE


AssociatedSamples

WG567869-1 10/19/2012 5:23:00 PM ALUMINUMIRONMAGNESIUMPOTASSIUMSODIUMZINC

2.75 mg/kg5.41 mg/kg1.81 mg/kg2.72 mg/kg6.12 mg/kg0.354 mg/kg

FC001SG-000015-20121002FC002SG-000015-20121002FC003SG-000015-20121002FC004SG-000015-20121002FC005SG-000015-20121002FC1004SG-000015-20121002SC001SG-000015-20121003SC002SG-000015-20121003SC003SG-000015-20121003SC004SG-000015-20121003SC005SG-000015-20121003SC006SG-000015-20121003SC007SG-000015-20121003WE001SG-000015-20121004WE003SG-000010-20121004WE004SG-000015-20121004WE005SG-000015-20121004WE006SG-000015-20121004WE007SG-000015-20121004WE008SG-000015-20121004

WG567890-1 10/22/2012 7:38:00 PM ARSENICBERYLLIUMCADMIUMCHROMIUMCOBALTCOPPERLEADNICKELVANADIUM

0.027 mg/kg0.015 mg/kg0.016 mg/kg0.055 mg/kg0.035 mg/kg0.082 mg/kg0.040 mg/kg0.059 mg/kg0.039 mg/kg

TN001SG-000015-20121004WE002SG-000015-20121004

Project Name and Number: 120782-01.01 - NEWTOWN CREEK RI11/9/2012 3:35:47 PM ADR version 1.6.0.185 Page 1 of 3




Method: SW8015M

Matrix: SE


AssociatedSamples

WG566238-1 10/15/2012 4:52:00 PM Diesel range organics (C10 - C28) 1.28 mg/kg FC001SG-000015-20121002FC002SG-000015-20121002FC003SG-000015-20121002FC004SG-000015-20121002FC005SG-000015-20121002FC1004SG-000015-20121002SC001SG-000015-20121003SC002SG-000015-20121003SC003SG-000015-20121003SC004SG-000015-20121003SC005SG-000015-20121003SC006SG-000015-20121003SC007SG-000015-20121003

WG566239-1 10/19/2012 3:50:00 PM Diesel range organics (C10 - C28) 0.315 mg/kg TN001SG-000015-20121004WE001SG-000015-20121004WE002SG-000015-20121004WE003SG-000010-20121004WE004SG-000015-20121004WE005SG-000015-20121004WE006SG-000015-20121004WE007SG-000015-20121004WE008SG-000015-20121004

Method: SW8260C

Matrix: SE


AssociatedSamples

WG565979-5 10/9/2012 8:58:00 AM CARBON DISULFIDE 0.66 ug/kg FC001SG-000015-20121002FC002SG-000015-20121002FC003SG-000015-20121002FC004SG-000015-20121002FC005SG-000015-20121002FC1004SG-000015-20121002SC001SG-000015-20121003SC002SG-000015-20121003SC003SG-000015-20121003SC004SG-000015-20121003SC005SG-000015-20121003SC006SG-000015-20121003SC007SG-000015-20121003

WG566341-5 10/10/2012 9:19:00 AM CARBON DISULFIDE 0.75 ug/kg TN001SG-000015-20121004WE001SG-000015-20121004WE002SG-000015-20121004WE003SG-000010-20121004WE004SG-000015-20121004WE005SG-000015-20121004WE006SG-000015-20121004WE007SG-000015-20121004WE008SG-000015-20121004

The following samples and their listed target analytes were qualified due to contamination reported in this blank

Sample ID AnalyteReported

ResultModified

Final Result

FC001SG-000015-20121002(RES/TOT) CARBON DISULFIDE 5.8 ug/kg 22U ug/kg

WE001SG-000015-20121004(RES/TOT) CARBON DISULFIDE 6.2 ug/kg 24U ug/kg





Method: SW8260C

Matrix: WS


AssociatedSamples

WG567074-5 10/15/2012 9:56:00 AM CHLOROMETHANE 0.29 ug/l SG-TB-20121002SG-TB-20121003SG-TB-20121004



ResultModified

Final Result

SG-TB-20121002(RES/TOT) CHLOROMETHANE 0.39 ug/l 2.5U ug/l




Method Blank Outlier ReportLab Reporting Batch ID: L1218042 Laboratory: AAL


Method: SM4500NH3HMatrix: SE


AssociatedSamples

WG567349-1 10/18/2012 9:40:00 PM Ammonia as nitrogen 1.4 mg/kg HB001SG-000015-20121006HB002SG-000015-20121006HB003SG-000015-20121006HB004SG-000015-20121006HB005SG-000015-20121006HB006SG-000015-20121006HB007SG-000015-20121006HB008SG-000015-20121006HB1005SG-000015-20121006TN002SG-000011-20121005TN003SG-000015-20121005TN004SG-000015-20121005TN005SG-000014-20121005TN006SG-000015-20121005

Method: SW6020AMatrix: SE


AssociatedSamples

WG568940-1 10/24/2012 5:26:00 PM ARSENICCOPPERIRONMANGANESENICKELPOTASSIUMSODIUMTHALLIUMVANADIUMZINC

0.014 mg/kg0.039 mg/kg2.96 mg/kg0.068 mg/kg0.041 mg/kg2.20 mg/kg3.39 mg/kg0.004 mg/kg0.108 mg/kg0.388 mg/kg

HB001SG-000015-20121006HB002SG-000015-20121006HB003SG-000015-20121006HB004SG-000015-20121006HB005SG-000015-20121006HB006SG-000015-20121006HB007SG-000015-20121006HB008SG-000015-20121006HB1005SG-000015-20121006TN002SG-000011-20121005TN003SG-000015-20121005TN004SG-000015-20121005TN005SG-000014-20121005TN006SG-000015-20121005

WG570724-1 10/31/2012 3:23:00 PM TIN 1.54 mg/kg HB001SG-000015-20121006HB002SG-000015-20121006HB003SG-000015-20121006HB004SG-000015-20121006HB005SG-000015-20121006HB006SG-000015-20121006HB007SG-000015-20121006HB008SG-000015-20121006HB1005SG-000015-20121006TN002SG-000011-20121005TN003SG-000015-20121005TN004SG-000015-20121005TN005SG-000014-20121005TN006SG-000015-20121005



ResultModified

Final Result

HB006SG-000015-20121006(RE/TOT) TIN 4.47 mg/kg 6.69U mg/kg

TN004SG-000015-20121005(RE/TOT) TIN 6.06 mg/kg 6.06U mg/kg


Project Name and Number: 120782-01.01 - NEWTOWN CREEK RI11/13/2012 8:54:59 AM ADR version 1.6.0.185 Page 1 of 4





AssociatedSamples



ResultModified

Final Result


Method: SW6020AMatrix: WS


AssociatedSamples

WG567654-1 10/23/2012 6:02:00 PM ARSENICBARIUMCOPPERIRONMAGNESIUMMANGANESENICKELSODIUMTHALLIUMVANADIUMZINC

0.0001 mg/l0.0001 mg/l0.0003 mg/l0.009 mg/l0.013 mg/l0.0004 mg/l0.0003 mg/l0.017 mg/l

0.00003 mg/l0.001 mg/l0.003 mg/l

SG-RB-20121006



ResultModified

Final Result

SG-RB-20121006(RES/TOT) BARIUM 0.0002 mg/l 0.0005U mg/l

SG-RB-20121006(RES/TOT) COPPER 0.001 mg/l 0.001U mg/l

SG-RB-20121006(RES/TOT) IRON 0.013 mg/l 0.050U mg/l

SG-RB-20121006(RES/TOT) MANGANESE 0.0008 mg/l 0.0008U mg/l

SG-RB-20121006(RES/TOT) NICKEL 0.0007 mg/l 0.0007U mg/l

SG-RB-20121006(RES/TOT) THALLIUM 0.00001 mg/l 0.00020U mg/l

SG-RB-20121006(RES/TOT) ZINC 0.005 mg/l 0.010U mg/l




Method: SW8015MMatrix: SE


AssociatedSamples

WG566754-1 10/19/2012 6:33:00 PM Diesel range organics (C10 - C28)Total petroleum hydrocarbons (C9-C40)

0.338 mg/kg0.525 mg/kg

HB001SG-000015-20121006HB002SG-000015-20121006HB003SG-000015-20121006HB004SG-000015-20121006HB005SG-000015-20121006HB006SG-000015-20121006HB007SG-000015-20121006HB008SG-000015-20121006HB1005SG-000015-20121006TN002SG-000011-20121005TN003SG-000015-20121005TN004SG-000015-20121005TN005SG-000014-20121005TN006SG-000015-20121005

Method: SW8015MMatrix: WS


AssociatedSamples

WG566066-1 10/11/2012 2:19:00 PM Diesel range organics (C10 - C28)n-Octadecane (C18)

0.010 mg/l0.001 mg/l

SG-RB-20121006



ResultModified

Final Result

SG-RB-20121006(RES/TOT) Diesel range organics (C10 - C28) 0.028 mg/l 0.028U mg/l

SG-RB-20121006(RES/TOT) n-Octadecane (C18) 0.001 mg/l 0.001U mg/l

Method: SW8260CMatrix: SE


AssociatedSamples

WG566791-5 10/11/2012 6:17:00 PM METHYLENE CHLORIDE 4.2 ug/kg HB001SG-000015-20121006HB002SG-000015-20121006HB003SG-000015-20121006HB004SG-000015-20121006HB005SG-000015-20121006HB006SG-000015-20121006HB007SG-000015-20121006HB008SG-000015-20121006HB1005SG-000015-20121006TN002SG-000011-20121005TN003SG-000015-20121005TN004SG-000015-20121005TN005SG-000014-20121005TN006SG-000015-20121005




Method: SW8270DSIMMatrix: WS


AssociatedSamples

WG566066-1 10/12/2012 6:29:00 PM Decalin, cis & trans- 2.30 ng/l SG-RB-20121006



ResultModified

Final Result

SG-RB-20121006(RES/TOT) Decalin, cis & trans- 3.02 ng/l 5.81U ng/l


Initial Calibration Verification Outliers



Method Category: GENCHEM

Method: SM4500PE

Analysis Date AnalyteRRF

(Limits)Percent*(Limits)

AssociatedSamples Flag

10/16/2012 12:00:00 PM

PHOSPHORUS - 127 (125.00) FC001SG-000015-20121002

FC002SG-000015-20121002

FC003SG-000015-20121002

FC004SG-000015-20121002

FC005SG-000015-20121002

FC1004SG-000015-20121002

SC001SG-000015-20121003

SC002SG-000015-20121003

SC003SG-000015-20121003

SC004SG-000015-20121003

SC005SG-000015-20121003

SC006SG-000015-20121003

SC007SG-000015-20121003

J (all detects)

* - Could refer to Percent DIfference or Percent Recovery depending on method requirements.


Continuing Calibration Verification Outliers



Method Category: GENCHEM

Method: SM4500PE




10/16/2012 12:00:00 PM

PHOSPHORUS - 132 (120.00) FC001SG-000015-20121002

FC002SG-000015-20121002

FC003SG-000015-20121002

FC004SG-000015-20121002

FC005SG-000015-20121002

FC1004SG-000015-20121002

SC001SG-000015-20121003

SC002SG-000015-20121003

SC003SG-000015-20121003

SC004SG-000015-20121003

SC005SG-000015-20121003

SC006SG-000015-20121003

SC007SG-000015-20121003

J (all detects)

Method Category: VOA

Method: SW8260C




10/15/2012 8:40:00 AM

2-BUTANONE - 22.48971 (20.00)

J (all detects)

10/9/2012 8:05:00 AM

BROMOMETHANE - 23.95292 (20.00)

J (all detects)

10/15/2012 8:40:00 AM

1,1,2,2-TETRACHLOROETHANE 0.22544 (0.30)

- J (all detects)UJ (all non-detects)

10/10/2012 8:25:00 AM

BROMOMETHANE - -21.86676 (-20.00)


10/15/2012 8:40:00 AM

BROMOMETHANE - -27.10272 (-20.00)




Continuing Calibration Verification OutliersLab Reporting Batch ID: L1218042 Laboratory: AAL


Method Category: VOA

Method: SW8260C




10/17/2012 5:54:00 AM

1,2-DIBROMO-3-CHLOROPROPANECARBON TETRACHLORIDECIS-1,3-DICHLOROPROPENEDIBROMOCHLOROMETHANETRANS-1,3-DICHLOROPROPENEVINYL ACETATE

------

20.53734 (20.00)

32.25594 (20.00)

24.34813 (20.00)

21.76936 (20.00)

25.26609 (20.00)

22.817 (20.00)

J (all detects)

10/11/2012 5:51:00 PM

VINYL CHLORIDE - 23.7073 (20.00) J (all detects)

10/11/2012 5:51:00 PM

ACETONECHLOROETHANEDICHLORODIFLUOROMETHANEMETHYLENE CHLORIDE

----

-26.28874 (-20.00)

-27.7214 (-20.00)

-49.42812 (-20.00)

-23.39735 (-20.00)




Lab Control Spike/Lab Control Spike Duplicate Outlier Report



Method: SM4500PE

Matrix: SE

QC Sample ID(Associated

Samples) CompoundLCS%R

%RLimits Flag

LCSD%R

AffectedCompounds

RPD(Limits)

WG567407-2 (FC001SG-000015-20121002 FC002SG-000015-20121002 FC003SG-000015-20121002 FC004SG-000015-20121002 FC005SG-000015-20121002 FC1004SG-000015-20121002 SC001SG-000015-20121003 SC002SG-000015-20121003 SC003SG-000015-20121003 SC004SG-000015-20121003 SC005SG-000015-20121003 SC006SG-000015-20121003 SC007SG-000015-20121003)

PHOSPHORUS 127 - 75.00-125.00 - PHOSPHORUS

J (all detects)


Lab Control Spike/Lab Control Spike Duplicate Outlier Report



Method: SW8260C

Matrix: SE


Samples) CompoundLCS%R

%RLimits Flag

LCSD%R

AffectedCompounds

RPD(Limits)

WG566791-4 (HB001SG-000015-20121006 HB002SG-000015-20121006 HB003SG-000015-20121006 HB004SG-000015-20121006 HB005SG-000015-20121006 HB006SG-000015-20121006 HB007SG-000015-20121006 HB008SG-000015-20121006 HB1005SG-000015-20121006 TN002SG-000011-20121005 TN003SG-000015-20121005 TN004SG-000015-20121005 TN005SG-000014-20121005 TN006SG-000015-20121005)

DICHLORODIFLUOROMETHANMETHYLENE CHLORIDE

--

161153

50.00-150.0050.00-150.00

--

DICHLORODIFLUOROMETHAMETHYLENE CHLORIDE

J (all detects)


Matrix Spike/Matrix Spike Duplicate Outlier Report



Method: SW9030B

Matrix: SE


Samples) CompoundMS%R

%RLimits Flag

MSD%R

AffectedCompounds

RPD(Limits)

SC001SG-000015-20121003MS (FC001SG-000015-20121002 FC002SG-000015-20121002 FC003SG-000015-20121002 FC004SG-000015-20121002 FC005SG-000015-20121002 FC1004SG-000015-20121002 SC001SG-000015-20121003 SC002SG-000015-20121003 SC003SG-000015-20121003 SC004SG-000015-20121003 SC005SG-000015-20121003 SC006SG-000015-20121003 SC007SG-000015-20121003)

SULFIDE 700 - 65.00-135.00 - SULFIDE

J (all detects)

WE003SG-000010-20121004MS (TN001SG-000015-20121004 WE001SG-000015-20121004 WE002SG-000015-20121004 WE003SG-000010-20121004 WE004SG-000015-20121004 WE005SG-000015-20121004 WE006SG-000015-20121004 WE007SG-000015-20121004 WE008SG-000015-20121004)

SULFIDE 0 - 65.00-135.00 - SULFIDE

J(all detects)R(all non-detects)

Method: SW8260C

Matrix: SE



%RLimits Flag

MSD%R

AffectedCompounds

RPD(Limits)

SC001SG-000015-20121003MS SC001SG-000015-20121003MSD (SC001SG-000015-20121003)

ACETONECYCLOHEXANEMETHYL ACETATE

000

000

50.00-150.0050.00-150.0050.00-150.00

---

ACETONECYCLOHEXANEMETHYL ACETATE


SC001SG-000015-20121003MS SC001SG-000015-20121003MSD (SC001SG-000015-20121003)

1,1,2,2-TETRACHLOROETHANE1,2,3-TRICHLOROBENZENE1,2,4-TRICHLOROBENZENE1,2-DIBROMO-3-CHLOROPROP1,2-DIBROMOETHANE1,2-DICHLOROBENZENE1,3-DICHLOROBENZENE1,4-DICHLOROBENZENE2-BUTANONE2-HEXANONE4-METHYL-2-PENTANONEBROMODICHLOROMETHANEBROMOFORMCHLOROBENZENECIS-1,3-DICHLOROPROPENEDIBROMOCHLOROMETHANEETHYL BENZENEISOPROPYLBENZENEm,p-XyleneMETHYL CYCLOHEXANEO-XYLENESTYRENETETRACHLOROETHENETRANS-1,3-DICHLOROPROPENVINYL ACETATE

45121440462525262847--

34434639454142434034-

4114

42101044442121211344494626394232413638393629433511

50.00-150.0050.00-150.0050.00-150.0050.00-150.0050.00-150.0050.00-150.0050.00-150.0050.00-150.0050.00-150.0050.00-150.0050.00-150.0050.00-150.0050.00-150.0050.00-150.0050.00-150.0050.00-150.0050.00-150.0050.00-150.0050.00-150.0050.00-150.0050.00-150.0050.00-150.0050.00-150.0050.00-150.0050.00-150.00

-------------------------

1,1,2,2-TETRACHLOROETHAN1,2,3-TRICHLOROBENZENE1,2,4-TRICHLOROBENZENE1,2-DIBROMO-3-CHLOROPRO1,2-DIBROMOETHANE1,2-DICHLOROBENZENE1,3-DICHLOROBENZENE1,4-DICHLOROBENZENE2-BUTANONE2-HEXANONE4-METHYL-2-PENTANONEBROMODICHLOROMETHANEBROMOFORMCHLOROBENZENECIS-1,3-DICHLOROPROPENEDIBROMOCHLOROMETHANEETHYL BENZENEISOPROPYLBENZENEm,p-XyleneMETHYL CYCLOHEXANEO-XYLENESTYRENETETRACHLOROETHENETRANS-1,3-DICHLOROPROPEVINYL ACETATE

J(all detects)UJ(all non-detects)





Method: SW8260C

Matrix: SE



%RLimits Flag

MSD%R

AffectedCompounds

RPD(Limits)

Method: SW8015M

Matrix: SE



%RLimits Flag

MSD%R

AffectedCompounds

RPD(Limits)

SC001SG-000015-20121003MS (SC001SG-000015-20121003)

n-Nonane (C9) 44.1 - 50.00-150.00 - n-Nonane (C9)J(all detects)

UJ(all non-detects)

Method: SW6020A

Matrix: SE



%RLimits Flag

MSD%R

AffectedCompounds

RPD(Limits)

SC001SG-000015-20121003MS (TOT) (FC001SG-000015-20121002 FC002SG-000015-20121002 FC003SG-000015-20121002 FC004SG-000015-20121002 FC005SG-000015-20121002 FC1004SG-000015-20121002 SC001SG-000015-20121003 SC002SG-000015-20121003 SC003SG-000015-20121003 SC004SG-000015-20121003 SC005SG-000015-20121003 SC006SG-000015-20121003 SC007SG-000015-20121003 WE001SG-000015-20121004 WE003SG-000010-20121004 WE004SG-000015-20121004 WE005SG-000015-20121004 WE006SG-000015-20121004 WE007SG-000015-20121004 WE008SG-000015-20121004)

ANTIMONY 24 - 75.00-125.00 - ANTIMONY






Method: SW6020A

Matrix: SE



%RLimits Flag

MSD%R

AffectedCompounds

RPD(Limits)


ALUMINUMIRON

177128

--

75.00-125.0075.00-125.00

--

ALUMINUMIRON

J(all detects)


TIN 0 - 75.00-125.00 - TIN






Method: SW9030B

Matrix: SE



%RLimits Flag

MSD%R

AffectedCompounds

RPD(Limits)

TN004SG-000015-20121005MS (HB001SG-000015-20121006 HB002SG-000015-20121006 HB003SG-000015-20121006 HB004SG-000015-20121006 HB005SG-000015-20121006 HB006SG-000015-20121006 HB007SG-000015-20121006 HB008SG-000015-20121006 HB1005SG-000015-20121006 TN002SG-000011-20121005 TN003SG-000015-20121005 TN004SG-000015-20121005 TN005SG-000014-20121005 TN006SG-000015-20121005)

SULFIDE 390 - 65.00-135.00 - SULFIDE

J (all detects)

Method: SM4500PE

Matrix: SE



%RLimits Flag

MSD%R

AffectedCompounds

RPD(Limits)

HB001SG-000015-20121006MS (HB001SG-000015-20121006 HB002SG-000015-20121006 HB003SG-000015-20121006 HB004SG-000015-20121006 HB005SG-000015-20121006 HB006SG-000015-20121006 HB007SG-000015-20121006 HB008SG-000015-20121006 HB1005SG-000015-20121006 TN002SG-000011-20121005 TN003SG-000015-20121005 TN004SG-000015-20121005 TN005SG-000014-20121005 TN006SG-000015-20121005)

PHOSPHORUS 14 - 65.00-135.00 - PHOSPHORUS






Method: SW6020A

Matrix: SE



%RLimits Flag

MSD%R

AffectedCompounds

RPD(Limits)

TN005SG-000014-20121005MS (TOT) (HB001SG-000015-20121006 HB002SG-000015-20121006 HB003SG-000015-20121006 HB004SG-000015-20121006 HB005SG-000015-20121006 HB006SG-000015-20121006 HB007SG-000015-20121006 HB008SG-000015-20121006 HB1005SG-000015-20121006 TN002SG-000011-20121005 TN003SG-000015-20121005 TN004SG-000015-20121005 TN005SG-000014-20121005 TN006SG-000015-20121005)

ANTIMONY 25 - 75.00-125.00 - ANTIMONY


TN005SG-000014-20121005MS (TOT) (HB001SG-000015-20121006 HB002SG-000015-20121006 HB003SG-000015-20121006 HB004SG-000015-20121006 HB005SG-000015-20121006 HB006SG-000015-20121006 HB007SG-000015-20121006 HB008SG-000015-20121006 HB1005SG-000015-20121006 TN002SG-000011-20121005 TN003SG-000015-20121005 TN004SG-000015-20121005 TN005SG-000014-20121005 TN006SG-000015-20121005)

ALUMINUMCALCIUMIRON

179752384

---

75.00-125.0075.00-125.0075.00-125.00

---

ALUMINUMCALCIUMIRON

J(all detects)


Lab Duplicate Outlier ReportLab Reporting Batch ID: L1218042 Laboratory: AAL


Method: SW9030BMatrix: SE

QC Sample ID(Associated Sample ID) Analyte

SampleRPD

eQAPPRPD Flag

TN003SG-000015-20121005DUP (HB001SG-000015-20121006 HB002SG-000015-20121006 HB003SG-000015-20121006 HB004SG-000015-20121006 HB005SG-000015-20121006 HB006SG-000015-20121006 HB007SG-000015-20121006 HB008SG-000015-20121006 HB1005SG-000015-20121006 TN002SG-000011-20121005 TN003SG-000015-20121005 TN004SG-000015-20121005 TN005SG-000014-20121005 TN006SG-000015-20121005)

SULFIDE 33 30.00


Method: SM4500NO3FMatrix: SE


SampleRPD

eQAPPRPD Flag

TN005SG-000014-20121005DUP (HB001SG-000015-20121006 HB002SG-000015-20121006 HB003SG-000015-20121006 HB004SG-000015-20121006 HB005SG-000015-20121006 HB006SG-000015-20121006 HB007SG-000015-20121006 HB008SG-000015-20121006 HB1005SG-000015-20121006 TN002SG-000011-20121005 TN003SG-000015-20121005 TN004SG-000015-20121005 TN005SG-000014-20121005 TN006SG-000015-20121005)

Nitrate + nitrite as nitrogen 30 20.00


Project Name and Number: 120782-01.01 - NEWTOWN CREEK RIADR version 1.6.0.18511/13/2012 8:53:56 AM Page 1 of 2

Lab Duplicate Outlier ReportLab Reporting Batch ID: L1218042 Laboratory: AAL


Method: SOOTCMatrix: SE


SampleRPD

eQAPPRPD Flag

TN005SG-000014-20121005DUP (HB001SG-000015-20121006 HB002SG-000015-20121006 HB003SG-000015-20121006 HB004SG-000015-20121006 HB005SG-000015-20121006 HB006SG-000015-20121006 HB007SG-000015-20121006 HB008SG-000015-20121006 HB1005SG-000015-20121006 SRM 1650B TN002SG-000011-20121005 TN003SG-000015-20121005 TN004SG-000015-20121005 TN005SG-000014-20121005 TN006SG-000015-20121005)

Soot Carbon 79 25.00




SampleRPD

eQAPPRPD Flag

TN005SG-000014-20121005DUP (TOT) (HB001SG-000015-20121006 HB002SG-000015-20121006 HB003SG-000015-20121006 HB004SG-000015-20121006 HB005SG-000015-20121006 HB006SG-000015-20121006 HB007SG-000015-20121006 HB008SG-000015-20121006 HB1005SG-000015-20121006 TN002SG-000011-20121005 TN003SG-000015-20121005 TN004SG-000015-20121005 TN005SG-000014-20121005 TN006SG-000015-20121005)

BARIUMBERYLLIUMCADMIUMCALCIUMLEADSELENIUMTHALLIUM

11254976693

129138

30.0030.0030.0030.0030.0030.0030.00



C1-Naphthalenes 0.0179 ug/L

C2-Naphthalenes 0.00665 J ug/L

C2-Phenanthrenes/Anthracenes 0.00415 J ug/L

C3-Naphthalenes 0.00458 J ug/L

Calcium 69 J ug/L

Chromium 1 J ug/L

Magnesium 134 ug/L

Potassium 68 J ug/L

Sodium 1110 ug/L

1-Methylnaphthalene 0.0111 J ug/L

2-Methylnaphthalene 0.0184 ug/L

Acenaphthene 0.003 J ug/L

Acenaphthylene 0.00252 J ug/L

Fluorene 0.00738 J ug/L

Naphthalene 0.0708 ug/L

Phenanthrene 0.00454 J ug/L

Pyrene 0.00169 J ug/L

Retene 0.00418 J ug/L

Unknown1 1.1 J ug/L

Total petroleum hydrocarbons (C9-C40) 0.035 J mg/L

Acetone 2.2 J ug/L

SG-RB-20121006

Rinse Blank Summary Table

Alkylated Polycyclic Aromatic Hydrocarbons (ug/L)

Total Metals (ug/L)

Polycyclic Aromatic Hydrocarbons (ug/L)

Total Petroleum Hydrocarbons (mg/L)

Volatile Organics (ug/L)

Field Duplicate RPD ReportLab Reporting Batch ID: L1217878 Laboratory: AAL


Method: SM2540G

Matrix: SE

Concentration (pct)

FC004SG-000015-20121002

FC1004SG-000015-20121002Analyte

SampleRPD

eQAPPRPD Flag

Total Solids 32.7 32.9 1 20.00 No Qualifiers Applied

Method: SM4500NH3H

Matrix: SE

Concentration (mg/kg)

FC004SG-000015-20121002

FC1004SG-000015-20121002Analyte

SampleRPD

eQAPPRPD Flag

Ammonia as nitrogen 170 170 0 50.00 No Qualifiers Applied

Method: SM4500NO3F

Matrix: SE


FC004SG-000015-20121002

FC1004SG-000015-20121002Analyte

SampleRPD

eQAPPRPD Flag

Nitrate + nitrite as nitrogen 10 9.1 9 50.00 No Qualifiers Applied

Method: SM4500NorgC

Matrix: SE


FC004SG-000015-20121002

FC1004SG-000015-20121002Analyte

SampleRPD

eQAPPRPD Flag

Nitrogen (Kjeldahl) 4800 3000 46 50.00 No Qualifiers Applied

Method: SM4500PE

Matrix: SE


FC004SG-000015-20121002

FC1004SG-000015-20121002Analyte

SampleRPD

eQAPPRPD Flag

PHOSPHORUS 1600 1700 6 50.00 No Qualifiers Applied

Method: SOOTC

Matrix: SE

Concentration (pct)

FC004SG-000015-20121002

FC1004SG-000015-20121002Analyte

SampleRPD

eQAPPRPD Flag

Soot Carbon 0.296 0.287 3 50.00 No Qualifiers Applied




Method: SW6020A

Matrix: SE


FC004SG-000015-20121002 (TOT)

FC1004SG-000015-20121002 (TOT)Analyte

SampleRPD

eQAPPRPD Flag

ALUMINUMANTIMONYARSENICBARIUMBERYLLIUMCADMIUMCALCIUMCHROMIUMCOBALTCOPPERIRONLEADMAGNESIUMMANGANESENICKELPOTASSIUMSELENIUMSILVERSODIUMTHALLIUMTINVANADIUMZINC

144000.78011.899.60.8353.14931094.410.7248

30400251

1140032291.134402.085.02

151000.47724.851.7605

159000.73212.3110

0.7693.16

1000097.611.4264

30900263

1260034095.437602.004.75

169000.52018.554.4600

1064108173662510559461192951

50.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.00

No Qualifiers Applied

Method: SW8015M

Matrix: SE


FC004SG-000015-20121002

FC1004SG-000015-20121002Analyte

SampleRPD

eQAPPRPD Flag

2,6,10-TrimethyltridecaneDiesel range organics (C10 - C28)Heptatriacontanen-Docosane (C22)n-Dotriacontane (C32)n-Eicosane (C20)n-Heneicosane (C21)n-Hentriacontane (C31)n-Heptacosane (C27)n-Heptadecane (C17)n-Hexacosane (C26)n-Hexatriacontane (C36)n-Nonacosane (C29)n-Octacosane (C28)n-Octadecane (C18)n-Octatriacontane (C38)Nonatriacontane (C39)n-Pentacosane (C25)n-Pentadecane (C15)n-Pentatriacontane (C35)n-Tetracontane (C40)n-Tetracosane (C24)n-Tetratriacontane (C34)n-Triacontane (Triacontane) (C30)n-Tricosane (C23)n-Tritriacontane (C33)PhytanePristaneTotal petroleum hydrocarbons (C9-C40)

0.94123100.8850.4531.850.8400.6279.882.864.951.012.757.470.6781.701.261.116.770.3851.681.090.6221.281.540.9774.631.280.8435360

0.81820800.8980.3791.65

0.6750.6738.472.674.44

0.9742.666.19

0.4861.591.151.096.30

0.3641.791.14

0.3981.381.40

0.7824.321.10

0.7744840

1410118112271571143193379276644481022715910

50.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.00





Method: SW8260C

Matrix: SE

Concentration (ug/kg)

FC004SG-000015-20121002

FC1004SG-000015-20121002Analyte

SampleRPD

eQAPPRPD Flag

2-BUTANONEACETONEBENZENECARBON DISULFIDE

59310

2.9 U16

763803.416

2520

2000

50.0050.0050.0050.00





Method: SW8270DSIM

Matrix: SE


FC004SG-000015-20121002

FC1004SG-000015-20121002Analyte

SampleRPD

eQAPPRPD Flag

1-Methyldibenzothiophene1-Methylnaphthalene1-Methylphenanthrene2 Methyldibenzothiophene & 3-Methyldibenzothio2,3,5-Trimethylnaphthalene2,6-Dimethylnaphthalene2-Methylanthracene2-METHYLNAPHTHALENE2-Methylphenanthrene4 Methylphenanthrene & 9-Methylphenanthrene4-MethyldibenzothiopheneACENAPHTHENEACENAPHTHYLENEANTHRACENEBenz[a]anthraceneBENZO(E)PYRENEBenzo(j,k)fluorantheneBenzo[a]pyreneBenzo[b]fluorantheneBenzo[g,h,i]peryleneBenzonaphthothiopheneBenzothiopheneC1-Benzo(a)anthracenes/ChrysenesC1-Benzo(b)thiophenesC1-DecalinsC1-DibenzothiophenesC1-Fluoranthenes/PyrenesC1-FluorenesC1-NaphthalenesC1-Phenanthrenes/AnthracenesC2-Benzo(a)anthracenes/ChrysenesC2-Benzo(b)thiophenesC2-DecalinsC2-DibenzothiophenesC2-FluorenesC2-NaphthalenesC2-Phenanthrenes/AnthracenesC3-Benzo(a)anthracenes/ChrysenesC3-Benzo(b)thiophenesC3-DecalinsC3-DibenzothiophenesC3-FluorenesC3-NaphthalenesC3-Phenanthrenes/AnthracenesC4-Benzo(a)anthracenes/ChrysenesC4-Benzo(b)thiophenesC4-DecalinsC4-DibenzothiophenesC4-NaphthalenesC4-Phenanthrenes/AnthracenesCARBAZOLECHRYSENEDecalin, cis & trans-Dibenzo(a,h)anthracene and dibenzo(a,c)anthracDIBENZOTHIOPHENEFLUORANTHENE

32.510418740.443.217113222122124185.916735057120102160229026902850199076813.3159046.380.61862420139201979118039.62434333262801120124066.523855556329381881369.2444407309529136239039.25841624420

29.591.516742.940.015212119920922576.7155311538

18501960218024802530182067912.6146058.580.3167

2190123179904

104037.7201380287248

1030108062.022947855026473070452.4391359274494135

224036.3547149

4210

1013116812910671171268105812912592301110121281351913131281474152101114281313127168785

50.0050.0050.0050.0050.0050.0050.0050.00

50.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.00





Method: SW8270DSIM

Matrix: SE

FLUORENEIndeno[1,2,3-cd]pyreneNAPHTHALENEPERYLENEPHENANTHRENEPYRENERetene

191190026271112504300295

1761720240635

12103970240

8109113821

50.0050.0050.0050.0050.0050.0050.00


Method: SW9030B

Matrix: SE


FC004SG-000015-20121002

FC1004SG-000015-20121002Analyte

SampleRPD

eQAPPRPD Flag

SULFIDE 4500 5100 12 50.00 No Qualifiers Applied

Method: SW9045C

Matrix: SE

Concentration (SU)

FC004SG-000015-20121002

FC1004SG-000015-20121002Analyte

SampleRPD

eQAPPRPD Flag

PH 7.7 7.6 1 50.00 No Qualifiers Applied

Method: SW9060

Matrix: SE

Concentration (pct)

FC004SG-000015-20121002

FC1004SG-000015-20121002Analyte

SampleRPD

eQAPPRPD Flag

TOTAL ORGANIC CARBON (TOC) 4.60 4.76 3 50.00 No Qualifiers Applied




Method: SM2540G

Matrix: SE

Concentration (pct)

HB005SG-000015-20121006

HB1005SG-000015-20121006Analyte

SampleRPD

eQAPPRPD Flag

Total Solids 25.5 25.2 1 20.00 No Qualifiers Applied

Method: SM4500NH3H

Matrix: SE


HB005SG-000015-20121006

HB1005SG-000015-20121006Analyte

SampleRPD

eQAPPRPD Flag

Ammonia as nitrogen 140 140 0 50.00 No Qualifiers Applied

Method: SM4500NO3F

Matrix: SE


HB005SG-000015-20121006

HB1005SG-000015-20121006Analyte

SampleRPD

eQAPPRPD Flag

Nitrate + nitrite as nitrogen 12 9.8 20 50.00 No Qualifiers Applied

Method: SM4500NorgC

Matrix: SE


HB005SG-000015-20121006

HB1005SG-000015-20121006Analyte

SampleRPD

eQAPPRPD Flag

Nitrogen (Kjeldahl) 7100 7000 1 50.00 No Qualifiers Applied

Method: SM4500PE

Matrix: SE


HB005SG-000015-20121006

HB1005SG-000015-20121006Analyte

SampleRPD

eQAPPRPD Flag

PHOSPHORUS 680 610 11 50.00 No Qualifiers Applied

Method: SOOTC

Matrix: SE

Concentration (pct)

HB005SG-000015-20121006

HB1005SG-000015-20121006Analyte

SampleRPD

eQAPPRPD Flag

Soot Carbon 0.136 0.193 35 50.00 No Qualifiers Applied




Method: SW6020A

Matrix: SE


HB005SG-000015-20121006 (TOT)

HB1005SG-000015-20121006 (TOT)Analyte

SampleRPD

eQAPPRPD Flag

ALUMINUMANTIMONYARSENICBARIUMBERYLLIUMCADMIUMCALCIUMCHROMIUMCOBALTCOPPERIRONLEADMAGNESIUMMANGANESENICKELPOTASSIUMSELENIUMSILVERSODIUMTHALLIUMTINVANADIUMZINC

115000.53115.237.70.6731.62433048.78.37121

34500127796021225.833902.911.93

227000.39212.162.5328

112000.56315.438.1

0.5971.66425048.58.75123

33700134

814021727.334902.782.00

232000.39924.661.9328

3611122204225226354226810

50.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.00


Method: SW8015M

Matrix: SE


HB005SG-000015-20121006

HB1005SG-000015-20121006Analyte

SampleRPD

eQAPPRPD Flag

2,6,10-TrimethyltridecaneDiesel range organics (C10 - C28)Heptatriacontanen-Docosane (C22)n-Dotriacontane (C32)n-Hentriacontane (C31)n-Heptacosane (C27)n-Heptadecane (C17)n-Hexacosane (C26)n-Hexatriacontane (C36)n-Nonacosane (C29)n-Nonadecane (C19)n-Octacosane (C28)n-Octadecane (C18)n-Octatriacontane (C38)Nonatriacontane (C39)n-Pentacosane (C25)n-Pentadecane (C15)n-Pentatriacontane (C35)n-Tetracontane (C40)n-Tetracosane (C24)n-Tetratriacontane (C34)n-Triacontane (Triacontane) (C30)n-Tricosane (C23)n-Tritriacontane (C33)PhytanePristaneTotal petroleum hydrocarbons (C9-C40)

0.35712201.100.1840.8066.825.141.100.7921.1714.00.3150.8510.5471.001.054.800.1471.370.6760.2606.851.210.5205.840.5950.2492980

0.35011700.8861.01 U0.9466.394.951.111.22

0.96512.5

0.2830.6570.5130.8791.174.09

0.1331.20

0.5281.01 U6.581.08

1.01 U4.13

0.5760.2662920

2422

2001674143191111266131116101325

200411

20034372

50.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.00





Method: SW8260C

Matrix: SE


HB005SG-000015-20121006

HB1005SG-000015-20121006Analyte

SampleRPD

eQAPPRPD Flag

2-BUTANONEACETONECARBON DISULFIDE

12058016

8137038

394481

50.0050.0050.00





Method: SW8270DSIM

Matrix: SE


HB005SG-000015-20121006

HB1005SG-000015-20121006Analyte

SampleRPD

eQAPPRPD Flag

1-Methyldibenzothiophene1-Methylnaphthalene1-Methylphenanthrene2 Methyldibenzothiophene & 3-Methyldibenzothio2,3,5-Trimethylnaphthalene2,6-Dimethylnaphthalene2-Methylanthracene2-METHYLNAPHTHALENE2-Methylphenanthrene4 Methylphenanthrene & 9-Methylphenanthrene4-MethyldibenzothiopheneACENAPHTHENEACENAPHTHYLENEANTHRACENEBenz[a]anthraceneBENZO(E)PYRENEBenzo(j,k)fluorantheneBenzo[a]pyreneBenzo[b]fluorantheneBenzo[g,h,i]peryleneBenzonaphthothiopheneC1-Benzo(a)anthracenes/ChrysenesC1-DecalinsC1-DibenzothiophenesC1-Fluoranthenes/PyrenesC1-FluorenesC1-NaphthalenesC1-Phenanthrenes/AnthracenesC2-Benzo(a)anthracenes/ChrysenesC2-Benzo(b)thiophenesC2-DecalinsC2-DibenzothiophenesC2-FluorenesC2-NaphthalenesC2-Phenanthrenes/AnthracenesC3-Benzo(a)anthracenes/ChrysenesC3-Benzo(b)thiophenesC3-DecalinsC3-DibenzothiophenesC3-FluorenesC3-NaphthalenesC3-Phenanthrenes/AnthracenesC4-Benzo(a)anthracenes/ChrysenesC4-DecalinsC4-DibenzothiophenesC4-NaphthalenesC4-Phenanthrenes/AnthracenesCARBAZOLECHRYSENEDecalin, cis & trans-Dibenzo(a,h)anthracene and dibenzo(a,c)anthracDIBENZOTHIOPHENEFLUORANTHENEFLUORENEIndeno[1,2,3-cd]pyreneNAPHTHALENE

16.7 U20.852.156.06.0515224.942.545.150.214.627.210215661897810101070125095023144518.880.272224.840.821933814.860.370.566.711928237128.672.410820547.021333812493.649.014347.890131.023630.4142045.297450.7

4.7220.447.266.64.0017726.742.446.055.415.327.3100159585860920936

120088522242918.989.468026.940.422232913.462.668.771.513026932224.881.210418945.620126512285.852.413649.181727.423631.4135043.291852.1

2002101741157021050225139134744111681131043795141411483624297531012035563

50.0050.0050.0050.0050.0050.0050.0050.00

50.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.00


PERYLENEPHENANTHRENEPYRENE

3243021510

279291

1430

1545

50.0050.0050.00





Method: SW9030B

Matrix: SE


HB005SG-000015-20121006

HB1005SG-000015-20121006Analyte

SampleRPD

eQAPPRPD Flag

SULFIDE 6000 7000 15 50.00 No Qualifiers Applied

Method: SW9045C

Matrix: SE

Concentration (SU)

HB005SG-000015-20121006

HB1005SG-000015-20121006Analyte

SampleRPD

eQAPPRPD Flag

PH 7.8 7.8 0 50.00 No Qualifiers Applied

Method: SW9060

Matrix: SE

Concentration (pct)

HB005SG-000015-20121006

HB1005SG-000015-20121006Analyte

SampleRPD

eQAPPRPD Flag

TOTAL ORGANIC CARBON (TOC) 5.10 4.39 15 50.00 No Qualifiers Applied



Changed by: Niki Masters

Analyte MethodAnalysis

Type Result UnitReason Code

Original Value

New Value

Edit Time

Field Sample ID: FC001SG-000015-20121002

ALUMINUM SW6020A DL/TOT 12500 mg/kg Matrix Spike Upper Estimation J 11/15/2012 17:47

Reason for change: Sample concentration >4x spike concentration.

IRON SW6020A DL/TOT 26600 mg/kg Matrix Spike Upper Estimation J 11/15/2012 17:47


NICKEL SW6020A DL2/TOT 26.7 mg/kg Professional Judgment J 11/15/2012 16:42

Reason for change: Serial dilution %D above the control limit.

SULFIDE SW9030B DL/TOT 790 mg/kg Matrix Spike Upper Estimation J 11/16/2012 9:20











ADR version 1.6.0.18511/27/2012 3:11:39 PM Page 1 of 10



Original Value

New Value

Edit Time



























Original Value

New Value

Edit Time















Field Sample ID: SC001SG-000015-20121003

ACETONE SW8260C RES/TOT 370 ug/kg Matrix Spike Lower Rejection J 11/16/2012 8:46











Original Value

New Value

Edit Time

























Original Value

New Value

Edit Time















Field Sample ID: TN001SG-000015-20121004

BROMOMETHANE SW8260C RES/TOT 4.1 ug/kg Continuing Calibration UJ 11/15/2012 15:41

Reason for change: Associated CV %D below control limit.

NICKEL SW6020A DL/TOT 23.6 mg/kg Professional Judgment J 11/15/2012 16:51


SILVER SW6020A RES/TOT 1.76 mg/kg Professional Judgment J 11/27/2012 14:58

Reason for change: Associated serial dilution %D above the control limit.

SULFIDE SW9030B DL/TOT 630 mg/kg Matrix Spike Lower Rejection J 11/16/2012 9:22





Original Value

New Value

Edit Time

Field Sample ID: WE001SG-000015-20121004














NICKEL SW6020A DL/TOT 30.6 mg/kg Professional Judgment J 11/15/2012 16:53


SILVER SW6020A RES/TOT 2.03 mg/kg Professional Judgment J 11/27/2012 14:58

Reason for change: Associated serial dilution %D above the control limit.









Original Value

New Value

Edit Time


























Changed by: Niki Masters



Original Value

New Value

Edit Time

Field Sample ID: HB001SG-000015-20121006

ACETONE SW8260C RES/TOT 410 ug/kg Continuing Calibration J 11/15/2012 16:19

Reason for change: Associated CV %D above control limit.



BARIUM SW6020A DL2/TOT 34.2 mg/kg Laboratory Duplicate Precision J 11/16/2012 10:48

Reason for change: Sample and duplicate results <5x QL and within +/- 2x QL.


Reason for change: Dup RPD above the control limit.

BERYLLIUM SW6020A DL2/TOT 0.663 mg/kg Laboratory Duplicate Precision J 11/16/2012 10:56


CALCIUM SW6020A DL/TOT 4770 mg/kg Matrix Spike Upper Estimation J 11/16/2012 10:22




Nitrate + nitrite as nitrogen SM4500NO3F RES/TOT 9.2 mg/kg Laboratory Duplicate Precision J 11/16/2012 10:45




ADR version 1.6.0.18511/16/2012 11:15:41 AM Page 1 of 15



Original Value

New Value

Edit Time


























Original Value

New Value

Edit Time










Nitrate + nitrite as nitrogen SM4500NO3F RES/TOT 12 mg/kg Laboratory Duplicate Precision J 11/16/2012 10:45
















Original Value

New Value

Edit Time


























Original Value

New Value

Edit Time






Field Sample ID: SG-RB-20121006

1,2-DIBROMO-3-CHLOROPROPANE SW8260C RES/TOT 2.5 ug/l Continuing Calibration UJ 11/15/2012 16:07


CARBON TETRACHLORIDE SW8260C RES/TOT 0.50 ug/l Continuing Calibration UJ 11/15/2012 16:07


CIS-1,3-DICHLOROPROPENE SW8260C RES/TOT 0.50 ug/l Continuing Calibration UJ 11/15/2012 16:08


COBALT SW6020A RE/TOT 0.00005 mg/l Calibration Blank Contamination U 11/15/2012 13:18

Reason for change: Sample concentration <5x concentration of ICB.

DIBROMOCHLOROMETHANE SW8260C RES/TOT 0.50 ug/l Continuing Calibration UJ 11/15/2012 16:08


LEAD SW6020A RES/TOT 0.0002 mg/l Calibration Blank Contamination U 11/15/2012 13:30

Reason for change: Sample concentration <5x concentration of CCB.

TIN SW6020A RES/TOT 0.0002 mg/l Calibration Blank Contamination U 11/15/2012 13:31

Reason for change: Sample concentration <5x concentration of CCB.

TRANS-1,3-DICHLOROPROPENE SW8260C RES/TOT 0.50 ug/l Continuing Calibration UJ 11/15/2012 16:08





Original Value

New Value

Edit Time

Field Sample ID: SG-RB-20121006

VINYL ACETATE SW8260C RES/TOT 5.0 ug/l Continuing Calibration UJ 11/15/2012 16:08


Field Sample ID: SG-TB-20121006

1,2-DIBROMO-3-CHLOROPROPANE SW8260C RES/TOT 2.5 ug/l Continuing Calibration UJ 11/15/2012 16:09


CARBON TETRACHLORIDE SW8260C RES/TOT 0.50 ug/l Continuing Calibration UJ 11/15/2012 16:09


CIS-1,3-DICHLOROPROPENE SW8260C RES/TOT 0.50 ug/l Continuing Calibration UJ 11/15/2012 16:09


DIBROMOCHLOROMETHANE SW8260C RES/TOT 0.50 ug/l Continuing Calibration UJ 11/15/2012 16:09


TRANS-1,3-DICHLOROPROPENE SW8260C RES/TOT 0.50 ug/l Continuing Calibration UJ 11/15/2012 16:10


VINYL ACETATE SW8260C RES/TOT 5.0 ug/l Continuing Calibration UJ 11/15/2012 16:10












Original Value

New Value

Edit Time


























Original Value

New Value

Edit Time











ACETONE SW8260C RES/TOT 7.9 ug/kg Continuing Calibration J 11/15/2012 16:19















Original Value

New Value

Edit Time















BERYLLIUM SW6020A DL2/TOT 0.137 mg/kg Calibration Blank Contamination U 11/15/2012 11:46

Reason for change: Sample concentration <5x concentration in ICB.










Original Value

New Value

Edit Time







Data Qualifier SummaryLab Reporting Batch ID: 'L1217878', 'L1218042' Laboratory: 'AAL'

EDD Filename: 'PrepL1217878', 'PrepL1218042' eQAPP Name: Newtown Creek - Alpha

SDG: L1217878

GENCHEMMethod Category:

Method: SM4500PE Matrix: SE

Sample ID:FC001SG-000015-20121002 Collected: 10/2/2012 10:54:00 Analysis Type: Dilution: 4.7DL/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

PHOSPHORUS 840 15 MDL 54 RDL mg/kg J Lcs, Icv, Ccv


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


Sample ID:FC004SG-000015-20121002 Collected: 10/2/2012 3:21:00 Analysis Type: Dilution: 5DL/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


Sample ID:SC001SG-000015-20121003 Collected: 10/3/2012 9:16:00 Analysis Type: Dilution: 5DL/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


* denotes a non-reportable result

Project Name and Number: -






Sample ID:SC002SG-000015-20121003 Collected: 10/3/2012 10:40:00 Analysis Type: Dilution: 4.6DL/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


Sample ID:SC004SG-000015-20121003 Collected: 10/3/2012 12:36:00 Analysis Type: Dilution: 5DL/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode








Method: SOOTC Matrix: SE

Sample ID:FC001SG-000015-20121002 Collected: 10/2/2012 10:54:00 Analysis Type: Dilution: 1RE/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

Soot Carbon 0.289 0.010 MDL 0.010 RDL pct J StoA

Sample ID:FC001SG-000015-20121002 Collected: 10/2/2012 10:54:00 Analysis Type: Dilution: 1RES/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode










AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


Sample ID:TN001SG-000015-20121004 Collected: 10/4/2012 4:08:00 Analysis Type: Dilution: 1RE/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


Sample ID:TN001SG-000015-20121004 Collected: 10/4/2012 4:08:00 Analysis Type: Dilution: 1RES/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode









Sample ID:WE001SG-000015-20121004 Collected: 10/4/2012 8:28:00 Analysis Type: Dilution: 1RE/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


Sample ID:WE001SG-000015-20121004 Collected: 10/4/2012 8:28:00 Analysis Type: Dilution: 1RES/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode










AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



Method: SW9012A Matrix: SE

Sample ID:SC005SG-000015-20121003 Collected: 10/3/2012 1:38:00 Analysis Type: Dilution: 1RES/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

CYANIDE 0.80 J 0.79 MDL 3.4 RDL mg/kg J Rl


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


METALSMethod Category:


Sample ID:FC001SG-000015-20121002 Collected: 10/2/2012 10:54:00 Analysis Type: Dilution: 10DL2/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

NICKEL 26.7 0.084 MDL 0.562 RDL mg/kg J ProfJudg

TIN 15.1 J 2.84 MDL 28.1 RDL mg/kg J Rl, Ms









AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

ANTIMONY 0.101 0.010 MDL 0.055 RDL mg/kg J Ms


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode











AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


Sample ID:SC001SG-000015-20121003 Collected: 10/3/2012 9:16:00 Analysis Type: Dilution: 10DL2/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


TIN 118 4.24 MDL 42.0 RDL mg/kg J Ms









AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode











AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


TIN 34.4 3.38 MDL 33.5 RDL mg/kg J Ms









AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


Sample ID:TN001SG-000015-20121004 Collected: 10/4/2012 4:08:00 Analysis Type: Dilution: 10DL/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


TIN 7.21 J 2.81 MDL 27.8 RDL mg/kg J Rl


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

SILVER 1.76 0.002 MDL 0.054 RDL mg/kg J ProfJudg

Sample ID:WE001SG-000015-20121004 Collected: 10/4/2012 8:28:00 Analysis Type: Dilution: 10DL2/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


Sample ID:WE002SG-000015-20121004 Collected: 10/4/2012 3:12:00 Analysis Type: Dilution: 10DL/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


TIN 11.2 J 3.16 MDL 31.3 RDL mg/kg J Rl









AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

SILVER 2.03 0.003 MDL 0.062 RDL mg/kg J ProfJudg


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode











AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

ANTIMONY 0.090 U 0.016 MDL 0.090 RDL mg/kg R Ms


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

ANTIMONY 0.088 U 0.016 MDL 0.088 RDL mg/kg R Ms


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

ANTIMONY 0.052 J 0.017 MDL 0.095 RDL mg/kg J Rl, Ms


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


TIN 78.1 5.08 MDL 50.4 RDL mg/kg J Ms









AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


SVOAMethod Category:

Method: SW8015M Matrix: SE


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

2,6,10-Trimethyltridecane 0.478 JG 0.064 MDL 0.537 RDL mg/kg J Rl

Heptatriacontane 0.130 J 0.119 MDL 0.537 RDL mg/kg J Rl

n-Docosane (C22) 0.105 J 0.056 MDL 0.537 RDL mg/kg J Rl

n-Dotriacontane (C32) 0.274 J 0.068 MDL 0.537 RDL mg/kg J Rl

n-Eicosane (C20) 0.256 J 0.076 MDL 0.537 RDL mg/kg J Rl

n-Heneicosane (C21) 0.127 J 0.064 MDL 0.537 RDL mg/kg J Rl

n-Heptacosane (C27) 0.524 J 0.065 MDL 0.537 RDL mg/kg J Rl

n-Hexacosane (C26) 0.236 J 0.079 MDL 0.537 RDL mg/kg J Rl

n-Hexadecane (C16) 0.090 J 0.081 MDL 0.537 RDL mg/kg J Rl

n-Octacosane (C28) 0.128 J 0.115 MDL 0.537 RDL mg/kg J Rl

n-Octatriacontane (C38) 0.174 J 0.125 MDL 0.537 RDL mg/kg J Rl

Nonatriacontane (C39) 0.277 J 0.174 MDL 0.537 RDL mg/kg J Rl

Norpristane 0.183 J 0.177 MDL 0.537 RDL mg/kg J Rl

n-Pentadecane (C15) 0.125 J 0.064 MDL 0.537 RDL mg/kg J Rl

n-Pentatriacontane (C35) 0.227 J 0.094 MDL 0.537 RDL mg/kg J Rl

n-Tetracontane (C40) 0.194 J 0.174 MDL 0.537 RDL mg/kg J Rl

n-Tetratriacontane (C34) 0.344 J 0.085 MDL 0.537 RDL mg/kg J Rl

n-Triacontane (Triacontane) (C30) 0.339 J 0.062 MDL 0.537 RDL mg/kg J Rl

n-Tricosane (C23) 0.469 J 0.068 MDL 0.537 RDL mg/kg J Rl

Phytane 0.474 JG 0.067 MDL 0.537 RDL mg/kg J Rl

Pristane 0.194 J 0.115 MDL 0.537 RDL mg/kg J Rl









AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode







n-Heptadecane (C17) 0.699 J 0.266 MDL 0.807 RDL mg/kg J Rl












AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



















Sample ID:FC003SG-000015-20121002 Collected: 10/2/2012 1:42:00 Analysis Type: Dilution: 1RES/TOT-

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


n-Tetracosane (C24) 0.192 J 0.132 MDL 0.788 RDL mg/kg J Rl







AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode









n-Octadecane (C18) 1.70 JG 0.471 MDL 2.35 RDL mg/kg J Rl




















AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode










n-Hexatriacontane (C36) 2.11 J 0.469 MDL 2.36 RDL mg/kg J Rl













AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode
















AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode















AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode









n-Nonane (C9) 0.814 U 0.242 MDL 0.814 RDL mg/kg UJ Ms














Sample ID:SC001SG-000015-20121003 Collected: 10/3/2012 9:16:00 Analysis Type: Dilution: 1RES/TOT-

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode







AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode





























AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode





















AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


















AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode














AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

























AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode






AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode





















AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode










AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


















Sample ID:TN001SG-000015-20121004 Collected: 10/4/2012 4:08:00 Analysis Type: Dilution: 1RES/TOT-

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode











n-Tritriacontane (C33) 0.444 J 0.071 MDL 0.503 RDL mg/kg J Rl









AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

2,6,10-Trimethyldodecane 0.130 J 0.126 MDL 0.839 RDL mg/kg J Rl














n-Tetradecane (C14) 0.168 J 0.126 MDL 0.839 RDL mg/kg J Rl




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode













Sample ID:WE002SG-000015-20121004 Collected: 10/4/2012 3:12:00 Analysis Type: Dilution: 1RES/TOT-

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode














AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode











n-Pentacosane (C25) 0.745 JG 0.452 MDL 0.853 RDL mg/kg J Rl














AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode






AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode







n-Nonadecane (C19) 1.03 J 0.339 MDL 1.32 RDL mg/kg J Rl






n-Tridecane (C13) 0.528 J 0.362 MDL 1.32 RDL mg/kg J Rl




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode














AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode












n-Tetradecane (C14) 0.183 JG 0.128 MDL 0.852 RDL mg/kg J Rl






AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode





















AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode









AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode






























AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode





AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


DODECANE 1.12 J 0.539 MDL 2.47 RDL mg/kg J Rl


n-Decane (C10) 0.794 J 0.789 MDL 2.47 RDL mg/kg J Rl








n-Undecane (C11) 1.09 J 0.738 MDL 2.47 RDL mg/kg J Rl


Method: SW8270DSIM Matrix: SE


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

1-Methyldibenzothiophene 32.5 J 9.71 MDL 35.2 RDL ug/kg J Rl

Benzothiophene 13.3 J 11.0 MDL 35.2 RDL ug/kg J Rl









AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode










AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


VOAMethod Category:

Method: SW8260C Matrix: SE


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

ACETONE 29 J 7.2 MDL 80 RDL ug/kg J Rl

CARBON DISULFIDE 5.8 J 0.57 MDL 22 RDL ug/kg U Mb


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

CARBON DISULFIDE 7.4 J 0.73 MDL 28 RDL ug/kg J Rl


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

CARBON DISULFIDE 16 J 0.80 MDL 31 RDL ug/kg J Rl






VOAMethod Category:



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

1,1,2,2-TETRACHLOROETHANE 3.1 U 0.89 MDL 3.1 RDL ug/kg UJ Ms

1,2,3-TRICHLOROBENZENE 15 U 2.8 MDL 15 RDL ug/kg UJ Ms

1,2,4-TRICHLOROBENZENE 15 U 2.7 MDL 15 RDL ug/kg UJ Ms

1,2-DIBROMO-3-CHLOROPROPANE 15 U 4.6 MDL 15 RDL ug/kg UJ Ms

1,2-DIBROMOETHANE 12 U 0.66 MDL 12 RDL ug/kg UJ Ms

1,2-DICHLOROBENZENE 15 U 1.1 MDL 15 RDL ug/kg UJ Ms



2-BUTANONE 68 12 MDL 31 RDL ug/kg J Ms

2-HEXANONE 31 U 3.9 MDL 31 RDL ug/kg UJ Ms

4-METHYL-2-PENTANONE 31 U 5.5 MDL 31 RDL ug/kg UJ Ms

BROMODICHLOROMETHANE 3.1 U 1.2 MDL 3.1 RDL ug/kg UJ Ms

BROMOFORM 12 U 3.4 MDL 12 RDL ug/kg UJ Ms


CHLOROBENZENE 3.1 U 0.76 MDL 3.1 RDL ug/kg UJ Ms

CIS-1,3-DICHLOROPROPENE 3.1 U 0.83 MDL 3.1 RDL ug/kg UJ Ms

CYCLOHEXANE 62 U 62 MDL 62 RDL ug/kg R Ms






VOAMethod Category:



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

DIBROMOCHLOROMETHANE 3.1 U 0.99 MDL 3.1 RDL ug/kg UJ Ms

ETHYL BENZENE 3.1 U 1.2 MDL 3.1 RDL ug/kg UJ Ms

ISOPROPYLBENZENE 3.1 U 0.60 MDL 3.1 RDL ug/kg UJ Ms

m,p-Xylene 6.2 U 1.4 MDL 6.2 RDL ug/kg UJ Ms

METHYL ACETATE 62 U 62 MDL 62 RDL ug/kg R Ms

METHYL CYCLOHEXANE 12 U 12 MDL 12 RDL ug/kg UJ Ms

O-XYLENE 6.2 U 1.8 MDL 6.2 RDL ug/kg UJ Ms

STYRENE 6.2 U 1.9 MDL 6.2 RDL ug/kg UJ Ms

TETRACHLOROETHENE 3.1 U 0.90 MDL 3.1 RDL ug/kg UJ Ms

TRANS-1,3-DICHLOROPROPENE 3.1 U 1.0 MDL 3.1 RDL ug/kg UJ Ms

VINYL ACETATE 31 U 4.2 MDL 31 RDL ug/kg UJ Ms


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode







VOAMethod Category:



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

1,4-DICHLOROBENZENE 3.8 J 0.91 MDL 15 RDL ug/kg J Rl

ISOPROPYLBENZENE 1.9 J 0.58 MDL 3.0 RDL ug/kg J Rl

m,p-Xylene 3.4 J 1.4 MDL 6.0 RDL ug/kg J Rl

O-XYLENE 1.7 J 1.7 MDL 6.0 RDL ug/kg J Rl


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


ISOPROPYLBENZENE 0.75 J 0.54 MDL 2.8 RDL ug/kg J Rl


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

2-BUTANONE 10 J 7.9 MDL 20 RDL ug/kg J Rl


BROMOMETHANE 4.1 U 1.2 MDL 4.1 RDL ug/kg UJ Ccv



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

2-BUTANONE 9.4 J 9.4 MDL 24 RDL ug/kg J Rl



CARBON DISULFIDE 6.2 J 0.62 MDL 24 RDL ug/kg U Mb


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode








VOAMethod Category:



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

2-BUTANONE 38 J 16 MDL 41 RDL ug/kg J Rl




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


TOLUENE 2.1 J 0.69 MDL 5.5 RDL ug/kg J Rl


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode







VOAMethod Category:



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

1,4-DICHLOROBENZENE 18 J 1.3 MDL 21 RDL ug/kg J Rl

4-METHYL-2-PENTANONE 10 J 7.3 MDL 41 RDL ug/kg J Rl

BENZENE 1.2 J 0.80 MDL 4.1 RDL ug/kg J Rl


m,p-Xylene 5.3 J 1.9 MDL 8.3 RDL ug/kg J Rl

O-XYLENE 2.7 J 2.4 MDL 8.3 RDL ug/kg J Rl

VOAMethod Category:

Method: SW8260C Matrix: WS

Sample ID:SG-TB-20121002 Collected: 10/2/2012 6:01:00 Analysis Type: Dilution: 1RES/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

ACETONE 1.8 J 1.6 MDL 5.0 RDL ug/l J Rl

CHLOROMETHANE 0.39 J 0.28 MDL 2.5 RDL ug/l U Mb


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



SDG: L1218042








Sample ID:HB001SG-000015-20121006 Collected: 10/6/2012 3:54:00 Analysis Type: Dilution: 4.6DL/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

PHOSPHORUS 610 22 MDL 77 RDL mg/kg J Ms


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


Sample ID:HB007SG-000015-20121006 Collected: 10/6/2012 10:45:00 Analysis Type: Dilution: 5DL/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode










AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


Sample ID:TN002SG-000011-20121005 Collected: 10/5/2012 10:41:00 Analysis Type: Dilution: 4.6DL/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

PHOSPHORUS 110 3.5 MDL 12 RDL mg/kg J Ms


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

PHOSPHORUS 130 3.6 MDL 13 RDL mg/kg J Ms








Sample ID:HB001SG-000015-20121006 Collected: 10/6/2012 3:54:00 Analysis Type: Dilution: 1RE/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

Soot Carbon 0.270 0.010 MDL 0.010 RDL pct J Ld, StoA

Sample ID:HB001SG-000015-20121006 Collected: 10/6/2012 3:54:00 Analysis Type: Dilution: 1RES/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode










AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode










AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


Sample ID:SRM 1650B Collected: 10/6/2012 12:00:00 Analysis Type: Dilution: 1RE/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


Sample ID:SRM 1650B Collected: 10/6/2012 12:00:00 Analysis Type: Dilution: 1RES/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode










AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode










AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode





AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



Method: SW9030B Matrix: SE


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

SULFIDE 5200 38 MDL 170 RDL mg/kg J Ld









AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode










AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

SULFIDE 35 0.29 MDL 1.3 RDL mg/kg J Ld









AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

CALCIUM 4770 258 MDL 2120 RDL mg/kg J Ld

Sample ID:HB001SG-000015-20121006 Collected: 10/6/2012 3:54:00 Analysis Type: Dilution: 10DL2/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

BARIUM 34.2 0.651 MDL 2.54 RDL mg/kg J Ld

CADMIUM 1.12 0.022 MDL 0.169 RDL mg/kg J Ld

LEAD 105 0.164 MDL 0.508 RDL mg/kg J Ld

SELENIUM 2.85 0.211 MDL 0.847 RDL mg/kg J Ld

THALLIUM 0.322 0.023 MDL 0.169 RDL mg/kg J Ld


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



LEAD 89.0 0.135 MDL 0.420 RDL mg/kg J Ld











AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode







AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode












AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode







AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode










AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode







AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

TIN 4.47 J 0.675 MDL 6.69 RDL mg/kg U Mb


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode














AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode







AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode












AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


Sample ID:TN002SG-000011-20121005 Collected: 10/5/2012 10:41:00 Analysis Type: Dilution: 10DL2/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode







AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode










AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode







AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode







AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

TIN 6.06 0.465 MDL 4.60 RDL mg/kg U Mb









AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

CALCIUM 15800 98.8 MDL 812 RDL mg/kg J Ld


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode







AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

TIN 5.14 0.328 MDL 3.25 RDL mg/kg U Mb


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode










AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


BERYLLIUM 0.137 0.029 MDL 0.100 RDL mg/kg U Cb



SELENIUM 0.268 J 0.083 MDL 0.335 RDL mg/kg J Rl, Ld



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

TIN 2.16 J 0.360 MDL 3.57 RDL mg/kg U Mb


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



Method: SW6020A Matrix: WS

Sample ID:SG-RB-20121006 Collected: 10/6/2012 9:05:00 Analysis Type: Dilution: 1RE/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

COBALT 0.00005 J 0.00002 MDL 0.00020 RDL mg/l U Cb

Sample ID:SG-RB-20121006 Collected: 10/6/2012 9:05:00 Analysis Type: Dilution: 1RES/TOT

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

BARIUM 0.0002 J 0.0001 MDL 0.0005 RDL mg/l U Mb

CALCIUM 0.069 J 0.019 MDL 0.100 RDL mg/l J Rl

COPPER 0.001 J 0.0003 MDL 0.001 RDL mg/l U Mb

IRON 0.013 J 0.008 MDL 0.050 RDL mg/l U Mb







Method: SW6020A Matrix: WS


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

LEAD 0.0002 J 0.0001 MDL 0.0010 RDL mg/l U Cb

MANGANESE 0.0008 0.0001 MDL 0.0005 RDL mg/l U Mb

NICKEL 0.0007 0.0002 MDL 0.0005 RDL mg/l U Mb

POTASSIUM 0.068 J 0.006 MDL 0.100 RDL mg/l J Rl

THALLIUM 0.00001 J 0.00001 MDL 0.00020 RDL mg/l U Mb

TIN 0.0002 J 0.0001 MDL 0.0005 RDL mg/l U Cb

ZINC 0.005 J 0.001 MDL 0.010 RDL mg/l U Mb




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

























AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



















AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



















Sample ID:HB003SG-000015-20121006 Collected: 10/6/2012 2:21:00 Analysis Type: Dilution: 1RES/TOT-

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode








AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode















AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode














AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode














AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

























AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode
















AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


















AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode









AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode














AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode














AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode






AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode















AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode
















AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode





AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



n-Hentriacontane (C31) 0.242 J 0.049 MDL 0.346 RDL mg/kg J Rl









AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



n-Hentriacontane (C31) 0.157 J 0.040 MDL 0.281 RDL mg/kg J Rl














Method: SW8015M Matrix: WS


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

Diesel range organics (C10 - C28) 0.028 0.004 MDL 0.024 RDL mg/l U Mb

n-Octadecane (C18) 0.001 JC 0.0001 MDL 0.001 RDL mg/l U Mb

Total petroleum hydrocarbons (C9-C40) 0.035 J 0.006 MDL 0.038 RDL mg/l J Rl




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

2,3,5-Trimethylnaphthalene 4.42 J 2.04 MDL 12.5 RDL ug/kg J Rl


C1-Decalins 10.2 J 3.14 MDL 12.5 RDL ug/kg J Rl

C2-Benzo(b)thiophenes 10.1 J 3.91 MDL 12.5 RDL ug/kg J Rl


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode






AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode













AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode






AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode





AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

1-Methylnaphthalene 6.18 J 3.88 MDL 12.3 RDL ug/kg J Rl

2-Methylanthracene 6.75 J 4.08 MDL 12.3 RDL ug/kg J Rl

2-METHYLNAPHTHALENE 11.7 J 3.18 MDL 12.3 RDL ug/kg J Rl


ACENAPHTHENE 9.33 J 2.17 MDL 12.3 RDL ug/kg J Rl


C1-Fluorenes 8.50 J 3.28 MDL 12.3 RDL ug/kg J Rl

C1-Naphthalenes 12.2 J 3.54 MDL 12.3 RDL ug/kg J Rl


CARBAZOLE 11.9 J 4.03 MDL 12.3 RDL ug/kg J Rl

DIBENZOTHIOPHENE 8.38 J 3.40 MDL 12.3 RDL ug/kg J Rl

Retene 8.32 J 3.02 MDL 12.3 RDL ug/kg J Rl


AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode










AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode





AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode





AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode










AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode







Method: SW8270DSIM Matrix: WS

Sample ID:SG-RB-20121006 Collected: 10/6/2012 9:05:00 Analysis Type: Dilution: 1RES/TOT-

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

1-Methylnaphthalene 11.1 J 1.88 MDL 11.6 RDL ng/l J Rl

ACENAPHTHENE 3.00 J 1.56 MDL 11.6 RDL ng/l J Rl

ACENAPHTHYLENE 2.52 J 2.44 MDL 11.6 RDL ng/l J Rl

C2-Naphthalenes 6.65 J 2.73 MDL 11.6 RDL ng/l J Rl

C2-Phenanthrenes/Anthracenes 4.15 J 2.76 MDL 11.6 RDL ng/l J Rl

C3-Naphthalenes 4.58 J 2.73 MDL 11.6 RDL ng/l J Rl

Decalin, cis & trans- 3.02 J 2.51 MDL 5.81 RDL ng/l U Mb

FLUORENE 7.38 J 2.53 MDL 11.6 RDL ng/l J Rl

PHENANTHRENE 4.54 J 2.76 MDL 11.6 RDL ng/l J Rl

PYRENE 1.69 J 1.05 MDL 11.6 RDL ng/l J Rl

Retene 4.18 J 2.63 MDL 11.6 RDL ng/l J Rl

VOAMethod Category:



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

ACETONE 410 11 MDL 120 RDL ug/kg J Ccv







VOAMethod Category:



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

ACETONE 320 9.1 MDL 100 RDL ug/kg J Ccv



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode








VOAMethod Category:



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

2-BUTANONE 32 J 14 MDL 35 RDL ug/kg J Rl




AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

2-BUTANONE 6.6 J 6.2 MDL 16 RDL ug/kg J Rl

ACETONE 33 J 5.2 MDL 58 RDL ug/kg J Rl, Ccv



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode





AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode









VOAMethod Category:



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

ACETONE 7.9 J 4.5 MDL 50 RDL ug/kg J Rl, Ccv



AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode


VOAMethod Category:

Method: SW8260C Matrix: WS

Sample ID:SG-RB-20121006 Collected: 10/6/2012 9:05:00 Analysis Type: Dilution: 1RES/TOT-

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

1,2-DIBROMO-3-CHLOROPROPANE 2.5 U 0.33 MDL 2.5 RDL ug/l UJ Ccv


CARBON TETRACHLORIDE 0.50 U 0.16 MDL 0.50 RDL ug/l UJ Ccv

CIS-1,3-DICHLOROPROPENE 0.50 U 0.14 MDL 0.50 RDL ug/l UJ Ccv

DIBROMOCHLOROMETHANE 0.50 U 0.19 MDL 0.50 RDL ug/l UJ Ccv

TRANS-1,3-DICHLOROPROPENE 0.50 U 0.16 MDL 0.50 RDL ug/l UJ Ccv

VINYL ACETATE 5.0 U 0.31 MDL 5.0 RDL ug/l UJ Ccv

Sample ID:SG-TB-20121006 Collected: 10/6/2012 4:23:00 Analysis Type: Dilution: 1RES/TOT-

AnalyteLab

Result DLDL

TypeRL

TypeRL UnitsLabQual

DataReview

QualReasonCode

1,2-DIBROMO-3-CHLOROPROPANE 2.5 U 0.33 MDL 2.5 RDL ug/l UJ Ccv


CARBON TETRACHLORIDE 0.50 U 0.16 MDL 0.50 RDL ug/l UJ Ccv

CIS-1,3-DICHLOROPROPENE 0.50 U 0.14 MDL 0.50 RDL ug/l UJ Ccv

DIBROMOCHLOROMETHANE 0.50 U 0.19 MDL 0.50 RDL ug/l UJ Ccv

TRANS-1,3-DICHLOROPROPENE 0.50 U 0.16 MDL 0.50 RDL ug/l UJ Ccv

VINYL ACETATE 5.0 U 0.31 MDL 5.0 RDL ug/l UJ Ccv






Reason Code Legend

Reason Code Description

Cb Calibration Blank Contamination

Ccv Continuing Calibration Verification Percent Difference Lower Estimation

Ccv Continuing Calibration Verification Percent Difference Upper Estimation

Ccv Continuing Calibration Verification Percent Recovery Upper Estimation

CcvRrf Continuing Calibration Verification Relative Response Factor

IcRrf Initial Calibration Relative Response Factor

Icv Initial Calibration Verification Percent Recovery Upper Estimation

Lcs Laboratory Control Spike Upper Estimation

Ld Laboratory Duplicate Precision

Mb Method Blank Contamination

Ms Matrix Spike Lower Estimation

Ms Matrix Spike Lower Rejection

Ms Matrix Spike Upper Estimation

ProfJudg Professional Judgment

Rl Reporting Limit Trace Value

StoA Sampling to Analysis Estimation




DATA VALIDATION REVIEW REPORT EPA STAGE2Bnewtowncreek.info/docs2/2 Remedial Investigation/Phase...

Documents

Transcript of DATA VALIDATION REVIEW REPORT EPA STAGE2Bnewtowncreek.info/docs2/2 Remedial Investigation/Phase...