Creating a Conference Poster Investigating Asphaltene ...

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Results Conclusions Experimental Setups Selected Publications Motivation Objective Investigating Asphaltene Stability in Crude Oil During Carbon Dioxide Injection Sherif M. Fakher│Advisor: Dr. Abdulmohsin Imqam Petroleum Engineering The reservoir thermodynamic conditions were found to have a strong impact on the stability of the asphaltene in the crude oil. Increasing the carbon dioxide injection pressure resulted in a decrease in the asphaltene filter cake thickness and an increase in the areal filtrate displacement. Heptane could not be used as an effective chemical agent for asphaltene mitigation since the asphaltene is insoluble in heptane. Although asphaltene was soluble in naphtha, the chemical agent could not mitigate the asphaltene plugging well. The two most effective chemical agents used in this research for asphaltene mitigation were kerosene and xylene. Overall, xylene was the best agent. Experimental Materials Acknowledgment I would like to thank MST for providing me with the Chancellor’s Distinguished Fellowship. Hydrocarbons are usually thought of as being a fluid (gas or liquid) Asphaltene is a solid component of the crude oil that is stabilized via resins or as a nano- colloid It can cause severe production problems and safety hazards in wellbores, equipment, and pipelines Investigate the factors that may impact asphaltene stability in the crude oil and quantify the effect of these factors. Determine how to reduce asphaltene precipitation and deposition and how to mitigate or alleviate asphaltene buildups Specially designed filtration setup Crude Oil from Kirk Lease, Kansas Stainless Steel tubings and connections High pressure CO 2 cylinder Filter membranes with pore sizes of 0.2, 10, and 100 nm, and 2.7 µm 1. Fakher, S. et al. Critical review of asphaltene properties and factors impacting its stability in crude oil. J Petrol Explor Prod Technol (2019). https ://doi.org/10.1007/s13202-019-00811-5. 2. Fakher, S. et al. An experimental investigation of asphaltene stability in heavy crude oil during carbon dioxide injection. J Petrol Explor Prod Technol (2019). https ://doi.org/10.1007/s13202-019-00782-7. 3. Fakher, S. and Imqam, A., 2018. An experimental investigation of immiscible carbon dioxide interactions with crude oil: Oil swelling and asphaltene agitation. https ://doi.org/10.1016/j.fuel.2020.117380. 4. Fakher, S. and Imqam, A., 2020. Asphaltene precipitation and deposition during CO2 injection in nano shale pore structure and its impact on oil recovery. https ://doi.org/10.1016/j.fuel.2018.10.039. 5. Fakher, S. et al., 2019. The Effect of Unconventional Oil Reservoirs’ Nano Pore Size on the Stability of Asphaltene During Carbon Dioxide Injection. Carbon Management Technology Conference. doi:10.7122/CMTC-558486-MS 6. Fakher, S.. Et al., 2019. Roadmap to Asphaltene Characteristics, Properties, and Presence in Crude Oils Based on an Updated Database From Laboratory Studies. Carbon Management Technology Conference. doi:10.7122/CMTC-558560-MS. 7. Fakher, S., 2019. Investigating Factors that May Impact the Success of Carbon Dioxide Enhanced Oil Recovery in Shale Reservoirs. Society of Petroleum Engineers. doi:10.2118/199781-STU. Chemistry World Asphaltene Stability Setup Asphaltene Mitigation Setup High precision camera Chemical agents (water, heptane, kerosene, naphtha, and xylene) Transparent 1000 ml glass beaker Pipettes (plastic and glass) Asphaltene Saturated Filter membranes Kerosene Naphtha Heptane Xylene Water (Reference Agent) 0 5 10 15 20 25 30 200 400 750 Asphaltene Concentration, wt% Pressure, psi 0 5 10 15 20 25 60 100 150 Asphaltene Concentration, wt% Temperature, ̊ C 0 2 4 6 8 10 12 14 16 18 20 10 100 Asphaltene Concentration, wt% Pore Size, nm 0 2 4 6 8 10 12 0.5 2 Asphaltene Concentration, wt% CO2 Soaking Time, hrs

Transcript of Creating a Conference Poster Investigating Asphaltene ...

Page 1: Creating a Conference Poster Investigating Asphaltene ...

Creating a Conference PosterAuthors or Reserachers

Department or Organization

Results

Conclusions

Experimental Setups

Selected Publications

Motivation

Objective

Investigating Asphaltene Stability in Crude Oil During

Carbon Dioxide InjectionSherif M. Fakher│Advisor: Dr. Abdulmohsin Imqam

Petroleum Engineering

▪ The reservoir thermodynamic conditions

were found to have a strong impact on the

stability of the asphaltene in the crude oil.

▪ Increasing the carbon dioxide injection

pressure resulted in a decrease in the

asphaltene filter cake thickness and an

increase in the areal filtrate displacement.

▪ Heptane could not be used as an effective

chemical agent for asphaltene mitigation

since the asphaltene is insoluble in heptane.

▪ Although asphaltene was soluble in

naphtha, the chemical agent could not

mitigate the asphaltene plugging well.

▪ The two most effective chemical agents

used in this research for asphaltene

mitigation were kerosene and xylene.

Overall, xylene was the best agent.

Experimental Materials

AcknowledgmentI would like to thank MST for providing me

with the Chancellor’s Distinguished Fellowship.

Hydrocarbons are

usually thought of as

being a fluid (gas or

liquid)

Asphaltene is a solid

component of the crude

oil that is stabilized via

resins or as a nano-

colloid

It can cause severe

production problems

and safety hazards in

wellbores, equipment,

and pipelines

▪ Investigate the factors that may impact

asphaltene stability in the crude oil and

quantify the effect of these factors.

▪ Determine how to reduce asphaltene

precipitation and deposition and how to

mitigate or alleviate asphaltene buildups

▪ Specially designed filtration setup

▪ Crude Oil from Kirk Lease, Kansas

▪ Stainless Steel tubings and connections

▪ High pressure CO2 cylinder

▪ Filter membranes with pore sizes of 0.2,

10, and 100 nm, and 2.7 µm

1. Fakher, S. et al. Critical review of asphaltene properties and factors

impacting its stability in crude oil. J Petrol Explor Prod Technol

(2019). https://doi.org/10.1007/s13202-019-00811-5.

2. Fakher, S. et al. An experimental investigation of asphaltene stability

in heavy crude oil during carbon dioxide injection. J Petrol Explor

Prod Technol (2019). https://doi.org/10.1007/s13202-019-00782-7.

3. Fakher, S. and Imqam, A., 2018. An experimental investigation of

immiscible carbon dioxide interactions with crude oil: Oil swelling

and asphaltene agitation. https://doi.org/10.1016/j.fuel.2020.117380.

4. Fakher, S. and Imqam, A., 2020. Asphaltene precipitation and

deposition during CO2 injection in nano shale pore structure and its

impact on oil recovery. https://doi.org/10.1016/j.fuel.2018.10.039.

5. Fakher, S. et al., 2019. The Effect of Unconventional Oil

Reservoirs’ Nano Pore Size on the Stability of Asphaltene

During Carbon Dioxide Injection. Carbon Management Technology

Conference. doi:10.7122/CMTC-558486-MS

6. Fakher, S.. Et al., 2019. Roadmap to Asphaltene Characteristics,

Properties, and Presence in Crude Oils Based on an Updated

Database From Laboratory Studies. Carbon Management Technology

Conference. doi:10.7122/CMTC-558560-MS.

7. Fakher, S., 2019. Investigating Factors that May Impact the Success

of Carbon Dioxide Enhanced Oil Recovery in Shale Reservoirs.

Society of Petroleum Engineers. doi:10.2118/199781-STU.

Chemistry World

Asphaltene Stability Setup Asphaltene Mitigation Setup

▪ High precision camera

▪ Chemical agents (water, heptane,

kerosene, naphtha, and xylene)

▪ Transparent 1000 ml glass beaker

▪ Pipettes (plastic and glass)

▪ Asphaltene Saturated Filter membranes

Kerosene

NaphthaHeptane

Xylene

Water

(Reference Agent)

0

5

10

15

20

25

30

200 400 750

Asp

hal

tene

Conce

ntr

atio

n, w

t%

Pressure, psi

0

5

10

15

20

25

60 100 150

Asp

hal

tene

Conce

ntr

atio

n, w

t%

Temperature, ̊ C

0

2

4

6

8

10

12

14

16

18

20

10 100

Asp

hal

tene

Conce

ntr

atio

n, w

t%

Pore Size, nm

0

2

4

6

8

10

12

0.5 2

Asp

hal

tene

Conce

ntr

atio

n, w

t%

CO2 Soaking Time, hrs