CONT SP-FE-0001,Rev .6 List of analysis parameters with Reference SP-DP12-0001List of... · LIST OF...
Transcript of CONT SP-FE-0001,Rev .6 List of analysis parameters with Reference SP-DP12-0001List of... · LIST OF...
Rev. No: 6
page :1 of 23
LIST OF ANALYSIS PARAMETERS WITH REFERENCE METHODS
Dubai Central laboratory
Doc.Ref : SP-FE-0001
Issue Date :04/04/2016
CONTROLLED COPYCONTROLLED COPY
Authorized by: HOSIssued by :SQO
Note: Printed copy of this document shall be treated as ‘Uncontrolled’. Always refer the controlled version ‘Online
CONTROLLED COPYCONTROLLED COPY
Rev. No: 6
page :2 of 23
LIST OF ANALYSIS PARAMETERS WITH REFERENCE METHODS
Dubai Central laboratory
Doc.Ref : SP-FE-0001
Issue Date :04/04/2016
S.No.Clause
AmendedDate Authorisaton
1 Heading 30/11/2011 HOS
2 All Clause 30/11/2011 HOS
3 - 30/11/2011 HOS
4 - 30/11/2011 HOS
5 Reference 30/11/2011 HOS
6 All Clause 18/11/2012 HOS
7 - 18/11/2012 HOS
18/11/2012 HOS
18/11/2012 HOS
18/11/2012 HOS
18/11/2012 HOS
9 18/11/2012 HOS
10 18/11/2012 HOS
22/11/2012 HOS
22/11/2012 HOS
Part 2-FCAU
Added sSOP-FE-2324 & SOP-FE-(2265,2347) & BSEN 13805:2002 to list
Part 3 -Env
8 Part 1-FMAU
Eliminated salmonella spp by Rabit technique and added 10 or as per dilution factor to solid
part of SOP-FE-3117.
Test duration (days) modified from 4 to7 days increased in SOP-FE-3105.
Added two new SOPs-FE-(1132,1133,1134) with the price in Env.unit
Modified tittle of two SOPs (3119 and 3120)
Test duration (days) incrased in Food chemical Analysis unit. Reference for
SOPs(2260,2261,2262,& 2263) replaced AOAC, 17th Edn. 2000 to AOAC, 16th Edn. 1998
11
Added three new SOPs-FE-(3122 &3123,3124) with the price in FMAU
Added Physical analysis fees
Added Government cost to list
Nature of Amendment
Change standard method 18th to 21 th
SP-DP12-0001(FE) changed to SP-FE-0001as per IMS requirement
AMENDMENT RECORD
SOPs numbring system changed from three digit number to four digit number system.
Added Chlorate(ClO30) and Chorite(Cl20) to SOP-FE-1130
Added two SOP-FE-2345 & 2346 with the price
Standard methods- 21 ST Edition instead of 18 th edition and MOOPAM 4th instead of 3rd
edition in Env list
22/11/2012 HOS
22/11/2012 HOS
22/11/2012 HOS
12 3.1 22/11/2012 HOS
13 - 22/11/2012 HOS
14 - 22/11/2012 HOS
15 20/01/2014 HOS
16 20/01/2014 HOS
17 20/01/2014 HOS
18 20/01/2014 HOS
19 Part 3 -Env 20/01/2014 HOS
20 Part 1-FMAU 09/02/2015 HOS
21 Part 2-FCAU 09/02/2015 HOS
22 Part 3 -Env 09/02/2015 HOS
23 All Clause 04/04/2016 HOS
24 Pari 1-FMAU 04/04/2016 HOS
25 Part2-FCAU 04/04/2016 HOS
26 Part 3 -ENVU 04/04/2016 HOS
Added new SOP-FE(3130 & 3131) with the price of tests and changed Test duation in
Yersinia entrocolitica.
Part 3 -Env
Method detection changed from 5 to 7,Changed reporting unit in SOP-FE-1124 from mg/l to
ug/L and removed waster water in sample type. Chaged method detection in SOP-FE-1128
z(Cd from 0.04 to 0.08,Zn from 0.04 to 0.05 ,Co from 0.1 to 0.12). Reduced method detection
in SOP-FE-1130 for (BrO3 from 5 to 3). TDS / EC Meter replaced of APHA-2130B in SOP-
FE-1105 for drinking water. Added sampling with price to list.
Added SOP-FE-2206 & Determination of traces elements of As*,Cd*,Hg*,Pb* by BS EN
15763:2009 with the price of tests
Added new SOPs (SOP-FE-2370 & 2371) to list
Changed the titles ,sample type and Duration time. Added Determination of salinity in water to
the list.
Added Enumeration of Legionella spp. & L pneumophila in water and wastewater by
(RT-PCR) as SOP-FE-1610 & Determination of Volatile Organic Compounds in Water
as SOP-FE-1136 & 1137.
Added detection of pork and horse as per SOP-FE-3132 &3133 ,Removed Detection of
Cronobacter sakazakii in Powdered Infant Formula for liquid.
Added Determination of Acrylamide & NSAIDS as SOP-FE-2373 &2374, corrected
standard method & input time (hrs) in the BS EN 15763:2009,pestiside residues in the
different foods as SOP-FE-2348,2349,2350 ,Determination of Residual Monomers
Migration from Food Packging into Food as SOP-FE-2450.
Added two new SOPs-FE-(1132,1133,1134) with the price in Env.unit
Added method detection of Cu -Cd ,Zn , Pb,N i,Cr & modified test duration (days) from 4 to 5
days incrased in SOP-FE-1304 in Env.unit.
Discontinuation the production of KIT from company for SOP-FE-3119
Issue By:SQO
Part 2-FCAU
Adde methosd detedtion to SOPs and replaced SOP-FE-2230 by AAS to SOP-FE-2231 by
ICPOES methods,added 3 SOP-FE-( 2231,2282,2372and 2392) to list.
Added drinking water analysis with price in ENVU
Added new SOP-FE-(3125,3126,3127,3128,3129) with the price of tests
Added SOP-FE-(1132,1133,1134,1135) with price in ENVU
Recalculated cost as 20% discount of analysis for all types of foods,drining water, animal
feed and food supplement as per law no14 year 2009.
Added remarks to list
Changed input time for Legionella from 2.2 to 2.30 hrs
11
Part 1-FMAU
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Rev. No: 6
page :3 of 23
LIST OF ANALYSIS PARAMETERS WITH REFERENCE METHODS
Dubai Central laboratory
Doc.Ref : SP-FE-0001
Issue Date :04/04/2016
S.No.Clause
AmendedDate Authorisaton
REVIEW DATENext Review
DateAuthorisation
-03/08/2009 -
18/10/2010 18/10/2011 HOS
Outcome of Review
Nature of Amendment
Reviewed no change required
-
REVIEW RECORD
AMENDMENT RECORD
18/10/2010 18/10/2011 HOS
30/11/2011 29/11/2012 HOS
22/11/2012 21/11/2013 HOS
22/11./2013 20/11/2014 HOS
20/01/2014 20/01/2015 HOS
09/02/2015 09/02/2016 HOS
04/04/2016 04/04/2017 HOS
Changed as per requirements
Associated Document
Reviewed no change required
Changed as per requirements
Changed as per requirements
Changed as per requirements
Reviewed no change required
Changed as per requirements
Issue By:SQO
���� IMS-DP-12-Laboratory Work Operations
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page :4 of 23
PARAMETER
TEST
METHOD
SOP-
REFERENCE SAMPLE TYPEREPORTING
UNIT
METHOD
DETECTION
INPUT
TIME
(Hrs)
ORIGINAL
COST
TEST
DURATI
ON
(Days)
REMARK
FDA (BAM on line) PPM Liquid cfu / ml 1
FDA (BAM on line) PPM Solid cfu / gm10 or as per
dilution factor
FDA (BAM on line) PPM cfu / ml 1
FDA (BAM on line) MPN cfu / ml 0.03
FDA (BAM on line) PPM cfu / gm10 or as per
dilution factor
FDA (BAM on line) MPN cfu / gm 0.3
FDA (BAM on line) MPN Liquid cfu / ml 0.03
FDA (BAM on line) MPN Solid cfu / gm 0.3
FDA (BAM on line) Liquid
Detected or
Not Detected /
ml
0.1
FDA (BAM on line) Solid
Detected or
Not Detected / 1
Enumeration of Coliforms
Bacteria
Enumeration of E.coli
Bacteria
Detection of of E.coli
Bacteria
LIST OF ANALYSIS PARAMETERS WITH REFERENCE METHODS
PART 1: FOOD MICROBIOLOGY ANALYSIS UNIT
0.5
Enumeration of Mesophilic
Areobic Colony
Count(ACC)
Dubai Central laboratory
FE-3103 * 70 2
Doc.Ref : SP-FE-0001
Issue Date : 04/04/2016
FE-3104 *
Liquid
4
Solid
0.5
40.5FE-3104 *
70
70
Rev. No: 6
FDA (BAM on line) Solid Not Detected /
gm
1
FDA (BAM on line) PPM Liquid cfu / ml 1
FDA (BAM on line) PPM Solid cfu / gm10 or as per
dilution factor
FDA (BAM on line) Liquid
Detected or
Not Detected
in 25ml
1
FDA (BAM on line) Solid
Detected or
Not Detected
in 25gm
1
FDA (BAM on line.) SPM Liquid cfu / ml 1
FDA (BAM on line.) SPM Solid cfu / gm10 or as per
dilution factor
FDA (BAM on line.) SPM Liquid cfu / ml 1
FDA (BAM on line.) SPM Solid cfu / gm10 or as per
dilution factor
Enumeration of Clostridium
perfringens
FDA 1998(BAM-
8th
ed)PPMcfu / ml 1
FDA 1998(BAM-
8th
ed)MPNcfu / ml 0.03
FDA 1998(BAM-
8th
ed)PPMcfu / gm
10 or as per
dilution factor
FDA 1998(BAM-
8th
ed)MPNcfu / gm 3
FDA (BAM - 8th
ed.) MPN Liquid cfu / ml 0.3
FDA (BAM - 8th
ed.) MPN Solid cfu / gm 3
0.5 70 4
Solid
Enumeration of Vibrio
parahaemolyticus FE-3110 0.5 70 4
FE-3109*
FE-3105 *
0.5
0.5
Liquid
Enumeration of Yeasts and
Moulds
Isolation and Identification
of Salmonella Species
Enumeration of Coagulase
Positive Staphylococcus
aureus
140
Enumeration of Bacillus
cereus
5
FE-3107 *
70
FE-3106 * 1
FE-3108 *
4
5700.5
Isuue by:SQO
70
4
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CONTROLLED COPY
page :5 of 23
PARAMETER
TEST
METHOD
SOP-
REFERENCE SAMPLE TYPEREPORTING
UNIT
METHOD
DETECTION
INPUT
TIME
(Hrs)
ORIGINAL
COST
TEST
DURATI
ON
(Days)
REMARK
LIST OF ANALYSIS PARAMETERS WITH REFERENCE METHODS
Dubai Central laboratory
Doc.Ref : SP-FE-0001
Issue Date : 04/04/2016
Rev. No: 6
FDA (BAM - 8th
ed.) MPN Liquid cfu / ml 0.3
FDA (BAM - 8th
ed.) MPN Solid cfu / gm 3
FDA (BAM - 8th
ed.) Liquid
Detected or
Not Detected
in 25ml
1
FDA (BAM - 8th
ed.) Solid
Detected or
Not Detected
in 25gm
1
FDA (BAM - 8th
ed.) Liquid
Detected or
Not Detected
in 25ml
1
FDA (BAM - 8th
ed.) Solid
Detected or
Not Detected
in 25gm
1
FDA (BAM - 8th
ed.) Liquid
Detected or
Not Detected
in 25ml
1
FDA (BAM - 8th
ed.) Solid
Detected or
Not Detected
in 25gm
1
FDA (BAM - 8th
ed.) Liquid
Detected or
Not Detected
in 25ml
1Detection of Yersinia
Isolation and Identification
of E.coli O157:H7 in
Foods
Isolation of Thermophilic
Campylobacter species
from Foods
Enumeration of Vibrio
parahaemolyticus
210
1.5 5
1.5FE-3112
Method for Isolation and
Detection of Listeria
Species.
FE-3111*
FE-3110 0.5
FE-3113*
1
210
5
4
140
70
5
in 25ml
FDA (BAM - 8th
ed.) Solid
Detected or
Not Detected
in 25gm
1
Enumeration of
Pseudomonas aeruginosa
and Pseudomonas species
in Food and water
FE-3115* 1992 (APHA- 20th
ed.) Liquid cfu /250ml 1 0.5 70 4
Don Whitley SC. 1997 Liquid cfu / ml 1
Don Whitley SC. 1997 Solid cfu / gm10 or as per
dilution factor
Don Whitley SC. 1997 Liquid cfu / ml 1
Don Whitley SC. 1997 Solid cfu / gm10 or as per
dilution factor
Don Whitley SC. 1997 Liquid cfu / ml 1
Don Whitley SC. 1997 Solid cfu / gm10 or as per
dilution factor
Don Whitley SC. 1997 Liquid cfu / ml 1
Don Whitley SC. 1997 Solid cfu / gm10 or as per
dilution factor
Detection of Meat Species in
cooked meats and meat
products by using Enzyme
Linked Immuno Sorbant
Assay (Elisa-Technique)
FE-3120 *Bio-Kits Procedure 2002
UKSolid
Suspected or
Not Detected
in 25 g
1% 0.5 70 3
Detection of Yersinia
entrocolitica in Food
Samples
0.5
1
Analysis of Food Samples
using Rapid Automated
Bacterial Impedance
Technique (RABIT) -
( Enumeration ofMolds and
Yeasts)
Analysis of Food Samples
using Rapid Automated
Bacterial Impedance
Technique (RABIT) -
(Enumeration of Mesophilic
Aerobic Colony Count /
Analysis of Food Samples
using Rapid Automated
Bacterial Impedance
Technique (RABIT) -
(Enumeration of Coliforms)
2
2
0.5 70
70
70
0.5
FE-3117*
0.5
Issue by:SQO
3
15FE-3114
FE-3117*
FE-3117*
FE-3117* 2
140
70
Analysis of Food Samples
using Rapid Automated
Bacterial Impedance
Technique (RABIT) -
(Enumeration/ Detection of
E.coli)
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PARAMETER
TEST
METHOD
SOP-
REFERENCE SAMPLE TYPEREPORTING
UNIT
METHOD
DETECTION
INPUT
TIME
(Hrs)
ORIGINAL
COST
TEST
DURATI
ON
(Days)
REMARK
LIST OF ANALYSIS PARAMETERS WITH REFERENCE METHODS
Dubai Central laboratory
Doc.Ref : SP-FE-0001
Issue Date : 04/04/2016
Rev. No: 6
Detection of Cronobacter
sakazakii in Powdered
Infant Formula
FE-3121 * FDA (BAM online) Solid
Detected or
Not detected
in 333gm
1 2 280 7
Liquid
Detected or
Not Detected
in 25ml
1
Solid
Detected or
Not Detected
in 25gm
1
USFDA- 8thed or AOAC Liquid cfu / ml 1
USFDA- 8thed or AOAC Solid cfu / gm10 or as per
dilution factor
USFDA- 8thed or AOAC Liquid cfu / ml 1
USFDA- 8thed or AOAC Solid cfu / gm10 or as per
dilution factor
USFDA- 8thed or AOAC Liquid
Detected or
not detected /
ml
1
USFDA- 8thed or AOAC Solid
Detected or
not detected /
gm
1
FE-3123*
Analysis of Food using
petriflim method 3M
( Enumeration o f
Mesophilic Areobic Colony
Count / ACC)
Detection of Salmonella
species by Using BAX
FE-3123* 2
2
70
FE-3122*AOAC Official Method
2003.092 280
0.5
2
70
Analysis of Food using
petriflim method 3M
(Enumeration of Coliforms
Bacteria)
0.5
FE-3123* 0.5 2
Analysis of Food using
petriflim method 3M (
Detection of E.coli Bacteria )
70gm
USFDA- 8thed or AOAC Liquid cfu / ml 1
USFDA- 8thed or AOAC Solid cfu / gm10 or as per
dilution factor
USFDA- 8thed or AOAC Liquid cfu / ml 1
USFDA- 8thed or AOAC Solid cfu / gm10 or as per
dilution factor
USFDA- 8thed or AOAC Liquid cfu / ml 1
USFDA- 8thed or AOAC Solid cfu / gm10 or as per
dilution factor
USFDA- 8thed or AOAC Liquid cfu / ml 1
USFDA- 8thed or AOAC Solid cfu / gm10 or as per
dilution factor
Solid
Detected or
Not Detected
in 25gm
1
Liquid
Detected or
Not Detected
in 25ml
1
Solid
Detected or
Not Detected
in 25gm
1
Liquid
Detected or
Not Detected
in 25ml
1
2 280FE-3126*
0.5
70
20.5
5
Enumeration of
Enterobacteriaceae in Foods FE-3124*
Analysis of Food using
petriflim method 3M
( Enumeration of E.coli
Bacteria )
Analysis of Food using
petriflim method 3M (
Enumeration of Yeasts and
Moulds )
FE-3123* 0.5 2
70
AOAC Official Method
2012.08
AOAC Official Method
2003.092
0.5
70
FE-3123*
70 2
280
2
2
Analysis of Food using
petriflim method 3M
( Enumeration of Coagulase
Positive Staphylococcus
aureus )
FE-3123*
Issue by:SQO
FE-3125*
Detection of Salmonella
spp. by VIDAS UP
Technique
Detection of Listeria
monocytogenes in Food
using BAX System
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CONTROLLED COPY
page :7 of 23
PARAMETER
TEST
METHOD
SOP-
REFERENCE SAMPLE TYPEREPORTING
UNIT
METHOD
DETECTION
INPUT
TIME
(Hrs)
ORIGINAL
COST
TEST
DURATI
ON
(Days)
REMARK
LIST OF ANALYSIS PARAMETERS WITH REFERENCE METHODS
Dubai Central laboratory
Doc.Ref : SP-FE-0001
Issue Date : 04/04/2016
Rev. No: 6
Solid
Detected or
Not Detected
in 10gm
1 ng
Liquid
Detected or
Not Detected
in 10ml
1 ng
Solid
Detected or
Not Detected
in 25gm
1
Liquid
Detected or
Not Detected
in 25ml
1
SureFood Animal ID Pork
kit (Manual S6014 Version
1.1E)
0.5%
Taqman Pork ID Kit (Pork
No. IMG-163-Rev. April
2013)
0.1%
Solid
Detected or
Not Detected 1
Detection of Pork
Contaminants in highly
processed Food and Feed by
Using Real-Time PCR
Technique
FE-3129* Solid
Detected or
Not detected
in 50-100 mg
2.5 350
FE-3128 1.5
Detection of Bacterial Enter
Toxin in food Using
TECRA Kit Method
210
AOAC Official Method
993.062
2SyLab Operation Manual
BacTrac 4000 Series
FE-3127 2 280
3
Detection of Different Micro-
organisms by Using Bac
Trac Method
(Detection of Salmonella
spp)
Solid Not Detected
in 25gm
1
Liquid
Detected or
Not Detected
in 25lm
1
Solid
Detected or
Not Detected
in 25gm
1
Liquid
Detected or
Not Detected
in 25 ml
1
Detection of Pork Gelatin in
Gelatinous Food Using Real-
Time PCR Technique
FE-3132
Taqman Pork ID Kit (Pork
No. IMG-163-Rev. April
2013)
Solid
Detected or
Not detected
in 50-100 mg
0.1% 2.5 350 3
Detection of Horse
contaminant Using Real-
Time PCR Technique
FE-3133Taqman Equine ID Kit
(SKU: A15570-Rev.2013)Solid
Detected or
Not detected
in 50-100 mg
0.1% 2.5 350 3
PPM: Pour Plate Method. SPM: Spread Plate Method. MPN: Most Probable Number .
Detection of E .coli
O157:H7 in Food Using
BAX System
FE-3130*AOAC Official Method
2009.112 280
Detection of Cronobacter
sakazakii in Baby Food
Using BAX System
280AOAC Official Method
20122FE-3131* 2
Issue by:SQO:
2
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CONTROLLED COPY
page :8 of 23
PARAMETER
TEST
METHOD
SOP-
REFERENCE SAMPLE TYPEREPORTING
UNIT
METHOD
DETECTION
INPUT
TIME
(Hrs)
ORIGINAL
COST
TEST
DURATI
ON
(Days)
REMARK
LIST OF ANALYSIS PARAMETERS WITH REFERENCE METHODS
Dubai Central laboratory
Doc.Ref : SP-FE-0001
Issue Date : 04/04/2016
Rev. No: 6
Determination of Moisture
/Total solids in Foods by
AIR-Oven methods
FE-2203 * AOAC, 17th Edn.2000 Solid / Liquid % w/w 0.02 0.4 56 4
Determination of moisture /
total solids in foods by
Vacuume -oven method
FE-2205AOAC , 17th Ed., (2000),
Gaithersburg, USA.Solid / Liquid % w/w 0.02 0.4 56 4
0.05 moisture
0.3 fat
0.5 protein
0.1 Ash
Determination of Fat content
in Foods by Ammonia
Digestion method
FE-2207 * AOAC, 17th Edn. 2000 Solid / Liquid %w/w 0.1 0.8 112 4
Determination of Fat in food
products (Meat & Cheese)FE-2208 AOAC, 15th Edn. 1990 Solid / Liquid %w/w 0.1 0.8 112 4
Determination of Total
Protein in Foods By
Kjeldahl method
FE-2210 * AOAC, 19th Ed ,2012 Solid / Liquid %w/w 0.1 0.8 112 4
Determination of Total Ash
in Foods by Incineration
method
FE-2211 * AOAC, 19th Ed ,2012 Solid / Liquid %w/w 0.05 0.7 98 4
Determination of Fat,Protein
and Acidity in selected Instrument Manual for FTIR 0.1 for Fat &
Determination of Moisture
Fat Protein and ash by FT-
NIR
FE-2206*
PART 2: FOOD CHEMICAL ANALYSIS UNIT
AOAC, 17th Edn.2000 Solid / Liquid % 0.15 21 5
and Acidity in selected
foods products by FTIR
Technique
FE-2212
Instrument Manual for FTIR
milkoscan FTIR20 Analyzer
FCMS-1
Solid / Liquid %w/w
0.1 for Fat &
Protein, 0.05 for
acidity
0.4 70 3
AOAC , 19 th Ed.,2012,
Gaithersburg, USA. 2.
David Pearson, The
Chemical Analysis of
Foods, 7th Ed., 1976
Determination of pH of
foodsFE-2214* APHA 4500 B-18th Edition Solid / Liquid - 0.1 0.3 42 2
Determination of Sugars by
HPLC in HoneyFE-2216*
Leatherhead Food RA, 2nd.,
1987Liquid %w/w
Fructose &
Glucose 1% and
Sucrose 0.5%
1.5 261 4
Determination of reducing
sugar and sucrose by Lane
& Eynon's
Solid / Liquid %w/w - 1.5 210 4
Determination of Non
reducing
sugar(Sucrose),Titrimetric
method
Solid / Liquid %w/w - 2.5 350 4
Determination of Water-
Soluble AshFE-2218 AOAC, 15th Edn. 1990 Solid / Liquid %w/w - 1.2 168 4
Determination of Acid-
Insoluble AshFE-2219 AOAC, 15th Edn. 1990 Solid / Liquid %w/w - 1.25 175 4
Determination of Alkalinity
of Water-Soluble AshFE-2220 AOAC, 15th Edn. 1990 Solid / Liquid %w/w - 1.5 210 4
FE-2217
AOAC, 15th Edn,1990,
Journal of the Society of
Chemical Industry, by J.
Lane and L. Eynon, 42, 325
AOAC, 15th Edn. 1990
Issue by:SQO
FE-2213*Determination of total
acidity in foodsSolid / Liquid %w/w 0.05 0.3 42 3
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CONTROLLED COPY
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PARAMETER
TEST
METHOD
SOP-
REFERENCE SAMPLE TYPEREPORTING
UNIT
METHOD
DETECTION
INPUT
TIME
(Hrs)
ORIGINAL
COST
TEST
DURATI
ON
(Days)
REMARK
LIST OF ANALYSIS PARAMETERS WITH REFERENCE METHODS
Dubai Central laboratory
Doc.Ref : SP-FE-0001
Issue Date : 04/04/2016
Rev. No: 6
Determination of Crude
FiberFE-2221
Pearson's Chemical Analysis
of Food, 7th Ed., 1976 Food
chemistry, by Lillian
Hoagland Mayer, CBS
Publishers & Dirtributors,
India, 1987
Solid / Liquid %w/w - 1.5 210 4
Determination of water
extract of tea and coffeeFE-2222 AOAC, 17th Edn.2000 Solid / Liquid %w/w - 0.55 77 4
Computationo solids not fat
and calorific value of foods
without crude Fiber
- Solid / Liquid Kcal/100g - 2.8 392 4
Computationo solids not fat
and calorific value of foods
with crude Fiber
Solid / Liquid Kcal/100g - 4.3 602 5
Computationo solids not fat
(S.N.F)Solid / Liquid %w/w 0.1 0.8 112 5
Determination of
Extraneous matter and
defects in Food grains
FE-2224 AOAC, 17th Edn.2000 Solid %w/w - 0.5 70 3
Determination of stones
(seeds) and shell content in
fruits/dried fruits and nuts.
FE-2225 - Solid / Liquid %w/w - 0.5 70 3
FE-2223
fruits/dried fruits and nuts.
Determination of Salt
content in edible Salt and
Foods
FE-2226 AOAC, 19th Ed ,2012 Solid / Liquid %w/w - 0.4 56 3
Determination of Drained
Weight in canned / Bottled
Foods
FE-2228 - Solid / Liquid %w/w - 0.25 35 3
Determination of Minerals
in Fortified Food Products
by ICPOES after Microwave
Digestion
FE-2231*J. of AOAC International,
vol 95, No. 1, 2012Solid / Liquid mg/kg As per standard 1.5 210 5
210 (Dhr)
for first
element, 32
(Dhr) per
extra
element
Detection and
Determination of Titanium
Dioxide in Food
FE-2232*AOAC Official Method
973.36 (2012) Solid / Liquid mg/kg 10 1.5 210 5
Detection of Titanium
dioxide- AOAC OM 973.36 Solid / Liquid
Detected/Not
detected- 1 140 7
Determination of Refractive
Index of Oils and FatsFE-2260* AOAC, 17th Edn. 2000 Solid / Liquid nD - 0.25 35 4
Determination of Free Fatty
Acid (FFA) in Fats and oilsFE-2261* AOAC, 19th Ed ,2012 Solid / Liquid %w/w 0.05 0.4 56 4
Determination of Peroxide
Value of Fats and OilsFE-2262* AOAC, 19th Ed ,2012 Solid / Liquid mq/Kg 0.1 0.4 56 4
Determination of Melting
Point of FatsFE-2263* AOAC, 17th Edn. 2000 Solid / Liquid °C - 0.5 70 4
Determination of Fatty Acid
Profile of Oils & FatsFE-2264* AOAC, 17th Edn. 2000 Solid / Liquid % - 1 140 4
Issue by:SQO
Note: Printed copy of this document shall be treated as ‘Uncontrolled’. Always refer the controlled version ‘Online
CONTROLLED COPY
page :10 of 23
PARAMETER
TEST
METHOD
SOP-
REFERENCE SAMPLE TYPEREPORTING
UNIT
METHOD
DETECTION
INPUT
TIME
(Hrs)
ORIGINAL
COST
TEST
DURATI
ON
(Days)
REMARK
LIST OF ANALYSIS PARAMETERS WITH REFERENCE METHODS
Dubai Central laboratory
Doc.Ref : SP-FE-0001
Issue Date : 04/04/2016
Rev. No: 6
AOAC, 17th Edn. 2000 Solid / Liquid % 0.2 1 140 4
Journal of AOAC
International,volume1 ,
2012. chapter 41, 27-28.
Solid / Liquid % 0.2 1 140 4
Determination of Iodine
value by FT-NIRFE-2265* AOCS cd 1e-01 Solid / Liquid
% Iodine
absoredAs per SOP 0.5 70 3
Determination of Ethanol
contents in non-alcholic I
beverage by using static
FE-2270*
AOAC Official Method
986.12,2000, HALAL”
CAC/GL 24-1997
Solid / Liquid v/v % 0.001 1 140 5
Determination of
Preservatives, Artificial
sweeteners and Caffeine in
Foods by HPLC method
FE-2280 * HPLC-DAD Manual Solid / Liquid mg/Kg
Liquids: BA,SA &
Caffeine:0.5 mg/L,
APM, Ace-K &
APM-1 mg/L.
SOLIDS:BA,SA &
Caffeine:5 mg/kg,
APM, Ace-K &
APM-5 mg/kg
0.8 112 5
For one
Preservatives,
Any extra
Preservatives
will increase
the time by
0.25 hr, and
charge by 35
(Dhr)
Determination of Vitamin C
in Soft DrinksFE-2281*
British Standard: BS EN
14130:2003Solid / Liquid mg/100g 5 1.5 210 5
FE-2264*
Determination of Fatty Acid
Profile of oils and fats,
omega fatty acids in
selected foods and food
supplements
Determination of Water
Soluble Vitamins in Foods
and food supplements
FE-2282*
Official Methods of AOAC
international, 19th Edition,
2012 Solid / Liquid mg/kgRefer validation
procedure1 140 5
For one
vitamin 140
AED and
35AED for
each
additional
vitamin
Identification of water
soluble Synthetic Colours in
Foods by Paper
Chromatography
FE-2285 *Pearson's Chemical Analysis
of food, 7th Ed, 1976Solid / Liquid - - 0.5 70 2
Solid mg/Kg 1 2.15 301 5
Liquid mg/L 1 2.15 301 5
Detection & Determination
of Sulphur Dioxide FE-2290 AOAC, 17th Edn. 2000 Solid / Liquid mg/Kg 5 1 140 5
Determination of total
soluble solids (Brix°) in
foods and moisture in
Honey
FE-2294*
Instruction manual for
automatic digital
refractomer RX-
50000,AOAC Official
Methods of Analysis (2000)
– AOAC Official Method
969.38
Solid / Liquid % - 0.25 35 3
Determination of Fat in
Butter / Ghee- AOAC OM 938.06 Solid / Liquid g/100g - 0.8 112 4
Determination of Aflatoxins
(B1, B2, G1, G2) in foods
by HPLC method
FE-2320* AOAC, 17th Edn. 2000 Solid µg/kg0.3 for B1 & G1 /
0.1 for B2 & G23.5 490 4
Determination of Synthetic
Food Colours by HPLCFE-2286 AOAC, 17th Edn. 2000
Issue by:SQO
Note: Printed copy of this document shall be treated as ‘Uncontrolled’. Always refer the controlled version ‘Online
CONTROLLED COPY
page :11 of 23
PARAMETER
TEST
METHOD
SOP-
REFERENCE SAMPLE TYPEREPORTING
UNIT
METHOD
DETECTION
INPUT
TIME
(Hrs)
ORIGINAL
COST
TEST
DURATI
ON
(Days)
REMARK
LIST OF ANALYSIS PARAMETERS WITH REFERENCE METHODS
Dubai Central laboratory
Doc.Ref : SP-FE-0001
Issue Date : 04/04/2016
Rev. No: 6
Solid 0.03 2.5 350 4
Liquid 0.003 2.5 350 4
Determination of Patulin in
Apple productsFE-2323
AOAC - BS EN
14177:2003 , BS EN
15890:2010
Solid / Liquid µg/kg 1 3.5 490 5
Determination of
Mycotoxins indifferent food
Commodities by Ultra-
Performance lquied
Chromatography and Tirple
Quadrupole Detector
FE-2324* RCM-2009; 23:1801-1809 Solid µg/kgAs per Annex-2
of SOP3.5 490 7
1-AED:490
for one toxin
2-115 for
each extra
toxins ( total
for 11 toxins
1755 Dh)
Determination of
Organochlorine and
Organophosphorous
Pisticide Residue in Cereals
(NON-Fatty dry Foods)
FE-2342 AOAC,15th Edn,1990 Cereals & Dry foods mg/KgAs per
Annex(III)of SOP 8 1120 7
Determination of N-
Methylcarbamatesin Fruits
and Vegetable Quenchers
Technique using LC-
MS/MS
FE-2343 *
AOAC 90, No. 2, 2007 In
house modified. Tripple
Quadrupole LC/MS System.Fruits & Vegetable mg/kg As per SOP 4 560 7
560 ( Dhr)
for N-
Methylcarba
matesin only
Determination of Aflatoxins
(M1, M2) in MilkFE-2321* AOAC, 15th Edn. 1990 µg/kg
MS/MS
Solid
Liquid
Multiresidue method for
analysis of pesticide residues
in fruits & Vegetables by
Acetonitrile extraction &
detection & GC-
ECD/NPD/MSD/PFPD
Detection -A QuEChERS
Approach
FE-2346*AOAC,Vol.90, No 2,2007.
In house modified. Fruits & Vegetable mg/kg
As per Annex
( I & II ) of SOP8 1120 7
Determination of N-
Methylcarbamatesin Fruits
and Vegetable Quenchers
Technique using LC-
MS/MS and Multiresidue
method for analysis of
pesticide residues in fruits &
Vegetables by Acetonitrile
extraction & detection &
GC-ECD/NPD/MSD/PFPD
Detection -A QuEChERS
Approach
FE-2343 * &
FE-2346*
AOAC 90, No. 2, 2007;In
house modified. Tripple
Quadrupole LC/MS System.Fruits & Vegetable mg/kg
10 and As per
Annex ( I &II) of
SOP
12 1680 7
For SOP-
FE-2343
(560 Dhr) +
SOP FE-
2346 (1120
(AED) =
1680
Multiresidue method for
analysis of pesticide residues
in fruits & Vegetables by
Acetonitrile extraction &
detection & GC-MSD
Detection -A QuEChERS
Approach
FE-2347*
AOAC 90, No.2, 2007 In
house modified. Single
Quadrupole GC/MS
System.
Fruits & Vegetable mg/kg As per SOP 6.75 945 7
Analysis of Pesticide
Residues in Spices by
Multiresidue Method -A
QuEChERS Approach
FE-2348*
AOAC Official Method
2007.012. In house
modified. Triple
Quadrupole GC/MS
System.
Spices mg/kg As per SOP 8 1120 7
Issue by:SQO
As per Annex of
SOP4 560 7
Determination of
Organochlorine Pestiside
and Polychlorinated
Biphenyl Residue in Milk -
Quechers.
FE-2345*AOAC,Vol.88, No 2,2005
In house modified.mg/kg
Note: Printed copy of this document shall be treated as ‘Uncontrolled’. Always refer the controlled version ‘Online
CONTROLLED COPY
page :12 of 23
PARAMETER
TEST
METHOD
SOP-
REFERENCE SAMPLE TYPEREPORTING
UNIT
METHOD
DETECTION
INPUT
TIME
(Hrs)
ORIGINAL
COST
TEST
DURATI
ON
(Days)
REMARK
LIST OF ANALYSIS PARAMETERS WITH REFERENCE METHODS
Dubai Central laboratory
Doc.Ref : SP-FE-0001
Issue Date : 04/04/2016
Rev. No: 6
Analysis of Pesticide &
PCBs Residues in Tissues
by Multiresidue Method -A
QuEChERS Approach
FE-2349*
AOAC Official Method
2007.012. In house
modified. Single
Quadrupole GC/MS
System.
Tissues ng/kg As per SOP 4 560 7
Analysis of Pesticide
Residues in Honey by GC-
MSD & LC-MSMS -A
Multiresidue QuEChERS
Approach
FE-2350*
EURL-2010 In house
modified. Tripple
Quadrupole LC/MS &
Single Quadripole GC/MS
System.
Honey and Dates
syrupmg/kg As per SOP 8 1120 7
Detection of Sulfonamide
Antibacterial in Raw Milk
by Charm II Test
FE-2360
by GC/MS - Thermo
Scientific, Technical
Note:10236, 2008.
Liquid µg / L _ 1.5 210 4
Detection of Tetracycline
antibacterial in Raw Milk by
Charm II Test
FE-2361arm II Test Operator’s
Manual for Tetracyclines Liquid µg / L _ 1.5 210 4
Detection of β-Lactams
Antibacterial in Raw Milk
by CharmII Test
FE-2362
Charm II Test
TBL8MRL06,
Rev.November 2004
(Charm Sciences Inc.)
Liquid µg / L _ 1.5 210 4
Detection of Macrolide
Antibacterial in Raw & FE-2364
Charm II Test Operator’s Liquid µg / L _ 1.5 210 4
Antibacterial in Raw &
Pasteurized Milk By Charm
II Test
FE-2364Charm II Test Operator’s
Manual for Macrolides Liquid µg / L _ 1.5 210 4
Liquid µg /L Milk 0.02
Fish: 0.04
Honey: 0.07
Liquid µg /L
Solid µg /L
Liquid mg/kg
Solid mg/kg
Liquid µg /L
Solid µg /L
Determination of
Antihelmintics-
Averrmectins- Residues in
Foods by LC-MSMS
FE-2372* Agilent Application Note Solid/Liquid µg/kgAs per Appendix
of SOP5 700 5
Determination of
Chloramphenicol in Foods
by LC-MS-MS
FE-2368*
AOAC, 2005, 2006,
Commission Decision
2002/657/EC, Commission
Decision2003 /181/EC,5 700
Issue by:SQO
Determination of Melamine
and Cyanuric Acid Residues
in Foods
FE-2370*
1-FDA LIB No. 4422,
Interim Method for
Determination of Melamine
and Cyanuric Acid Residues
In Foods using LC-
0.1 5 700 5
Determination of
Sulfonamides &
Trimethoprim in Milk and
Tissues by LC-MSMS
FE-2369*
Analysis of veterinary drug
residues in shrimp, Journal
of Chromatography B, 836
(2006) 22–3
As per Appendix-
2 of SOP
5
Solid µg /kg
5 700 5
Determination of
Tetracyclines in foods by LC-
MSMS
FE-2371*
10.2 Official Methods of
Analysis, 19th Edition
(2012), Method 995.09.
As per Appendix-
1 & 2 of SOP5 700 5
Note: Printed copy of this document shall be treated as ‘Uncontrolled’. Always refer the controlled version ‘Online
CONTROLLED COPY
page :13 of 23
PARAMETER
TEST
METHOD
SOP-
REFERENCE SAMPLE TYPEREPORTING
UNIT
METHOD
DETECTION
INPUT
TIME
(Hrs)
ORIGINAL
COST
TEST
DURATI
ON
(Days)
REMARK
LIST OF ANALYSIS PARAMETERS WITH REFERENCE METHODS
Dubai Central laboratory
Doc.Ref : SP-FE-0001
Issue Date : 04/04/2016
Rev. No: 6
Determination of
Acrylamide in Selected
Foods by LCMSMS
FE-2373*
Institue of Food safety &
health, Illinois Institue of
Technology, bedford park
Solid µg/kg 25 3 420 5
Determination of
NSAIDS(Non-Steroidal
Anti-Inflammatory Drugs)
Residues in Milk by
LCMSMS
FE-2374 Anal. Biochem 2012 Solid/Liquid µg/kgAs per Appendix
2 of SOP5 700 5
Determination of Benzo (a)
Pyrene in Oils and FatsFE-2390* BS EN ISO 25302 :2010 Solid / Liquid µg/kg 0.4 4.5 630 5
Determination of 3-MCPD
in Soy Sauce by GC-MSFE-2391* AOAC, 17th End 2000 Liquid mg/Kg 0.03 6 840 5
Determination of Polycyclic
Aromatic Hydrocarbons in
Edible Oils and fats
FE-2392*BS EN ISO 25302 :2010. In
house modified.Solid / Liquid µg/kg Refer SOP 4.5 630 5
Determination of Sudan
Dyes in Selected
Spices/Condiments &
Selected Foods
FE-2400*
Statutory Analysis
Government Chemist
Programme – LGC Limited
2006- Food Standards
Agency - information
Solid / Liquid mg / Kg 1 2 280 7
Solid Bq/kg 2.5
Liquid Bq/L 2.5
Idenfication of Rhodamine
B in Foods by paper
Chromatography
FE-2403*
David Pearson, the
Chemical Analysis of Foods
, 7th Edn, (1976),Churchill
Livingstone ,
Developments in food
colours, Vol I & II, Avi.
Publishers.
Solid / Liquid mg/kg 2 0.5 70 3
Determination of traces
elements of
As*,Cd*,Hg*,Pb* in food
stuffs by ICP-MS after
pressure digestion
-
As 15
Cd 5
Hg 15
Pb 15
Idenfication of
Rhodamine B in Foods
by paper
Chromatography
FE-2403*
David Pearson, the
Chemical Analysis of Foods
, 7th Edn, (1976),Churchill
Livingstone ,
Developments in food
colours, Vol I & II, Avi.
Publishers.
Solid / Liquid mg/kg 2 0.5 70 3
Issue by:SQO
Determination of Gamma
Radiation in Foods by using
sodium iodide gamma
Spectrometer
FE-2401*
Berthold LB 2045 Gamma
Spectrometer instruction
manual.Method for
detection of permissible
radionuclides limits in food
part 1; gamma spectrometry
analysis GSO 998-1998
1 140 2
BS EN
15763:2009BSEN 15763:2009 Solid / Liquid ug/kg 3.33 466 5
466 for one
test, more
than one test
115
Note: Printed copy of this document shall be treated as ‘Uncontrolled’. Always refer the controlled version ‘Online
CONTROLLED COPY
page :14 of 23
PARAMETER
TEST
METHOD
SOP-
REFERENCE SAMPLE TYPEREPORTING
UNIT
METHOD
DETECTION
INPUT
TIME
(Hrs)
ORIGINAL
COST
TEST
DURATI
ON
(Days)
REMARK
LIST OF ANALYSIS PARAMETERS WITH REFERENCE METHODS
Dubai Central laboratory
Doc.Ref : SP-FE-0001
Issue Date : 04/04/2016
Rev. No: 6
Determination of Residual
Monomers Migration from
Food Packging into Food
Simulants by GC-MS
FE-2450*BSEN : 13130-1:2004,
BSEN 13130-5:2004Food contact materials µg/kg
0.5 for Benzene
&Et Benzene, 1.0
for Styrene, 1.5
for Toluene
1.5 210 5
Physical analysis SP-FE-0004 - - - - 0.3 42 1
Determination of Total Ash
in Foods by Incineration
method
FE-2211* AOAC, 17th Edn. 2000 Solid / Liquid %w/w - 0.7 98 4
Determination of Aflatoxins
(B1, B2, G1, G2) in foods
by HPLC method
FE-2320* AOAC, 17th Edn. 2000 Solid µg/kg0.3 for B1 & G1 /
0.1 for B2 & G23.5 490 4
Determination of
Mycotoxins indifferent food
1-AED:490
for one toxin
ANIMAL FEED ANALYSIS
Mycotoxins indifferent food
Commodities by Ultra-
Performance lquied
Chromatography and Tirple
Quadrupole Detector
FE-2324* RCM-2009; 23:1801-1809 Solid µg/kgAs per Annex-2
of SOP3.5 490 7
2-115 for
each extra
toxins ( total
for 11 toxins
1755 Dh)
*-Test is listed in DAC accreditation schedule No. LB-014 -TEST
Issue by:SQO
# -Solution basis
Note: Printed copy of this document shall be treated as ‘Uncontrolled’. Always refer the controlled version ‘Online
CONTROLLED COPY
page :15 of 23
PARAMETER
TEST
METHOD
SOP-
REFERENCE SAMPLE TYPEREPORTING
UNIT
METHOD
DETECTION
INPUT
TIME
(Hrs)
ORIGINAL
COST
TEST
DURATI
ON
(Days)
REMARK
LIST OF ANALYSIS PARAMETERS WITH REFERENCE METHODS
Dubai Central laboratory
Doc.Ref : SP-FE-0001
Issue Date : 04/04/2016
Rev. No: 6
Water / Waste water 52 3
Drinking water 42 3
Water µS/cm 5 52 3
Drinking water µS/cm 5 42 3
Waste water mS/cm 0.01 52 3
Determination of salinity in
waterFE-1102 Salinity meter Water / Waste water ppt 5 0.3 52 3
Water / Waste water 44 3
Drinking water 35 3
Determination of Total
Suspended Solids in water
and waste water
FE-1104 * APHA-2540 D Water / Waste water mg/L 11 0.6 104 5
0.25
Determination of
Conductivity in waterFE-1102* APHA-2510 B 0.3
Determination of Turbidity FE-1103 APHA-2130 B NTU 0.5
PART 3:ENVIRONMENT UNIT
Determination of pH in
waterFE-1101 * APHA-4500-H+ - 1 to 14 0.3
and waste water
Water mg/L 10
Waste water mg/L 51
FE-1105 TDS / EC Meter Drinking water mg/L 5 0.6 84 5
Determination of Total
Solids in water and waste
water
FE-1106 APHA-2540 B Water / Waste water mg/L 51 0.6 104 5
Water / Waste water mg/L 5 0.5 87 3
Drinking water mg/L 5 0.5 70 3
Determination of Acidity in
water and waste waterFE-1108 APHA-2310 B Water / Waste water mg/L 5 0.5 87 3
Determination of Alkalinity
in water and waste waterFE-1109 APHA-2320 B Water / Waste water mg/L 5 0.5 87 3
Determination of Chloride FE-1110 APHA-4500-Cl- B Water / Waste water mg/L 6 0.5 87 3
Determination of Nitrogen-
Ammonia in water and
waste water
FE-1112 APHA-4500-NH3- B, C Water / Waste water mg/L 0.2 0.64 111 5
Determination of Nitrate-
Nitrogen in water
wastewater
FE-1113 APHA-4110 Water / Waste water mg/L 0.05 0.77 134 5
Determination of Total
Nitrogen FE-1115
T.R.Parsons 2.1, 1984,
APHA 4110 BWater / Waste water mg/L 0.13 0.9 157 5
Determination of Total
Kjeldahl NitrogenFE-1116 APHA - 4500 - Norg B, C Water / Waste water mg/L 1 1.2 209 5
Issue By:SQO
APHA-2340FE-1107
Determination of Total
Hardness in water and
waste water
Determination of Total
Dissolved Solids in water
and waste water
FE-1105 * APHA-2540 C 0.6 104 5
Note: Printed copy of this document shall be treated as ‘Uncontrolled’. Always refer the controlled version ‘Online
CONTROLLED COPY
page :16 of 23
PARAMETER
TEST
METHOD
SOP-
REFERENCE SAMPLE TYPEREPORTING
UNIT
METHOD
DETECTION
INPUT
TIME
(Hrs)
ORIGINAL
COST
TEST
DURATI
ON
(Days)
REMARK
LIST OF ANALYSIS PARAMETERS WITH REFERENCE METHODS
Dubai Central laboratory
Doc.Ref : SP-FE-0001
Issue Date : 04/04/2016
Rev. No: 6
Determination of Phosphate-
phosphorousMOOPAM 4
th ED. 3.2.8-A Water / Waste water mg/L 0.02 0.64 111 5
Determination of Total
Phosphorus in water/ waste
water
APHA - 4500 - P (B, D) Water / Waste water mg/L 0.1 0.99 172 5
Determination of Sulfide FE-1120 APHA - 4500 S2-
F Water / Waste water mg/L 1 0.5 87 5
Determination of Oil and
Grease in water and waste
water
FE-1121 * APHA - 5520 B Water / Waste water mg/L 12 1.2 209 5
Determination of
Biochemical Oxygen
Demand (BOD)
FE-1122 * APHA - 5210 B Water / Waste water mg/L 7 0.5 87 7
Determination of Chemical
Oxygen Demand (COD)FE-1123 * APHA - 5220 B Water / Waste water mg/L 12 0.44 77 5
Water ug/L 0.1 6 1044 7
drinking water ug/L 0.1 6 840 7
Determination of
Phytopigments FE-1125 T.R.Parsons (4.1,4.2), 1984 Water mg/m
3 0.5 1.2 209 5
Determination of Petroleum
Hydrocarbons in waterFE-1126
MOOPAM 4th
ED. -Section
6.6, 6.9Water / Waste water mg/L 5 0.8 139 5
Determination of
Organochlorine Pesticides in
Water By GC-ECD-Solvent
Extraction
APHA 6630 BFE-1124*
FE-1117
Hydrocarbons in waterFE-1126
6.6, 6.9Water / Waste water mg/L 5 0.8 139 5
Determination of Heavy
Metals (Cu, Cd, Pb, Ni, Zn,
Cr)*
FE 1128 APHA - 3030 E, 3111 Water / Waste water mg/Las per each
element307 7
Determination of Copper
(Cu) *Water / Waste water mg/L 0.1
Determination of Cadmium
(Cd) *Water / Waste water mg/L 0.08
Determination of Zinc (Zn)
*Water / Waste water mg/L 0.05
Determination of
Manganese (Mn)*Water / Waste water mg/L 0.05
Determination of Nickel
(Ni) * Water / Waste water mg/L 0.2
Determination of Chromium
(Cr)*Water / Waste water mg/L 0.2
Determination of Iron (Fe)* Water / Waste water mg/L 0.1
Determination of Cobalt
(Co)* Water / Waste water mg/L 0.12
Determination of Lead (Pb) * Water / Waste water mg/L 0.5
Determination of Silver (Ag)* FE-1128 APHA - 3030 E, 3111 water / waste water mg/L 0.1 0.5 87 5
0.5 87 7
87 AED for
one Element
& 44 AED
for each
extra
elements
Issue by:SQO
FE-1128 APHA - 3030 E, 3111
Note: Printed copy of this document shall be treated as ‘Uncontrolled’. Always refer the controlled version ‘Online
CONTROLLED COPY
page :17 of 23
PARAMETER
TEST
METHOD
SOP-
REFERENCE SAMPLE TYPEREPORTING
UNIT
METHOD
DETECTION
INPUT
TIME
(Hrs)
ORIGINAL
COST
TEST
DURATI
ON
(Days)
REMARK
LIST OF ANALYSIS PARAMETERS WITH REFERENCE METHODS
Dubai Central laboratory
Doc.Ref : SP-FE-0001
Issue Date : 04/04/2016
Rev. No: 6
Determination of Fluoride (
F)* in water by Ion
chromatography
Dionex manual water mg/L 0.1
Determination of Chloride
(Cl)* in water by Ion
chromatography
Dionex manual water mg/L 0.1
Determination of Nitrate
(NO3) * in water by Ion
chromatography
Dionex manual water mg/L 0.1
Determination of Sulfate
(SO4)*in water by Ion
chromatography
Dionex manual water mg/L 0.1
Determination of Bromate
(BrO3)* in water by Ion
chromatography
Dionex manual water ug/L 3
Determination of Bromide
(Br)* in water by Ion
chromatography
Dionex manual water mg/L 0.1
Determination of Chlorite
(ClO2)in water by Ion
chromatography
Dionex manual water ug/L 5
Determination of
Chlorate(ClO3) in water by
Ion chromatography
Dionex manual water ug/L 5
5
131 AED
for one
Element &
44 AED for
each extra
elements,
DRINKING WATER (SOP-FE-1130)
FE-1130 0.75 131
Determination of Fluoride
( F)* in water by Ion
chromatography
Dionex manual Drinking water mg/L 0.1
Determination of Chloride
(Cl)* in water by Ion
chromatography
Dionex manual Drinking water mg/L 0.1
Determination of Nitrate
(NO3) * in water by Ion
chromatography
Dionex manual Drinking water mg/L 0.1
Determination of Sulfate
(SO4)*in water by Ion
chromatography
Dionex manual Drinking water mg/L 0.1
Determination of Bromate
(BrO3)* in water by Ion
chromatography
Dionex manual Drinking water ug/L 3
Determination of Bromide
(Br)* in water by Ion
chromatography
Dionex manual Drinking water mg/L 0.1
Determination of Chlorite
(ClO2)in water by Ion
chromatography
Dionex manual Drinking water ug/L 5
Determination of
Chlorate(ClO3) in water by
Ion chromatography
Dionex manual Drinking water ug/L 5
Determination of Heavy
Metals (Cu, Cd, Pb, Ni, Zn,
Cr)* in water / waste water
by ICP-OES
APHA - 3030 E, 3120 Water / Waste water mg/Las per each
element131
Determination of Metals
(Cu, Fe, Zn, Ca, Mg, Na)*in
drinking water by ICP-OES
APHA - 3030 E, 3121 Drinking water mg/Las per each
element105
FE-1130 0.75 105 5
105 AED
for one
Element &
35 AED for
each extra
elements,
FE-1131 0.75 5
Issue by:SQO
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PARAMETER
TEST
METHOD
SOP-
REFERENCE SAMPLE TYPEREPORTING
UNIT
METHOD
DETECTION
INPUT
TIME
(Hrs)
ORIGINAL
COST
TEST
DURATI
ON
(Days)
REMARK
LIST OF ANALYSIS PARAMETERS WITH REFERENCE METHODS
Dubai Central laboratory
Doc.Ref : SP-FE-0001
Issue Date : 04/04/2016
Rev. No: 6
water µg/L 5
Waste water mg/L 0.1
Determination of Arsenic
(As) by ICP-OES water / waste water µg/L 8
Water µg/L 2
Waste water mg/L 0.05
Water µg/L 2
Waste water mg/L 0.1
Water µg/L 6
Waste water mg/L 0.1
Determination of Cadmium
(Cd*) by ICP-OES
Determination of
Manganese (Mn*) by ICP-
OES
Determination of Silver
(Ag*) by ICP-OES
FE-1131 APHA 3120 0.75 131 5
Determination of Lead (
Pb*) by ICP-OES
131 AED
for one
Element &
44 AED for
each extra
elements
Waste water mg/L 0.1
Determination of Calcium
(Ca*) by ICP OESWater mg/L 0.05
Determination of
Magnesium (Mg*) by ICP-
OES
water mg/L 0.05
Determination of Iron (Fe*)
by ICP-OESWater mg/L 0.05
Determination of Zinc
(Zn*) by ICP-OESWaste water mg/L 0.05
Determination of Nickel
(Ni*) by ICP-OESWaste water mg/L 0.1
Determination of
Chromium (Cr*) by ICP-
OES
Waste water mg/L 0.1
Determination of Copper
(Cu*) by ICP-OESWaste water mg/L 0.05
Determination of
Molybdenum (Mo) by ICP-
OES
water µg/L 10
Determination of Sodium
(Na) by ICP-OESwater µg/L 10
Determination of
Barium(Ba) by ICP OESwater µg/L 10
Determination of
Potassium(K) by ICP OESwater µg/L 10
1131 APHA 3120 0.75 131 5
131 AED
for one
Element
&44AED
for each
extra
elements,
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PARAMETER
TEST
METHOD
SOP-
REFERENCE SAMPLE TYPEREPORTING
UNIT
METHOD
DETECTION
INPUT
TIME
(Hrs)
ORIGINAL
COST
TEST
DURATI
ON
(Days)
REMARK
LIST OF ANALYSIS PARAMETERS WITH REFERENCE METHODS
Dubai Central laboratory
Doc.Ref : SP-FE-0001
Issue Date : 04/04/2016
Rev. No: 6
Determination of Cadmium
(Cd*) by ICP-OES Drinking water µg/L 2
Determination of
Manganese (Mn*) by ICP-
OES
Drinking water µg/L 2
Determination of Lead (
Pb*) by ICP-OES Drinking water µg/L 6
Determination of Calcium
(Ca*) by ICP OES Drinking water mg/L 0.05
Determination of
Magnesium (Mg*) by ICP-
OES
Drinking water mg/L 0.05
Determination of Nickel
(Ni*) by ICP-OES Drinking water µg/L 10
Determination of Iron (Fe*)
by ICP-OES Drinking water mg/L 0.05
Determination of Zinc
(Zn*) by ICP-OES Drinking water µg/L 10
Determination of
Chromium (Cr*) by ICP-
OES
Drinking water µg/L 10
0.75 105 5
DRINKING WATER (SOP-FE-1131)
105 AED
for one
Element
&35 AED
for each
extra
elements,
1131 APHA 3120
Determination of Copper
(Cu*) by ICP-OES Drinking water µg/L 10
Determination of
Molybdenum (Mo) by ICP-
OES
Drinking water µg/L 10
Determination of Sodium
(Na) by ICP-OES Drinking water µg/L 10
Determination of
Barium(Ba) by ICP OES Drinking water µg/L 10
Determination of
Potassium(K) by ICP OES Drinking water µg/L 10
Water Colour Units 1 0.7 122 3
Drinking water Colour Units 1 0.7 98 3
APHA - 4500 Cl -G Water mg/L 0.2 0.7 122 3
APHA - 4500 Cl -G Drinking water mg/L 0.2 0.7 98 3
APHA - 4500 Cl -G Water mg/L 0.2 0.7 122 3
APHA - 4500 Cl -G Drinking water mg/L 0.2 0.7 98 3
Determination of Carbonate
and Bicarbonate in water
by Titrimetry
FE-1134 AOAC 920.194 Water mg/L 5 0.5 87 3
FE-1133
Determination of
Monochoramine
Determination of Colour FE-1132 APHA - 2120 B
Determination of Free
Chlorine
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page :20 of 23
PARAMETER
TEST
METHOD
SOP-
REFERENCE SAMPLE TYPEREPORTING
UNIT
METHOD
DETECTION
INPUT
TIME
(Hrs)
ORIGINAL
COST
TEST
DURATI
ON
(Days)
REMARK
LIST OF ANALYSIS PARAMETERS WITH REFERENCE METHODS
Dubai Central laboratory
Doc.Ref : SP-FE-0001
Issue Date : 04/04/2016
Rev. No: 6
Drinking water ug/L 0.5 7.3 1022 7
Water ug/L 0.5 7.3 1270 7
Drinking water ug/L 0.5 4 560 7
Water ug/L 0.5 4 696 7
Determination of Volatile
Organic Compounds in
Water with Headspace Trap
GCMS
FE-1136 APHA 6200 B Drinking water ug/L As per SOP 7 890 7
Determination of total
organic carbon(TOC) in
water
FE-1137 APHA - 5310 B water / waste water mg/L 1 1 174 5
Determination of Moisture
in SoilFE-1301
Chemical analysis of
polluted soils. EPA-
Publication.139-4.
Soil/ Sludge/Sediment % - 0.5 87 5
Determination of pH in
SoilFE-1302 EPA-SW-846-9045 C Soil/ Sludge/Sediment - 1 to 14 0.5 87 5
Determination of Total
Phosphorus in Soil /
Sediment
FE-1303
Chemical analysis of
ecological materials-3,
APHA - 4500 P D
Soil / Sludge /
Sedimentmg/Kg 1 1.7 296 5
Determination of Trace
elements (Sb, As, Ba, Be, Cd,
Cr, Pb, Mn, Mo, Ni, Se, Ag, Sn,
U ) by ICP-MS
FE-1135 APHA - 3125
Determination of Trace
elements Mercury (Hg) in
by ICP-MS
FE-1135 APHA - 3125
Sediment APHA - 4500 P D
Cu-4
Cd-2
Zn-4
Pb-15
Ni-16
Cr-9
Determination of Total
Petroleum Hydrocarbons in
Soil
FE-1305MOOPAM 4
th ED.
–Section 6.7, 6.9
Soil / Sludge /
Sedimentmg/Kg 0.2 2.1 365 7
Determination of Oil and
Grease in Soil / SludgeFE-1306 APHA - 5520 E
Soil / Sludge /
Sedimentmg/kg ** 1.1 191 7
Determination of Sludge-
Leachate test FE-1307 DM, EPSS TG-No-43
Soil / Sludge /
Sedimentmg/L - 4.55 792 7
Determination of Water
soluble chloride FE-1308
EPA,Melbourne publication
139-17Soil/ Sludge/Sediment mg/kg ** 0.6 104 5
Determination of Electrical
conductivity of soilFE-1309
EPA,Melbourne publication
139-6
Soil / Sludge /
SedimentmS/cm 0.1 0.5 87 5
Determination of Mercury
in oilFE-1310
ASTM 1992.Section
11.APHA 3111Oil ng/g ** 2.1 365 7
Determination of Heavy
Metals [Copper (Cu),
Cadmium (Cd), Lead (Pb),
Zinc (Zn) ] in fish
FE-1401MOOPAM 4
th ED. - Section
5.3, 5.4
Fish / Biological
Samplemg/g ** 2.1 497 10
Determination of
Hydrocarbons in fishFE-1402
MOOPAM 4th
ED. - Section
6.8, 6.9
Fish / Biological
Samplemg/g 0.2 2.6 452 10
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10
Determination of Total
Heavy Metals [Copper
(Cu), Cadmium (Cd),
Lead (Pb),Nickel
(Ni),Zinc (Zn), Chromium
(Cr)] in Soil / Sediment
FE-1304*
EPA-139-13
Melbourne.1981,
MOOPAM 4th
edition &
APHA -3111
Soil / Sludge /
Sedimentmg/kg 2.1 585
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page :21 of 23
PARAMETER
TEST
METHOD
SOP-
REFERENCE SAMPLE TYPEREPORTING
UNIT
METHOD
DETECTION
INPUT
TIME
(Hrs)
ORIGINAL
COST
TEST
DURATI
ON
(Days)
REMARK
LIST OF ANALYSIS PARAMETERS WITH REFERENCE METHODS
Dubai Central laboratory
Doc.Ref : SP-FE-0001
Issue Date : 04/04/2016
Rev. No: 6
Organic Matter and ash in
Organic Fertilizers Growing
Media
FE-1701
AOAC, 19th
Edn (2012)
967.04 / 967.05 & British
Standard BS EN 13039 :
2000
Organic Fertilizers % - 0.5 87 5
Water/waste water CFU/100 mL 1/100 ml 0.35 61 3
Drinking water CFU/100 mL 1/100 ml 0.35 49 3
Water/waste water CFU/ mL 1/1ml 0.35 61 4
Drinking water CFU/ mL 1/1ml 0.35 49
Water/waste water CFU/100 mL 1 /100ml 104
Drinking water CFU/250 mL 1 /250ml 84
Detection and Enumeration
of Legionella species FE-1605*
BSI BS 6068 section 4.12
:1998Water /Waste water CFU/L 1 /L 2.3 400 16
Detection and Enumeration
of Coliforms and E.ColiFE-1601* APHA - 9223 B
APHA - 9215 A & BFE-1603*Enumeration of Aerobic
Colony Count
Detection and Enumeration
of Pseudomonas aeruginosa FE-1604*
BSI BS 6068 section 4.7
:19890.6 5
Water/waste water CFU/100 mL 1 /100ml 104
Drinking water CFU/250 mL 1 /250ml 84
Detection and Enumeration
of Sulphite reducing
clostridia in drinking water
FE-1609*BSEN 26461 Part 2 1993
water quality detectionDrinking water CFU/250 mL 1 /250ml 0.6 84 5
Detection & Enumeration of
Legionella spp. & L
pneumophila in water and
wastewater by
(RT-PCR)
FE-1610
Detection & Enumeration of
Legionella spp. & L
pneumophila (BIO-RAD
manual)
Water /Waste water UG/L 1 2.8 487 3
1Hr 174
Determination of Mercury
in oilFE-1310
ASTM 1992.Section
11.APHA 3111Oil ng/g ** 2.1 365 7
Determination of Heavy
Metals [Copper (Cu),
Cadmium (Cd), Lead (Pb),
Zinc (Zn) ] in fish
FE-1401MOOPAM 4
th ED. - Section
5.3, 5.4
Fish / Biological
Samplemg/g ** 2.1 497 10
Determination of
Hydrocarbons in fishFE-1402
MOOPAM 4th
ED. - Section
6.8, 6.9
Fish / Biological
Samplemg/g 0.2 2.6 452 10
Organic Matter and ash in
Organic Fertilizers Growing
Media
FE-1701
AOAC, 19th
Edn (2012)
967.04 / 967.05 & British
Standard BS EN 13039 :
2000
Organic Fertilizers % - 0.5 87 5
Detection and Enumuration
of Faecal StreptococciFE-1606*
BSI BS 6068 section 4.4
:19890.6 5
Sampling NA NA NA NA NA NA
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PARAMETER
TEST
METHOD
SOP-
REFERENCE SAMPLE TYPEREPORTING
UNIT
METHOD
DETECTION
INPUT
TIME
(Hrs)
ORIGINAL
COST
TEST
DURATI
ON
(Days)
REMARK
LIST OF ANALYSIS PARAMETERS WITH REFERENCE METHODS
Dubai Central laboratory
Doc.Ref : SP-FE-0001
Issue Date : 04/04/2016
Rev. No: 6
Drinking water 0.35 49 3
Water/waste water/ 0.35 61 3
Drinking water 0.35 49
Water/waste water 0.35 61 4
Water/waste water CFU/100 mL 1 /100ml 0.6 104
Drinking water CFU/250 mL 1 /250ml 0.6 84
Detection and Enumeration
of Legionella species FE-1605*
BSI BS 6068 section 4.12
:1998Water /Waste water CFU/L 1 /L 2.3 400 16
Detection and Enumeration
of Coliforms and E.ColiCFU/100 mL 1/100 mlFE-1601* APHA - 9223 B
Enumeration of Aerobic
Colony Count FE-1603* APHA - 9215 A & B CFU/ mL 1/1ml
Detection and Enumeration
of Pseudomonas aeruginosa FE-1604*
BSI BS 6068 section 4.7
:19895
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Water/waste water CFU/100 mL 1 /100ml 104
Drinking water CFU/250 mL 1 /250ml 84
Detection and Enumeration
of Sulphite reducing
clostridia in drinking water
FE-1609*BSEN 26461 Part 2 1993
water quality detectionDrinking water CFU/250 mL 1 /250ml 0.6 84 5
Detection & Enumeration of
Legionella spp. & L
pneumophila in water and
wastewater by
(RT-PCR)
FE-1610
Detection & Enumeration of
Legionella spp. & L
pneumophila (BIO-RAD
manual)
Water /Waste water UG/L 1 2.8 500 3
1Hr 174
2Hr 348
3 Hr 522
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NA NA NA NA
** The method detection limit will be calculated during the analysis depending on the
type and weight of sample.
Detection and Enumuration
of Faecal StreptococciFE-1606*
BSI BS 6068 section 4.4
:19890.6 5
Sampling NA NA
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PARAMETER
TEST
METHOD
SOP-
REFERENCE SAMPLE TYPEREPORTING
UNIT
METHOD
DETECTION
INPUT
TIME
(Hrs)
ORIGINAL
COST
TEST
DURATI
ON
(Days)
REMARK
LIST OF ANALYSIS PARAMETERS WITH REFERENCE METHODS
Dubai Central laboratory
Doc.Ref : SP-FE-0001
Issue Date : 04/04/2016
Rev. No: 6
Prepared By:
S. No. Employee No.
1 1447
3 465
2 -
Reviewed By:
S. No. Employee No.
1 1789
TECHICAL APPOVALS
Makeya Abdulrahman AlRais
Name
Dr.Hamed Mohammed Ibrahim
Signature
Lilly George
Dr.Alamuri Gopalakrishnamacharyulu
Name Signature
This procedure was Prepared, Reviewed and Approved for technical content by the following Staff:
1 1789
2 9394
3 16064
4 5426
5 6262
6 13871
S. No. Employee No.
1 9550
2 5426
3 4762
Issue by:SQO
Shaikha Khalfan AlJallaf
Aisha Ibrahim Al Beshr
Name
Farida Mohammed Alamadi
Approved By HOUs( Food Chemical Analysis , Food Microbiology Analysis and Environment Unit)
Signature
Makeya Abdulrahman AlRais
Majida Mohammed AlHarmoodi
Wedad Saeed AbdulRahman
Shaikha Khalfan Al Jallaf
Vaidehi Garimella
Fatma Hassan AlObaidly
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