Background Report Reference AP-42 Section Number: 10.6.1 ... · 1 - 5, CFR Title 40, Part . 60,...
Transcript of Background Report Reference AP-42 Section Number: 10.6.1 ... · 1 - 5, CFR Title 40, Part . 60,...
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1 I . _ -
Background Report Reference
AP-42 Section Number: 10.6.1
Background Report Section: 4
Reference Number: 65
Title: Results of the May 14,1996 Air Emission Enginering Testing At The Louisiana Pacific OSB Plant In Hayward, Wisconsin
Interpoll Laboratories, Inc.
June 1996
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Interpol1 Laboratories, Inc. 4500 Ball Road N.E.
Circle Pines, Minnesota 55014-1819
TEL: (612) 786-6020 FAX: (612) 786-7854
RESULTS OF THE MAY 14, 1996 AIR EMISSION ENGINEERING TESTING
AT THE LOUISIANA PACIFIC OSB PLANT IN HAYWARD, WISCONSIN
Submitted to:
4 - q
GEOENERGY INTERNATIONAL CORPORATION 1819 South Central, Suite No. 143
Kent, Washington 98032
Attention:
Gary Raemhild .
Reviewed by:
Report Number 6-7684 June 3, 1996 SWsll
- !Manager Stationary Source Testing Department
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.- .
. . . . .... TABLE OF CONTENTS
. . .... . .
. . .........
ABBREVIATIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . iii
1 INTRODUCTION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
2 SUMMARY AND DISCUSSION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
3 RESULTS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13 3.1 Results of Orsat and Moisture Analyses . . . . . . . . . . . . . . . . . . . . . 14
Results of Particulate Loading Determinations . . . . . . . . . . . . . . . . . 18
3.4 Results of Carbon Monoxide Determinations . . . . . . . . . . . . . . . . . 26
3.2 3.3 Results of Oxides of Nitrogen Determinations . . . . . . . . . . . . . . . . . 22
4 RESULTS OF NITRATE ANALYSES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30
APPENDICES: A - Results of Volumetric Flow Rate Determinations 8 - Field Data Sheets C - Interpoll Laboratories Analytical Data D - NOx and CO Datalogger Printouts E - Measurement System Performance Specifications F - Calibration Gas Certification Sheets
C - Sampling Train Calibration Data
H - Line 2 Core Dryer E-Tube Outlet Monitoring
. . . .. . . . . II
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AB B R EVI AT1 0 N S
ACFM cc (ml) DSCFibI DSML DEC-F ( O F )
DIA. FP FT/SEC
C PM CUACF CWDSCF g/dscm HP H RS IN. IN.HC. IN.WC. LB LB/DSCF LB/HR LB/1 O'BTU LB/MMBTU LTPD MW mg/Nm3 ug/Nm3 microns (urn) MIN. ng ohm-cm PM PPH PPM
0 0
PPmC ppmd PPm,w PPt PSI SQ.Ff. TP D ug viv w/w <
actual cubic feet per minute cubic centimeter (milliliter) dry standard cubic foot of dry gas per minute dry standard milliliter degrees Fahrenheit diameter finished product for plant feet per second gram gallons per minute grains per actual cubic foot grains per dry standard cubic foot grams per dry standard cubic meter horsepower hours inches inches of mercury inches of water pound pounds per dry standard cubic foot pounds per hour pounds per million British Thermal Units heat input pounds per million British Thermal Units heat input long tons per day megawatt milligrams per dry standard cubic meter micrograms per dry standard cubic meter micrometer minutes nanograms ohm-centimeter particulate matter pounds per hour parts per million parts per million carbon parts per million, dry parts per million, wet parts per trillion pounds per square inch square feet tons per day micrograms percent by volume percent by weight
(when following a cumber)
Standard conditions are defined as 68'F (20°C) and 29.92 IN. of mercury pressure.
g:kmd0rm\mircbbbm.h
... 1 1 1
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1 INTRODUCTION
. , . . . . > :
:.: .::.
On May 14, 1996, Interpoll Laboratories conducted Air Emission Engineering Tests
at the Louisiana Pacific OSB Plant in Hayward, Wisconsin on the following sources:
Source Parameters Line 2 E-Tube Outlet
Line 2 Surface Dryer E-Tube Inlet
Line 2 Core Dryer €-Tube Inlet
PM, NO,,CO
PM,NO,,CO
PM, N ox, CO
On-site testing was performed by Bob Aschenbach, Ed Juers, Scott Fjelsta, Jamie Bainville,
Steve Kelker, Jim Lorenz, Mark Peterson, and Ken Nuessmeier. Coordination between testing
activities and plant operation was provided by Gary Raemhild of Ceoenergy. The tests were
not witnessed by a member of the Wisconsin Department of Natural Resources.
Particulate determinations were performed in accordance with €PA Methods 1 - 5,
CFR Title 40, Part 60, Appendix A (revised July 1, 1995). Preliminary volumetric flow rate
determinations were used to select the appropriate nozzle diameter for isokinetic sample
withdrawal. Interpoll Labs Model 3 M5 sampling trains which meet or exceed specifications
in the above-cited reference were used to extract particulate samples by means of heated
stainless steel probe. Wet catch samples were collected in the back half of the Method 5
sampling train at the stack test site and analyzed as per Wisconsin DNR protocol.
Oxides of nitrogen, carbon monoxide, oxygen, and carbon dioxide concentrations
were determined in accordance with Methods 7E, 10, and 3A (Ibid). A slip stream of sample
gas was withdrawn from the exhaust gas stream using a heated stainless steel probe equipped
with a filter to remove interfering particulate material. The particulatefree gas was transport-
ed to the analyzers by means of a heat-traced probe and filter assembly. After passing
through the filter, the gas passed through a chilled condenser-type moisture removal system.
The particulatefree dry gas was then transported to the analyzers with the excess exhausted
to the atmosphere through a calibrated orifice which was used to ensure that the flow from
the stack exceeds the requirements of the analyzers. A three-way valve on the probe was
used to introduce standard gas for the "system bias check".
1
. .
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. . :.. .. . ..
-
The analog response of each analyzer was recorded with a computer datalogger and
backed up with a strip chart recorder. The NO,, CO, 0, and CO, analyzers were calibrated
with National Specialty Gases and Air Products and Chemicals standard gases. The
instrument was calibrated before and after each run as per EPA Method 7E, 10, and 3A. The
sample probe was moved through a three-point traverse (1/6, 3/6, 516 of the stack diameter)
to measure oxides of nitrogen and carbon monoxide concentrations.
Integrated flue gas samples were extracted simultaneously with particulate sampling
using a specially designed gas sampling system. Integrated flue gas samples were collected
in 44-liter Tedlar bags. Prior to sampling, the Tedlar bags are leak checked at 15 IN.HC.
vacuum with an in-line rotameter. Bags with any detectable inleakage are discarded. After
sampling was complete, the bags were sealed and returned to the laboratory for Orsat
analysis.
A summary and discussion of all of the important results of this compliance test i s
given in the following section. More detailed results of the various samplings are presented
in Section 3, together with pertinent sampling parameters. Supplemental information such
as field data sheets, laboratory results, procedures and calculation equations are presented
in the appendices.
2
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2 SUMMARY AND DISCUSSION
The results of the air emission compliance tests are presented in Tables 1 - 5. An
overview of the results is presented in the table below:
PARAMETER MEASURED LINE 2 E-TUBE OUTLET Particulate
DRY -+ WETCATCH 0.023 . . . . . . . . . . . . . . . . . . . . . (CWDSCF)
11.7 . . . . . . . . . . . . . . . . . . . . . . . (LB/HR)
(CWDSCR 0.0058 . . . . . . . . . . . . . . . . . . . . . . . 3.0 (LBIHR)
. . . . . . . . . . . . . . . . . . . . . . . (LB/HR)
. . . . . . . . . . . . . . . . . . . . . . . (ppm,d)
. . . . . . . . . . . . . . . . . . . . . . . (LB/HR)
DRY CATCH ONLY . . . . . . . . . . . . . . . . . . . . .
Oxides of Nitrogen
Carbon Monoxide
. . . . . . . . . . . . . . . . . . . . . . . (ppm,d) a. 1
io98
3.5
290
LINE 2 SURFACE DRYER E-TUBE INLET Particulate
DRY + WETCATCH . . . . . . . . . . . . . . . . . . . . . (GWDSCF) . . . . . . . . . . . . . . . . . . . . . . . (LB/HR) DRY CATCH ONLY . . . . . . . . . . . . . . . . . . . . . (CWDSCF) . . . . . . . . . . . . . . . . . . . . . . . (LB/HR)
. . . . . . . . . . . . . . . . . . . . . . . (ppm,d)
. . . . . . . . . . . . . . . . . . . . . . . (LB/HR)
Oxides of Nitrogen
Carbon Monoxide . . . . . . . . . . . . . . . . . . . . . . . !ppm,d) . . . . . . . . . . . . . . . . . . . . . . . (LB/HR)
LINE 2 CORE DRYER E-TUBE INLET Particulate
DRY + WETCATCH . . . . . . . . . . . . . . . . . . . . . (CWDSCF) . . . . . . . . . . . . . . . . . . . . . . . (LB/HR) DRY CATCH ONLY . . . . . . . . . . . . . . . . . . . . . (CWDSCF) . . . . . . . . . . . . . . . . . . . . . . . (LB/HK)
Oxides of Nitrogen
Carbon (Monoxide
. . . . . . . . . . . . . . . . . . . . . . . (ppm,d)
(ppm,d)
. . . . . . . . . . . . . . . . . . . . . . . (LB/HR)
. . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . . . . (LBIHR)
0.428 87.6
0.305 62.4
24.9 4.3
1016 106
0.344 78.6
0.263 60.2
20.7 4.0
a34 97
3
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. :..
.. No difficulties were encountered in the field or in the laboratory evaluation of the
samples. O n the basis of these facts and a complete review of the data and results, it is our
opinion that the concentrations and emission rates reported herein are accurate and closely
reflect the actual values which existed at the time the tests were performed.
.. .
. . 4
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e o O S . r Y VI V I +
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L I
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L a o v = + I
W O T W O +I s 2 e _ r + I o s
V I S - *@a. s c u VI 0 - o e =+I.-
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CCCP
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l. u m m m . e m N 4 - 0 0 In
r t N . d w KJN
m w m m 0 0 0 N w r - u r t r o m m m o l . .
m o KJ m 0 0 0 0 p1- N
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4 w I- u w m m . . ln K J N N dl. 0 0 w
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-
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m
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.- /_.
Table 4. Summary of the Results of the May 14, 1996 Oxides of Nitrogen Determina-
tions at the Louisiana Pacific Plant in Hayward, Wisconsin.
Concentration Emission Rate
Date Time bDm,d) (LB/HR) (Line 2 E-Tube Outlet)
5-1 4-96 1200-1346 9.2 4.0 5-14-96 1500-1641 8.5 3.7 5-1 4-96 181 5-1 920 6.5 2.8
Avg 8.1 3.5
(Line 2 Surface Dryer E-Tube Inlet) 5-14-96 1200-1346 25.9 4.5 5-14-96 1500-1641 26.4 4.4 5-1 4-96 181 5-1920 22.4 3.8
Avg 24.9 4.3
(Line 2 Core Dryer E-Tube Inlet) 5-1 4-96 1200-1 346 22.5 4.3 5-14-96 1500-1 641 18.8 3.6 5-1 4-96 1815-1920 20.9 4.0
Avg 20.7 4.0
11
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..
. ..
. .. . . . .
.. _...
..
Table 5. Summary of the Results of the May 14, 1996 Carbon Monoxide Determina-
tions at the Louisiana Pacific Plant in Hayward, Wisconsin.
Concentration Emission Rate
Date Time (DDm,d (LBIHR) (Line 2 E-Tube Outlet)
5-14-96 1200-1 346 1014 268 5-14-96 1500-1 641 973 256 5-14-96 1815-1 920 1308 346
Avg 1098 290
(Line 2 Surface Dryer E-Tube Inlet) 5-1 4-96 1200-1346 1042 110 5-1 4-96 1 500-1 641 928 95 5-14-96 181 5-1 920 1079 112
Avg 1016 106
(Line 2 Core Dryer €-Tube Inlet) 5- 1 4-96 1200-1346 788 92 5-14-96 1500-1641 820 96 5- 1 4-96 181 5-1 920 894 103
Avg 834 97
12
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3 RESULTS
. . . ..
. . . . ... . ..
The results of all field and laboratory evaluations are presented in this section. Cas
composition results (Orsat and moisture) are presented first followed by the computer
printout of the gas composition, particulate, oxides of nitrogen, carbon monoxide determinat-
ions . Preliminary measurements including test port locations are given in the appendices.
The results have been calculated on a personal computer using programs written in
Extended BASIC specifically for source testing calculations. €PA-published equations have
been used as the basis of the calculation techniques in these program. Emission rates have
been calculated using the product of the concentration times flow method.
13
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3.1 Results of Orsat and Moisture Analvses .,- . .
. . . , .
. ... . . . .
14
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. . . . . . . . . : .: :..
. . . . . . . .
I n t e r p o l 1 Labs R e p o r t No. 6-7684 G e o e n e r g y - LP
Hayward , WI
T e s t N o . 1 L i n e 2 E-Tube O u t l e t
R e s u l t s o f O r s a t S M o i s t u r e Ana lyses - - - - -Me thods 3 & 4(%v/v)
D a t e o f r u n
D r y b a s i s ( o r s a t )
Run 1 Run 2 Run 3 05-14-96 05-14-96 05-14-96
c a r b o n d i o x i d e . ........... 4.00
o x y g e n .................... 16.50
n i t r o g e n . . . . . . . . . . . . . . . . . . 79.50
Wet b a s i s ( o r s a t )
c a r b o n d i o x i d e . . . . . . . . . . . . 2.95
o x y g e n .................... 12.18
n i t r o g e n . . . . . . . . . . . . . . . . . . 58.10
w a t e r v a p o r . .............. 26.17
D r y m o l e c u l a r w e i g h t ........ 29.30
Wet m o l e c u l a r w e i g h t . . . . . . . . 26.34
S p e c i f i c g r a v i t y . . . . ........ 0.910
W a t e r mass f l o w . . . . . . (LB/HR) 60286
F O 1.100
3.80 3.70
16.50 16.70
19.70 79.60
2.79 2.77
12.12 12.49
58.54 59.54
26.55 25.20
29.21 29.26
26.28 26.42
0.908 0.913
61218 57391
1.158 1.135
15
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I n t e r p o l l Labs R e p o r t No. 6-7684 G e o e n e r g y - L P
Hayward , W I
T e s t No. 3 L i n e 2 S u r f a c e D r y e r E-Tube I n l e t
R e s u l t s o f O r s a t
D a t e o f r u n
Dry b a s i s ( o r s a t
c a r b o n d i o x i d e . . . . . . . . . . . o x y g e n .................... n i t r o g e n . . . . . . . . . . . . . . . . . .
Wet b a s i s ( o r s a t )
!L. --
. .
. . . . . . . .
S M o i s t u r e Ana lyses - - - - -Me thods 3 S 4 ( t v / v )
c a r b o n d i o x i d e . ........... o x y g e n . . . . . . . . . . . . . . . . . . . . n i t r o g e n . . . . . . . . . . . . . . . . . . w a t e r v a p o r . . . . . . . . . . . . . . .
D r y m o l e c u l a r w e i g h t . . ...... Wet m o l e c u l a r w e i g h t . . . . . . . . S p e c i f i c g r a v i t y . . . . . . . . . . . . W a t e r mass f l o w . . . . . . (LB/HR)
Run 1 Run 2 Run 3 05-14-96 05-14-96 05-14-96
4.70
15.70
79.60
3.37
11.24
57.01
28.39
29.38
26.15
0.903
26993
5.00
15.40
79.60
3.48
10.73
55.45
30.34
29.42
25.95
0.896
28706
5.40
15.00
79.60
3.80
10.57
56.07
29.57
29.46
26.07
0.901
28050
FO 1.106 1.100
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. . ~ . . .
. . . . .~ . :.
.~ . . . . . . . . . ~.
. . . . . . .
I n t e r p o l l Labs R e p o r t No. 6-7684 G e o e n e r g y - L P
Hayward , W I
T e s t No. 5 L i n e 2 C o r e D r y e r € -Tube I n l e t
R e s u l t s o f O r s a t B M o i s t u r e Ana lyses - - - - -Me thods 3 S 4 ( Z v / v )
D a t e o f r u n Run 1 Run 2 Run 3
05-14-96 05-14-96 05-14-96
D r y b a s i s ( o r s a t )
c a r b o n d i o x i d e . . . . . . . . . . . . 4.20 4.30 4.40
o x y g e n 16.20 16.00 15.90
n i t r o g e n . . . . . . . . . . . . . . . . . . 19.60 7 9 . 7 0 79.70
....................
Wet b a s i s ( o r s a t )
c a r b o n d i o x i d e . ........... 3.06 3.10 3.19
o x y g e n .................... 11.80 11.52 11.55
n i t r o g e n . . . . . . . . . . . . . . . . . . 57.97 57.40 57.87
w a t e r v a p o r . .............. 27.18 27 * 98 27.39
D r y m o l e c u l a r w e i g h t . . ...... 29.32 29.33 29.34
Wet m o l e c u l a r w e i g h t ........ 26.24 26.16 26.23
S p e c i f i c g r a v i t y . . . . . . . . . . . . 0.907 0.904 0.906
W a t e r mass f l o w . . . . . . (LB /HR) 28129 29152 27920
FO
. .
17 .~
1.119 1.140 1.136 I
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. . . ::: ::.:
3.2 Results of Particulate Loading Determinations
18
1
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. . . . . . . .
. . . ~ . . . .
I n t e r p o l l Labs R e p o r t No. 6 - 7 6 8 4 G e o e n e r g y - LP
Hayward , W I
T e s t No. 1 L i n e 2 E-Tube O u t l e t
R e s u l t s o f P a r t i c u l a t e L o a d i n g D e t e r m i n a t i o n s - - - - - - - M e t h o d 5
D a t e o f r u n Run 1
0 5 - 1 4 - 9 6
T i m e run s t a r t / e n d . , ... (HRS) 1 2 0 0 / 1 3 5 0
S t a t i c p r e s s u r e . . . . . . (1N.WC) C r o s s s e c t i o n a l a r e a ( S Q . F T ) P i t o t t u b e c o e f f i c i e n t . . . . . . W a t e r i n sample gas
c o n d e n s e r . . . . . . . . . . . . . (ML) i r n p i n g e r s . . . . . . . . . . (GRAMS) d e s i c c a n t . . . . . . . . . . (GRAMS) t o t a l . . . . . . . . . . . . . . (GRAMS)
T o t a l p a r t i c u l a t e m a t e r i a l . . . . . . . . . . . . c o l l e c t e d ( g r a m s )
G a s m e t e r c o e f f i c i e n t . . . . . . . B a r o m e t r i c p r e s s u r e . . (1N.HG) Avg. o r i f . p r e s . d r o p . . ( I N . W C ) Avg. gas m e t e r temp. . (DEF-F)
Volume t h r o u g h g a s m e t e r . . . . a t m e t e r c o n d i t i o n s . . . ( C F ) s t a n d a r d c o n d i t i o n s . ( D S C F )
T o t a l s a m p l i n g t i m e . . . . ( M I N ) N o z z l e d i a m e t e r . . . . . . . . . ( I N ) A v g . s t a c k gas t e m p . . (DEG-F)
V o l u m e t r i c f l o w r a t e . . . . . . . . a c t u a l . . . . . . . . . . . . . . ( A C F M ) d r y s t a n d a r d . . . . . . . ( O S C F M )
I s o k i n e t i c v a r i a t i o n . . . . . ( % )
P a r t i c u l a t e c o n c e n t r a t i o n . . . a c t u a l . . . . . . . . . . . . ( G R / A C F ) d r y s t a n d a r d . . . . . ( G R / D S C F )
P a r t i c l e mass r a t e . . . ( L B / H R )
- 1 . 5 0 2 2 . 8 7
. 8 4 0
0.0 2 7 2 . 0
1 0 . 0 2 8 2 . 0
0.0601
1 . 0 0 0 5 2 8 . 9 3
0 . 8 7 6 8 . 8
3 8 . 7 7 3 7 . 5 2
7 2 . 0 0 * 1 8 9
1 6 2
1 0 0 5 0 5 6 0 6 4 2
1 0 0 . 9
0 . 0 1 4 9 1 0 . 0 2 4 7 2
2 . 8 4 8
Run 2 0 5 - 1 4 - 9 6
1500/1652
- 1 . 5 0
. 8 4 0 2 2 . a 7
0 .0 2 7 5 . 0
1 2 . 0 2 8 7 . 0
0 . 0 5 1 9
1 . 0 0 0 5 2 8 . 9 3
0 . 8 8 7 3 . 1
3 9 . 0 0 3 7 , 4 4
7 2 . 0 0 . 1 8 9
1 6 3
1 0 0 7 6 9 6 0 3 7 7
101.1
0 . 0 1 2 8 1 0 . 0 2 1 3 9
1 1 . 0 7 1
Run 3 0 5 - 1 4 - 9 6
1 8 1 5 / 1 9 3 8
- 1 . 5 0 2 2 . 8 7
. 8 4 0
0 . 0 2 4 7 . 0
13 .-0 2 6 0 . 0
0 . 0 5 1 3
1 . 0 0 0 5 2 8 . 9 3
0 . 8 2 7 0 . 8
37 .76 3 6 . 4 0
7 2 . 0 0 . 1 8 9
1 6 5
9 9 8 4 6 6 0 7 5 3
9 7 . 7
0 . 0 1 3 2 3 0 . 0 2 1 7 5
1 1 . 3 2 5
19
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T e s t L i n e
Re su
D a t e
T i me
-. .... j j I
; ..
..
........
No. 3 2 S u r f a c e D r y e r E-Tube
t s o f P a r t i c u l a t e L o a d
o f r u n
run s t a r t / e n d . . . . . ( H R S )
S t a t i c p r e s s u r e . . . . . . ( I N . W C ) C r o s s s e c t i o n a l a r e a ( S Q . F T ) P i t o t t u b e c o e f f i c i e n t . . .... W a t e r i n samp le g a s
c o n d e n s e r . ............ ( M L ) i m p i n g e r s . . . . . . . . . . (GRAMS) d e s i c c a n t . . . . . . . . . . (GRAMS) t o t a l . . . . . . . . . . . . . . (GRAMS)
T o t a l p a r t i c u l a t e m a t e r i a l . . . . . . . . . . . . c o l l e c t e d ( g r a m s )
Gas m e t e r c o e f f i c i e n t . . . . . . . B a r o m e t r i c p r e s s u r e . . ( I N . H G ) Avg. o r i f . p r e s . d r o p . . ( I N . W C ) Avg. g a s m e t e r temp. . (DEF-F)
Volume t h r o u g h gas m e t e r . . . . a t m e t e r c o n d i t i o n s ... ( C F ) s t a n d a r d c o n d i t i o n s . ( D S C F )
T o t a l s a m p l i n g t i m e . . . . ( M I N ) N o z z l e d i a m e t e r . . . . . . . . . ( I N ) A v g . s t a c k gas t e m p . . D E G - F )
V o l u m e t r i c f l o w r a t e . a c t u a l . . . . . . . . . . . . . d r y s t a n d a r d . . . . . . .
I s o k i n e t i c v a r i a t i o n
. . . . . . (ACFM) DSCFM)
. . . ( % )
P a r t i c u l a t e c o n c e n t r a t i o n . . . a c t u a l . . . . . . . . . . . . (GR/ACF) d r y s t a n d a r d . . . . . ( G R / D S C F )
P a r t i c l e mass r a t e . . . (LE /HR)
I n t e r p o l 1 L a b s R e p o r t No. 6-7684 G e o e n e r g y - L P
Hayward , W I
I n l e t
ng D e t e r m i n a t i o n s - - - - - - - M e t h o d 5
Run 1 05-14-96
l200/ 135 1
-9.00 9.62 .840
0.0 284.0 18.0
302.0
0.9618
0.9935 28.93
0 . 8 0 59.7
36.75 35.93
72.00 .190 245
47903 24279
100.5
0.20928 0.41309
85.966
Run 2 05-14-96
1500/ 1652
-9.00 9.62 .840
0.0 313 .O 16.0
329.0
0.9263
0.9935 28.93 0.78 55.6
36.15 35.62
72.00 .190 243
47567 23498
102.9
0.19815 0.40128
80.821
Run 3 05-14-96
1815/1935
-9.00 9.62 . E40
0 .,o 296.0 15 .b
311.0
1.0660
0.9935 28.93 0.75 58.1
35.63 34.93
72.00 .190 245
47772 23823
99.6
0.23471 0.47085
96.146
. . . 20
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....
. .
I n t e r p o l 1 Labs R e p o r t No. 6-7684 G e o e n e r g y - L P
Hayward , WI
T e s t No. 5 L i n e 2 C o r e D r y e r € -Tube I n l e t
R e s u l t s o f P a r t i c u l a t e L o a d i n g D e t e r m i n a t i o n s - - - - - - - M e t h o d 5
D a t e o f r u n
T ime r u n s t a r t / e n d . . . . . ( H R S )
S t a t i c p r e s s u r e . . . . . . ( 1 N . W C ) C r o s s s e c t i o n a l a r e a ( S Q . F T ) P i t o t t u b e c o e f f i c i e n t . . . . . . W a t e r i n samp le g a s
c o n d e n s e r . . . . . . . . . . . . . ( M L ) i m p i n g e r s . . . . . . . . . . (GRAMS) d e s i c c a n t . . . . . . . . . . (GRAMS) t o t a l . . . . . . . . . . . . . . (GRAMS)
T o t a l p a r t i c u l a t e m a t e r i a l . . . . ......... c o l l e c t e d ( g r a m s )
Gas m e t e r c o e f f i c i e n t . . . . . . . B a r o m e t r i c p r e s s u r e . . ( I N . H G ) Avg. o r i f . p r e s . d r o p . . ( IN .WC) Avg. gas m e t e r temp. . (DEF-F)
Volume t h r o u g h g a s m e t e r . . . . a t m e t e r c o n d i t i o n s . . . ( C F ) s t a n d a r d c o n d i t i o n s . ( D S C F )
T o t a l s a m p l i n g t i m e . . . . ( M I N ) N o z z l e d i a m e t e r . . . . . . . . . ( I N ) A v g . s t a c k gas temp . . ( D E G - F )
V o l u m e t r i c f l o w r a t e . . . . . . . . a c t u a l . . . . . . . . . . . . . . ( A C F M ) d r y s t a n d a r d . . . . . . . (DSCFM)
I s o k i n e t i c v a r i a t i o n . . . . . ( % )
P a r t i c u l a t e c o n c e n t r a t i o n . . . a c t u a l . . . . . . . . . . . . (GR/ACF) d r y s t a n d a r d . . . . . (GR/DSCF)
P a r t i c l e mass r a t e . . . ( L B / H R )
Run 1 05-14-96
1200/ 1352
-11.00 9.62 .840
0.0 297.0 21 .o
318.0
0.8860.
1.0019 28.93 1.01 62.5
40.95 40.17
72.00 .192 235
51669 26870
99.4
0.17689 0.34029
78.373
Run 2 05-14-96
1500 / 165 3
-11.00 9.62 .E40
0.0 307.0 25.0
332.0
0.8868
1 :0019 28.93 1.01 62.9
41.11 40.30
72.00 .192 239
52313 26756
100.2
0.17359 0.33953
77.867
Run 3 05-14-96
1815/1931
-11.00 9.62 .840
0.0 307;O
8.0 315..0
0.8987
1.0019 28.93 0.97 62.0
40.10 39.37
72.00 .192 2 40
51226 26388
99.2
0.18135 0.35218
79.657
2 1
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3.3 Results of Oxides of Nitrogen Determinations
. . . . . ~. . . . .
. . . .::.
22
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Interpoll Labs Report No. 6-7684
Ceoenergy / Louisiana Pacific Corporation
Hayward, Wisconsin
Test No. 2
Line 2 E-Tube Outlet
Results of Oxides of Nitrogen Determinations Method7E
Date of run
Time run stadend (HRS)
Total sampling time (MINI
Run 1 Run 2 Run 3
5-14-96 5-14-96 5-14-96
1200-1 346 1500-1 641 181 5-1 920
60 60 60
Moisture content (%VM 26.2 26.6 25.2
Oxygen content (%VN) 16.5 16.5 16.3
Volumetric flow rate (DSCFM) 60642 60377 60753
NO, concentration @pm,d) 9.2 8.5 6.5
NO, emission rate (LB/HR) 4.0 3.7 2.8 . . . . .
. . . . . . ~.
23 I
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. . .:. ..::
-
. . . . . . .
. . . .. . ... . . .
Interpoll Labs Report No. 6-7684
Ceoenergy / Louisiana Pacific Corporation
Hayward, Wisconsin
Test No. 4
Line 2 Surface Dryer €-Tube Inlet
Results of Oxides of Nitrogen Determinations Method7E
Date of run
Time run stadend (HRS)
Total sampling time (MIN)
Moisture content (%VN)
Oxygen content (%VN)
Volumetric flow rate (DSCFM)
NO, concentration (ppm,d)
NO, emission rate (LBIHR)
Run 1
5-1 4 9 6
1200-1 346
60
28.4
16.1
24279
25.9
4.5
Run 2
5-1 4-96
1500-1 641
60
30.3
16.2
23498
26.4
4.4
Run 3
5-1 4-96
I 815-1920
60
29.6
15.9
23823
22.4
3.8
24
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..
Interpoll Labs Report No. 6-7684
Ceoenergy / Louisiana Pacific Corporation
Hayward, Wisconsin
Test No. 6
Line 2 Core Dryer €-Tube Inlet
Results of Oxides of Nitrogen Determinations Method7E
Date of run
Time run stadend (HRS)
Total sampling time (MINI
Moisture content (%VM
Oxygen content (%VM
Volumetric flow rate (DSCFM)
NO, concentration (ppm,d)
NO, emission rate (LBIHR)
Run 1
5-14-96
1200-1346
60
27.2
15.0
26870
22.5
4.3
Run 2
5-1 4-96
1500-1 641
60
28.0
15.3
26756
18.8
3.6
Run 3
5-1 4-96
I81 5-1 920
60
27.4
14.5
26388
20.9
4.0 . . . . . .
.. ..::
25
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3.4 Results of Carbon Monoxide Determinations
. .. . . . . .
. , . . . . . . . .
26
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interpoll Labs Report No. 6-7684
Ceoenergy / Louisiana Pacific Corporation
Hayward, Wisconsin
Test No. 2
Line 2 E-Tube Outlet
Results of Carbon Monoxide Determinations Method1 0
Date of run
Run 1 Run 2 Run 3
5-14-96 5-1 4-96 5-14-96
Time run stadend (HRS) 1200-1346 1500-1 641 1815-1920
Total sampling time (MIN) 60 60 60
Moisture content (%VN) 26.2 26.6 25.2
Oxygen content (%VN) 16.5 16.5 16.3
Volumetric flow rate (DSCFM) 60642 60377 60753
CO concentration (ppm,d) 1014 973 1308
CO emission rate (LB/HR) 268 256 346
27
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Interpol1 Labs Report No. 6-7684
Ceoenergy / Louisiana Pacific Corporation
Hayward, Wisconsin
Test No. 4
Line 2 Surface Dryer €-Tube Inlet
Results of Carbon Monoxide Determinations Method1 0
Date of run
Run 1 Run 2 Run 3
5-1 4-96 5-14-96 5-14-96
Time run stadend (HRS) 1200-1 346 1700-16.11 181 5-1920
Total sampling time (MIN) 60 60 60
Moisture content (%V/V) 28.4 30.3 29.6
Oxygen content ( % V N 16.1 16.2 15.9
Volumetric flow rate (DSCFM) 24279 23498 23823
CO concentration (ppm,d) 1042 928 1079
CO emission rate (LB/HR) 110 95 112
28
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!
: :..
. . ... . . , . . . . .
.~ . . . .
. . : . . . .
Interpol1 Labs Report No. 6-7684
Geoenergy / Louisiana Pacific Corporation
Hayward, Wisconsin
Test No. 6
Line 2 Core Dryer E-Tube Inlet
Results of Carbon Monoxide Determinations Method1 0
Date of run
Time run stadend (HRS)
Total sampling time (MIN)
Moisture content ( % V M
Oxygen content ( % V M
Volumetric flow rate (DSCFM)
CO concentration (ppm,d)
CO emission rate (LB/HR)
Run 1
5-14-96
1200-1 346
60
27.2
15.0
26870
788
92
Run 2
5-1 4-96
1500-1641
60
28.0
15.3
26756
a20
96
Run 3
5-1 4-96
1815-1920
60
27.4
14.5
26388
a94
103 -
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:-: ::.:
-.
4 RESULTS OF NITRATE ANALYSES
' ,... -
30
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. -. I
.. .. ~I . . .
INTERPOLL WBORATORIES, INC. (612)786-6020
Louisiana Pacific, Hayward Laboratory Log No. 7684
Results of Nitmte Analysis
Sample Nitrate" Loe No. Identification Samule Tvue (rng/L)
j / -\, 7684-22 Recycle Water 3300
7684-23 Recycle Water 3200
Respectfully submitted,
.. . . .
. . .. . ~ .
David J. Schneider, Manager Chemistry Department
DJSIcg
"Analysis performed by EPA Method 300.0.
31
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's cx .4 I'
C
?s 0 . A .
2
32
:
- P L! c -
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APPENDIX A
RESULTS OF VOLUMETRIC FLOW RATE DETERMINATIONS
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I n t e r p o l 1 Labs R e p o r t No . 6-7684 Geoenergy . LP
Hayward . W I
T e s t No . 3 L i n e 2 S u r f a c e D r y e r E-Tube I n l e t
R e s u l t s o f V o l u m e t r i c F l o w R a t e Determination....... M e t h o d 2
D a t e o f D e t e r m i n a t i o n . ........... Time o f D e t e r m i n a t i o n . . . . . . . ( H R S )
B a r o m e t r i c p r e s s u r e . ..... .(I N . H G )
P i t o t t u b e c o e f f i c i e n t . . .........
Number o f s a m p l i n g p o r t s ......... T o t a l number o f p o i n t s . . . . . . . . . . . Shape o f d u c t .................... S t a c k d i a m e t e r ............... ( I N )
D u c t a r e a . ................ ( S Q . F T )
D i r e c t i o n o f f l o w . . . . . . . . . . . . . . . .
S t a t i c p r e s s u r e . .......... ( 1 N . W C )
Avg . g a s temp ............. ( D E G - F )
M o i s t u r e c o n t e n t .......... ( % V / V )
Avg. . l i n e a r v e l o c i t y ..... (FT/SEC)
Gas d e n s i t y . . . . . . . . . . . . . . (LB/ACF)
M o l e c u l a r w e i g h t . . . . . . (LB/LBMOLE)
Mass f l o w o f gas . . . . . . . . . . (LB/HR)
v o l u m e t r i c f l o w r a t e . . . . . . . . . . . . . a c t u a l . . . . . . . . . . . . . . . . . . . ( A C F M ) d r y s t a n d a r d . . . . . . . . . . . . ( D S C F M )
05-14-96
1130
28.93
.84
1
6
Round
4'2
9.62
HORIZONTAL
-9
242
28.69
84.1
. 04819 29.38
140456
48575 24614
A- 1
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> I
. ,
. .
I n t e r p o l 1 Labs R e p o r t No. 6-7684 G e o e n e r g y - LP
Hayward , W I
T e s t No. 5 L i n e 2 C o r e D r y e r E-Tube I n l e t
Aesu l t s o f V o l u m e t r i c F1 o w Rate D e t e r m i n a t i o n - - - - - - - Method 2
Date o f D e t e r m i n a t i o n . . . . . . . . . . . . T i m e o f D e t e r m i n a t i o n . . . . . . . (HRS)
B a r o m e t r i c p r e s s u r e . . . . . . . ( 1 N . H G )
P i t o t t u b e c o e f f i c i e n t ...........
Number o f s a m p l i n g p o r t s . . . ...... T o t a l number o f p o i n t s . .......... Shape o f d u c t .................... S t a c k d i a m e t e r . . . . . . . . . . . . . . . ( I N )
D u c t a r e a . ................ (SQ.FT)
D i r e c t i o n o f f l o w . . . . . . . . . . . . . . . .
S t a t i c p r e s s u r e . . . . . . . . . . . ( I N . W C )
Avg. gas temp . . . . . . . . . . . . . ( D E G - F )
M o i s t u r e c o n t e n t . . ........ ( % V / V )
Avg. l i n e a r v e l o c i t y . . . . . (FT/SEC)
Gas d e n s i t y . . . . . . . . . . . . . . (LE/ACF)
M o l e c u l a r w e i g h t . . . . . . (LB/LBMOLE)
Mass f l o w o f gas . . . . . . . . . . (LB/HR)
V o l u m e t r i c f l o w r a t e . . . . . . . . . . . . . a c t u a l . . . . . . . . . . . . . . . . . . . ( A C F M ) d r y s t a n d a r d . . . . . . . . . . . . (DSCFMJ
05-14-96
1130
28.93
.84
2
12
Round
4 2.
9.62 ' . .
HORIZONTAL
-11
239
25. a6
90.2
.04866
29.32
152086
52093 27419
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APPENDIX B
FIELD DATA SHEETS
TABLE OF CONTENTS
Line 2 E-Tube Outlet. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
35
. . . . . . . . . . . . . . . . . . . . . . . . . . . . 45
Line 2 Surface Dryer E-Tube Inlet . . . . . . . . . . . . . . . . . . . . . . . . . . . Line 2 Core Dryer E-Tube Inlet
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INTERPOLL LABORATORIES, INC. (61 2) 786-6020
EPA Method 2 Field Data Sheet
ob L.P. Avyhv6 6- srz\a d Source f!Yd z'oIy,;m &*?+?
Dry Bulb O F Wet bulb O F
Test I RunhDate S-lV-% Stack Dimen. 6% 74 IN.
Manometer @-Reg. OExp OEiec. Barometric Pressure 2g.q 3 IN.HC
IN.WC Static Pressure - Operators €.XU,rs T, L9rnA-L Pitot No. 2qv-g c. .gm
Drawing of Test Site
Elevation Cross-section
03 2594-C:\STACK\WP\FORMS\S-392.1
B- 1
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... . . . . . . '/[ f - " L
8-3
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. .
.::. . .. .~ . .
.-
. ~ . , . . . . .
i ' . " I 1 I-:
, . , :
I i i , . .
...
..: . .
. . .. -:: ~.
..
Final Tare
INTERPOLL UEOFL4TORIES, INC. (61 2) 786-6020
Interpoll Laboratories EPA Method 5/17 Sample Log Sheet
Job L ? / d ! 9 Date Y-IY-PL Test 3 Run I Source L, z S<-G- ad-- E .- U o . of traverse points J L
Method 5 Filter holdexS.5. Filter type: S.S. Tk,.+A
Post test: o e cfm at / I IN. HG (vac) ,d
Sample Train Leak Check: Pretest: < 0.02 cfm at 15 lN.HG (vac)
Difference
Particulate Catch Data: Yo. of filters used
3y ! / o
No. of probe wash bottles: Sample recovered by: Condensate Data:
In t
Item
Impinger No. 1
Impinger No. 2
Impinger No. 3
Desiccant
Total
rated Gas Sampling I
Recovery jolvent(s)
d c e t o n e Oother(s)
Bag Pump No. 22 (3 Box No. ry Bag No./
Pretest leak check: 0 . u u cdmin at /b IN.HG Bag Material: 5-laver Aluminized Tedlar Size: - M L
Time s~art: /a LI (HRS) Time end: I 3r/ (ms) Sampling rate: Y o 3 cdmin Operator: SF
S/N of O1 Analyzer used to monitor train outlet: 8 OS239eC.UTAC~WP\FC)RMNb046RR
B-9
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INTERPOLL LABORATORIES, INC. (6 12) 786-6020
Interpoll Laboratories EPA Method 5/17 Sample Log Sheet
Job L7/d- J DateK-/+-%Test 3 Run L , Source L., 1 s - c Q.,- r.rsr.UNo. of traverse points Merhod Filter holder: A> Filter type: KS. =.-LA
Sample Train Leak Check: Pretest: 5 0.02 cfm at 15 IN.HG (vac) S post test: a e cfm at / 7 IN. HG (vac) $f Particulate Catch Data: No. of filters used:
/L
Recovery solvent(s)
wacetone @other(s)
No of probe wash bottles:
Condensate Data: Sample recovered b y Y P
weight (g)
Final Tare Difference
303 2 0 3
/t3 / O c Impinger No. 2
Desiccant / y 5/ /y3< / b
3 2 :*p,*. y*.*.. y.&H *%.... ,..,&MA::WH4x&&&%%*rn
Integrated as Sampling Data:
Bag Pump No. 2.5 f? Box No. a Lr Bag N 0 . L
Pretest leak check: R - O U ccimin at & N.HG 44. L Bag Material: 5-laver .4luminized Tedlar Size: -
Time S ~ M : d (FiRS) Time end: / C J - L W S ) Sampling rare: L/U& cc’min Operator: S F
2 7 SIX of 0: Analyzer used to monitor train outlet:
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.. . . . . . ~....
. .
.- .
... ...
.~
. . ..
I .
I .~ .
. .
. . . . .
. . . . . . .
INTERPOLL LABORATORIES, INC. (6 T 21 786-6020
Interpol1 Laboratories EPA Method 5/17 Sample Log Sheet
Job L?/h/,, Dates-l%/-Fc Test 3 Run -3
Source L-, LS w L 0 ,- r.7-b. z - d No. of traverse points / L
Method 5 Filter holder5.S. Filter me: s.3 7;c --IL Sample Train Leak Check Pretesr: s 0.02 c h at 15 N.HG (vac) ,!B Post test:a= c h at /6 IN. HG (vac) &!? Particulate Catch Data: 30. of filters used Recovery jolvent(s)
/4
No. of probe wash bottles: Sample recovered by: Condensate Data:
JGacetone Oother(s)
Weight (8)
Final Tare Difference
kcL3/
Impinger No. 1
Desiccant / 3 13 .w 4
3 I f .*'.*%<A* ..%-**1K* &,-+y ~ C ~ : ~ ~ ~ S : : ~ ~ ~ ~ ~ ~ ~ ~ ~ . . ~ ~
z-=z Box No. tY Bag No.-? Bag Pump No.
Pretest leak check: d . Qo cc'min at /6 IN.HG Bag Material: Slaver Aluminized Tedlar Size: - 44L
Time stm: / 8 / ( (HRS) Time end: /93r (HRS) cc'min Operator: 3 4 - Sampling rate: -
SIN of 0, Analyzer used to monitor tiain outlet: b+ 05139eG:\STAC~WF"IFC)RMS15-0046RR
8-13
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. . ::. . .. . .
INTERPOLL LABORATORIES, INC. (61 2) 786-6020
€PA Method 2 Field Data Sheet
I ~~~ RunJ .. Stack Dirnen. - Dry Bulb 2 7 4 O F Wet bulb !f> "F
IExp C1Elec. 3 IN.HC
IN.WC
Job Source rc Test Stack Dirnen. IN. Dry Bulb 277 O F Wet bulb !f> "F Manometer 9 Reg. C1Elec. Barometric Pressure IN.HC Static Pressure IN.WC Operators Pitot No.
Drawing of Test Site
Cross-section Elevation View B
os
I' I
. .
I
.~ . . .
.. . .
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. . ... . .
. .
. . . .
. . . . . .
. .
. .
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APPENDIX C
INTERPOLL LABORATORIES ANALYTICAL DATA
. . __
. . .
.. .
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I N l t K P U L L LABUKAIUKlt3, INL. (612) 786-6020
EPA Method 3 Data Reporting Sheet - Orsat Analysis GKd)E-%xh’r / L P fff i6kr-O Source bn pe4 -flq-o .~ . . . .
lob Team Leader F3 Test Site iT Z L C T Date Submitted 15- /c/ -9L Dare oi Ten c - f Y ’ 4 6 Ten No. h No. of Runs Completed 2
. .. ~~ ..
Date of Analysis 5 - - 1 7 - ? G Technician E A
. ...
. . . .
. . . . . . . - :..
Orsat Analyzer System Leak Check Fuel Type FO Range F, Within €PA M-3 Guidelines for iuel type.
0 0 Coal:
Anthracitelignite 1.016-1.130 Bituminous 1.083-1.230
Where Fo - 20.9-0. coi
F - Flask 1250 CC all glass)
- Tedlar Bag 15 layer)
Oil: Dinillate 1.260-1 A13 Residual 1.210.1.370
Natural 1.600-1 336 Propane 1.434-1.586 Butane 1.405-1.53
WwdMlood Bark 1.00~1.130
cas:
11 1595t:L5TACKlWP\FORMS\S-jgg c-1
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INTERPOLL LABORATORIES, INC (61 2) 786-6020
EPA Method 3 Data Reporting Sheet - Orsat Analysis
1
. . .. . ..::
. . . :.. . .
. . . .
. .
...
. . . .
.. :. . .
.. .
lob C7 ' 0 ENE~G 9.A P trem Source CohC 0 k)Cq F T u d C
Dare Submitted 4 /) f 9 b Dare ai Test Test NO.
Test Site 3 M L C - r
No. oi Runs Completed 2 Y- /Y - 4r,
Team leader 5 K
Dare oi Analysis rA)7- 'i b Technician 3 x T e d Sample No. Buret Readings (ml) Conc Conc. 0, Fo Run Log No. of co, sbvtv %VtV Dry
and Tvoe An. Zero Pt. Alter CO. Aker 0.
I I I , I I I I I I I II I I I I I I I II I I II iI I I
I I I I I1 I I I I II
I I I I I I II I 7 -. I II II I , II I
I I
0 a
Orsat Analyzer System Leak Check Fo Within €PA M-3 Guidelines for fuel type.
Where F. - 20.9-01 co:
F - Flask (250 cc all glass)
B - Tedla; Bag (5 layer1
Fuel Type Coal:
Anrhracitekignite Bituminous
Disrillate Residual
Natural Propane Butane
Oil:
Gas:
WoodWood Bark
FO Range
1.016-1.130 1.083-1.230
1.260-1.413 1.210-1.370
1.6ac+i.836 1.4341.586 1.405-1. j j 3 1.000-1.130
11 1595C;\STAC:~WP\FORMS~-j69 c-3
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INTERPOLL LABORATORIES, INC. (6 12) 786-6020
Solvent Rinse Data Reporting Sheet
Y k P A Method 5 Probe Wash 0 EPA Method 29 Probe Wash 0 €PA Method 202 Cup & Tube Wash
Job Date Submined Test No.
0 &+4IW&%CI I,.&* P* U G Y / SourcdSite c/.,L/c Z a Z y k /z/c Z u L e r
Date of Analysis 6 - 3 - 'i Technician 5 4
Transpon Leakage@ NonQ ml Solvent
. . . ...
'Solvent Residue=ug/ml -[(Sample Wt.&$ (106)]NoI. of Sol. E m 1 EPA-M5 Acetone Residue Blank Spec. 5 7.8 u g h 1
4 5 Results of Solvent Rinse 8
RUN 8 RUN RUN 2 RUN -? . 9003 c-5 ,o 5,6 . o/c7 . W 6 7
/
. . . . . . .... . . . . . . . . . . . . . .~ . . . . . . . . . . . . . . . . . . .~ .~
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INTERPOLL LABORATORIES, INC. (61 2) 786-6020
Filter Gravimetrics Reporting Sheet
. Test: I Run: 0 Fiiter No: O3 5-.? Field Blank Filter Twe: W M 4. E Lac No: '74% Y - 61 1: Filter + Samoie Wr: ./L/L/F E
, color: b1-1 ITY Filter Tare Wt: . "%d c
Fiter Type: &EPA Method 5 0 EPA Method 29 0 €PA Method 202 0 Other
lob, 44.44Wrn/G<G e,wc-rc / Sourcdsite &Me f ~ & t r Z+V - 6 c I 6 Date Submitted Ten No. / Date of Analysis 6 - 3 - 9 b Technician L& 3
I
4 Results of Filter Analpis ?-
RUN D RUN 00 I RUN I RUN 7 . eoo r c c c z$ I .oar' - C o b 0
-
Total Mass #
r I I I * ,I
1 0.0601 I 0.0519 0.0 5/3
C-6 1 1 2 9 9 4 G E T A C K \ W P \ F O I 9 1
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INTERPOLL LABORATORIES, INC. (61 2) 786-6020
Filter Gravimetrics Reporting Sheet
Test: / Run: 7 Field Blank
Loc No: - 0 +/F ...
Color: L h & d
Test: Run:
Loe No:
Color:
Fiter Type: @ €PA Method 5 0 EPA Method 29 €PA Method 202 0 Other
Filter No: 0 3 T/
Filter + Samole Wt: * /yq/ Filter Tvoe: q7AA CY.
e
Samole Wt: eo0 Y C D
Filter Tare Wt: , /US/ c
Filter NO:
Filter Tvoe:
Filter c Samole Wt: e
Filter Tare Wt: c
Sample Wt: g
Color: Filter + Sample Wt: g
!I Sample Wt:
Test: Run:
Log No:
Color:
Filter No:
Filter Type:
Filter + Samole Wt: K
Filter Tare Wt:
49 RUN -? RUN RUN RUN
Results of Filter Analysis g , o o . - l O 1.
I RUN I RUN I RUN I RUN
Total Mass g
c-7 11 2994C:\STACK\WP\FORMSW91
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-. .
INTERPOLL LABORATORIES, INC. (612) 786-6020
lrnpinger Catch Data Reporting Sheet Protocol: OMinnesota UWisconsin Olowa $PA Method 202 UOther
Date Submitted
. . . . . .
-
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .~ . . . . . ~. . .
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. . . . . . . . .. . . . . . . . . :. . . .: . .. . . . . . . . .,...
~~~~ ~ ~ ~ ~~~
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Test: 3 Run:
LOG No: YL/ - 0 e? . Volume of Soivent 115- ml . . . . .
'Solvent Residue udml
Test: -3 Run: ( VoI. of Solvent
Loe Number
Comments
IC? 0 mi
- 0 4 ?
Tesr: 3 Run:
Val. of Solvent ITo mi
Log Number - I v r' Comments
Test 7 Run: 3 Voi. of Solvent /?'a& Lo4 Number - ' /I'
c
RUN 0 RUN ( RUN 2 RUN 7
Dish No: 7 9s'.
Dish Tare Wt: @ vz . 3 yvs- D
Dish + Samole Wt: i/ 2- J f L / 7 4
Samole Wt: . o o o L 0
Dish NO:
Dish * Samole Wt: 2 7. 7 7 4 -/ 4
DishTare Wt: 37. 16 7 8 s Samole Wt , 2 / / L 0
Dish NO: 72 Dish Samole Wt: 7 9 . / 9 / 0 4
Dish Tare Wt: 770vq/G g
Samole Wt: ' /+ 7/ e
Dish i Sample Wt L/ 7. L 2. g
rile Wr. , / t i 7 0 0
Dish NO: 4. d 3 6
Dish Tare Wt: ?7- YLL. e
. .. . . . . . . . . . . . :. . . . . . . . .. . . . . . . . . .
~ ~ ~ ~ ~~~~~~
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INTERPOLL LABORATORIES, INC. (61 2) 786-6020
Filter Gravimetrics Reporting Sheet
& Results of Filter Analysis g
Fiter Type: kf €?A Method 5 0 €?A Method 29 0 €?A Method 202 &Other -‘7 l o b , L P +f lqu.+ad SourdSite L<b* Z 5 4 F A c r &- E-;-o*,c Date Submitted Test No. 3 Z - U G ef
Date of Analysis & - 3 - 5 c Technician S c 3 ._
- RUN 0 RUN / RUN / 1 RUN z ~
. d o o r ? . 2 5-c 7 I .tg79 ,5-u/--
, 1
11 2994C:Ki’ACK\WP\FORMS6491 c- 10
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INTERPOLL LABORATORIES, INC. (612) 786-6020
Filter Gravirnetrics Reporting Sheet
. . . .
Fiter Type: 0 EPA Method 5 €PA Method 29 0 €PA Method 202 H e r ./%' - /7
Test: 3 Run: 3 Fiiter NO: ' 7 Field Blank: Filter Tvw: A ..C T % ' ~ ~ l . z / ~
Loe No: 76 d c/- / /F Filter c Samole Wt: 32. '(73-18 e Color: Filter Tare Wt: 3 7 . 7612 e
Samole Wr: . 5 / Y C s -
Color: Filter t Samole Wt: 4
Sample Wt:
Color:
Sample Wt:
Filter + Sample Wt: g
Test Run:
Log No:
Color:
Filter NO:
Fiiter Type:
Filter + Sample Wt: 4
Filter Tare Wt: g
J P ' /
Results o i Fiiter Analysis g
- RUN RUN RUN RUN
.5/Y6
RUN RUN RUN RUN
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INTERPOLL LABORATORIES, INC (612) 786-6020
lmpinger Catch Data Reporting Sheet
Date Submined s!t T . 9 cr Test No. 3- Date of Analysis 5-1 -f ' 96 Technician m M la3
. . . .. . . .
. . . . . . . . . . . . . . . . . . . . . : - . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . : : . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
I
1
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. . . . . . . : . . . .
~~
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INTERPOLL LABORATORIES, INC. (61 2) 7866020
Solvent Rinse Data Reporting Sheet
Test: c Run: a Dish No: 2 7 Loe NO: 76- . fL{- /0 ‘ Dish i Samole Wt: ?i/7 e
/ z c rnl Dish Tare Wt: %P. 6s ? Z Volume oi Solvent m
-00 e L̂ ‘Solvent Residue 4
Test: f Run: / . I Dish No: q” udmi I Samole wt:
Vel. of Solvent - /~J’’~I 1 Dish + Samole Wt: 4 7 7 L / S e
Lo4 Number e /&> I Dish Tare Wt: u7. 6# ’ 2c Comments I Samole wt: ,: / /92c e
Log Number 172 Dish Tare Wt: L/d. C y / J g
Vol. of Solvent /70d Dish + Sample Wt: qf. 6137.- g
Loe Number - / y?’ Dish Tare Wt: 4 Y. L/Y 7 2 E
<-le wt. ” / 753 D
e
Test: Y Run: Dish No: 33 VoI. of Solvent /?a ml Dish i Samole Wt: q L e 20 3 9 e
I Sarnole wt: . //LC Comments m
Test: R u m 3 Dish No: 6 ( 3
I h m m p - r c
, 4 P A Method 5 Probe Wash €PA (Method 29 Probe Wash UEPA Method 202 Cup & Tube Wash
r
. . . . . . . . . . . . . . . . . . . . . . . . - .
. . . . . . . . .~ . .
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. . . . . . . .
. .
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...
Test: Run: /
INTERPOLL LABORATORIES, INC. (6 12) 786-6020
Filter Cravimetrics Reporting Sheet
Filter NO: 7
Fiter Type: 0 EPA Method 5 EPA Method 29 EPA Method 202 A O t h e r A’- ’7
Job, L j //4+4.d/& -/ Source/Site ~ / J Q ~ ~ ~ ~ c i i i A- -7u,y< %&-r
Date of Analysis 6 - 3 - 7 ~ Technician <c /? Date Submitted Test No. s
Field Blank
~ 0 4 ~ 0 : 76f “/-/6F Color: /Tho Lr-/
Filter Twe: 5. 5- 7‘ Filter + Samole Wt:’$’o . ’037 4
Filter Tare Wt: 3 9- 9 8 5 7 e
Calor: / c r r r d Filter + Samole Wt: 4/. / 6 s z 4
Filter Tare Wt: 4/- 08s 7 e
Sample Wt: . 0 6 3 P g
Test: Run: 3 Log No: - / g F Calor:
Filter No: 7 Filter Type: -5.L W ~ 4 3 c e
Filter T& Wr ua. 2 2 3 8 Filter + Samole Wt: 7//< 4
8 do,-
Results of Filter Analysis 8 &./dx ‘063$ I , VL f/ 4 f77
RUN @ I RUN 7 RUN ?a RUN
Total Mass 0 . 8 0 6 6 I 0.8967
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Interpol 1 Laboratories . Inc - <612)786--6020
Ion Chromatography Laboratory
F] Flow Rate Eluent
AS3 ml/min 2 . 4 nM NazC03 & 3.0 mM NaHCO3
1 . 8 mM NaZCOa B 1.7 mM NaHCO3 /’ AS4A -- ASS ml/min 100 nM NaOH
DIONEX W E L 4ooo1 W I T H ANION MICRO MEMBRANE SUPRESSION
Flow Rate Suppressor Acid
ml/min 12.5 ml.l Sulfuric Acid
ml /ml n
Isocrati c
Results of Sulfate Deterrlnation
’f 1 i ~~~
, .i - 3 IC . ; :, . . I
Total ug = (Sample Vol.) x (Dilution) x (Solution Conc.) meq = Total ug / 48000
LSC-OERR
C-15
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I n t e r p o l 1 Laborator-l es I n c - <612)7a6-6020
I on Chromatography Laboratory
)/jFl
AS3
J' AS4A
ASS
- ow Rate Eluent Flow Rate Suppressor Acid
m l / m l n 2.4 mM NazCO3 & 3.0 mM NaHCO3 m l / m i n 12.5 mM Sul fu r ic Acid
&nl/mln 1.8 W4 Na~C03 & 1.7 mM NaHCO3 m l /mi n
ml/min 100 mM NaOH I s o c r a t l c
m l /ml n Gradlent(L1 s t program below) --
Results of Srlfate Deterrlnatlon
Tota l ug = (Sample Vol . ) x (D i l u t l on ) x (Solut ion Conc.) mq = Tota l ug / 48000
LSC-OBRR
C- 16
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. .
c
C-17
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. . . . . ~
w i-
0' i
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c-19
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r
c-20
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APPENDIX D
NO, AND CO DATALOCCER PRINTOUTS
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:.. . :
.-
...
RePOn NO. 6-7684 GeaenergvlLP . Haywerd
Line 2 E -Tube Outlet Test 2 Run 1
I I NOX I 0 2 I CO 1 co2 OATE i TIME 1 Ippm) I 19bl I lppml 1 1%)
AVERAGES1 8.41 16.51 1010.81 4.1
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.. .. . .
D-2
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D- 3
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Reporr No. 6-7684 GeoenergylLP - Hayward
Tests 4 and 6 Run 1
l ~ i n e 2 Surface Dryer E . Tube Inlet I Line 2 Core Dryer E - Tube Inlet I 0 2 I co 1 c02 NOX 1 0 2 1 co 1 c02 19/01 I (PPrnl I 1%1 lpprnl I 1%) I Imm) I (%I
I I 1 1 I
I ! /I I 1 5.6
1 AVERAGES I 25.41 1ti.1' 1042.6 5.011 24.11 15.01 785.31
D-4
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Repon No. 6-7684 GeoenergylLP . Hayward
Tests 4 and 6 Run 2
i I I NOX 1 0 2 j CO I c02 11 NOX I 0 2 1 CO i C 0 2
DATE 1 TIME I IPPml I [ % I I IOOml I 1% I( ioom) I 1%) I lpprnl I 1%)
ILine 2 Surface Dryer E . Tube Inlet I /lLine 2 Core Over E .Tube Inlet I
11
.. .
I I I 25.51 16.21 330.01 4.d 20.4; 15.31 815.91 5.6
I AVERAGES
0- 5
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Repon NO. 6-7684 ~ e o e n e r g y l ~ P - Havward
Tesrs 4 and 6 Run 3
ILlne 2 Surface Dryer E - Tube Inlet I Line 2 Care Dryer E .Tube Inlet I I NOX 1 02 I CO 1 c02 NOX I 02 1 co 1 c02
DATE 1 TIME 1 room) I 1%) I loprnl I l%l loprnl I 1%) I (porn) I 1 % ) I I I
. .
I 6.1 I AVERAGES I 22.91 15.91 1082.91 4.711 21.61 14.51 887.81
D-6
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APPENDIX E
MEASUREMENT SYSTEM PERFORMANCE SPECIFICATIONS
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INTERPOLL LABORATORIES, INC. (6 12) 786-6020
EPA Method 2 Field Data Sheet Drawing of Test Site
lob :7 EO EM d t% -f L
Test %lFtjRun-Date r- IY-96 Stack Dimen. Dry Bulb "F Wet bulb O F
iblanometer 0 Reg. 0 Exp DElec. Barometric Pressure IN.HC Static Pressure IN.WC Ooerators Pitot No. C,
r - Source - L fx E-7u& &f IC4
B I , C
*a;. M.f
IN. I 1
. . .
. . . . .
03 25 94C:\sTACK\W P\FORMS\s-3 9 2.1
E - 1
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Q/ &Jk ,a/ J Source J T ~ C L ’ ‘&,%‘e 07.24 / E39 c7-a Job
Test Stack Dirnen. Dry Bulb “F Wet bulb “ F Manometer Reg. OExp OElec. Barometric Pressure IN.HC Static Pressure IN.WC Operators #x ‘L L c , Pitot No. C
Y Run Datec/<i-SC “ ‘ T i ? V - L IN.
~
Cross-section Elevation View View
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Job Source Test Stack Dimen. Dry Bulb
Traverse Point *o
INTERPOLL LABORATORIES, INC. (612) 786-6020
EPA Method 2 Field Data Sheet Drawing of Test Site
Cross-section Elevation L 9 / rtah\(l.”v& G Z 6 +
L ;e ‘ 2. CITY. -or\lv, +?73 &&CY
b Run-Date ! T - / V - ? A Y’ d IN.
O F Wet bulb “F
Distance From Stack Distance Z:lr Wall (IN.) From End of Port (IN.) Velocity Temp. of Cas
.................... ........................................ ........................................ .................... . . . . . . . . . . . . . . . . . ....................
I
I I
Port Length: IN. . Time Start: HRS
I1 I
Temp. Meas. Device & SIN: Time End. H RS
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Calibration Error Check
Test & Run C Date 5'-/Y-?t' Job
Operator 5 . RhTd V U L k
%Calibration: Time (HRSI
Response
NO, Calibration: Time (HW
Response Value (PPM) (PPM) IPPM)
0, Calibration: Time (HRS)
/ .I Cylinder Difference Value Response (PPMI (PPM) (PPM) (PPMI
CO? Calibration Time (HRS . .
.. Response (PPMI
. .
Zero Cas 0
Mid Level IO . F; High Level 1 b- $
CO Calibration Time (HRS
Response (PPM) (PPM)
..
E-4
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INTERPOLL MBORATORIES, INC (61 21 786-6020
12
>\ 0 s . .,'
Zero Cas 0 I m Upscale I WE3
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I NTERPOLL UBO KAT0 R I €5, I N C (6 12) 786-6020
/J& Cal Drift Check
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INTERPOLL MBORATORIES, INC (61 2) 786-6020 0 Cal Drift Check
Dare T7 Y -7 G Site e D T N C L 3
lob L? / &./ Luw4 Source 2 E o / ~ i z c e Q'yCy
-3z?un F 7ZLk Tesr
3eracor ,
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INTERPOLL U8ORATORlE5, INC (6121 786-6020
09 1 j?jC:‘STAC:GWP,FO RMSU-5 9a
E-11
,
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INTERPOLL LABORATORIES, INC (612) 786-6020
0 k Cai Drift Check
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INTERPOLL LABORATORIES, INC 161 2) 786-6020
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INTERPOLL LABORATORIES, INC (61 2) 786-6020
C O Z Cal Drift Check
..:.
E-15
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INTERPOLL UBORATORIES, INC
Instrument
J\/c")c
L o
0,
C O Y
Cylinder Analyzer Resp (PPM) Diff. Span % Value CE-SB Val. of (ppp,i) Cal. Err. Sys. Bias ( p p ~ )
* * *
(PPM) Span
Zero Gas 0 0 3 a- $60 ,E% Upscale 7e.q % \ A 7g.g 3 4 950 l J L %
upscale ) q 7 \q& \*'& 0 rl: c 0% Zero Gas 0 b ,3 ,3 BW '2% Upscale 13,7r 13.L 1 3 4 - I !g% *4% Zero Gas 0 0 -. 1 . \ wK .5-q Upscale l o . e \D,% \o ,$ 0 a 0 5 0%
Zero Gas 0 0 0 0 5OG 0%
Zero Gas 0
Upscale
Zero Gas 0
Upscale
Zero Gas 0
Upscale
Zero Gas 0
Upscale
Zero Gas 0
Upscale
Zero Gas 0
I Upscale I Zero Cas 1 o Upscale I Zero Gas 0 I
E-17
~
I ~
I Upscale I I I
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.. (61 2) 786-6020
Calibration Error Check
Job LQ/ & , r i l r f 7 - 0
Test Date +-(<-?A <->:,P> I Operator - ,/
SO; Calibration: Time WRn
Response Value (PPMI (PPM) (PPM)
NO, Calibration: Time (HR.9
Value Response Value (PPMI (PPM) (PPMI (PPMI
O? Calibration: lime (HRS
Response IPPMI IPPMI IPPMI Soan
. . . .
CO? Calibration Time (HR.9
Response Value (PPMI
CO Calibration Time !HW - Response
IPPMI IPPMI (PPMI IPPMI Soan
E- 18
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I
E-l?
Operator &A- Instrument Cylinder Analyzer Resp (PPM) 01%. Span 96
Value CE-SB Val. of (PPM) Cal. Err. Sys. Bias (PPM)
ai.=
(PPM) Span
Zero Gas 0 0
Zero Gas 0 0
0 Upscale / 3 . 7 /3- c Zero Gas 0 f I '
Zero Gas 0 I
p.. Upscale 77.7 79 I
Upscale 3 9 d ~
Zero Gas 0
J d - od, U& Upscale /o 7 / i . 7
Upscale
Zero Gas 0
Upscale
Zero cas 1 o Upscale
Zero Gas 0
Upscale
Zero Gas 0
Upscale I Upscale I I
Zero Gas 0 I
Zero Gas 0
Zero Cas 0
Upscale
I - I Upscale kwsr be within 5% or the span ror the zero or upscale cal. gas.
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Test
Operator - SO? Calibration: Time (HRS)
Response (PPMI (PPMI Span
I I1 I 1 Mid Level 1 1 1 I . 1 , 1 NO, Calibration: Time (HRS)
High Level
Response (PPMI (PPM) (PPMI
O2 calibration: Time (HRSI
Value Value (PPMI IPPMI
High Level -1 CO, Calibration Time (HRSI
Response
Mid Level . / c
CO Calibration Time (HRSI
Response IPPM) IPPM) (PPMI
05?39~-C:\5T~Ci;\\2ImFOR,~S\5~20-10
High Level
E-20
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1
E-21
Cylinder Analyzer Resp (PPM) Diff. Span % Value CE-SB Val. Of
- = = Instrument
(PPM) Span (PPM) Cal. Err. Sys. Bias (PPM)
Zero Cas 0 I
Zero Cas O I - fVO< Upscale x 7 ?5-
Zero Gas 0 I / I CG Upscale 5-73 2 7
COJ Upscale /d: 7 /f- 4
UL Upscale 3- 7 / 3.6 Zero Gas 0 ,L
Zero Gas 0
Upscale
Zero Cas 0
Upscale
Zero Cas 0
Upscale
Zero Cas 0
Upscale
Zero Cas 0
Upscale I Zero Cas 0
Upscale
Zero Cas 0
Upscale
Zero Cas
Upscale 0 I I
i Must be within 5% or the span ror the zero or upscale cal. gas.
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APPENDIX F
CALIBRATION GAS CERTIFICATION SHEETS
. .
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.:.:
..
. .
c ~ w
m N
t;
!
5
N “ S ” “ O F :
u v ( * v u :
( * N O e:“
F- 1
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INTERPOLL L4BOFATORIES, INC. (61 2) 786-6020
Certificate of Analysis for High Range Standard Gas for Method 3A
Vendor p s - / , 2 d * I
Date of Preparation 1 -&32
Blend Specification a 1 . 1 3, o, /6-7 22 C q
Cylinder No. L c /O? 'SbC,
Label
I . - L
Results are within 5% of the vendor tag value; use tag value ..-
El
0
0
Results are not within 5% of the vendor tag value; d u c t another se! of triplicate analyses.
All results within f 5% of the average; relabel as above.
All results not within * 5% of the average; perform another set of triplicate analyses.
Date:
Approved by: Or. PI
F-2
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161 7) 786-6020 EPA Method 3 Data Reporting Sheet - Orsat Analysis
-P7? N Zcurce C ' C / C 7 ~ @ Tes; 3i:e 7 he3
.: lob - a chs7 > #?am Leader .5//3
D3:e si re.; / - ' ~ k - 5 6 "Ye Scbnixed - dte ai .Analvris
. . . .
F, Wilhin EPA M-3 Guidelines for iuel type. An:hracire/Lignire 1.01b1.130
Coal: - C
Bituminous I .083-1.230 Where F, - Oil:
co: Distii1a:c 1.26C-1.LI3 ?.esidi;al I.IlC-l.li0
CdS: Xarural 1.60~-1.a36
.. - Flask (250 cc all glass) Propane 1.4311.586 Burane l.~O3-l.~53
8 - Tedlar Bag (3 layer1 LVoadUiocd Bark 1 .0001.130
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1 NATIONAL SPECIALTY GASES 630 U7"TED D)EITyE D-M, N.C. 27713 (919) 54-43772
TO: TWINCITYOXYGEN
CERTIFICATE O F ANALYSIS
DATE REPORTED:9/29/94 REFERENCE #8&34131
MAT- SUBMITTED:OXYGEN, CARBON DIOXIDE Dl NITROGEN, CERTIFIED CYL. #CC109860
1
INFORMATION REQUESTEDzRATIO AXALYSIS
METHOD OF ANALYSIS:OXYGEN &YZER
RESULT OF INVESTIGATION:
t
. * - .-
COMPONENT
OXYGEN CARBON DIOXIDE
NIlXOGEN
SPECIFICATION
21% 17%
CONCENTRATION
21.1% 16.9%
BALANCE
F-4
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INTERPOLL LABORATORIES, INC. (6121 786-6020
Certificate of Analysis for Standard Gas
A4Jdk .56 'r/r )bCr2 \-+% i ,-a-7s hi\k-?,e &:A 0
7 3 . 3 nLlM IC+ k.? P 2 r , I
Date of Analysis
Vendor
Cylinder No.
Date of Preparation
Label
Blend Specification
Run /c/o\ y-9-4 b '-I- Y-$6 r-4 -7 C"
1 7d.YLIY 2 m 3373 3 7a. c b e ~ ' 4
I ll I I
5 I II 6
Analyst
El U
0
Results are within 2% of the vendor tag value; use tag value.
Results are not within 2% of the vendor tag value; conduct another set of triplicate analyses.
All results within
All results not within
2% of the average; relabel as above.
2% of the average; perform another set of triplicate analyses
F- 5
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I WTERpOLLLirBs
TANK C€WT TANKNUMBERSG9151692
41436
4 / q s 12o:oopM
4/4/96 1:20:06pM
4436 l:ZO12pM
4/4/98 120:18pM
4/4#36 120:24PM
U436 1:2030pM
4/4/96 1:20:36FM
4/4/96 1:2042pM
V436 1:20:48pM
0 71.973 0 0 0
0 74008 0 0 0
0 716M 0 0 0
0 73.194 0 0 0
0 72787 0 0 0
0 72.38 0 0 0
0 71.973 0 0 0
0 72787 0 0 0
0 7238 0 0 0
0 71.566 0 0 0
0 72.38 0 0 0
0 7238 0 0 0
0 72787 0 0 0
0 73.1 94 0 0 0
0 n.16 0 0 0
0 7238 0 0 0
0 7238 0 0 0
0 71.973 0 0 0
0 7238 0 0 0
0 71.566 0 0 0
4/4/96 12k54pM
4/* 1:21:00w
44196 121:OGFM
4/4/96 121:lZpM
4/4/96 1:21:18pM
4438 1:21:24PM
4/4/96 l21:30pM
4/4/96 1:21:36PM
4436 1:21:42PM
44446 121:48pM
4/4/96 1:21:54W
72.46145
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TANK ERT TPNKMJMRER SO9151692
44196
1:41:05 PM
1:41:11 FM 72787
1:41:17 FM 73.1 94
1:4123FM 7230
1:4129W 72787
1 :4135 W 73.194
1:41:41 FM 71.973
1:4:47PM
1:41:53 FM n.973
1:41SgpM 73.194
1:42% PM 71 373
1:42ll FM
1:4a 7 PM 71.973
1:42P PM 72787
1:+29W
1:ms PM 73.194
1:4241 PM 73.601
1:4247 plr( 72.787
1:4253 RA 71.373
1:4259 w 7238
723e
n.sn
72787
72787
m03as
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
a
0
0
0
0
0
0
a
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0 .
0
0
0
0
0
0
0
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0
- w
r c a o a
. 4 . Y O a 0 . b e 4 Y e E . . m n
* c 0
u o Q
u r n .. % m
3 n rl
m P 4- $ t ..
I .
I
I I F-8
i m C 4
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INTERPOLL LABORATORIES, INC. (6 12) 786-6020
I I -
Certificate of Analysis for Standard Cas
Vendor A* ? r " A Q A q . . Cylinder No. SG 9 \ ' ;Aqoa,
Date of Preparation
Label Wihr: c Ox,La 7- 1a-7 y
Blend Specification I q18%? C-I h l l
Date of Analysis
Y-Y-9 b
-il-?6 4-.1-sc
Run (vex 1 r.\4. F l - L L
2 IYb. 3 I V Y . og 7J 4 I 5 II
Analyst &a& #- 4 0
0
Results are within 2% of the vendor tag value; use tag value.
Results are not within 2% of the vendor tag value; conduct another set of triplicate analyses.
All results within 5 2% of the average; relabel as above.
All results not within 296 of the average; perform another set of triplicate analyses.
Date:
Approved by: -
01 2696*;.\STAC(\WP\FORMS\S-L25
F-9
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1 TANK C3T TANKNUMRE!4SG932402
44496
4 4 9 6 12:49:05PM 0 14725 0
4/4/96 124S l lPM 0 146.436 0
444% 1249:17pM 0 146.843
12:43:23 pM 14725
124g:z9 Phi 147.25
124935 RA 146.843
12:49:41 PM 146.843
124347RA 146.436
124953 pM 146.436
124953pM 146.436
1250:05 FM 146.436
1250:11 RA 146.843
125017 PM 14125
1250:23 Phi 146.843
125029 RA 146.029
1250% PM 146.436
1250:41 Phi 147.25
12so:47 RA 146.843
0 0
0 0
0 , o
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
F- 10 I ..
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TPNK CERT TbNKNUMRERSGS132402
4/4/96
1:03:04 W 146.843
1:03:10FM 147.25
1:0316PM 146.029
1 : o m PM 146.843
146.436 1 :ON4 PM
146.843 1:U340..IDFM
146.843 1 : O M FM
146.436 1:0352PM
146436 1:03sew
146.843 1:0404 W
145622 1:0410 FM
146.843
146.843 lP422PM
146436 1:0428 FM
147.25 1:04:34 PM
14725 1:04:40W
146.843 1:04:46PM
146.436 1:04:62 W
146.843 1:0458 PM
i:o3oe FM
I :O~ I~FM
1 4 6 . ~ ~ 1
146.65385
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
F-11
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TANK CERT TANK NUMBER SG9132402
44/96
qw 0
44/96 0
q4B6 0
4IVS 0
44% 0
44/96 0
4/4/96 0
4496 0
4/4/96 0
44/96 0
44/96 0
4436 0
4/4/96 0
4496 0
44/96 0
qV6 0
44/96 0
U496 0
0 W 6
0
1:11:05 FM
1:11:11 FM 147.657
1:11:17FM 146.843
1:11:WFM 146.843
1:ll:29FM 14725
1:11:35Fhi 146.436
1:11:41 FM 146.843
1:11:47 FM 147725
1:11:n FM 1 4725
1:ll:59FM 147.25
1:12J5FM 14725
1:12:11 FM 146.843
1:1217FM 146.843
1:1223FM 14725
1:1229FM 147.657
1:lUfiFM 146.843
1:1241 FM 147.25
1:12'47pM 146.843
1:1253FM 147.25
1:1259FM 14725
147.0872
146.1143 0 0 0
0 0 0
0 0 0
0 0 0
0 0 0 .
0 0 0
0 0 0
0 0 0
0 0 0
0 0 0
0 0 0
0 0 0
0 0 0
0 0 0
0 0 0
0 0 0
0 0 0
0 , 0 0
0 0 0
a 0 0
F-12
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... .
-
0 fi n .
> E + L c U LI e c #
E
e e C E
n
d
L C D
C
C
C ( 6 c L E
5
:
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U 0 ct 9i 4
U O 8 0 1 - 8 W O
c 4
m x m a m
s a a 0 0 Y)
0 4
a4 0 ln rl
3 0
PI n U m m a
m
A
m P Y 0 C
F-13
U
m z m
2 Y U m 0 a n
.. >. m
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v, 0 a
z a r o o m z z
2 .. ..
u m p.
Ln . l n
m c l z a r
z n w a 2 0 v a
E n
E C PI m 0 b4 Y .4 z Q
u PI 0 C
.. m
m m 4
m ..4 m a
I O 1 x 7 I 4
F-14
.. .
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.. . . . . :. . . . . . . ...
d e H . .
VI
U 4 0 z 4 .. .. c o o m z z
n
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m
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e . E . o . w - 0 m u . o r u + , 4 4 Y Y Y C n a u m m u m u m u v c c o
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c - m -
0 w 0 .e -
u x 4 0 1 z
0 e . .
C m m 0 u Y 4
z
m D 0
m 0 C 9 3 4 m
.. 1
F-15
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NATIONAL SWCIAL.TY GASES 630 UNITED D m DURHAM, NC 27713 (919)544-3772
CERTIFICATE OF ANALYSIS-EPA F'RUIWCoL MIXTURES
REFERENCE a: 8840607 C " D E R kCc16348 C Y L PRESSURE2000PSIG EWlR4TION D A T 3 612~98 CUSTOMER TWIN CITY OXYGEN
LAST ANALYSIS DATE612195 P.O.# 17405
METHOD: AN&YZF,D ACCORDING TO EPA TRACEABILITY PROTOCOL FOR ASSAY AND CERTIFICATION OF GASEOUS CALIBRATION STANDAFfDSSEFTEMBER 1993G-1. THIS STANDARD SHOULD NOT BE USED W" ITS GAS PRESSURE IS BELOW 1.0 MEGAPASCALS (150 BIG) .
STANDARD: INSTRUMETPICBECKMAN NDIR BECKMAN PARAMAGNETIC SRMk 1675B 2859A MODEL #380 755 ma: CLM6413 CLM6737 SERIAL 82000418 1001419 CONC.: 14.01% 2U.72% LAST cAL.:5/22/95 6IU95
c o M P o m . c o 2 COMPONENT: 0 2 COMPONENT: MEAN CONC:l6.8% MEANCONC 21.0% MEAN CONC: REPLICATE CONC. REPLICATE CONC. REPLICATE CONC. DATE6mJ95 DATE: DATE.6mJ95 DATE. DATE: DATE: 16.8% 16.8% 16.9%
BALANCE GAS32
REPLICATE DATA
DATE: 6/2/95 Z 0 R R 168.5 Z Z 0 C
REPUCATE DATA
DATE: 6l2i95 Z 0 R ~
R 210.5 2 Z 0 C
REPLICATE DATA
DATE Z R R Z Z C
21.0% 21.08 21.1%
C O M P O N F m ~
DATE: 168.0 c 201.5 Z R 0 C 202.1 R Z 203.9 R 169.0 Z C
COMPONENT92
DATE: 210.0 c 212.8 Z R 0 C 213.0 R Z 214.9 R 211.0 Z C
COMPONENT.
DATE C C
Z R
R 2 ~
R Z C
Z=ZERO C=CANDIDATE &REFERENCE . .-
C C R
C C R
C C R
F-17
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Vendor
Cylinder No.
Date of Preparation
Label
Blend Specification
INTERPOLL LABORATORIES, INC. (61 2) 786-6020
Certificate of Analysis for Standard Gas
A
Analyst
6
a n
Results are within 296 of the vendor tag value; use tag value.
Results are not within 2% of the vendor tag value; conduct another set of triplicate analyses.
All results within
Al l results not within
2% of the average; relabel as above.
2% of the average; perform another set of triplicate analyses.
Date:
Approved by:
01 2696C?STACK\WP?FORMS\S-125
F-18
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. :. . ::. : .
.-
. . . .:
TANK CERT TANKNUMBERcc117755
445136
45/96 0
45/96 0
1~42ilOAM 79.704
la42364 79298
10:QlZPM 73.704
104218W 79298
10:4224M 78.891
10:4230AM 78.891
1k4236.N 70.64
10:4242AM 78404
10:4248AM 78.484
lkM4W 79.298
1tUPoM 79298
10:4306PM 78404
10:4112AM 77.67
lt4318AM 70.484
lOA324PM 78.484
lR4330AM 78.077
10:4336AM 78.484
. .
10:43:48pM 70.484
104154PM 70.404
0 0 0
0 0 0
0 0 0
0 0 0
0 0 0
0 0 0
0 0 0
0 0 0
0 0 0
0 0 0
0 0 0
0 0 0
0 0 0
0 0 0
0 0 0
0 0 0
0 O 0
0 0 0
0 0 0
0 0 0
78.7281
F-19
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4 5 8 6 0
0 w
W6 0
0 4m
0
0 0 0
0 0 0
0 0 0
F-20 ~
0 D 0
0 0 0
0 0 0
0 0 0
0 0 0
0 0 0
a 0 0
0 0 0
0 0 0
0 0 0
0 0 0
0 0 0
0 0 0
0 0 0
0 0 0
0 0 0
0 0 0
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TANKQRT TANKNUhiBEFtCC117755
4536
4&36 105k42iW 0 77.67
+@36 106948AM 0 78.484
q5p6 I D m 5 4 N 0 78.077
78.230
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
4
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
F-21
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INTERPOLL LABORATORIES, INC. (6 12) 786-6020
Certificate of Analysis for Standard Gas
Date of Analysis
‘ I -5-96
I
Vendor
Cylinder No. 56 9/c1 37 -7 5 Date of Preparation / / - 7 - 9 7 Label ,/L-k,;L 0X:Jp - Blend Specification I CIT’,,Rn/l - 7 B/Lk&C* / b,
Run /t& 1 Y3- 303
,EL
0
Results are within 296 of the vendor tag value; use tag value.
Results are not within 2% of the vendor tag value; conduct another set of triplicate analyses.
All results within 2% of the average; relabel as above.
e All results not within 5 246 of the average; perform another set of triplicate analyses.
Date:
Approved by: -
01 2 6 9 6 C ? S T A C ~ ~ V ~ F O R M S ~ ~ 2 5
F-23
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122930PM 144809
122936pM 144.909
IrnlZFM 141809
143.335 122924FM
1 4 m 1 2 2 9 3 PM
122UEpM 143.335
122942FM lam
122948pM
122954pM 142774
12-pM
1230?JSpM 142774
1 m 1 2 p M 14Z.367
l23P18pM 142774
lWM4PM 142774
123030 FM 142774
1230SPM 142367
1 2 3 4 2 PM
12304 PM 14237
1 M O S P M 142367
143.33
i z m a p M
inim
i 4 m 8
i 4 m
inim
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
G
0
0
0
0
0
0
0
0
0
0
0
0
0
0
8
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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. . . . . .
TMK #RT TANKNUMBD1909162776
45/36
0 142361 45196 123642W
0 142774 4536 1236.40FM
0 143.181 @@ l U 6 5 4 W
0 142361 WF, 1m3oFM
0 143.1 ffl 45% 123796FM
0 142.367 y6/96 123732FM
U 1 4 W 45/96 lM:18FM
0 1 4 2 3 7 4588 123724FM
0 142367 4&36 1 U 7 3 F M
0 1 4 2 3 7 45/96 123756FM
0 142367
0 142774 45/96 123754FM
0 i 4 z m
1428554
U
0
0
0
0
0
0
0
0
a
0
0
0
0
0
0
0
0
0
0
F-25
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
a 0
0
0
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w6 1242pOpM 0 144.809
4526 124206FM 0 144402
142.95715 I-- ~ F-26
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
a
0
0
0
0
0
0
0
0
0
0
n
0
0
0
0
0
0
0
0
a
0
0
0
0
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0
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0
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0
0
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0
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0
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0
0
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: : u 5 -H
...
* 4 L . 8 . * ' y I o
" C C
C i
i
: ; 0 a c
cc. 02% u o a 0 u o uln C . m m 011.
2 -
5 I 3
o r . Y N I I 0 3
?: n m
n u ) ~m
I. .. 3 0 : z 4s u u 1 u 4 a ) m
P U L l c a m a v n U C E m m
u z w
" a PI u 0 z
J Y ~
I - N . c f r - i u m o m 4 z Z E 4 E CI
3 a
2 a 0 m 3
U
$ a m Ja u 0 C
5 rl
0' .c 0
U u a U C U Ul
m
*
F-27
.. 21 m
.. 2 n
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U G n . m
m a U
n
n
E O 0 m z z z .. ..
o m z - Y O
Ln . m
m c l z a : z :: z n w u 2 0 u a
m 0 rl
C VI
.t I
z c a o a -4
.I u o * Y O 8 ULn c . * o r (
urn c r l 0
t a u
L m o
e a m * u u c m m
m m r u u C 0 LI 0 4 W a: a
* z a a c c * o % W - I Q
m u . c.4 m o o u u + 1 ..( -4 u u u c c m u m~ u Q J u - i u u c E O .. m u
r l u m e a 0
U
* PI .4 W
rxl
x PI
I I I I I I I I I I I I I I I I I I I I I I I I I !
.. x m
2 2 >
a a a:
C m m 0 Y U .4 z
rn m W
m 0 C
rl
..
m m
01 d
a 0 VI 4
rn
3 0 0 R W m
rl
rn a
n m
Y 0 C
2 Y 0 .c m W u m C
U (0
a
m
I
F-28
U m x d
C a: m
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.~
. .
.:. .,
. I I
I 3 a: a
" m m u 0 2
0 rl 0 VI .-I
v1
E N Z E
0 i d a
a: a m ::
Z W
u a
C 0, m
Y 4 z E
.. m m u W U C 4a a rl ".
.. x m
V W a I PI P U 0 C
F-29
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APPENDIX G
SAMPLING TRAIN CALIBRATION DATA
. . . .
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INTERPOLL L%3O!UTORIES, INC (61 21 7866520
:. . . EPA Method 3 Cas IMetering System Quality Control Check Data Sheet
-_
lob L.P k4ud-J / L r , i / Dare S / Y - 7s Operaror ,Module No. 2 .. . Instructions: Operare :he control module rr i flow rare equal to 4H@ for 10 minures before arZding ihe umbiliczl.
Record the following data:
Bar press 28.91; in.Hg E - /I=S AH@ /- 7 2 in.\NC.
~
. .
i Time I Volume I
if y, I S nor within the rang5 o i 0.97 to 1.03, "the volume merering vynem h u l d be invsigared before begjnning."
CF?. Tide 10, Parr 60, .Appendix A, ,Merhod 5 , S m o n 1.1.1
G- 1
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INTERPOLL LABORATORIES, INC. (6 12) 786-6020
EPA Method 5 Gas Metering System Quality Control Check Data Sheet
Ti me Volume
L?/ Wc.4-2 Date S-/Y-FC lob Operator T. 422 IModuIe No. 5/
Meter Temp ( O D
Instructions: Operate the control module at a flow rate equal to AH@ for 10 minutes before attaching the umbilical.
Inlet ( m i d (Cn
Record the following data:
Bar press Zp.*pJ in.Hg 8- d . 9 9 3 r AH@ /. 77 in.WC.
Outlet
Calculate Y, as follows:
. . . .
y, = 1.786
( ) IO3
) - 460 0 t (
Y,- /UU6&7
If Y,, i s not within the range of 0.97 to 1.03, "the volume metering system should be investigated before beginning."
CFR Title 40, Part 60, Appendix A, IMethod 5, Section 4.4.1
01 1995-C:\STAC,~WP.FORMSU~32
G- 2
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INTERPOLL L4BORATORIE5, INC. (6 1 2) ia6-6020
EPA Method 3 Cas IMetering System Quality Control Check Data Sheet . . . . ..: . .
lob Lm E n t w . ,/ @A, I L. -lr J Dare 47 //?/?b hioduie so. 8 Operator r;u
I nsiructions: Operate :he control module ar a flow m e equal to AH@ faor 10 minutes before arcaching the umbiiicil.
Record the following data.
8ar press -25, $3 in.sg E - OH@ I, 7 7 in.‘NC.
Time I Volume I JMerer Temp (“I? ll Inlet I Ourlet it (CrS I (min)
,I of3 I 65- I bo I !]- 2.5 I
Calculate Y, as follows:
. . .. -.
yG7 = ‘ 97qq if Y, is nor within the beginnins.“
c?X Tide LO, Parr 60. .Acoendix ,A. ,b\/lerhod 5, Sedan 4.4.1
oi 0.97 to 1.03, “:he volume rnererins syynem should be invesrigared before
..
6-3
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1
Y - 1 m v) W M a 3 -0 C m C 0 .- 1 e 4 - G :: m ki : 1
6-4
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. .
rn 3 m
W M
- z
a 3 -0 C m C 0 ._ e 0 - 0 8
3
m L W -
G-5 I
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6-6
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. . . , . . .
G-7
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I 1: 0 a
Z
6-8
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. ..
II I I
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...
Interpoll Laboratories (61 2) 786-6020
Nozzle Calibration Data Sheet
Date of Calibration: 05-14-96 Technician: Scott Fjelsta Nozzle Number: 4-3
The nozzle i s rotated in 60 degree increments and the diameter at each point is measured to the nearest 0.001 inch. The observed readings and average are shown below.
Position Diameter (inches)
1 0.192
2 0.190
3 0.188
Average 0.190
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Interpoll Laboratories (612) 786-6020
Nozzle Calibration Data Sheet
Date of Calibration: 05-14-96 Technician: Ed Juers Nozzle Number: 8-3
The nozzle is rotated in 60 degree increments and the diameter at each point is measured to the nearest 0.001 inch. The observed readings and average are shown below.
Position Diameter (inches)
1 0.188
2 0.189
3 0.190
Average 0.189
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Interpoll Laboratories (612) 786-6020
Nozzle Calibration Data Sheet
Date of Calibration: 05-14-96 Technician: Steve Kelker Nozzle Number: 9-3
The nozzle is rotated in 60 degree increments and the diameter at each point is measured to the nearest 0.001 inch. The observed readings and average are shown below.
Position Diameter (inches)
1 0.191
2 0.192
3 0.193
Average 0.192
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is cold juncion compensated. Caliontion accuracy i s 5 0.196 of span (2100'fl 5 1 deogee Ifor negative temperatures add 2 2 degrees). The CL-300 sirnulars exacly the millivohge of a Type K thermocouple at h e indiet& remperarure.
Desired Temp Temperature o i Response ai Unit Under Deviation
Standard or Simulated Ten ('0 ~ [*fl Nominal nt c-n (%)
0 - 3 3 .69 Temp ("'3
t 06 9 7 ? . $3 I 0
100
200 20 0 I44 I I I .I5 300 3 0 zq 7 I
500 I 500 4q 7 I
aoo $0 0 600 I
3 .39
3 .35
3 n - 5 \
200 % 0 397
600 600 5-94 I I . 0 4
I I 1 1 6 9 8 2 '00 700
0 0 I .07' 000 400 899.
1000 lo@ ~~~ ~
1100 / too. 10 98
1300 /?OO 127%
/ooo 0 0 I z .I3 I
0 0
2 . I !
. .. 1 4 0 I 400 /YO/ I .o 5 I .os
I200 1200 I tog I
I500 /5OU IY44 I
1 io0 / 7nu 17Ul I
1900 f W 0 I /YO/ I 1000 l~ 2cJoO 1 20CO I
I 2100 Z I l f l I @4<
t I 474
I I .os z I .oq
0 l o 1
! 600 /bOU l a 2
1800 1800 /goz.
1 1 .OY
I .OY ~~ ~ ~~
I
I . r s 3 !I Averass: I * $ OF - 013 scale response by unit under 1 s t ("0 .&nit in tolerance
Z dev - 100 dl1460 i I) OUnit was nor in :olerance: recalibrated - See new cdlibration sheet.
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INTERPOLL LABORATORIES, INC (612) 786-6020.
Temperature Measurement Device Calibration Sheet Unit Under Tat: Y? . .
?ndor C,IC'c-+ .,ode1 4 h el Serial Number 7i JY.ly& 7
Range 0 - LIZL' 'F Thermocouple Type i<:
Method oi Calibration: POT No. ?? Care oi Calibration 1 /2L' I .)b Tednician f l r t r PFTTRSGsw
C
E
, Comparison against ASiM mercury &glass thermome!er using a rhermosaued and insulated aluminum block design& IO provide uniionn remperature. The temperature is adjusted by adjusting the voltage on the blo& heater m i d g e . Omega Model CL-300 Type KThermocouple Simulator which provides 22 precise ternpentwe equivalent millivolt signals. The CL-300 is cold junction cornpensared. Calibration accuracy is + 0.1% of span (2100'R + 1 d e s (for negative remperatures add 5 2
I empe.ature or Response a i h i t Under
. .
. .
Averages: 1.18 Z dW - 100 nfA460 + tl
I OF - 03 scale response by unit under test ("0 - ;Unir in rolennce OUnit was not in tolennce: reralibnted -See new sl ibnt ion sheet.
01 1995C:!STACICIWWORMS&l33
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1 INTERPOLL LABORATORIES, INC (612) 70€-6020
Temperature Measurement Device Calibration Sheet Unit Under T e s t psi Vendor
Range e . 'LOCC 'F Thermocouple Type 4 Dare a i Cilibration Method o i Calibration: PDT No.
Model C! * L e a Serial Number 75 5 s ?//a
/loLln 1 7 - 1 4 9 6 Technician hlJ .5 i
, Comparison against H M mercsy in.glass thermometer using a rhermosactd and insulated ajurninum b l o d aesignd io provide uniform remperarure. Tne temperature is adjuned by adjusting rhe volege on the blo& heater -ridge. O m e ~ a Model CL-300 Type KThermocouple Simuiator whic.. provides 22 precise temperature equivalent millivolt signals. The CL-300 is cold juncion compensated. Calibration accuracy is 2 0.1% of span (2100'fl e 1 dea,ree (for negative temperatures add 2 decrees). The CL-300 simulates exaaly :he millivoltage o i a Type K rherrnocouole at the indicatd temperature.
c
. . ..
OF - OS scale response bv unit under test (On
E G t In tolerance % dev - 100 nr4-160 GUnir was nor in tolerance: recalibrated - See new Qlibrarion shet.
11
01 1995C?STACICIWWORMN~33
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interpoll Laboratories, Inc. (612) 786-6020
S-Tvoe Pitot Tube lnsoection Sheet
Pitot Tube N o . 3 2 -
Pitot tube dimensions:
I . External tubing diameter (DJ
2. Base to Side h opening plane (PA)
3. Base to Side 8 opening plane (PJ
: Tf' IN.
qhd IN.
'dho IN.
Alienment:
4. u, < loo + 5. 0, < l o o
6. B, < 5' k 7. B, < 5= a
.-
a. z <.125".& 9. w <.0625".&Z
Distance from Pitot to Probe Cornoonents:
I 7 5 B IN. 10. Pitot to 0.500 IN. nozzle
1 1. Pitot to probe sheath '3.d IN.
12. Pitot to thermocouple (parallel to probe) z ' D IN.
13. Pitot to thermocouple (perpendicular to probe) 7ko IN.
.:. .
?% Meets all EPA design criteria thus C, - 0.84 0 Does not meet EPA design criteria - thus calibrate in wind tunnel.
c, -
Inspected by: Date of Inspection:
CFR Title 40 Pan 60 Appenidix A Merhod 2 5-348
6-17
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Interpoll laboratories, Inc. (612) 78G-6020
5-Tvoe Pitot Tube lnsoection Sheet
Pitot Tube N o . A Y - 9
Pitot tube dimensions:
I . External tubing diameter (D,) + .3lJ IN.
2. Base to Side h opening plane (PA) i ?k'B IN.
3. Base to Side B opening plane (Pd qd8 IN.
Alienmen t:
4. 0, < loo L 9 5. u2 < loo //
8. Z <.l25" d / 9. W <.0625" . 2
10.
1 I . Pitot to probe sheath 3. @ IN.
Pitot to 0.500 IN. nozzle ' 73-22 IN.
12. Pitot to thermocouple (parallel to probe) 3. IN.
13. Pitot to thermocouple (perpendicular to probe) '7@ IN.
0 0
Meets all EPA design criteria thus C, - 0.84 Does not meet EPA design criteria - thus calibrate in wind tunnel. c, -
Date of Inspection: Inspected by:
CFR Title 40 Part 60 Appenidix A Method 2 5-348
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Interpoll Laboratories, Inc. (612) 786-6020
S-Tvoe Pitot Tube lnmection Sheet
Pitot Tube No. 3 1- Pitot tube dimensions:
1. External tubing diameter (D,) 3 1 6 IN.
2. Base to Side A opening plane (PA) I 5 4 0 IN.
3. Base to Side B opening plane (P,) 1 q& IN.
Alienment:
4. (I, < l o o n 5. (I, < l o o ,"
6. B, < 5' D 7. B, < 5 O 7 8. Z <.125" i a / 9. W <.0625"&
Distance from Pitot to Probe Comoonenn:
10. Pitot to 0.500 IN. nozzle 7.53 IN.
11. Pitot to probe sheath 7; a IN.
12. Pitot to thermocouple (parallel to probe) 3J 8 IN.
13. Pitot to thermocouple (perpendicular to probe) T53 IN.
, b e e t s all EPA design criteria thus C, - 0.84 0 Does not meet EPA design criteria - thus calibrate in wind tunnel.
c, -
Date of Inspection: Inspected by:
L/- 7 - f j CFR Jirle 40 Pari 60 Appenidix A Method 2
5-348
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INTERPOLL LABORATORIES, INC. (612) 786-6020
Stack Sampling Department - QA Aneroid Barometer Calibration Sheet
Actual Mercury Ambient Temperature Adjusted Mercury Initial Aneroid Barometer Read Temp. Correction Barometer Read Barometer Read
Factor
37.77 69 , / 07 37-6 8 2% 6 7
Date &-2--9b
Mercuv Column Barometer No. G7.Mna -< I I Technician &R
Aneroid Barometer No. JO7.!L%?j 0 ks
Difference (P, - P,,)
I o/
Has this barometer shown any consistent problems with calibration? YedNo. If yes, explain.
~ ~~
Has problem been alleviated? Yes/No. How?
Note: Aneroid barometers will be calibrated periodically against a mercury column barometer. The aneroid barometer to be calibrated should be placed in close proximity to the mercury barometer and left to equilibrate for 20 - 30 minutes before calibrating. Aneroid barometer will be calibrated to the adjusted mercury barometer readings.
01 1794-C:UTACIC\M'P\FORMN-312
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.-
INTERPOLL LABORATORIES, INC. (61 2) 786-6020
Stack Sampling Department - QA Aneroid Barometer Calibration Sheet
Date Y-8 -.7& Technician 5 ; Mercury Column Barometer No. r .\I,- ';L Aneroid Barometer No. 3 @ 9 0 1 @ I O
c
~
Actual Mercury Ambient Temperature Adjusted Mercury Initial Aneroid Difference Barometer Read Temp. Correction Barometer Read
Factor
Has this barometer shown any consistent problems with calibration? YedNo. If yes, explain.
Has problem been alleviated? Yes/No. How?
Note: Aneroid barometers will be calibrated periodically againsta mercury column barometer. The aneroid barometer to be calibrated should be placed in close proximity to the mercury barometer and left to equilibrate for 20 - 30 minutes before calibrating. Aneroid barometer will be calibrated to the adjusted mercury barometer readings.
01 1794C:\STACh"WP\FORMS\S-312
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INTERPOLL LABORATORIES, INC. (612) 786-6020
Stack Sampling Department - QA Aneroid Barometer Calibration Sheet
Actual Mercury Ambient Temperature Adjusted Mercury Barometer Read Temp. Correction Barometer Read
Factor
L 9.94 8 2 . 36 28.
Date 2-Ci -4 6 Technician &.Td\65 Mercury Column Barometer No. I Aneroid Barometer No. I 07 2 4 0 d
Initial Aneroid Difference Barometer Read (Pba - Pbm)
2 g. a5 0
Has problem been alleviated? Yes/No. How?
..
Note: Aneroid barometers will be calibrated periodically against a mercury column barometer. The aneroid barometer to be calibrated should be placed in close proximity to the mercury barometer and left to equilibrate for 20 - 30 minutes before calibrating. Aneroid barometer will be Calibrated to the adjusted mercury barometer readings.
01 1794-C:\STAC~WPIFORMN-312
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. .
. :.. . . .
-
Actual Mercury Barometer Read
INTERPOLL LABORATORIES, INC. (6 12) 786-6020
Stack Sampling Department - QA Aneroid Barometer Calibration Sheet
Ambient Temperature Adjusted Mercury lnirial Aneroid Difference Temp. Correction Barometer Read Barometer Read (Pba - PJ
Factor
Date /o -1 7-7s Technician Gb I d
Aneroid Barometer No. sa 2Cfi
c r
Mercury Column Barometer No. A-MUA-]
Has this barometer shown any consistent problems with calibration? YedNo. If yes, explain.
2ArnWFJ7FR l-fA hm
Has problem been alleviated! YesINo. How? . .
Note: Aneroid barometers will be calibrated periodically against a mercury column barometer. The aneroid barometer to be calibrated should be placed in close proximity to the mercury barometer and left to equilibrate for 20 - 30 minutes before calibrating. Aneroid barometer will be calibrated to the adjusted mercury barometer readings.
01 179Ct:UTACK\WP\FORMN-312
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APPENDIX H
LINE 2 CORE DRYER E-TUBE OUTLET MONITORING
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CeoenergvILP-Hayward Line 2 core Dryer E-Tube Outlet
Page 1
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Page 2
H-2
GeoenergvlLP-Haward Line 2 Core Drver E-Tube Outlet
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CeoenergvILPHawrd Line 2 Core Dryer E-Tube Outlet
_. , _. - -, -. , , ... , 5114/9618:14:38 PMI
5/14/96181441 PMI
5/14/961814:44 PMI
5/14/96 81467 PMI
v i d m u.4d.w PMI I
20.8941
01 0.203 20.8741 01 0.081
01 0.407 20.8941 0.8141 0,081
01 0.2031 20.935 01 0.081
Page 3
H- 3
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CeoenergyILPHawara Line 2 Core ONer E-TuBe Outlet
Page A
H-4
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ceoenergv/tP-Haywara tine 2 core Drier E-Tube outlet
Page 5
H-5
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CeoenergyLP-Hayward tine 2 core Drier &Tube Outlet
Page 6
H-6
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. . :.. . .
. -.
.. .
Ceaenergv/LP.Hawara tine 2 core Orver E-TuBe ouuet
Page 7
H - 7
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- _
Geoenergv/LPHawrd Line 2 Core Dryer ETUbe outlet
Page 8
H-8
.~ ~~
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Ceoenergy/LP+award Line 2 Core D r i e r E-Tube Outlet
i
Page 9
H-9
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CeoenergvlLP-Haward Line 2 core Dryer E-Tube OuUet
I
Page 10
H- 10
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-
. . . . . . .~... . . .
-..
teoenergyn.PHavwara tine 2 core Dryer E-Tube Outlet
H-11
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ceaenergy/LP-HayWard Line 2 care m e r E-Tuue Outlet
Page 12
H- 12
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Geoenergylw.Hawara Line 2 Core Dryer E-Tune outlet
Page 13
H-13
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Ceoenergy/tP-Hawara tine 2 care over E-Tube outlet
Page l a
H- 14
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. . .
...
Ceoenergy/LP-Hayward Line 2 Core Ower E-Tube Outlet
_. - - _ _ . ... 5/14/961 83205 PMI
5/14/96 8:32:08 PM
<l’ld/QFI 11.Z7.09 D M I
5.1881 17.1811 294.1891 3.516
01 4.8831 17.0591 301.5141 3.516 -. - - , . , .. 51141961 8 3 2 1 1 PMI
5/14/961832:13 PMI
511U961 8:3215 PMI
51141961 8:3218 PMI
<l ld,9Fl 11.z7.19 D M I I
4.5781 17.121 324.7071 3.516
01 4.8831 17.121 340.5761 3.442 -. . -. _- , . - , ... , 51141961 8 3 2 2 1 PMI
51141961 8 3 2 2 4 PMI
<lld19CI 11.Z7.75 DMI I I -. . -. -_, -. _- . , .. , 5114/961 8 3 2 2 7 PMI
4.2721 17.2121 382.081 3.369 F l l d l C E l R.Z7.2< DMI , -. , _. --, -.-_.- . , ... ,
01 4.8831 17.2731 388.1841 3.394
Page 15
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Ceoenergv/LP-Hawrcl Line 2 Core Dryer E-Tube Outlet
Page 16
H-16
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GeoenergvlLP-Hawrd Line 2 Core Dryer E-Tube Ouuet
Page 17
H-17
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-- CeoenergylLP-Hayward
tine 2 core Dryer E-TUbe outlet
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-1 GeOenergylLP-HayWard
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GeOenergylLP-Hayward Line 2 core Dryer E-Tube outlet
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Ceoenergy LP-Hawar0 ..ne 2 core Dryer E-TuOe Ouner
5/14/961 841:56 PMI
5/14/961 8:41:57 PMI
VldlQRI X.Al.50 DMI
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5/14/9618:4239 PMI
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01 4.8831 16.9981 645.7521 3.564
01 4.8831 17.0591 642.091 3.564 5/14/961 8:42:43 PMI I I
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GeoenergWLP-Haward Line 2 core over E-Tube outlet
5/14/961 8 4 2 4 5 PMI
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4.2721 17.0291 622.5591 3.613
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01 4.5781 17.0591 528.5641 3.613
01 4.2721 16.9681 523.6821 3.589
01 3.9671 16.9371 518.7991 3.589
01 4.5781 17.0291 515.1371 3.589
01 4.8831 16.9981 510.2541 3.564
5114/9618:43:45 PMI I I
51141961 843:47 PMI I I
51141961 6 4 3 5 0 PMI I I 5114l961 6 4 3 5 1 PMI I I
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Geoenergyw-Hayward Line 2 core Dryer E-Tube Outlet
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51141961 84717 PMI 502 INOX 102 co
l m m i 11%) (uurn) 01 7.0191 17.395 312.5
51141961 8:4719 PMI ai 7.3241 17.3651 312.5
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3.271
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GeoenergyAP-Hayward Line 2 core Drier E-Tube outlet
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Gec%Iergy/LP-Haward Line 2 core ower E-Tube outlet
IlDDml 11%) Ilppm) 01 5.4931 17.3031 388.184
5/14/961 8:4935 PMI I
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5/14/96i 8:49:41 PMI
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Ceoenergy/LP.HayWard Line 2 Core Dryer €-Tune OuUet
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GeOenergyILP-Hawrd tine 2 core Dryer E-Tuoe Outlet
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GeoenergylLP-Hayward Line 2 core Drfer E-Tube Outlet
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Geoenergym-Hawara Line 2 Core Dryer E.Tube Outlet
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ceoenergy/LP-Havward tine 2 core Dryer E-Tube outlet
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Geoenergy/LP-Haward Line 2 core Orver E-Tube Outlet
5/14/961 8:59:37 PMI
5/14/96185940 PMI
5114196i 8 5 9 4 1 PMI
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0 1 a.5781 16.9371 938.7211 3.638
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01 3.9671 17.2421 410.1561 3.418 /14/961 9 0 1 5 1 PMI I I
0 1 a.8831 17.3031 404.0531 3.467
01 4.5781 17.1811 379.6391 3.54
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1 GeOenergyILP-HayWard
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01 4,8831 16.9071 483.3981 3.638
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Ceoenergvnwaward Line 2 Core Dryer €-Tune Outlet
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START 4- 1 4-2 4-3 4-4 4-5 4-6
CAL END CAL
4-7 4-8 4-9
4-1 0 4-1 1 4-1 2 4-13 4-1 4 4-1 5
19:47 Baseline
19:58 20:03 20:05
20:06:30 20:08:30 20:10:00 20:21 :oo
2096 20:28:30 20:30:30 20:40:00 20:44:00
20:46:00-20:52:00 -20:53:30
20:55 21:05
GeoenergylLP - Hayward Test 7 Run 1
Line 2 Core Dryer E - Tube Outlet 05/14/96
Core Field Intensity 50 kv
40.1 kv 30.3 kv
20 kv 10 kv
30 kv 10 kv 50 kv
1 cfm ,L Ammonia Injection 45 cfm 7 1.8 cfm 2.5 cfm
lost tube CAL
1 H- 50