CIP Report of RO

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    CIP REPORT OF RO PLANT AT EEAP 

    Engro Eximp Agriproducts Utilities Department March 02, 2016 

    Prepared by:  Reviewed by: 

     Adeel Ahmed Muhammad Uzair

     AM Utilities Manager Utilities 

    M.Uzair Sha

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    The Team 

     Adeel Ahmed AM (Lead) Khalid Javed FC

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    Table of Contents 

    Topic  Page•  Team  2 

    •  Why we need CIP  4 

    •  P & ID of RO Plant  5 

    •  CIP Procedure  6 

    •  CIP Activity  7 

    •  Data Comparison 9

    •  Conclusion  9 

    •  Recommendation  10 

    •  Preservation  10 

    •  Preservation Procedure 11

    •   Annexures (A)  12 

    •   Annexures (B)  14 

    •   Annexures (C)  15 

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    Why We Need CIP 

    This report contains the CIP for the RO plant at EEAP. The RO plant

    CIP required when the surface of RO membrane is subjected to

    fouling by foreign materials which may be present in the field water

    such as Hydrates of metal oxides, Calcium precipitates, Organic and

    biological matters. (The term” fouling” here includes the buildup of all

    kinds of layers on the membrane surface, including scaling. 

    CIP of RO plant mostly required on the Basis of following 3 points: 

    •  When the ∆p across the membranes increases 10% 

    •  Permeate flow decreases 10% 

    •  TDS increases abnormally. 

    In normal operation, the membrane in reverse osmosis elements can

    become fouled by suspended solids, microorganisms, and mineral scale.

    These deposits build up during operation and cause loss in water output or

    salt rejection, or both. Regular cleaning of the membrane elements

    minimizes the loss of performance and extends membrane life. 

    Membrane cleaning systems are designed to be used with any RO system

    to clean membranes without removing them from the system. Our cleaning

    systems are provided with hoses and quick disconnect fittings to allow easy

    connection to the membrane system. 

    Background

    -

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    P & ID of RO Plant 

    CIP Procedure 

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    CIP Procedure 

    Genesol 703 (Alkaline cleaning) first bath for Reverse Osmosis plant 

    Genesol 703 quantity required: 10 Kg 

    Total Time Required  02 Hrs 

    Soaking time:  15 min 

    Recirculation time:  15 min 

    Genesol 703 (Alkaline cleaning) second bath for Reverse Osmosis

    plant 

    Genesol 703 quantity required: 15 Kg 

    Total Time Required  04 Hrs 

    Soaking time:  30 min 

    Recirculation time:  15 min 

    Genesol 30 (Biocide) bath for Reverse Osmosis plant 

    Genesol 30 quantity required: 01 Kg 

    Total Time Required  50 min 

    Soaking time:  20 min 

    Recirculation time:  05 min 

    Genesol 37 (Acid cleaning) bath for Reverse Osmosis plant 

    Genesol 37 quantity required: 30 Kg 

    Total Time Required  05 Hrs 

    Soaking time:  40 min 

    Recirculation time:  30 min 

    Chemicals Used : ListCIP Regime

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    CIP Activity 

    •  RO plant CIP activity started at 0900 hrs. at 1st March

    •  First of we fill the cleaning tank with permeate water. 

    •  Chemical used for CIP are Genesol 703, Genesol 37, Genesol 30 

    •  Take samples for Analysis before the CIP 

    •  Before CIP starts note down all the parameters of RO plant. •   After that starts the first bath with Gensol 703 for 02 hours by adding

    10 kg. 

    •  In this bath 15 minutes are for circulation and fifteen minutes for

    soaking. 

    •   After that starts the 2nd batch by adding 15 kg chemical time required

    for that bath was 4 hrs. 

    •  During this cleaning we frequently note down the ph. of solution, that

    was alkaline solution and PH remains from 10.5 to 12 

    •   After this complete flushing of system take place. 

    •   After that we started the acidic cleaning with Genesol 37. 

    •  Total time required for this activity was 05 hrs. 

    •  30 minutes for circulation and 40 minutes for soaking. 

    •   After that bath with acidic chemical complete flushing was done, 

    •  The RO plant cleaning activity was end at 00:30 hrs.  

    •  Then we take RO back in service and note down its parameters after

    cleaning. 

    •  Took the sample for lab analysis after cleaning.

    Procedure

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    RO Cleaning Tank

     Alkaline Cleaner Acid Cleaner

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    Data Comparison before and after CIP 

    Data and LAB Results

    Conclusion 

    •   After CIP the completion it was observed that the permeate flow is

    increased from 10 GPM to 20 GPM. 

    •  ∆p across the membrane is decreased from 105 psi to 95 psi. 

    •  Permeate TDS are also decreased. 

    Parameters Unit Before CIP After CIP

    Membrane inlet

    Pressure psi 120 120

    ∆p across the

    membrane psi 105 95

    Permeate flow GPM 10 20

    Reject flow GPM 74 64

    TDS mg/L 15.4 11

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    Recommendation 

    It is recommended that when a RO machine is going to shutdown,

    carefully consideration must be paid. And For the membrane storage

    procedure in order to minimize the potential for micro biological growth in

    the system. 

    Preservation 

    Short term shut down of an RO system (24-48 hours) generally does not

    require special membrane storage procedures. The RO should be cycled

    (run in operational mode) for at least 15 minutes every 24-48 hours to

    reduce the potential for bio-growth and stagnation within the system. Some

    systems use a permeate flush during shutdown. This type of cycling will

    allow the system to remain “operationally” ready, and it will allow for a

    slightly longer time between flush cycles.

    For prolonged storage (i.e. several days to several months), the following

    procedures are recommended. These procedures will help protect and

    preserve the elements from bacterial growth. The elements can be left in

    their housings or unloaded and stored separately.

    Typically, one of the following lay-up solutions is used depending upon

    application

    Regulatory limitations, preference, and chemical availability:

    1. 0.5 to 1.0% sodium bisulfite or Biocide. 

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    Preservation procedure 

    The following procedure is recommended for RO storage with biocide

    solution.

    •  Prepare the appropriate strength sodium bisulfite or biocide solution

    in the Cleaning tank by diluting with permeates water.

    •  Circulate the solution through the RO system for 15 to 20 minutes.

    •  When the RO system is filled with this solution, close the valves to

    retain the solution in the RO.

    •  Repeat Steps 2 and 3 with fresh solution every 15 days

    •  When the RO system is ready to be returned to service, flush the

    system to drain until the 

    •  Permeate water meets quality specifications, then return the machine

    to service

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    Annexures 

    Annexures (A) 

    Mail Endorsement 

    From: t_Adeel Ahmed [mailto:[email protected]

    Sent: Tuesday, March 01, 2016 11:47 AM 

    To: [email protected] 

    Cc: Mohammad Uzair Shaikh; Muhammad Munir Ahmed; Muhammad Asim Zeb 

    Subject: RO cleaning and preservation. 

    Dear Faisal Farooq 

    As per our telephonic conversation I have sent you the procedure for RO

    cleaning and Ro preservation, kindly review these and reply me if you want to add

    some points or any suggestion .we are using Gensol membrane cleaner chemicals

    for RO CIP. 

    Also please confirm your visit at plant sight tomorrow for ROpreservation activity.

     

    Regards 

    Adeel Ahmed 

    AM utilities. 

    EEAP Muridke. 

    https://mail.google.com/mail/u/0/h/1kybxp84vgumh/?&cs=wh&v=b&[email protected]://mail.google.com/mail/u/0/h/1kybxp84vgumh/?&cs=wh&v=b&[email protected]://mail.google.com/mail/u/0/h/1kybxp84vgumh/?&cs=wh&v=b&[email protected]://mail.google.com/mail/u/0/h/1kybxp84vgumh/?&cs=wh&v=b&[email protected]://mail.google.com/mail/u/0/h/1kybxp84vgumh/?&cs=wh&v=b&[email protected]://mail.google.com/mail/u/0/h/1kybxp84vgumh/?&cs=wh&v=b&[email protected]

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    From: Faisal [mailto:[email protected]

    Sent: Tuesday, March 01, 2016 2:22 PM To: t_Adeel Ahmed 

    Cc: Mohammad Uzair Shaikh; Muhammad Munir Ahmed; Muhammad Asim

    Zeb; [email protected]; 'Sajid Khan' 

    Subject: RE: RO cleaning and preservation. 

    Dear Mr. Adeel 

    Reference to your given below email, please find the attached file for RO CIP and

    RO preservation procedure. Furthermore charges for the visit would be 5000 Rs.

    Kindly confirm us by return email. 

    With Best Regards. 

    Engr. Faisal Farooq 

    Product Engineer 

    Voice +92-301-8461341 

    Email  [email protected]  

    Water Regime Pvt Ltd 

    130/R-3, Johar Town, 

    Lahore, Pakistan 

    Tel: 0092-42-35955584-5 

    Fax: 0092-42-35955586 

    www.waterregime.com 

    https://mail.google.com/mail/u/0/h/1kybxp84vgumh/?&cs=wh&v=b&[email protected]://mail.google.com/mail/u/0/h/1kybxp84vgumh/?&cs=wh&v=b&[email protected]://mail.google.com/mail/u/0/h/1kybxp84vgumh/?&cs=wh&v=b&[email protected]://mail.google.com/mail/u/0/h/1kybxp84vgumh/?&cs=wh&v=b&[email protected]://mail.google.com/mail/u/0/h/1kybxp84vgumh/?&cs=wh&v=b&[email protected]://www.google.com/url?q=http://www.waterregime.com/&sa=D&sntz=1&usg=AFQjCNGjTwmJ-6TZ3uOCp0XH13loZnkchAhttp://www.google.com/url?q=http://www.waterregime.com/&sa=D&sntz=1&usg=AFQjCNGjTwmJ-6TZ3uOCp0XH13loZnkchAhttp://www.google.com/url?q=http://www.waterregime.com/&sa=D&sntz=1&usg=AFQjCNGjTwmJ-6TZ3uOCp0XH13loZnkchAhttps://mail.google.com/mail/u/0/h/1kybxp84vgumh/?&cs=wh&v=b&[email protected]://mail.google.com/mail/u/0/h/1kybxp84vgumh/?&cs=wh&v=b&[email protected]://mail.google.com/mail/u/0/h/1kybxp84vgumh/?&cs=wh&v=b&[email protected]

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    Annexures (B) 

    RO Log Sheet 

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    Annexures (C) 

    LAB Results