Appendix J: Residential Bores - Laboratory Test ...

Appendix J: Residential Bores - Laboratory Test Certificates and

CoC Documentation

Certificate of Analysis

Coffey Environments Pty Ltd VIC

Level 1, 436 Johnston Street

Abbotsford

VIC 3067

Attention: Ian Newby

Report 566029-W

Project name DOD TINDAL

Project ID 754-MELEN199420 TASK 140.01

Received Date Oct 03, 2017

Client Sample ID 0990_PB059_170929

Sample Matrix Water

Eurofins | mgt Sample No. M17-Oc03107

Date Sampled Sep 29, 2017

Test/Reference LOR Unit

Perfluoroalkyl carboxylic acids (PFCAs)

Perfluorobutanoic acid (PFBA)N11 0.05 ug/L < 0.05

Perfluoropentanoic acid (PFPeA)N11 0.01 ug/L < 0.01

Perfluorohexanoic acid (PFHxA)N11 0.01 ug/L < 0.01

Perfluoroheptanoic acid (PFHpA)N11 0.01 ug/L < 0.01

Perfluorooctanoic acid (PFOA)N11 0.01 ug/L < 0.01

Perfluorononanoic acid (PFNA)N11 0.01 ug/L < 0.01

Perfluorodecanoic acid (PFDA)N11 0.01 ug/L < 0.01

Perfluoroundecanoic acid (PFUnA)N11 0.01 ug/L < 0.01

Perfluorododecanoic acid (PFDoA)N11 0.01 ug/L < 0.01

Perfluorotridecanoic acid (PFTrDA) 0.01 ug/L < 0.01

Perfluorotetradecanoic acid (PFTeDA)N11 0.01 ug/L < 0.01

13C4-PFBA (surr.) 1 % 118

13C5-PFPeA (surr.) 1 % 137

13C5-PFHxA (surr.) 1 % 150

13C4-PFHpA (surr.) 1 % 115

13C8-PFOA (surr.) 1 % 101

13C5-PFNA (surr.) 1 % 129

13C6-PFDA (surr.) 1 % 64

13C2-PFUnDA (surr.) 1 % 45

13C2-PFDoDA (surr.) 1 % 30

13C2-PFTeDA (surr.) 1 % INT

Perfluoroalkane sulfonamides (PFASAs)

Perfluorooctane sulfonamide (FOSA)N11 0.05 ug/L < 0.05

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA)N11 0.05 ug/L < 0.05

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA)N11 0.05 ug/L < 0.05

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol(N-MeFOSE)N11 0.05 ug/L < 0.05

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE)N11 0.05 ug/L < 0.05

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA)N11 0.05 ug/L < 0.05

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA)N11 0.05 ug/L < 0.05

13C8-FOSA (surr.) 1 % 77

D3-N-MeFOSA (surr.) 1 % 17

Date Reported: Oct 12, 2017

Eurofins | mgt 2-5 Kingston Town Close, Oakleigh, Victoria, Australia, 3166

ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 11

Report Number: 566029-W

NATA AccreditedAccreditation Number 1261Site Number 1254

Accredited for compliance with ISO/IEC 17025 – TestingThe results of the tests, calibrations and/ormeasurements included in this document are traceableto Australian/national standards.


Sample Matrix Water





D5-N-EtFOSA (surr.) 1 % INT

D7-N-MeFOSE (surr.) 1 % 30

D9-N-EtFOSE (surr.) 1 % 19

D5-N-EtFOSAA (surr.) 1 % 43

D3-N-MeFOSAA (surr.) 1 % 47

Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates (PFSAs)

Perfluorobutanesulfonic acid (PFBS)N11 0.01 ug/L < 0.01

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L < 0.01

Perfluorohexanesulfonic acid (PFHxS)N11 0.01 ug/L < 0.01

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L < 0.01

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L < 0.01

Perfluorodecanesulfonic acid (PFDS) 0.01 ug/L < 0.01

13C3-PFBS (surr.) 1 % 171

18O2-PFHxS (surr.) 1 % 132

13C8-PFOS (surr.) 1 % 95

n:2 Fluorotelomer sulfonic acids

1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS)N11 0.01 ug/L < 0.01

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS)N11 0.05 ug/L < 0.05

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS)N11 0.01 ug/L < 0.01

1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2FTS) 0.01 ug/L < 0.01

13C2-4:2 FTS (surr.) 1 % 129

13C2-6:2 FTS (surr.) 1 % 95

13C2-8:2 FTS (surr.) 1 % INT

PFASs Summations

Sum (PFHxS + PFOS) 0.01 ug/L < 0.01

Sum of US EPA PFAS (PFOS + PFOA) 0.01 ug/L < 0.01

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 0.01 ug/L < 0.01

Sum of WA DER PFAS (n=10) 0.05 ug/L < 0.05

Sum of PFASs (n=28) 0.1 ug/L < 0.1

Ammonia (as N) 0.01 mg/L < 0.01

Chloride 1 mg/L 45

Nitrate (as N) 0.02 mg/L 0.63

Sulphate (as SO4) 5 mg/L 13

Alkalinity (speciated)

Bicarbonate Alkalinity (as CaCO3) 20 mg/L 460

Carbonate Alkalinity (as CaCO3) 10 mg/L < 10

Alkali Metals

Calcium 0.5 mg/L 83

Magnesium 0.5 mg/L 48

Potassium 0.5 mg/L 4.5

Sodium 0.5 mg/L 34



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 11


Sample HistoryWhere samples are submitted/analysed over several days, the last date of extraction and analysis is reported.A recent review of our LIMS has resulted in the correction or clarification of some method identifications. Due to this, some of the method reference information on reports has changed. However,no substantive change has been made to our laboratory methods, and as such there is no change in the validity of current or previous results (regarding both quality and NATA accreditation).

If the date and time of sampling are not provided, the Laboratory will not be responsible for compromised results should testing be performed outside the recommended holding time.

Description Testing Site Extracted Holding Time

Per- and Polyfluorinated Alkyl Substances (PFASs)

Perfluoroalkyl carboxylic acids (PFCAs) Brisbane Oct 09, 2017 14 Day

- Method: LTM-ORG-2100 Per- and Polyfluorinated Alkyl Substances by LC-MS/MS

Perfluoroalkane sulfonamides (PFASAs) Brisbane Oct 09, 2017 14 Day


Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates (PFSAs) Brisbane Oct 09, 2017 14 Day


n:2 Fluorotelomer sulfonic acids Brisbane Oct 09, 2017 14 Day


Eurofins | mgt Suite B11

Ammonia (as N) Melbourne Oct 06, 2017 28 Day

- Method: APHA 4500-NH3 Ammonia Nitrogen by FIA

Chloride Melbourne Oct 06, 2017 28 Day

- Method: LTM-INO-4090 Chloride by Discrete Analyser

Nitrate (as N) Melbourne Oct 06, 2017 7 Day

- Method: APHA 4500-NO3 Nitrate Nitrogen by FIA

Sulphate (as SO4) Melbourne Oct 11, 2017 28 Day

- Method: LTM-INO-4110 Sulfate by Discrete Analyser

Alkalinity (speciated) Melbourne Oct 06, 2017 14 Day

- Method: APHA 2320 Alkalinity by Titration

Alkali Metals Melbourne Oct 06, 2017 180 Day

- Method: USEPA 6010 Alkali Metals



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 11


.Company Name: Coffey Environments Pty Ltd VIC Order No.: Received: Oct 3, 2017 8:33 AMAddress: Level 1, 436 Johnston Street Report #: 566029 Due: Oct 10, 2017

Abbotsford Phone: 03 8413 6900 Priority: 5 DayVIC 3067 Fax: Contact Name: Ian Newby

Project Name: DOD TINDELProject ID: 754-MELEN199420 TASK 140.01

Eurofins | mgt Analytical Services Manager : Mary Makarios

Sample Detail

Major A

nions

Major C

ations

Per- and P

olyfluorinated Alkyl S

ubstances(P

FA

Ss)

Melbourne Laboratory - NATA Site # 1254 & 14271 X X

Sydney Laboratory - NATA Site # 18217

Brisbane Laboratory - NATA Site # 20794 X

Perth Laboratory - NATA Site # 23736

External Laboratory

No Sample ID Sample Date SamplingTime

Matrix LAB ID

1 0990_PB059_170929

Sep 29, 2017 Water M17-Oc03107 X X X

Test Counts 1 1 1

ABN– 50 005 085 521e.mail : [email protected] : www.eurofins.com.au

MelbourneMelbourneMelbourneMelbourne2-5 Kingston Town CloseOakleigh VIC 3166Phone : +61 3 8564 5000NATA # 1261Site # 1254 & 14271

SydneySydneySydneySydneyUnit F3, Building F16 Mars RoadLane Cove West NSW 2066Phone : +61 2 9900 8400NATA # 1261 Site # 18217

BrisbaneBrisbaneBrisbaneBrisbane1/21 Smallwood PlaceMurarrie QLD 4172Phone : +61 7 3902 4600NATA # 1261 Site # 20794

PerthPerthPerthPerth2/91 Leach HighwayKewdale WA 6105Phone : +61 8 9251 9600NATA # 1261Site # 23736

Date Reported:Oct 12, 2017


ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 11


Internal Quality Control Review and Glossary

General

Holding Times

Units

Terms

QC - Acceptance Criteria

QC Data General Comments

1. Laboratory QC results for Method Blanks, Duplicates, Matrix Spikes, and Laboratory Control Samples are included in this QC report where applicable. Additional QC data may be available on

request.

2. All soil results are reported on a dry basis, unless otherwise stated.

3. All biota results are reported on a wet weight basis on the edible portion, unless otherwise stated.

4. Actual LORs are matrix dependant. Quoted LORs may be raised where sample extracts are diluted due to interferences.

5. Results are uncorrected for matrix spikes or surrogate recoveries except for PFAS compounds.

6. SVOC analysis on waters are performed on homogenised, unfiltered samples, unless noted otherwise.

7. Samples were analysed on an 'as received' basis.

8. This report replaces any interim results previously issued.

Please refer to 'Sample Preservation and Container Guide' for holding times (QS3001).

For samples received on the last day of holding time, notification of testing requirements should have been received at least 6 hours prior to sample receipt deadlines as stated on the Sample

Receipt Advice.

If the Laboratory did not receive the information in the required timeframe, and regardless of any other integrity issues, suitably qualified results may still be reported.

Holding times apply from the date of sampling, therefore compliance to these may be outside the laboratory's control.

**NOTE: pH duplicates are reported as a range NOT as RPD

mg/kg: milligrams per kilogram mg/L: milligrams per litre

ug/L: micrograms per litre ppm: Parts per million

ppb: Parts per billion %: Percentage

org/100mL: Organisms per 100 millilitres NTU: Nephelometric Turbidity Units

MPN/100mL: Most Probable Number of organisms per 100 millilitres

Dry Where a moisture has been determined on a solid sample the result is expressed on a dry basis.

LOR Limit of Reporting.

SPIKE Addition of the analyte to the sample and reported as percentage recovery.

RPD Relative Percent Difference between two Duplicate pieces of analysis.

LCS Laboratory Control Sample - reported as percent recovery.

CRM Certified Reference Material - reported as percent recovery.

Method Blank In the case of solid samples these are performed on laboratory certified clean sands and in the case of water samples these are performed on de-ionised water.

Surr - Surrogate The addition of a like compound to the analyte target and reported as percentage recovery.

Duplicate A second piece of analysis from the same sample and reported in the same units as the result to show comparison.

USEPA United States Environmental Protection Agency

APHA American Public Health Association

TCLP Toxicity Characteristic Leaching Procedure

COC Chain of Custody

SRA Sample Receipt Advice

QSM Quality Systems Manual ver 5.1 US Department of Defense

CP Client Parent - QC was performed on samples pertaining to this report

NCP Non-Client Parent - QC performed on samples not pertaining to this report, QC is representative of the sequence or batch that client samples were analysed within.

TEQ Toxic Equivalency Quotient

RPD Duplicates: Global RPD Duplicates Acceptance Criteria is 30% however the following acceptance guidelines are equally applicable:

Results <10 times the LOR : No Limit

Results between 10-20 times the LOR : RPD must lie between 0-50%

Results >20 times the LOR : RPD must lie between 0-30%

Surrogate Recoveries: Recoveries must lie between 50-150%-Phenols & PFASs

PFAS field samples that contain surrogate recoveries in excess of the QC limit designated in QSM 5.1 where no positive PFAS results have been reported have been reviewed and no data was

affected.

1. Where a result is reported as a less than (<), higher than the nominated LOR, this is due to either matrix interference, extract dilution required due to interferences or contaminant levels within

the sample, high moisture content or insufficient sample provided.

2. Duplicate data shown within this report that states the word "BATCH" is a Batch Duplicate from outside of your sample batch, but within the laboratory sample batch at a 1:10 ratio. The Parent

and Duplicate data shown is not data from your samples.

3. Organochlorine Pesticide analysis - where reporting LCS data, Toxaphene & Chlordane are not added to the LCS.

4. Organochlorine Pesticide analysis - where reporting Spike data, Toxaphene is not added to the Spike.

5. Total Recoverable Hydrocarbons - where reporting Spike & LCS data, a single spike of commercial Hydrocarbon products in the range of C12-C30 is added and it's Total Recovery is reported

in the C10-C14 cell of the Report.

6. pH and Free Chlorine analysed in the laboratory - Analysis on this test must begin within 30 minutes of sampling.Therefore laboratory analysis is unlikely to be completed within holding time.

Analysis will begin as soon as possible after sample receipt.

7. Recovery Data (Spikes & Surrogates) - where chromatographic interference does not allow the determination of Recovery the term "INT" appears against that analyte.

8. Polychlorinated Biphenyls are spiked only using Aroclor 1260 in Matrix Spikes and LCS.

9. For Matrix Spikes and LCS results a dash " -" in the report means that the specific analyte was not added to the QC sample.

10. Duplicate RPDs are calculated from raw analytical data thus it is possible to have two sets of data.



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 11


Quality Control Results

Test Units Result 1 AcceptanceLimits

PassLimits

QualifyingCode

Method Blank


Perfluorobutanoic acid (PFBA) ug/L < 0.05 0.05 Pass

Perfluoropentanoic acid (PFPeA) ug/L < 0.01 0.01 Pass

Perfluorohexanoic acid (PFHxA) ug/L < 0.01 0.01 Pass

Perfluoroheptanoic acid (PFHpA) ug/L < 0.01 0.01 Pass

Perfluorooctanoic acid (PFOA) ug/L < 0.01 0.01 Pass

Perfluorononanoic acid (PFNA) ug/L < 0.01 0.01 Pass

Perfluorodecanoic acid (PFDA) ug/L < 0.01 0.01 Pass

Perfluoroundecanoic acid (PFUnA) ug/L < 0.01 0.01 Pass

Perfluorododecanoic acid (PFDoA) ug/L < 0.01 0.01 Pass

Perfluorotridecanoic acid (PFTrDA) ug/L < 0.01 0.01 Pass

Perfluorotetradecanoic acid (PFTeDA) ug/L < 0.01 0.01 Pass

Method Blank


Perfluorooctane sulfonamide (FOSA) ug/L < 0.05 0.05 Pass

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA) ug/L < 0.05 0.05 Pass

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA) ug/L < 0.05 0.05 Pass

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol (N-MeFOSE) ug/L < 0.05 0.05 Pass

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE) ug/L < 0.05 0.05 Pass

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA) ug/L < 0.05 0.05 Pass

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA) ug/L < 0.05 0.05 Pass

Method Blank


Perfluorobutanesulfonic acid (PFBS) ug/L < 0.01 0.01 Pass

Perfluoropentanesulfonic acid (PFPeS) ug/L < 0.01 0.01 Pass

Perfluorohexanesulfonic acid (PFHxS) ug/L < 0.01 0.01 Pass

Perfluoroheptanesulfonic acid (PFHpS) ug/L < 0.01 0.01 Pass

Perfluorooctanesulfonic acid (PFOS) ug/L < 0.01 0.01 Pass

Perfluorodecanesulfonic acid (PFDS) ug/L < 0.01 0.01 Pass

Method Blank


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2 FTS) ug/L < 0.01 0.01 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) ug/L < 0.05 0.05 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) ug/L < 0.01 0.01 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2 FTS) ug/L < 0.01 0.01 Pass

Method Blank

Ammonia (as N) mg/L < 0.01 0.01 Pass

Chloride mg/L < 1 1 Pass

Nitrate (as N) mg/L < 0.02 0.02 Pass

Sulphate (as SO4) mg/L < 5 5 Pass

Method Blank


Bicarbonate Alkalinity (as CaCO3) mg/L < 20 20 Pass

Carbonate Alkalinity (as CaCO3) mg/L < 10 10 Pass

Method Blank

Alkali Metals

Calcium mg/L < 0.5 0.5 Pass

Magnesium mg/L < 0.5 0.5 Pass

Potassium mg/L < 0.5 0.5 Pass

Sodium mg/L < 0.5 0.5 Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 11



PassLimits

QualifyingCode

LCS - % Recovery


Perfluorobutanoic acid (PFBA) % 78 50-150 Pass

Perfluoropentanoic acid (PFPeA) % 95 50-150 Pass

Perfluorohexanoic acid (PFHxA) % 90 50-150 Pass

Perfluoroheptanoic acid (PFHpA) % 95 50-150 Pass

Perfluorooctanoic acid (PFOA) % 110 50-150 Pass

Perfluorononanoic acid (PFNA) % 109 50-150 Pass

Perfluorodecanoic acid (PFDA) % 86 50-150 Pass

Perfluoroundecanoic acid (PFUnA) % 105 50-150 Pass

Perfluorododecanoic acid (PFDoA) % 101 50-150 Pass

Perfluorotridecanoic acid (PFTrDA) % 121 50-150 Pass

Perfluorotetradecanoic acid (PFTeDA) % 107 50-150 Pass

LCS - % Recovery


Perfluorooctane sulfonamide (FOSA) % 85 50-150 Pass

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA) % 118 50-150 Pass

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA) % 111 50-150 Pass

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol (N-MeFOSE) % 135 50-150 Pass

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE) % 111 50-150 Pass

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA) % 108 50-150 Pass

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA) % 100 50-150 Pass

LCS - % Recovery


Perfluorobutanesulfonic acid (PFBS) % 64 50-150 Pass

Perfluoropentanesulfonic acid (PFPeS) % 93 50-150 Pass

Perfluorohexanesulfonic acid (PFHxS) % 84 50-150 Pass

Perfluoroheptanesulfonic acid (PFHpS) % 84 50-150 Pass

Perfluorooctanesulfonic acid (PFOS) % 87 50-150 Pass

Perfluorodecanesulfonic acid (PFDS) % 114 50-150 Pass

LCS - % Recovery


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2 FTS) % 83 50-150 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) % 106 50-150 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) % 51 50-150 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2 FTS) % 115 50-150 Pass

LCS - % Recovery

Ammonia (as N) % 95 70-130 Pass

Chloride % 125 70-130 Pass

Nitrate (as N) % 96 70-130 Pass

Sulphate (as SO4) % 124 70-130 Pass

LCS - % Recovery


Carbonate Alkalinity (as CaCO3) % 88 70-130 Pass

LCS - % Recovery

Alkali Metals

Calcium % 98 70-130 Pass

Magnesium % 104 70-130 Pass

Potassium % 96 70-130 Pass

Sodium % 115 70-130 Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 11


Test Lab Sample ID QASource Units Result 1 Acceptance

LimitsPass

LimitsQualifying

Code

Spike - % Recovery

Perfluoroalkyl carboxylic acids (PFCAs) Result 1

Perfluorobutanoic acid (PFBA) M17-Oc03152 NCP % 91 50-150 Pass

Perfluoropentanoic acid (PFPeA) M17-Oc03152 NCP % 114 50-150 Pass

Perfluorohexanoic acid (PFHxA) M17-Oc03152 NCP % 96 50-150 Pass

Perfluoroheptanoic acid (PFHpA) M17-Oc03152 NCP % 115 50-150 Pass

Perfluorooctanoic acid (PFOA) M17-Oc03152 NCP % 133 50-150 Pass

Perfluorononanoic acid (PFNA) M17-Oc03152 NCP % 108 50-150 Pass

Perfluorodecanoic acid (PFDA) M17-Oc03152 NCP % 104 50-150 Pass

Perfluoroundecanoic acid (PFUnA) M17-Oc03152 NCP % 121 50-150 Pass

Perfluorododecanoic acid (PFDoA) M17-Oc03152 NCP % 110 50-150 Pass

Perfluorotridecanoic acid (PFTrDA) M17-Oc03152 NCP % 106 50-150 Pass

Perfluorotetradecanoic acid(PFTeDA) M17-Oc03152 NCP % 120 50-150 Pass

Spike - % Recovery

Perfluoroalkane sulfonamides (PFASAs) Result 1

Perfluorooctane sulfonamide(FOSA) M17-Oc03152 NCP % 96 50-150 Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) M17-Oc03152 NCP % 116 50-150 Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) M17-Oc03152 NCP % 110 50-150 Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) M17-Oc03152 NCP % 121 50-150 Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) M17-Oc03152 NCP % 113 50-150 Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-Oc03152 NCP % 130 50-150 Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-Oc03152 NCP % 121 50-150 Pass

Spike - % Recovery

Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates (PFSAs) Result 1

Perfluorobutanesulfonic acid(PFBS) M17-Oc03152 NCP % 78 50-150 Pass

Perfluoropentanesulfonic acid(PFPeS) M17-Oc03152 NCP % 95 50-150 Pass

Perfluorohexanesulfonic acid(PFHxS) M17-Oc03152 NCP % 104 50-150 Pass

Perfluoroheptanesulfonic acid(PFHpS) M17-Oc03152 NCP % 97 50-150 Pass

Perfluorooctanesulfonic acid(PFOS) M17-Oc03152 NCP % 106 50-150 Pass

Perfluorodecanesulfonic acid(PFDS) M17-Oc03152 NCP % 112 50-150 Pass

Spike - % Recovery

n:2 Fluorotelomer sulfonic acids Result 1

1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-Oc03152 NCP % 99 50-150 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-Oc03152 NCP % 110 50-150 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-Oc03152 NCP % 52 50-150 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) M17-Oc03152 NCP % 110 50-150 Pass

Spike - % Recovery

Result 1



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 11



LimitsPass

LimitsQualifying

Code

Ammonia (as N) P17-Oc04002 NCP % 90 70-130 Pass

Chloride S17-Oc01852 NCP % 116 70-130 Pass

Nitrate (as N) M17-Oc01935 NCP % 92 70-130 Pass

Sulphate (as SO4) P17-Oc02333 NCP % 115 70-130 Pass

Spike - % Recovery

Alkali Metals Result 1

Calcium S17-Oc01851 NCP % 70 70-130 Pass

Magnesium S17-Oc01851 NCP % 101 70-130 Pass

Potassium M17-Se32574 NCP % 116 70-130 Pass

Sodium M17-Se32574 NCP % 120 70-130 Pass


LimitsPass

LimitsQualifying

Code

Duplicate

Perfluoroalkyl carboxylic acids (PFCAs) Result 1 Result 2 RPD

Perfluorobutanoic acid (PFBA) M17-Oc02460 NCP ug/L < 0.05 < 0.05 <1 30% Pass

Perfluoropentanoic acid (PFPeA) M17-Oc02460 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanoic acid (PFHxA) M17-Oc02460 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanoic acid (PFHpA) M17-Oc02460 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanoic acid (PFOA) M17-Oc02460 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorononanoic acid (PFNA) M17-Oc02460 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanoic acid (PFDA) M17-Oc02460 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroundecanoic acid (PFUnA) M17-Oc02460 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorododecanoic acid (PFDoA) M17-Oc02460 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) M17-Oc02460 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) M17-Oc02460 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate

Perfluoroalkane sulfonamides (PFASAs) Result 1 Result 2 RPD

Perfluorooctane sulfonamide(FOSA) M17-Oc02460 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) M17-Oc02460 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) M17-Oc02460 NCP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) M17-Oc02460 NCP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) M17-Oc02460 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-Oc02460 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-Oc02460 NCP ug/L < 0.05 < 0.05 <1 30% Pass

Duplicate

Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates (PFSAs) Result 1 Result 2 RPD

Perfluorobutanesulfonic acid(PFBS) M17-Oc02460 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoropentanesulfonic acid(PFPeS) M17-Oc02460 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanesulfonic acid(PFHxS) M17-Oc02460 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) M17-Oc02460 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanesulfonic acid(PFOS) M17-Oc02460 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanesulfonic acid(PFDS) M17-Oc02460 NCP ug/L < 0.01 < 0.01 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 11


Duplicate

n:2 Fluorotelomer sulfonic acids Result 1 Result 2 RPD

1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-Oc02460 NCP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-Oc02460 NCP ug/L < 0.05 < 0.05 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-Oc02460 NCP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) M17-Oc02460 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate

Result 1 Result 2 RPD

Ammonia (as N) P17-Oc04012 NCP mg/L < 0.01 < 0.01 <1 30% Pass

Chloride M17-Oc03107 CP mg/L 45 47 4.7 30% Pass

Nitrate (as N) P17-Oc04002 NCP mg/L 35 36 4.0 30% Pass

Sulphate (as SO4) M17-Oc03107 CP mg/L 13 13 2.8 30% Pass

Duplicate

Alkalinity (speciated) Result 1 Result 2 RPD

Bicarbonate Alkalinity (as CaCO3) M17-Oc03107 CP mg/L 460 470 3.0 30% Pass

Carbonate Alkalinity (as CaCO3) M17-Oc03107 CP mg/L < 10 < 10 <1 30% Pass

Duplicate

Alkali Metals Result 1 Result 2 RPD

Calcium M17-Oc03147 NCP mg/L 90 92 2.0 30% Pass

Magnesium M17-Oc03147 NCP mg/L 39 40 1.0 30% Pass

Potassium M17-Oc03147 NCP mg/L 1.5 1.6 2.0 30% Pass

Sodium M17-Oc03147 NCP mg/L 3.5 3.5 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 11


Comments

Sample IntegrityCustody Seals Intact (if used) N/A

Attempt to Chill was evident Yes

Sample correctly preserved Yes

Appropriate sample containers have been used Yes

Sample containers for volatile analysis received with minimal headspace Yes

Samples received within HoldingTime Yes

Some samples have been subcontracted No

Qualifier Codes/Comments

Code Description

N11

Isotope dilution is used for calibration of each native compound for which an exact labelled analogue is available (Isotope Dilution Quantitation). The isotopically labelledanalogues allow identification and recovery correction of the concentration of the associated native PFAS compounds. Where the native PFAS compound does not have labelledanalogue then the quantification is made using the Extracted Internal Standard Analyte with the closest retention time to the analyte and no recovery correction has been made(Internal Standard Quantitation).

Authorised By

Mary Makarios Analytical Services Manager

Alex Petridis Senior Analyst-Metal (VIC)

Jonathon Angell Senior Analyst-Organic (QLD)

Huong Le Senior Analyst-Inorganic (VIC)

Glenn Jackson

National Operations Manager

- Indicates Not Requested

* Indicates NATA accreditation does not cover the performance of this service

Measurement uncertainty of test data is available on request or please click here.Eurofins | mgt shall not be liable for loss, cost, damages or expenses incurred by the client, or any other person or company, resulting from the use of any information or interpretation given in this report. In no case shall Eurofins | mgt be liable for consequential damages including, but notlimited to, lost profits, damages for failure to meet deadlines and lost production arising from this report. This document shall not be reproduced except in full and relates only to the items tested. Unless indicated otherwise, the tests were performed on the samples as received.



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 11


http://www.eurofins.com.au/media/311687/reporting-measurement-uncertainty-of-chemical-and-microbiology-test-results.pdf




Abbotsford

VIC 3067


Report 566032-W


Project ID 754-MELEN199420


Client Sample ID 0990_PP063_171002

Sample Matrix Water


Date Sampled Oct 02, 2017





Perfluorohexanoic acid (PFHxA)N11 0.01 ug/L N090.02


Perfluorooctanoic acid (PFOA)N11 0.01 ug/L N09< 0.01







13C4-PFBA (surr.) 1 % 73

13C5-PFPeA (surr.) 1 % 98

13C5-PFHxA (surr.) 1 % 96

13C4-PFHpA (surr.) 1 % 113

13C8-PFOA (surr.) 1 % 100

13C5-PFNA (surr.) 1 % 84

13C6-PFDA (surr.) 1 % 64



13C2-PFTeDA (surr.) 1 % 13









13C8-FOSA (surr.) 1 % 67




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 11




Client Sample ID 0990_PP063_171002

Sample Matrix Water











Perfluorobutanesulfonic acid (PFBS)N11 0.01 ug/L 0.03

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L N090.03

Perfluorohexanesulfonic acid (PFHxS)N11 0.01 ug/L N090.15

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L N090.01

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N090.25


13C3-PFBS (surr.) 1 % 98

18O2-PFHxS (surr.) 1 % 86

13C8-PFOS (surr.) 1 % 86






13C2-4:2 FTS (surr.) 1 % 56

13C2-6:2 FTS (surr.) 1 % 54

13C2-8:2 FTS (surr.) 1 % INT

PFASs Summations

Sum (PFHxS + PFOS) 0.01 ug/L 0.4

Sum of US EPA PFAS (PFOS + PFOA) 0.01 ug/L 0.25

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 0.01 ug/L 0.4

Sum of WA DER PFAS (n=10) 0.05 ug/L 0.45

Sum of PFASs (n=28) 0.1 ug/L 0.49


Chloride 1 mg/L 19


Sulphate (as SO4) 5 mg/L < 5




Alkali Metals

Calcium 0.5 mg/L 83



Sodium 0.5 mg/L 5.2



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 11





























ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 11




Project Name: DOD TINDELProject ID: 754-MELEN199420


Sample Detail

Major A

nions

Major C

ations

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_PP063_171002

Oct 02, 2017 Water M17-Oc03141 X X X

Test Counts 1 1 1








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 11



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 11




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank





Method Blank




Method Blank

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 11



PassLimits

QualifyingCode

LCS - % Recovery













LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery





LCS - % Recovery



LCS - % Recovery

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 11



LimitsPass

LimitsQualifying

Code

Spike - % Recovery


Perfluorobutanoic acid (PFBA) B17-Se35410 NCP % 116 50-150 Pass

Perfluoropentanoic acid (PFPeA) B17-Se35410 NCP % 107 50-150 Pass

Perfluorohexanoic acid (PFHxA) B17-Se35410 NCP % 105 50-150 Pass

Perfluoroheptanoic acid (PFHpA) B17-Se35410 NCP % 113 50-150 Pass

Perfluorooctanoic acid (PFOA) B17-Se35410 NCP % 110 50-150 Pass

Perfluorononanoic acid (PFNA) B17-Se35410 NCP % 121 50-150 Pass

Perfluorodecanoic acid (PFDA) B17-Se35410 NCP % 114 50-150 Pass

Perfluoroundecanoic acid (PFUnA) B17-Se35410 NCP % 103 50-150 Pass

Perfluorododecanoic acid (PFDoA) B17-Se35410 NCP % 117 50-150 Pass

Perfluorotridecanoic acid (PFTrDA) B17-Se35410 NCP % 65 50-150 Pass

Perfluorotetradecanoic acid(PFTeDA) B17-Se35410 NCP % 107 50-150 Pass

Spike - % Recovery


Perfluorooctane sulfonamide(FOSA) B17-Se35410 NCP % 97 50-150 Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) B17-Se35410 NCP % 104 50-150 Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) B17-Se35410 NCP % 54 50-150 Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) B17-Se35410 NCP % 70 50-150 Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) B17-Se35410 NCP % 90 50-150 Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) B17-Se35410 NCP % 104 50-150 Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) B17-Se35410 NCP % 96 50-150 Pass

Spike - % Recovery


Perfluorobutanesulfonic acid(PFBS) B17-Se35410 NCP % 113 50-150 Pass

Perfluoropentanesulfonic acid(PFPeS) B17-Se35410 NCP % 120 50-150 Pass

Perfluorohexanesulfonic acid(PFHxS) B17-Se35410 NCP % 109 50-150 Pass

Perfluoroheptanesulfonic acid(PFHpS) B17-Se35410 NCP % 130 50-150 Pass

Perfluorooctanesulfonic acid(PFOS) B17-Se35410 NCP % 107 50-150 Pass

Perfluorodecanesulfonic acid(PFDS) B17-Se35410 NCP % 82 50-150 Pass

Spike - % Recovery


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) B17-Se35410 NCP % 76 50-150 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) B17-Se35410 NCP % 75 50-150 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) B17-Se35410 NCP % 78 50-150 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) B17-Se35410 NCP % 57 50-150 Pass

Spike - % Recovery

Result 1



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 11



LimitsPass

LimitsQualifying

Code


Chloride M17-Oc07407 NCP % 113 70-130 Pass


Sulphate (as SO4) M17-Oc04090 NCP % 129 70-130 Pass

Spike - % Recovery







LimitsPass

LimitsQualifying

Code

Duplicate


Perfluorobutanoic acid (PFBA) B17-Se35409 NCP ug/L < 0.05 < 0.05 <1 30% Pass

Perfluoropentanoic acid (PFPeA) B17-Se35409 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanoic acid (PFHxA) B17-Se35409 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanoic acid (PFHpA) B17-Se35409 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanoic acid (PFOA) B17-Se35409 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorononanoic acid (PFNA) B17-Se35409 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanoic acid (PFDA) B17-Se35409 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroundecanoic acid (PFUnA) B17-Se35409 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorododecanoic acid (PFDoA) B17-Se35409 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) B17-Se35409 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) B17-Se35409 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


Perfluorooctane sulfonamide(FOSA) B17-Se35409 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) B17-Se35409 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) B17-Se35409 NCP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) B17-Se35409 NCP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) B17-Se35409 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) B17-Se35409 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) B17-Se35409 NCP ug/L < 0.05 < 0.05 <1 30% Pass

Duplicate


Perfluorobutanesulfonic acid(PFBS) B17-Se35409 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoropentanesulfonic acid(PFPeS) B17-Se35409 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanesulfonic acid(PFHxS) B17-Se35409 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) B17-Se35409 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanesulfonic acid(PFOS) B17-Se35409 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanesulfonic acid(PFDS) B17-Se35409 NCP ug/L < 0.01 < 0.01 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 11


Duplicate


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) B17-Se35409 NCP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) B17-Se35409 NCP ug/L < 0.05 < 0.05 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) B17-Se35409 NCP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) B17-Se35409 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate



Chloride M17-Oc04156 NCP mg/L 100 92 12 30% Pass


Sulphate (as SO4) M17-Oc04156 NCP mg/L 31 29 6.7 30% Pass

Duplicate


Bicarbonate Alkalinity (as CaCO3) M17-Oc03099 NCP mg/L 42 49 15 30% Pass

Carbonate Alkalinity (as CaCO3) M17-Oc03099 NCP mg/L < 10 < 10 <1 30% Pass

Duplicate








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 11


Comments









Code DescriptionN09 Quantification of linear and branched isomers has been conducted as a single total response using the relative response factor for the corresponding linear/branched standard.

N11


Authorised By





Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 11






Abbotsford

VIC 3067


Report 566035-W





Sample Matrix Water
















13C4-PFBA (surr.) 1 % 99



13C4-PFHpA (surr.) 1 % 125

13C8-PFOA (surr.) 1 % 124

13C5-PFNA (surr.) 1 % 106

13C6-PFDA (surr.) 1 % 76












13C8-FOSA (surr.) 1 % 78




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 11





Sample Matrix Water





D5-N-EtFOSA (surr.) 1 % 23












13C3-PFBS (surr.) 1 % 98

18O2-PFHxS (surr.) 1 % 120

13C8-PFOS (surr.) 1 % 80






13C2-4:2 FTS (surr.) 1 % 110

13C2-6:2 FTS (surr.) 1 % 84

13C2-8:2 FTS (surr.) 1 % 42

PFASs Summations







Chloride 1 mg/L 22


Sulphate (as S) 5 mg/L < 5




Alkali Metals

Calcium 0.5 mg/L 85



Sodium 0.5 mg/L 8.6



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 11














Major Cations





Major Anions





Sulphate (as S) Melbourne Oct 06, 2017 28 Day






ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 11


.Company Name: Coffey Environments Pty Ltd VIC Order No.: Received: Oct 3, 2017 8:30 PMAddress: Level 1, 436 Johnston Street Report #: 566035 Due: Oct 11, 2017


Project Name: DOD TINDALProject ID: 754-MELEN199420


Sample Detail

Major A

nions

Major C

ations

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_PB062_171002

Oct 02, 2017 Water M17-Oc03142 X X X

Test Counts 1 1 1








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 11



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 11




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank




Sulphate (as S) mg/L < 5 5 Pass

Method Blank




Method Blank

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 11



PassLimits

QualifyingCode

LCS - % Recovery













LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery




Sulphate (as S) % 124 70-130 Pass

LCS - % Recovery



LCS - % Recovery

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 11



LimitsPass

LimitsQualifying

Code

Spike - % Recovery


Perfluorobutanoic acid (PFBA) M17-Oc03147 NCP % 120 50-150 Pass

Perfluoropentanoic acid (PFPeA) M17-Oc03147 NCP % 104 50-150 Pass

Perfluorohexanoic acid (PFHxA) M17-Oc03147 NCP % 120 50-150 Pass

Perfluoroheptanoic acid (PFHpA) M17-Oc03147 NCP % 98 50-150 Pass

Perfluorooctanoic acid (PFOA) M17-Oc03147 NCP % 115 50-150 Pass

Perfluorononanoic acid (PFNA) M17-Oc03147 NCP % 118 50-150 Pass

Perfluorodecanoic acid (PFDA) M17-Oc03147 NCP % 109 50-150 Pass

Perfluoroundecanoic acid (PFUnA) M17-Oc03147 NCP % 112 50-150 Pass

Perfluorododecanoic acid (PFDoA) M17-Oc03147 NCP % 111 50-150 Pass

Perfluorotridecanoic acid (PFTrDA) M17-Oc03147 NCP % 116 50-150 Pass

Perfluorotetradecanoic acid(PFTeDA) M17-Oc03147 NCP % 118 50-150 Pass

Spike - % Recovery


Perfluorooctane sulfonamide(FOSA) M17-Oc03147 NCP % 114 50-150 Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) M17-Oc03147 NCP % 107 50-150 Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) M17-Oc03147 NCP % 111 50-150 Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) M17-Oc03147 NCP % 102 50-150 Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) M17-Oc03147 NCP % 105 50-150 Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-Oc03147 NCP % 101 50-150 Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-Oc03147 NCP % 116 50-150 Pass

Spike - % Recovery


Perfluorobutanesulfonic acid(PFBS) M17-Oc03147 NCP % 95 50-150 Pass

Perfluoropentanesulfonic acid(PFPeS) M17-Oc03147 NCP % 96 50-150 Pass

Perfluorohexanesulfonic acid(PFHxS) M17-Oc03147 NCP % 118 50-150 Pass

Perfluoroheptanesulfonic acid(PFHpS) M17-Oc03147 NCP % 106 50-150 Pass

Perfluorooctanesulfonic acid(PFOS) M17-Oc03147 NCP % 99 50-150 Pass

Perfluorodecanesulfonic acid(PFDS) M17-Oc03147 NCP % 114 50-150 Pass

Spike - % Recovery


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-Oc03147 NCP % 102 50-150 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-Oc03147 NCP % 107 50-150 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-Oc03147 NCP % 73 50-150 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) M17-Oc03147 NCP % 85 50-150 Pass

Spike - % Recovery

Result 1



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 11



LimitsPass

LimitsQualifying

Code




Sulphate (as S) M17-Oc03142 CP % 96 70-130 Pass

Spike - % Recovery







LimitsPass

LimitsQualifying

Code

Duplicate


Perfluorobutanoic acid (PFBA) M17-Oc03142 CP ug/L < 0.05 < 0.05 <1 30% Pass

Perfluoropentanoic acid (PFPeA) M17-Oc03142 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanoic acid (PFHxA) M17-Oc03142 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanoic acid (PFHpA) M17-Oc03142 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanoic acid (PFOA) M17-Oc03142 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorononanoic acid (PFNA) M17-Oc03142 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanoic acid (PFDA) M17-Oc03142 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroundecanoic acid (PFUnA) M17-Oc03142 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorododecanoic acid (PFDoA) M17-Oc03142 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) M17-Oc03142 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) M17-Oc03142 CP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


Perfluorooctane sulfonamide(FOSA) M17-Oc03142 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) M17-Oc03142 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) M17-Oc03142 CP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) M17-Oc03142 CP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) M17-Oc03142 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-Oc03142 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-Oc03142 CP ug/L < 0.05 < 0.05 <1 30% Pass

Duplicate


Perfluorobutanesulfonic acid(PFBS) M17-Oc03142 CP ug/L 0.01 0.01 4.0 30% Pass

Perfluoropentanesulfonic acid(PFPeS) M17-Oc03142 CP ug/L 0.01 < 0.01 4.0 30% Pass

Perfluorohexanesulfonic acid(PFHxS) M17-Oc03142 CP ug/L 0.07 0.08 11 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) M17-Oc03142 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanesulfonic acid(PFOS) M17-Oc03142 CP ug/L 0.05 0.05 1.0 30% Pass

Perfluorodecanesulfonic acid(PFDS) M17-Oc03142 CP ug/L < 0.01 < 0.01 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 11


Duplicate


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-Oc03142 CP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-Oc03142 CP ug/L < 0.05 < 0.05 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-Oc03142 CP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) M17-Oc03142 CP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate



Chloride M17-Oc03107 NCP mg/L 45 47 4.7 30% Pass


Sulphate (as S) M17-Oc03107 NCP mg/L < 5 < 5 <1 30% Pass

Duplicate


Bicarbonate Alkalinity (as CaCO3) S17-Oc01854 NCP mg/L < 20 < 20 <1 30% Pass

Carbonate Alkalinity (as CaCO3) S17-Oc01854 NCP mg/L < 10 < 10 <1 30% Pass

Duplicate








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 11


Comments










N11


Authorised By





Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 11






Abbotsford

VIC 3067


Report 566036-W





Sample Matrix Water
















13C4-PFBA (surr.) 1 % 91



13C4-PFHpA (surr.) 1 % 117

13C8-PFOA (surr.) 1 % 115

13C5-PFNA (surr.) 1 % 91

13C6-PFDA (surr.) 1 % 63












13C8-FOSA (surr.) 1 % 46




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 11





Sample Matrix Water

















13C3-PFBS (surr.) 1 % 100

18O2-PFHxS (surr.) 1 % 114

13C8-PFOS (surr.) 1 % 63






13C2-4:2 FTS (surr.) 1 % 82

13C2-6:2 FTS (surr.) 1 % 71

13C2-8:2 FTS (surr.) 1 % 40

PFASs Summations







Chloride 1 mg/L 11


Sulphate (as S) 5 mg/L < 5




Alkali Metals

Calcium 0.5 mg/L 90



Sodium 0.5 mg/L 3.5



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 11














Major Cations





Major Anions





Sulphate (as S) Melbourne Oct 06, 2017 28 Day






ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 11


.Company Name: Coffey Environments Pty Ltd VIC Order No.: Received: Oct 3, 2017 8:33 PMAddress: Level 1, 436 Johnston Street Report #: 566036 Due: Oct 11, 2017


Project Name: TOT TINDALProject ID: 754-MELEN199420


Sample Detail

Major A

nions

Major C

ations

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_PB061_170930

Sep 30, 2017 Water M17-Oc03147 X X X

Test Counts 1 1 1








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 11



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 11




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank




Sulphate (as S) mg/L < 5 5 Pass

Method Blank




Method Blank

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 11



PassLimits

QualifyingCode

LCS - % Recovery













LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery




Sulphate (as S) % 124 70-130 Pass

LCS - % Recovery



LCS - % Recovery

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 11



LimitsPass

LimitsQualifying

Code

Spike - % Recovery


Perfluorobutanoic acid (PFBA) M17-Oc03147 CP % 120 50-150 Pass

Perfluoropentanoic acid (PFPeA) M17-Oc03147 CP % 104 50-150 Pass

Perfluorohexanoic acid (PFHxA) M17-Oc03147 CP % 120 50-150 Pass

Perfluoroheptanoic acid (PFHpA) M17-Oc03147 CP % 98 50-150 Pass

Perfluorooctanoic acid (PFOA) M17-Oc03147 CP % 115 50-150 Pass

Perfluorononanoic acid (PFNA) M17-Oc03147 CP % 118 50-150 Pass

Perfluorodecanoic acid (PFDA) M17-Oc03147 CP % 109 50-150 Pass

Perfluoroundecanoic acid (PFUnA) M17-Oc03147 CP % 112 50-150 Pass

Perfluorododecanoic acid (PFDoA) M17-Oc03147 CP % 111 50-150 Pass

Perfluorotridecanoic acid (PFTrDA) M17-Oc03147 CP % 116 50-150 Pass

Perfluorotetradecanoic acid(PFTeDA) M17-Oc03147 CP % 118 50-150 Pass

Spike - % Recovery


Perfluorooctane sulfonamide(FOSA) M17-Oc03147 CP % 114 50-150 Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) M17-Oc03147 CP % 107 50-150 Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) M17-Oc03147 CP % 111 50-150 Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) M17-Oc03147 CP % 102 50-150 Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) M17-Oc03147 CP % 105 50-150 Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-Oc03147 CP % 101 50-150 Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-Oc03147 CP % 116 50-150 Pass

Spike - % Recovery


Perfluorobutanesulfonic acid(PFBS) M17-Oc03147 CP % 95 50-150 Pass

Perfluoropentanesulfonic acid(PFPeS) M17-Oc03147 CP % 96 50-150 Pass

Perfluorohexanesulfonic acid(PFHxS) M17-Oc03147 CP % 118 50-150 Pass

Perfluoroheptanesulfonic acid(PFHpS) M17-Oc03147 CP % 106 50-150 Pass

Perfluorooctanesulfonic acid(PFOS) M17-Oc03147 CP % 99 50-150 Pass

Perfluorodecanesulfonic acid(PFDS) M17-Oc03147 CP % 114 50-150 Pass

Spike - % Recovery


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-Oc03147 CP % 102 50-150 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-Oc03147 CP % 107 50-150 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-Oc03147 CP % 73 50-150 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) M17-Oc03147 CP % 85 50-150 Pass

Spike - % Recovery

Result 1



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 11



LimitsPass

LimitsQualifying

Code




Sulphate (as S) P17-Oc02333 NCP % 115 70-130 Pass

Spike - % Recovery


Calcium M17-Oc03147 CP % 136 70-130 Fail Q08

Magnesium M17-Oc03147 CP % 131 70-130 Fail Q08

Potassium M17-Oc03147 CP % 128 70-130 Pass

Sodium M17-Oc03147 CP % 127 70-130 Pass


LimitsPass

LimitsQualifying

Code

Duplicate













Duplicate









Duplicate


Perfluorobutanesulfonic acid(PFBS) M17-Oc03142 NCP ug/L 0.01 0.01 4.0 30% Pass

Perfluoropentanesulfonic acid(PFPeS) M17-Oc03142 NCP ug/L 0.01 < 0.01 4.0 30% Pass

Perfluorohexanesulfonic acid(PFHxS) M17-Oc03142 NCP ug/L 0.07 0.08 11 30% Pass


Perfluorooctanesulfonic acid(PFOS) M17-Oc03142 NCP ug/L 0.05 0.05 1.0 30% Pass




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 11


Duplicate






Duplicate



Chloride M17-Oc03107 NCP mg/L 45 47 4.7 30% Pass


Sulphate (as S) M17-Oc03107 NCP mg/L < 5 < 5 <1 30% Pass

Duplicate


Bicarbonate Alkalinity (as CaCO3) S17-Oc01854 NCP mg/L < 20 < 20 <1 30% Pass

Carbonate Alkalinity (as CaCO3) S17-Oc01854 NCP mg/L < 10 < 10 <1 30% Pass

Duplicate


Calcium M17-Oc03147 CP mg/L 90 92 2.0 30% Pass

Magnesium M17-Oc03147 CP mg/L 39 40 1.0 30% Pass

Potassium M17-Oc03147 CP mg/L 1.5 1.6 2.0 30% Pass

Sodium M17-Oc03147 CP mg/L 3.5 3.5 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 11


Comments










N11


Q08The matrix spike recovery is outside of the recommended acceptance criteria. An acceptable recovery was obtained for the laboratory control sample indicating a sample matrixinterference

Authorised By





Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 11






Abbotsford

VIC 3067


Report 566039-W





0990_QCPB309_170930

0990_QCPB308_170930

Sample Matrix Water Water Water

Eurofins | mgt Sample No. M17-Oc03152 M17-Oc03153 M17-Oc03154

Date Sampled Sep 30, 2017 Sep 30, 2017 Sep 30, 2017



Perfluorobutanoic acid (PFBA)N11 0.05 ug/L < 0.05 < 0.05 < 0.05

Perfluoropentanoic acid (PFPeA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01

Perfluorohexanoic acid (PFHxA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01

Perfluoroheptanoic acid (PFHpA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01

Perfluorooctanoic acid (PFOA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01

Perfluorononanoic acid (PFNA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01

Perfluorodecanoic acid (PFDA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01

Perfluoroundecanoic acid (PFUnA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01

Perfluorododecanoic acid (PFDoA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01

Perfluorotridecanoic acid (PFTrDA) 0.01 ug/L < 0.01 < 0.01 < 0.01

Perfluorotetradecanoic acid (PFTeDA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01

13C4-PFBA (surr.) 1 % 103 107 102

13C5-PFPeA (surr.) 1 % 157 141 141

13C5-PFHxA (surr.) 1 % 172 153 149

13C4-PFHpA (surr.) 1 % 117 118 115

13C8-PFOA (surr.) 1 % 95 101 101

13C5-PFNA (surr.) 1 % 109 115 130

13C6-PFDA (surr.) 1 % 51 64 64

13C2-PFUnDA (surr.) 1 % 26 41 38

13C2-PFDoDA (surr.) 1 % 17 26 27

13C2-PFTeDA (surr.) 1 % INT INT INT


Perfluorooctane sulfonamide (FOSA)N11 0.05 ug/L < 0.05 < 0.05 < 0.05

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA)N11 0.05 ug/L < 0.05 < 0.05 < 0.05

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA)N11 0.05 ug/L < 0.05 < 0.05 < 0.05

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol(N-MeFOSE)N11 0.05 ug/L < 0.05 < 0.05 < 0.05

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE)N11 0.05 ug/L < 0.05 < 0.05 < 0.05

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA)N11 0.05 ug/L < 0.05 < 0.05 < 0.05

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA)N11 0.05 ug/L < 0.05 < 0.05 < 0.05

13C8-FOSA (surr.) 1 % 67 80 80

D3-N-MeFOSA (surr.) 1 % 11 17 14



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 11





0990_QCPB309_170930

0990_QCPB308_170930


Eurofins | mgt Sample No. M17-Oc03152 M17-Oc03153 M17-Oc03154

Date Sampled Sep 30, 2017 Sep 30, 2017 Sep 30, 2017



D5-N-EtFOSA (surr.) 1 % INT INT INT

D7-N-MeFOSE (surr.) 1 % 15 25 23

D9-N-EtFOSE (surr.) 1 % INT 15 14

D5-N-EtFOSAA (surr.) 1 % 28 40 38

D3-N-MeFOSAA (surr.) 1 % 38 43 45


Perfluorobutanesulfonic acid (PFBS)N11 0.01 ug/L < 0.01 < 0.01 < 0.01

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L < 0.01 < 0.01 < 0.01

Perfluorohexanesulfonic acid (PFHxS)N11 0.01 ug/L < 0.01 < 0.01 < 0.01

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L < 0.01 < 0.01 < 0.01

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L < 0.01 < 0.01 < 0.01

Perfluorodecanesulfonic acid (PFDS) 0.01 ug/L < 0.01 < 0.01 < 0.01

13C3-PFBS (surr.) 1 % 185 174 167

18O2-PFHxS (surr.) 1 % 131 131 132

13C8-PFOS (surr.) 1 % 74 93 91


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS)N11 0.01 ug/L < 0.01 < 0.01 < 0.01

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS)N11 0.05 ug/L < 0.05 < 0.05 < 0.05

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS)N11 0.01 ug/L < 0.01 < 0.01 < 0.01

1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2FTS) 0.01 ug/L < 0.01 < 0.01 < 0.01

13C2-4:2 FTS (surr.) 1 % INT 134 134

13C2-6:2 FTS (surr.) 1 % 95 88 93

13C2-8:2 FTS (surr.) 1 % INT INT INT

PFASs Summations

Sum (PFHxS + PFOS) 0.01 ug/L < 0.01 < 0.01 < 0.01

Sum of US EPA PFAS (PFOS + PFOA) 0.01 ug/L < 0.01 < 0.01 < 0.01

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 0.01 ug/L < 0.01 < 0.01 < 0.01

Sum of WA DER PFAS (n=10) 0.05 ug/L < 0.05 < 0.05 < 0.05

Sum of PFASs (n=28) 0.1 ug/L < 0.1 < 0.1 < 0.1

Chloride 1 mg/L 22 - 20

Sulphate (as SO4) 5 mg/L < 5 - < 5


Total Alkalinity (as CaCO3) 20 mg/L 360 - 350

Alkali Metals

Calcium 0.5 mg/L 62 - 68

Magnesium 0.5 mg/L 40 - 40

Potassium 0.5 mg/L 2.4 - 2.4

Sodium 0.5 mg/L 6.3 - 6.4



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 11
























ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 11






Sample Detail

Chloride

Sulphate (as S

O4)

Total A

lkalinity (as CaC

O3)

Alkali M

etals

Per- and P


ubstances(P

FA

Ss)

Melbourne Laboratory - NATA Site # 1254 & 14271 X X X X




External Laboratory


Matrix LAB ID

1 0990_PB060_170930

Sep 30, 2017 Water M17-Oc03152 X X X X X

2 0990_QCPB309_170930

Sep 30, 2017 Water M17-Oc03153 X

3 0990_QCPB308_170930

Sep 30, 2017 Water M17-Oc03154 X X X X X

Test Counts 2 2 2 2 3








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 11



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 11




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank



Method Blank


Total Alkalinity (as CaCO3) mg/L < 20 20 Pass

Method Blank

Alkali Metals





LCS - % Recovery





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 11



PassLimits

QualifyingCode











LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery



LCS - % Recovery


Total Alkalinity (as CaCO3) % 91 70-130 Pass

LCS - % Recovery

Alkali Metals






LimitsPass

LimitsQualifying

Code

Spike - % Recovery


Perfluorobutanoic acid (PFBA) M17-Oc03152 CP % 91 50-150 Pass

Perfluoropentanoic acid (PFPeA) M17-Oc03152 CP % 114 50-150 Pass

Perfluorohexanoic acid (PFHxA) M17-Oc03152 CP % 96 50-150 Pass

Perfluoroheptanoic acid (PFHpA) M17-Oc03152 CP % 115 50-150 Pass

Perfluorooctanoic acid (PFOA) M17-Oc03152 CP % 133 50-150 Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 11



LimitsPass

LimitsQualifying

Code

Perfluorononanoic acid (PFNA) M17-Oc03152 CP % 108 50-150 Pass

Perfluorodecanoic acid (PFDA) M17-Oc03152 CP % 104 50-150 Pass

Perfluoroundecanoic acid (PFUnA) M17-Oc03152 CP % 121 50-150 Pass

Perfluorododecanoic acid (PFDoA) M17-Oc03152 CP % 110 50-150 Pass

Perfluorotridecanoic acid (PFTrDA) M17-Oc03152 CP % 106 50-150 Pass

Perfluorotetradecanoic acid(PFTeDA) M17-Oc03152 CP % 120 50-150 Pass

Spike - % Recovery


Perfluorooctane sulfonamide(FOSA) M17-Oc03152 CP % 96 50-150 Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) M17-Oc03152 CP % 116 50-150 Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) M17-Oc03152 CP % 110 50-150 Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) M17-Oc03152 CP % 121 50-150 Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) M17-Oc03152 CP % 113 50-150 Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-Oc03152 CP % 130 50-150 Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-Oc03152 CP % 121 50-150 Pass

Spike - % Recovery


Perfluorobutanesulfonic acid(PFBS) M17-Oc03152 CP % 78 50-150 Pass

Perfluoropentanesulfonic acid(PFPeS) M17-Oc03152 CP % 95 50-150 Pass

Perfluorohexanesulfonic acid(PFHxS) M17-Oc03152 CP % 104 50-150 Pass

Perfluoroheptanesulfonic acid(PFHpS) M17-Oc03152 CP % 97 50-150 Pass

Perfluorooctanesulfonic acid(PFOS) M17-Oc03152 CP % 106 50-150 Pass

Perfluorodecanesulfonic acid(PFDS) M17-Oc03152 CP % 112 50-150 Pass

Spike - % Recovery


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-Oc03152 CP % 99 50-150 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-Oc03152 CP % 110 50-150 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-Oc03152 CP % 52 50-150 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) M17-Oc03152 CP % 110 50-150 Pass

Spike - % Recovery

Result 1

Chloride S17-Oc01852 NCP % 116 70-130 Pass


Spike - % Recovery


Calcium M17-Oc03147 NCP % 136 70-130 Fail Q08

Magnesium M17-Oc03147 NCP % 131 70-130 Fail Q08

Potassium M17-Oc03147 NCP % 128 70-130 Pass

Sodium M17-Oc03147 NCP % 127 70-130 Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 11



LimitsPass

LimitsQualifying

Code

Duplicate













Duplicate









Duplicate








Duplicate








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 11


Duplicate


Chloride B17-Se32562 NCP mg/L 3500 3400 <1 30% Pass

Sulphate (as SO4) M17-Oc04726 NCP mg/L 390 370 5.3 30% Pass

Duplicate


Total Alkalinity (as CaCO3) M17-Oc03152 CP mg/L 360 340 5.0 30% Pass

Duplicate








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 11


Comments









Code Description

N11



Authorised By





Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 11






Abbotsford

VIC 3067


Report 566224-W





Sample Matrix Water
















13C4-PFBA (surr.) 1 % 110

13C5-PFPeA (surr.) 1 % 181

13C5-PFHxA (surr.) 1 % 139

13C4-PFHpA (surr.) 1 % 151

13C8-PFOA (surr.) 1 % 153

13C5-PFNA (surr.) 1 % 124

13C6-PFDA (surr.) 1 % 85












13C8-FOSA (surr.) 1 % 88




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 11





Sample Matrix Water

















13C3-PFBS (surr.) 1 % 114

18O2-PFHxS (surr.) 1 % 145

13C8-PFOS (surr.) 1 % 74



1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS)N11 0.05 ug/L 0.31



13C2-4:2 FTS (surr.) 1 % INT

13C2-6:2 FTS (surr.) 1 % 147

13C2-8:2 FTS (surr.) 1 % INT

PFASs Summations






Chloride 1 mg/L 72



Total Alkalinity (as CaCO3) 20 mg/L 670

Alkali Metals

Calcium 0.5 mg/L 58


Potassium 0.5 mg/L 10

Sodium 0.5 mg/L 28



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 11
























ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 11






Sample Detail

Chloride

Sulphate (as S

O4)

Total A

lkalinity (as CaC

O3)

Alkali M

etals

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_PB064_171002

Oct 02, 2017 Water M17-Oc04329 X X X X X









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 11



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 11




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank



Method Blank



Method Blank

Alkali Metals





LCS - % Recovery





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 11



PassLimits

QualifyingCode











LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery



LCS - % Recovery



LCS - % Recovery

Alkali Metals






LimitsPass

LimitsQualifying

Code

Spike - % Recovery


Perfluorobutanoic acid (PFBA) B17-Oc11112 NCP % 100 50-150 Pass

Perfluoropentanoic acid (PFPeA) B17-Oc11112 NCP % 90 50-150 Pass

Perfluorohexanoic acid (PFHxA) B17-Oc11112 NCP % 98 50-150 Pass

Perfluoroheptanoic acid (PFHpA) B17-Oc11112 NCP % 100 50-150 Pass

Perfluorooctanoic acid (PFOA) B17-Oc11112 NCP % 97 50-150 Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 11



LimitsPass

LimitsQualifying

Code

Perfluorononanoic acid (PFNA) B17-Oc11112 NCP % 117 50-150 Pass

Perfluorodecanoic acid (PFDA) B17-Oc11112 NCP % 108 50-150 Pass

Perfluoroundecanoic acid (PFUnA) B17-Oc11112 NCP % 97 50-150 Pass

Perfluorododecanoic acid (PFDoA) B17-Oc11112 NCP % 87 50-150 Pass

Perfluorotridecanoic acid (PFTrDA) B17-Oc11112 NCP % 99 50-150 Pass

Perfluorotetradecanoic acid(PFTeDA) B17-Oc11112 NCP % 76 50-150 Pass

Spike - % Recovery


Perfluorooctane sulfonamide(FOSA) B17-Oc11112 NCP % 94 50-150 Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) B17-Oc11112 NCP % 91 50-150 Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) B17-Oc11112 NCP % 87 50-150 Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) B17-Oc11112 NCP % 72 50-150 Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) B17-Oc11112 NCP % 82 50-150 Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) B17-Oc11112 NCP % 83 50-150 Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) B17-Oc11112 NCP % 96 50-150 Pass

Spike - % Recovery


Perfluorobutanesulfonic acid(PFBS) B17-Oc11112 NCP % 103 50-150 Pass

Perfluoropentanesulfonic acid(PFPeS) B17-Oc11112 NCP % 83 50-150 Pass

Perfluorohexanesulfonic acid(PFHxS) B17-Oc11112 NCP % 93 50-150 Pass

Perfluoroheptanesulfonic acid(PFHpS) B17-Oc11112 NCP % 92 50-150 Pass

Perfluorooctanesulfonic acid(PFOS) B17-Oc11112 NCP % 100 50-150 Pass

Perfluorodecanesulfonic acid(PFDS) B17-Oc11112 NCP % 56 50-150 Pass

Spike - % Recovery


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) B17-Oc11112 NCP % 100 50-150 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) B17-Oc11112 NCP % 129 50-150 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) B17-Oc11112 NCP % 61 50-150 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) B17-Oc11112 NCP % 98 50-150 Pass

Spike - % Recovery

Result 1



Spike - % Recovery

Alkalinity (speciated) Result 1

Total Alkalinity (as CaCO3) P17-Oc05212 NCP % 112 70-130 Pass

Spike - % Recovery




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 11



LimitsPass

LimitsQualifying

Code

Calcium M17-Oc05322 NCP % 115 70-130 Pass

Magnesium M17-Oc05322 NCP % 113 70-130 Pass

Potassium M17-Oc05322 NCP % 108 70-130 Pass

Sodium M17-Oc05322 NCP % 113 70-130 Pass


LimitsPass

LimitsQualifying

Code

Duplicate













Duplicate









Duplicate










ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 11


Duplicate






Duplicate


Chloride M17-Oc04329 CP mg/L 72 71 <1 30% Pass

Sulphate (as SO4) M17-Oc04329 CP mg/L < 5 < 5 <1 30% Pass

Duplicate


Total Alkalinity (as CaCO3) M17-Oc04329 CP mg/L 670 650 2.0 30% Pass

Duplicate




Potassium M17-Oc05322 NCP mg/L 230 230 3.0 30% Pass

Sodium M17-Oc05322 NCP mg/L 1500 1600 4.0 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 11


Comments









Code Description

N11


Authorised By





Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 11






Abbotsford

VIC 3067


Report 567120-W-V2

Project name 754-MELEN199420



Sample Matrix Water

Eurofins | mgt Sample No. B17-Oc11817

Date Sampled Aug 31, 2017














13C4-PFBA (surr.) 1 % 119

13C5-PFPeA (surr.) 1 % 160

13C5-PFHxA (surr.) 1 % 167

13C4-PFHpA (surr.) 1 % 138

13C8-PFOA (surr.) 1 % 119

13C5-PFNA (surr.) 1 % 120

13C6-PFDA (surr.) 1 % 73












13C8-FOSA (surr.) 1 % 63



First Reported: Oct 16, 2017


Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172

ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 1 of 11

Report Number: 567120-W-V2




Sample Matrix Water

Eurofins | mgt Sample No. B17-Oc11817















13C3-PFBS (surr.) 1 % 143

18O2-PFHxS (surr.) 1 % 126

13C8-PFOS (surr.) 1 % 84






13C2-4:2 FTS (surr.) 1 % INT

13C2-6:2 FTS (surr.) 1 % 123

13C2-8:2 FTS (surr.) 1 % 67

PFASs Summations









ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 2 of 11

















ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 3 of 11



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.


















ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 4 of 11




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






LCS - % Recovery













LCS - % Recovery





ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 5 of 11



PassLimits

QualifyingCode








LCS - % Recovery








LCS - % Recovery







LimitsPass

LimitsQualifying

Code

Spike - % Recovery


Perfluorobutanoic acid (PFBA) B17-Oc12761 NCP % 94 50-150 Pass

Perfluoropentanoic acid (PFPeA) B17-Oc12761 NCP % 119 50-150 Pass

Perfluorohexanoic acid (PFHxA) B17-Oc12761 NCP % 98 50-150 Pass

Perfluoroheptanoic acid (PFHpA) B17-Oc12761 NCP % 105 50-150 Pass

Perfluorooctanoic acid (PFOA) B17-Oc12761 NCP % 108 50-150 Pass

Perfluorononanoic acid (PFNA) B17-Oc12761 NCP % 107 50-150 Pass

Perfluorodecanoic acid (PFDA) B17-Oc12761 NCP % 93 50-150 Pass

Perfluoroundecanoic acid (PFUnA) B17-Oc12761 NCP % 87 50-150 Pass

Perfluorododecanoic acid (PFDoA) B17-Oc12761 NCP % 91 50-150 Pass

Perfluorotridecanoic acid (PFTrDA) B17-Oc12761 NCP % 113 50-150 Pass

Perfluorotetradecanoic acid(PFTeDA) B17-Oc12761 NCP % 104 50-150 Pass

Spike - % Recovery


Perfluorooctane sulfonamide(FOSA) B17-Oc12761 NCP % 90 50-150 Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) B17-Oc12761 NCP % 104 50-150 Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) B17-Oc12761 NCP % 127 50-150 Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) B17-Oc12761 NCP % 112 50-150 Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) B17-Oc12761 NCP % 95 50-150 Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) B17-Oc12761 NCP % 93 50-150 Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) B17-Oc12761 NCP % 90 50-150 Pass

Spike - % Recovery





ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 6 of 11



LimitsPass

LimitsQualifying

Code

Perfluorobutanesulfonic acid(PFBS) B17-Oc12761 NCP % 83 50-150 Pass

Perfluoropentanesulfonic acid(PFPeS) B17-Oc12761 NCP % 105 50-150 Pass

Perfluorohexanesulfonic acid(PFHxS) B17-Oc12761 NCP % 95 50-150 Pass

Perfluoroheptanesulfonic acid(PFHpS) B17-Oc12761 NCP % 75 50-150 Pass

Perfluorooctanesulfonic acid(PFOS) B17-Oc12761 NCP % 91 50-150 Pass

Perfluorodecanesulfonic acid(PFDS) B17-Oc12761 NCP % 101 50-150 Pass

Spike - % Recovery


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) B17-Oc12761 NCP % 101 50-150 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) B17-Oc12761 NCP % 99 50-150 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) B17-Oc12761 NCP % 96 50-150 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) B17-Oc12761 NCP % 86 50-150 Pass

Spike - % Recovery


Perfluorobutanoic acid (PFBA) B17-Oc11819 CP % 94 50-150 Pass

Perfluoropentanoic acid (PFPeA) B17-Oc11819 CP % 127 50-150 Pass

Perfluorohexanoic acid (PFHxA) B17-Oc11819 CP % 82 50-150 Pass

Perfluoroheptanoic acid (PFHpA) B17-Oc11819 CP % 100 50-150 Pass

Perfluorooctanoic acid (PFOA) B17-Oc11819 CP % 118 50-150 Pass

Perfluorononanoic acid (PFNA) B17-Oc11819 CP % 104 50-150 Pass

Perfluorodecanoic acid (PFDA) B17-Oc11819 CP % 89 50-150 Pass

Perfluoroundecanoic acid (PFUnA) B17-Oc11819 CP % 71 50-150 Pass

Perfluorododecanoic acid (PFDoA) B17-Oc11819 CP % 66 50-150 Pass

Perfluorotridecanoic acid (PFTrDA) B17-Oc11819 CP % 117 50-150 Pass

Perfluorotetradecanoic acid(PFTeDA) B17-Oc11819 CP % 94 50-150 Pass

Spike - % Recovery


Perfluorooctane sulfonamide(FOSA) B17-Oc11819 CP % 72 50-150 Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) B17-Oc11819 CP % 90 50-150 Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) B17-Oc11819 CP % 107 50-150 Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) B17-Oc11819 CP % 85 50-150 Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) B17-Oc11819 CP % 75 50-150 Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) B17-Oc11819 CP % 83 50-150 Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) B17-Oc11819 CP % 76 50-150 Pass

Spike - % Recovery


Perfluorobutanesulfonic acid(PFBS) B17-Oc11819 CP % 79 50-150 Pass




ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 7 of 11



LimitsPass

LimitsQualifying

Code

Perfluoropentanesulfonic acid(PFPeS) B17-Oc11819 CP % 90 50-150 Pass

Perfluorohexanesulfonic acid(PFHxS) B17-Oc11819 CP % 89 50-150 Pass

Perfluoroheptanesulfonic acid(PFHpS) B17-Oc11819 CP % 77 50-150 Pass

Perfluorooctanesulfonic acid(PFOS) B17-Oc11819 CP % 85 50-150 Pass

Perfluorodecanesulfonic acid(PFDS) B17-Oc11819 CP % 80 50-150 Pass

Spike - % Recovery


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) B17-Oc11819 CP % 97 50-150 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) B17-Oc11819 CP % 111 50-150 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) B17-Oc11819 CP % 96 50-150 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) B17-Oc11819 CP % 62 50-150 Pass


LimitsPass

LimitsQualifying

Code

Duplicate


Perfluorobutanoic acid (PFBA) B17-Oc12760 NCP ug/L < 0.05 < 0.05 <1 30% Pass

Perfluoropentanoic acid (PFPeA) B17-Oc12760 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanoic acid (PFHxA) B17-Oc12760 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanoic acid (PFHpA) B17-Oc12760 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanoic acid (PFOA) B17-Oc12760 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorononanoic acid (PFNA) B17-Oc12760 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanoic acid (PFDA) B17-Oc12760 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroundecanoic acid (PFUnA) B17-Oc12760 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorododecanoic acid (PFDoA) B17-Oc12760 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) B17-Oc12760 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) B17-Oc12760 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


Perfluorooctane sulfonamide(FOSA) B17-Oc12760 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) B17-Oc12760 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) B17-Oc12760 NCP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) B17-Oc12760 NCP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) B17-Oc12760 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) B17-Oc12760 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) B17-Oc12760 NCP ug/L < 0.05 < 0.05 <1 30% Pass




ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 8 of 11


Duplicate


Perfluorobutanesulfonic acid(PFBS) B17-Oc12760 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoropentanesulfonic acid(PFPeS) B17-Oc12760 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanesulfonic acid(PFHxS) B17-Oc12760 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) B17-Oc12760 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanesulfonic acid(PFOS) B17-Oc12760 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanesulfonic acid(PFDS) B17-Oc12760 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) B17-Oc12760 NCP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) B17-Oc12760 NCP ug/L < 0.05 < 0.05 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) B17-Oc12760 NCP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) B17-Oc12760 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


Perfluorobutanoic acid (PFBA) B17-Oc11818 CP ug/L < 0.05 < 0.05 <1 30% Pass

Perfluoropentanoic acid (PFPeA) B17-Oc11818 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanoic acid (PFHxA) B17-Oc11818 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanoic acid (PFHpA) B17-Oc11818 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanoic acid (PFOA) B17-Oc11818 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorononanoic acid (PFNA) B17-Oc11818 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanoic acid (PFDA) B17-Oc11818 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroundecanoic acid (PFUnA) B17-Oc11818 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorododecanoic acid (PFDoA) B17-Oc11818 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) B17-Oc11818 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) B17-Oc11818 CP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


Perfluorooctane sulfonamide(FOSA) B17-Oc11818 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) B17-Oc11818 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) B17-Oc11818 CP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) B17-Oc11818 CP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) B17-Oc11818 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) B17-Oc11818 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) B17-Oc11818 CP ug/L < 0.05 < 0.05 <1 30% Pass




ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 9 of 11


Duplicate


Perfluorobutanesulfonic acid(PFBS) B17-Oc11818 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoropentanesulfonic acid(PFPeS) B17-Oc11818 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanesulfonic acid(PFHxS) B17-Oc11818 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) B17-Oc11818 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanesulfonic acid(PFOS) B17-Oc11818 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanesulfonic acid(PFDS) B17-Oc11818 CP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) B17-Oc11818 CP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) B17-Oc11818 CP ug/L < 0.05 < 0.05 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) B17-Oc11818 CP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) B17-Oc11818 CP ug/L < 0.01 < 0.01 <1 30% Pass




ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 10 of 11


Comments

Split Report










N11


Authorised By



Glenn Jackson








ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 11 of 11





3G Marine Pde

Abbotsford

VIC 3067


Report 542977-W

Project name DOD TINDAl

Project ID 754_MELEN199420

Received Date Apr 20, 2017

Client Sample ID TDL_2145URALLA

Sample Matrix Water

Eurofins | mgt Sample No. B17-Ap15804

Date Sampled Apr 13, 2017



Perfluorobutanoic acid (PFBA) 0.05 ug/L < 0.05

13C4-PFBA (surr.) 1 % 58

Perfluoropentanoic acid (PFPeA) 0.01 ug/L < 0.01


Perfluorohexanoic acid (PFHxA) 0.01 ug/L < 0.01


Perfluoroheptanoic acid (PFHpA) 0.01 ug/L < 0.01

13C4-PFHpA (surr.) 1 % 65

Perfluorooctanoic acid (PFOA) 0.01 ug/L < 0.01

13C8-PFOA (surr.) 1 % 63

Perfluorononanoic acid (PFNA) 0.01 ug/L < 0.01

13C5-PFNA (surr.) 1 % 58

Perfluorodecanoic acid (PFDA) 0.01 ug/L < 0.01

13C6-PFDA (surr.) 1 % 41

Perfluoroundecanoic acid (PFUnA) 0.01 ug/L < 0.01


Perfluorododecanoic acid (PFDoA) 0.01 ug/L < 0.01



Perfluorotetradecanoic acid (PFTeDA) 0.01 ug/L < 0.01



Perfluorooctane sulfonamide (FOSA) 0.05 ug/L < 0.05

13C8-FOSA (surr.) 1 % 40

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA) 0.05 ug/L < 0.05


N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA) 0.05 ug/L < 0.05


2-(N-methylperfluoro-1-octane sulfonamido)-ethanol(N-MeFOSE) 0.05 ug/L < 0.05


2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE) 0.05 ug/L < 0.05


N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA) 0.05 ug/L < 0.05

Date Reported: May 04, 2017


ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 1 of 10




emma.delborrello

Rectangle

Client Sample ID TDL_2145URALLA

Sample Matrix Water






N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA) 0.05 ug/L < 0.05



Perfluorobutanesulfonic acid (PFBS) 0.01 ug/L < 0.01

13C3-PFBS (surr.) 1 % 56


Perfluorohexanesulfonic acid (PFHxS) 0.01 ug/L < 0.01




13C8-PFOS (surr.) 1 % 39



1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2 FTS) 0.01 ug/L < 0.01

13C2-4:2 FTS (surr.) 1 % 108

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) 0.05 ug/L < 0.05

13C2-6:2 FTS (surr.) 1 % 84

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) 0.01 ug/L < 0.01

13C2-8:2 FTS (surr.) 1 % 45




ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 2 of 10


emma.delborrello

Rectangle





Perfluoroalkyl carboxylic acids (PFCAs) Brisbane May 03, 2017 14 Day


Perfluoroalkane sulfonamides (PFASAs) Brisbane May 03, 2017 14 Day


Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates (PFSAs) Brisbane May 03, 2017 14 Day


n:2 Fluorotelomer sulfonic acids Brisbane May 03, 2017 14 Day




ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 3 of 10


.Company Name: Coffey Environments Pty Ltd VIC Order No.: Received: Apr 20, 2017 9:00 AMAddress: 3G Marine Pde Report #: 542977 Due: Apr 28, 2017


Project Name: DOD TINDAlProject ID: 754_MELEN199420


Sample Detail

Per- and P


ubstances(P

FA

Ss)

Melbourne Laboratory - NATA Site # 1254 & 14271




External Laboratory


Matrix LAB ID

1 TDL_2145URALLA

Apr 13, 2017 Water B17-Ap15804 X

Test Counts 1






Date Reported:May 04, 2017


ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 4 of 10


emma.delborrello

Rectangle


General

Holding Times

Units

Terms




request.



4. Results are uncorrected for matrix spikes or surrogate recoveries.


6. Samples were analysed on an 'as received' basis. 7. This report replaces any interim results previously issued.



Receipt Advice.




mg/kg: milligrams per Kilogram mg/l: milligrams per litre

ug/l: micrograms per litre ppm: Parts per million


org/100ml: Organisms per 100 millilitres NTU: Nephelometric Turbidity Units






LCS Laboratory Control Sample - reported as percent recovery

CRM Certified Reference Material - reported as percent recovery

Method Blank In the case of solid samples these are performed on laboratory certified clean sands.

In the case of water samples these are performed on de-ionised water.



Batch Duplicate A second piece of analysis from a sample outside of the clients batch of samples but run within the laboratory batch of analysis.

Batch SPIKE Spike recovery reported on a sample from outside of the clients batch of samples but run within the laboratory batch of analysis.







NCP Non-Client Parent - QC performed on samples not pertaining to this report, QC is representative of the sequence or batch that client samples were analysed within






Surrogate Recoveries: Recoveries must lie between 50-150%-Phenols & PFASs 20-130%

















ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 5 of 10




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






LCS - % Recovery













LCS - % Recovery




ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 6 of 10



PassLimits

QualifyingCode








LCS - % Recovery








LCS - % Recovery







LimitsPass

LimitsQualifying

Code

Spike - % Recovery


Perfluorobutanoic acid (PFBA) B17-Ap19703 NCP % 118 50-150 Pass

Perfluoropentanoic acid (PFPeA) B17-Ap19703 NCP % 124 50-150 Pass

Perfluorohexanoic acid (PFHxA) B17-Ap19703 NCP % 113 50-150 Pass

Perfluoroheptanoic acid (PFHpA) B17-Ap19703 NCP % 114 50-150 Pass

Perfluorooctanoic acid (PFOA) B17-Ap19703 NCP % 112 50-150 Pass

Perfluorononanoic acid (PFNA) B17-Ap19703 NCP % 110 50-150 Pass

Perfluorodecanoic acid (PFDA) B17-Ap19703 NCP % 113 50-150 Pass

Perfluoroundecanoic acid (PFUnA) B17-Ap19703 NCP % 115 50-150 Pass

Perfluorododecanoic acid (PFDoA) B17-Ap19703 NCP % 115 50-150 Pass

Perfluorotridecanoic acid (PFTrDA) B17-Ap19703 NCP % 91 50-150 Pass

Perfluorotetradecanoic acid(PFTeDA) B17-Ap19703 NCP % 112 50-150 Pass

Spike - % Recovery


Perfluorooctane sulfonamide(FOSA) B17-Ap19703 NCP % 115 50-150 Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) B17-Ap19703 NCP % 118 50-150 Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) B17-Ap19703 NCP % 120 50-150 Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) B17-Ap19703 NCP % 122 50-150 Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) B17-Ap19703 NCP % 101 50-150 Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) B17-Ap19703 NCP % 110 50-150 Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) B17-Ap19703 NCP % 109 50-150 Pass

Spike - % Recovery




ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 7 of 10



LimitsPass

LimitsQualifying

Code

Perfluorobutanesulfonic acid(PFBS) B17-Ap19703 NCP % 115 50-150 Pass

Perfluoropentanesulfonic acid(PFPeS) B17-Ap19703 NCP % 107 50-150 Pass

Perfluorohexanesulfonic acid(PFHxS) B17-Ap19703 NCP % 109 50-150 Pass

Perfluoroheptanesulfonic acid(PFHpS) B17-Ap19703 NCP % 100 50-150 Pass

Perfluorooctanesulfonic acid(PFOS) B17-Ap19703 NCP % 107 50-150 Pass

Perfluorodecanesulfonic acid(PFDS) B17-Ap19703 NCP % 110 50-150 Pass

Spike - % Recovery


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) B17-Ap19703 NCP % 109 50-150 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) B17-Ap19703 NCP % 108 50-150 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) B17-Ap19703 NCP % 90 50-150 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) B17-Ap19703 NCP % 58 50-150 Pass


LimitsPass

LimitsQualifying

Code

Duplicate


Perfluorobutanoic acid (PFBA) B17-Ap19702 NCP ug/L < 0.05 < 0.05 <1 30% Pass

Perfluoropentanoic acid (PFPeA) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanoic acid (PFHxA) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanoic acid (PFHpA) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanoic acid (PFOA) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorononanoic acid (PFNA) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanoic acid (PFDA) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroundecanoic acid (PFUnA) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorododecanoic acid (PFDoA) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


Perfluorooctane sulfonamide(FOSA) B17-Ap19702 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) B17-Ap19702 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) B17-Ap19702 NCP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) B17-Ap19702 NCP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) B17-Ap19702 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) B17-Ap19702 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) B17-Ap19702 NCP ug/L < 0.05 < 0.05 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 8 of 10


Duplicate


Perfluorobutanesulfonic acid(PFBS) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoropentanesulfonic acid(PFPeS) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanesulfonic acid(PFHxS) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanesulfonic acid(PFOS) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanesulfonic acid(PFDS) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) B17-Ap19702 NCP ug/L < 0.05 < 0.05 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 9 of 10


Comments









Code Description

N11


Authorised By



Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 10 of 10





3G Marine Pde

Abbotsford

VIC 3067


Report 542977-W-V2

Project name DOD TINDAl

Project ID 754_MELEN199420

Received Date Apr 20, 2017

Client Sample ID TDL_2145URALLA_BORE

Sample Matrix Water
















13C4-PFBA (surr.) 1 % 58




13C8-PFOA (surr.) 1 % 63

13C5-PFNA (surr.) 1 % 58

13C6-PFDA (surr.) 1 % 41












13C8-FOSA (surr.) 1 % 40



First Reported: May 04, 2017



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 1 of 10




emma.delborrello

Rectangle

Client Sample ID TDL_2145URALLA_BORE

Sample Matrix Water
















13C3-PFBS (surr.) 1 % 56


13C8-PFOS (surr.) 1 % 39






13C2-4:2 FTS (surr.) 1 % 108

13C2-6:2 FTS (surr.) 1 % 84

13C2-8:2 FTS (surr.) 1 % 45




ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 2 of 10


emma.delborrello

Rectangle
















ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 3 of 10


.Company Name: Coffey Environments Pty Ltd VIC Order No.: Received: Apr 20, 2017 9:00 AMAddress: 3G Marine Pde Report #: 542977 Due: Apr 28, 2017


Project Name: DOD TINDAlProject ID: 754_MELEN199420


Sample Detail

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 TDL_2145URALLA

Apr 13, 2017 Water B17-Ap15804 X

Test Counts 1






First Reported:May 04, 2017



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 4 of 10


emma.delborrello

Rectangle


General

Holding Times

Units

Terms




request.










Receipt Advice.



















































ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 5 of 10




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






LCS - % Recovery













LCS - % Recovery





ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 6 of 10



PassLimits

QualifyingCode








LCS - % Recovery








LCS - % Recovery







LimitsPass

LimitsQualifying

Code

Spike - % Recovery


Perfluorobutanoic acid (PFBA) B17-Ap19703 NCP % 118 50-150 Pass

Perfluoropentanoic acid (PFPeA) B17-Ap19703 NCP % 124 50-150 Pass

Perfluorohexanoic acid (PFHxA) B17-Ap19703 NCP % 113 50-150 Pass

Perfluoroheptanoic acid (PFHpA) B17-Ap19703 NCP % 114 50-150 Pass

Perfluorooctanoic acid (PFOA) B17-Ap19703 NCP % 112 50-150 Pass

Perfluorononanoic acid (PFNA) B17-Ap19703 NCP % 110 50-150 Pass

Perfluorodecanoic acid (PFDA) B17-Ap19703 NCP % 113 50-150 Pass

Perfluoroundecanoic acid (PFUnA) B17-Ap19703 NCP % 115 50-150 Pass

Perfluorododecanoic acid (PFDoA) B17-Ap19703 NCP % 115 50-150 Pass

Perfluorotridecanoic acid (PFTrDA) B17-Ap19703 NCP % 91 50-150 Pass

Perfluorotetradecanoic acid(PFTeDA) B17-Ap19703 NCP % 112 50-150 Pass

Spike - % Recovery


Perfluorooctane sulfonamide(FOSA) B17-Ap19703 NCP % 115 50-150 Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) B17-Ap19703 NCP % 118 50-150 Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) B17-Ap19703 NCP % 120 50-150 Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) B17-Ap19703 NCP % 122 50-150 Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) B17-Ap19703 NCP % 101 50-150 Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) B17-Ap19703 NCP % 110 50-150 Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) B17-Ap19703 NCP % 109 50-150 Pass

Spike - % Recovery





ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 7 of 10



LimitsPass

LimitsQualifying

Code

Perfluorobutanesulfonic acid(PFBS) B17-Ap19703 NCP % 115 50-150 Pass

Perfluoropentanesulfonic acid(PFPeS) B17-Ap19703 NCP % 107 50-150 Pass

Perfluorohexanesulfonic acid(PFHxS) B17-Ap19703 NCP % 109 50-150 Pass

Perfluoroheptanesulfonic acid(PFHpS) B17-Ap19703 NCP % 100 50-150 Pass

Perfluorooctanesulfonic acid(PFOS) B17-Ap19703 NCP % 107 50-150 Pass

Perfluorodecanesulfonic acid(PFDS) B17-Ap19703 NCP % 110 50-150 Pass

Spike - % Recovery


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) B17-Ap19703 NCP % 109 50-150 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) B17-Ap19703 NCP % 108 50-150 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) B17-Ap19703 NCP % 90 50-150 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) B17-Ap19703 NCP % 58 50-150 Pass


LimitsPass

LimitsQualifying

Code

Duplicate


Perfluorobutanoic acid (PFBA) B17-Ap19702 NCP ug/L < 0.05 < 0.05 <1 30% Pass

Perfluoropentanoic acid (PFPeA) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanoic acid (PFHxA) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanoic acid (PFHpA) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanoic acid (PFOA) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorononanoic acid (PFNA) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanoic acid (PFDA) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroundecanoic acid (PFUnA) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorododecanoic acid (PFDoA) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


Perfluorooctane sulfonamide(FOSA) B17-Ap19702 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) B17-Ap19702 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) B17-Ap19702 NCP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) B17-Ap19702 NCP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) B17-Ap19702 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) B17-Ap19702 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) B17-Ap19702 NCP ug/L < 0.05 < 0.05 <1 30% Pass




ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 8 of 10


Duplicate


Perfluorobutanesulfonic acid(PFBS) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoropentanesulfonic acid(PFPeS) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanesulfonic acid(PFHxS) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanesulfonic acid(PFOS) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanesulfonic acid(PFDS) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) B17-Ap19702 NCP ug/L < 0.05 < 0.05 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) B17-Ap19702 NCP ug/L < 0.01 < 0.01 <1 30% Pass




ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 9 of 10


Comments

Report amended to correct sample ID









Code Description

N11


Authorised By



Glenn Jackson








ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 10 of 10





3G Marine Pde

Abbotsford

VIC 3067

Attention: Chris Molloy

Report 544592-W



Received Date May 03, 2017

Client Sample ID 0990_053MW01_170427

0990_053MW06_170428

0990_070MW01_170428

0990_BCPMW01_170428

Sample Matrix Water Water Water Water

Eurofins | mgt Sample No. M17-My03446 M17-My03448 M17-My03449 M17-My03450

Date Sampled Apr 28, 2017 Apr 28, 2017 Apr 28, 2017 Apr 28, 2017



Perfluorobutanoic acid (PFBA) 0.05 ug/L 0.09 < 0.05 < 0.05 < 0.05

13C4-PFBA (surr.) 1 % 99 83 85 110

Perfluoropentanoic acid (PFPeA) 0.01 ug/L N090.11 N090.01 N090.02 N090.02

13C5-PFPeA (surr.) 1 % 103 102 105 112

Perfluorohexanoic acid (PFHxA) 0.01 ug/L N090.17 N090.04 N090.09 N090.02

13C5-PFHxA (surr.) 1 % 96 105 105 110

Perfluoroheptanoic acid (PFHpA) 0.01 ug/L N090.03 < 0.01 < 0.01 < 0.01

13C4-PFHpA (surr.) 1 % 98 105 106 111

Perfluorooctanoic acid (PFOA) 0.01 ug/L N090.03 < 0.01 N090.01 < 0.01

13C8-PFOA (surr.) 1 % 95 129 111 124

Perfluorononanoic acid (PFNA) 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

13C5-PFNA (surr.) 1 % 88 79 86 100

Perfluorodecanoic acid (PFDA) 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

13C6-PFDA (surr.) 1 % 92 120 63 104

Perfluoroundecanoic acid (PFUnA) 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

13C2-PFUnDA (surr.) 1 % 80 103 57 93

Perfluorododecanoic acid (PFDoA) 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

13C2-PFDoDA (surr.) 1 % 60 94 49 85

Perfluorotridecanoic acid (PFTrDA) 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

Perfluorotetradecanoic acid (PFTeDA) 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

13C2-PFTeDA (surr.) 1 % 52 42 27 44


Perfluorooctane sulfonamide (FOSA) 0.05 ug/L < 0.05 < 0.05 < 0.05 < 0.05

13C8-FOSA (surr.) 1 % 64 79 52 57

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA) 0.05 ug/L < 0.05 < 0.05 < 0.05 < 0.05

D3-N-MeFOSA (surr.) 1 % 58 51 42 62

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA) 0.05 ug/L < 0.05 < 0.05 < 0.05 < 0.05

D5-N-EtFOSA (surr.) 1 % 41 31 26 57

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol(N-MeFOSE) 0.05 ug/L < 0.05 < 0.05 < 0.05 < 0.05

D7-N-MeFOSE (surr.) 1 % 36 44 35 48

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE) 0.05 ug/L < 0.05 < 0.05 < 0.05 < 0.05

D9-N-EtFOSE (surr.) 1 % 42 43 34 47

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA) 0.05 ug/L < 0.05 < 0.05 < 0.05 < 0.05



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 70





0990_053MW06_170428

0990_070MW01_170428

0990_BCPMW01_170428






D5-N-EtFOSAA (surr.) 1 % 62 86 54 61

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA) 0.05 ug/L < 0.05 < 0.05 < 0.05 < 0.05

D3-N-MeFOSAA (surr.) 1 % 76 107 62 90


Perfluorobutanesulfonic acid (PFBS) 0.01 ug/L N090.08 N090.03 N090.08 N090.01

13C3-PFBS (surr.) 1 % 96 103 103 104

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L N090.07 N090.02 N090.05 N090.01

Perfluorohexanesulfonic acid (PFHxS) 0.01 ug/L N090.50 N090.12 N090.18 N090.06

18O2-PFHxS (surr.) 1 % 86 104 98 104

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N090.13 N090.14 N090.07 N090.03

13C8-PFOS (surr.) 1 % 89 107 73 108

Perfluorodecanesulfonic acid (PFDS) 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2 FTS) 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

13C2-4:2 FTS (surr.) 1 % 83 100 82 97

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) 0.05 ug/L < 0.05 < 0.05 < 0.05 < 0.05

13C2-6:2 FTS (surr.) 1 % 93 85 91 98

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

13C2-8:2 FTS (surr.) 1 % 87 102 55 86

1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2FTS) 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

Conductivity (at 25°C) 1 uS/cm 1000 980 - 850

pH 0.1 pH Units 6.9 7.2 - 6.9

Client Sample ID 0990_BCRUMW01_170428

0990_BORE06_170428

0990_BORE05_170428

0990_NT0073MW02_170428






Perfluorobutanoic acid (PFBA) 0.05 ug/L < 0.05 0.08 < 0.05 < 0.05

13C4-PFBA (surr.) 1 % 109 105 124 129

Perfluoropentanoic acid (PFPeA) 0.01 ug/L N090.02 N090.02 < 0.01 < 0.01

13C5-PFPeA (surr.) 1 % 107 106 119 123

Perfluorohexanoic acid (PFHxA) 0.01 ug/L N090.05 N090.03 N090.01 < 0.01

13C5-PFHxA (surr.) 1 % 110 101 117 119

Perfluoroheptanoic acid (PFHpA) 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

13C4-PFHpA (surr.) 1 % 109 99 119 119

Perfluorooctanoic acid (PFOA) 0.01 ug/L N090.02 N090.01 < 0.01 < 0.01

13C8-PFOA (surr.) 1 % 115 101 138 132


13C5-PFNA (surr.) 1 % 102 54 33 90


13C6-PFDA (surr.) 1 % 113 56 127 113



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 70


Client Sample ID 0990_BCRUMW01_170428

0990_BORE06_170428

0990_BORE05_170428

0990_NT0073MW02_170428







13C2-PFUnDA (surr.) 1 % 101 38 99 123


13C2-PFDoDA (surr.) 1 % 75 45 86 93



13C2-PFTeDA (surr.) 1 % 69 38 76 104



13C8-FOSA (surr.) 1 % 71 38 70 63


D3-N-MeFOSA (surr.) 1 % 55 38 67 65


D5-N-EtFOSA (surr.) 1 % 45 33 38 45


D7-N-MeFOSE (surr.) 1 % 43 30 44 39


D9-N-EtFOSE (surr.) 1 % 56 31 45 49


D5-N-EtFOSAA (surr.) 1 % 62 34 70 61


D3-N-MeFOSAA (surr.) 1 % 83 43 98 83


Perfluorobutanesulfonic acid (PFBS) 0.01 ug/L N090.03 N090.03 < 0.01 < 0.01

13C3-PFBS (surr.) 1 % 110 104 111 113

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L N090.02 N090.02 < 0.01 < 0.01

Perfluorohexanesulfonic acid (PFHxS) 0.01 ug/L N090.19 N090.11 N090.03 < 0.01

18O2-PFHxS (surr.) 1 % 95 92 112 107

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L N090.02 < 0.01 < 0.01 < 0.01


13C8-PFOS (surr.) 1 % 92 58 101 104




13C2-4:2 FTS (surr.) 1 % 94 80 115 160


13C2-6:2 FTS (surr.) 1 % 96 76 115 155


13C2-8:2 FTS (surr.) 1 % 109 32 95 132


Conductivity (at 25°C) 1 uS/cm 780 - 770 650

pH 0.1 pH Units 7.1 - 7.2 7.3



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 70


Client Sample ID 0990_NT0050MW02_170429

R160990_NT0065MW02_170428

R160990_NT0065MW04_170428

R160990_NT0269MW01_170428






Perfluorobutanoic acid (PFBA) 0.05 ug/L < 0.05 2.7 0.84 < 0.3

13C4-PFBA (surr.) 1 % 121 103 110 111

Perfluoropentanoic acid (PFPeA) 0.01 ug/L < 0.01 N096.3 N091.7 N090.65

13C5-PFPeA (surr.) 1 % 113 82 87 91

Perfluorohexanoic acid (PFHxA) 0.01 ug/L < 0.01 N0919 N096.8 N091.2

13C5-PFHxA (surr.) 1 % 111 78 85 91

Perfluoroheptanoic acid (PFHpA) 0.01 ug/L < 0.01 N093.5 N090.93 < 0.3

13C4-PFHpA (surr.) 1 % 114 103 111 114

Perfluorooctanoic acid (PFOA) 0.01 ug/L < 0.01 N098.2 N092.3 N090.66

13C8-PFOA (surr.) 1 % 124 92 110 116

Perfluorononanoic acid (PFNA) 0.01 ug/L < 0.01 0.41 < 0.3 < 0.3

13C5-PFNA (surr.) 1 % 102 110 107 118


13C6-PFDA (surr.) 1 % 96 77 101 117


13C2-PFUnDA (surr.) 1 % 66 100 124 115


13C2-PFDoDA (surr.) 1 % 57 66 80 80



13C2-PFTeDA (surr.) 1 % 47 14 22 20



13C8-FOSA (surr.) 1 % 56 85 95 106


D3-N-MeFOSA (surr.) 1 % 43 48 55 57


D5-N-EtFOSA (surr.) 1 % 39 30 30 31


D7-N-MeFOSE (surr.) 1 % 56 40 49 39


D9-N-EtFOSE (surr.) 1 % 57 51 52 48


D5-N-EtFOSAA (surr.) 1 % 35 72 87 78


D3-N-MeFOSAA (surr.) 1 % 42 73 95 98


Perfluorobutanesulfonic acid (PFBS) 0.01 ug/L < 0.01 N096.6 N091.8 0.38

13C3-PFBS (surr.) 1 % 111 98 104 108

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L < 0.01 N096.7 N091.8 N090.43

Perfluorohexanesulfonic acid (PFHxS) 0.01 ug/L < 0.01 N0950 N0911 N093.3

18O2-PFHxS (surr.) 1 % 106 90 103 109

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L < 0.01 N093.6 N090.84 N090.25

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N090.02 N09170 N0935 N099.5

13C8-PFOS (surr.) 1 % 78 74 99 104




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 70



R160990_NT0065MW02_170428

R160990_NT0065MW04_170428

R160990_NT0269MW01_170428







13C2-4:2 FTS (surr.) 1 % 118 84 88 91


13C2-6:2 FTS (surr.) 1 % 129 87 90 92


13C2-8:2 FTS (surr.) 1 % 90 79 97 96



pH 0.1 pH Units 7.1 - 7.0 7.0


0990_BORE24_170428

0990_NT0048MW1_170428

0990_NT0064MW11_170429






Perfluorobutanoic acid (PFBA) 0.05 ug/L 0.23 < 0.05 < 0.05 0.22

13C4-PFBA (surr.) 1 % 106 107 123 116


13C5-PFPeA (surr.) 1 % 100 102 116 106


13C5-PFHxA (surr.) 1 % 94 95 113 90

Perfluoroheptanoic acid (PFHpA) 0.01 ug/L N090.04 N090.04 N090.01 N090.19

13C4-PFHpA (surr.) 1 % 99 91 114 98

Perfluorooctanoic acid (PFOA) 0.01 ug/L N090.10 N090.06 N090.04 N090.52

13C8-PFOA (surr.) 1 % 79 91 98 66

Perfluorononanoic acid (PFNA) 0.01 ug/L < 0.01 0.02 < 0.01 < 0.01

13C5-PFNA (surr.) 1 % 68 73 56 70


13C6-PFDA (surr.) 1 % 64 78 93 37


13C2-PFUnDA (surr.) 1 % 50 60 103 59


13C2-PFDoDA (surr.) 1 % 53 56 84 52



13C2-PFTeDA (surr.) 1 % 48 57 120 45



13C8-FOSA (surr.) 1 % 42 50 70 37


D3-N-MeFOSA (surr.) 1 % 37 50 46 36


D5-N-EtFOSA (surr.) 1 % 34 38 28 37



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 70



0990_BORE24_170428

0990_NT0048MW1_170428

0990_NT0064MW11_170429







D7-N-MeFOSE (surr.) 1 % 33 40 32 31


D9-N-EtFOSE (surr.) 1 % 37 53 46 32


D5-N-EtFOSAA (surr.) 1 % 36 43 73 34


D3-N-MeFOSAA (surr.) 1 % 49 56 75 42



13C3-PFBS (surr.) 1 % 98 101 107 94



18O2-PFHxS (surr.) 1 % 79 86 89 103

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L N090.04 N090.03 N090.04 N090.32

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N090.18 N090.99 N091.1 N0912

13C8-PFOS (surr.) 1 % 57 69 85 53




13C2-4:2 FTS (surr.) 1 % 86 85 167 116

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) 0.05 ug/L < 0.05 0.09 < 0.05 < 0.05

13C2-6:2 FTS (surr.) 1 % 74 80 145 116

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) 0.01 ug/L < 0.01 < 0.01 < 0.01 0.02

13C2-8:2 FTS (surr.) 1 % 56 59 110 52



pH 0.1 pH Units 7.0 - 8.0 7.0

Client Sample IDR160990_NT0064MW12_170429

R160990_NT0064MW13_170429

R160990_NT0064MW14_170429

0990_BORE10_170429






Perfluorobutanoic acid (PFBA) 0.05 ug/L 30 12 0.44 < 0.05

13C4-PFBA (surr.) 1 % 103 106 109 120

Perfluoropentanoic acid (PFPeA) 0.01 ug/L N0965 N0926 N090.85 < 0.01

13C5-PFPeA (surr.) 1 % 81 89 94 109

Perfluorohexanoic acid (PFHxA) 0.01 ug/L N09280 N0964 N092.8 N090.01

13C5-PFHxA (surr.) 1 % 64 85 95 107

Perfluoroheptanoic acid (PFHpA) 0.01 ug/L N0947 N0912 N090.45 < 0.01



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 70



R160990_NT0064MW13_170429

R160990_NT0064MW14_170429

0990_BORE10_170429






13C4-PFHpA (surr.) 1 % 90 105 112 104

Perfluorooctanoic acid (PFOA) 0.01 ug/L N0987 N0945 N091.6 < 0.01

13C8-PFOA (surr.) 1 % 68 77 110 102

Perfluorononanoic acid (PFNA) 0.01 ug/L N091.1 N092.0 < 0.3 < 0.01

13C5-PFNA (surr.) 1 % 99 107 116 65


13C6-PFDA (surr.) 1 % 76 66 110 53


13C2-PFUnDA (surr.) 1 % 119 109 118 57


13C2-PFDoDA (surr.) 1 % 109 45 110 47



13C2-PFTeDA (surr.) 1 % 46 30 35 46



13C8-FOSA (surr.) 1 % 86 92 98 39


D3-N-MeFOSA (surr.) 1 % 38 59 35 36


D5-N-EtFOSA (surr.) 1 % 31 39 23 29


D7-N-MeFOSE (surr.) 1 % 46 55 45 26


D9-N-EtFOSE (surr.) 1 % 58 58 59 28


D5-N-EtFOSAA (surr.) 1 % 83 94 91 34


D3-N-MeFOSAA (surr.) 1 % 92 73 95 45


Perfluorobutanesulfonic acid (PFBS) 0.01 ug/L N0961 N0915 N092.0 < 0.01

13C3-PFBS (surr.) 1 % 90 104 106 105

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L N0957 N0916 N091.8 < 0.01

Perfluorohexanesulfonic acid (PFHxS) 0.01 ug/L N09240 N09170 N0916 N090.03

18O2-PFHxS (surr.) 1 % 103 79 102 91

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L N0924 N098.2 N090.62 < 0.01

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N09270 N091200 N093.7 N090.12

13C8-PFOS (surr.) 1 % 102 80 100 59




13C2-4:2 FTS (surr.) 1 % 89 89 94 118

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) 0.05 ug/L 7.8 < 1.5 < 1.5 < 0.05

13C2-6:2 FTS (surr.) 1 % 87 91 94 105




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 70



R160990_NT0064MW13_170429

R160990_NT0064MW14_170429

0990_BORE10_170429






13C2-8:2 FTS (surr.) 1 % 84 78 92 59


Conductivity (at 25°C) 1 uS/cm - 360 - 830

pH 0.1 pH Units - 7.1 - 7.1

Client Sample ID 0990_BORE11_170429

0990_QC1GW_170428

0990_QC2GW_170428

0990_QCSGW_170428





PFOS/PFOA/6:2FTS

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L - - - < 0.01

Perfluorooctanoic acid (PFOA) 0.01 ug/L - - - < 0.01

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) 0.05 ug/L - - - < 0.05

13C8-PFOS (surr.) 1 % - - - 95

13C8-PFOA (surr.) 1 % - - - 109

13C2-6:2 FTS (surr.) 1 % - - - 95


Perfluorobutanoic acid (PFBA) 0.05 ug/L < 0.05 < 0.05 < 0.05 -

13C4-PFBA (surr.) 1 % 123 116 113 -

Perfluoropentanoic acid (PFPeA) 0.01 ug/L < 0.01 N090.10 N090.02 -

13C5-PFPeA (surr.) 1 % 107 104 105 -

Perfluorohexanoic acid (PFHxA) 0.01 ug/L < 0.01 N090.17 N090.06 -

13C5-PFHxA (surr.) 1 % 108 98 101 -

Perfluoroheptanoic acid (PFHpA) 0.01 ug/L < 0.01 N090.04 < 0.01 -

13C4-PFHpA (surr.) 1 % 106 99 100 -

Perfluorooctanoic acid (PFOA) 0.01 ug/L < 0.01 N090.06 N090.01 -

13C8-PFOA (surr.) 1 % 112 86 102 -

Perfluorononanoic acid (PFNA) 0.01 ug/L < 0.01 0.02 < 0.01 -

13C5-PFNA (surr.) 1 % 71 72 102 -

Perfluorodecanoic acid (PFDA) 0.01 ug/L < 0.01 < 0.01 < 0.01 -

13C6-PFDA (surr.) 1 % 59 55 98 -

Perfluoroundecanoic acid (PFUnA) 0.01 ug/L < 0.01 < 0.01 < 0.01 -

13C2-PFUnDA (surr.) 1 % 52 54 96 -

Perfluorododecanoic acid (PFDoA) 0.01 ug/L < 0.01 < 0.01 < 0.01 -

13C2-PFDoDA (surr.) 1 % 46 49 69 -

Perfluorotridecanoic acid (PFTrDA) 0.01 ug/L < 0.01 < 0.01 < 0.01 -

Perfluorotetradecanoic acid (PFTeDA) 0.01 ug/L < 0.01 < 0.01 < 0.01 -

13C2-PFTeDA (surr.) 1 % 40 42 46 -


Perfluorooctane sulfonamide (FOSA) 0.05 ug/L < 0.05 < 0.05 < 0.05 -

13C8-FOSA (surr.) 1 % 52 38 86 -

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA) 0.05 ug/L < 0.05 < 0.05 < 0.05 -

D3-N-MeFOSA (surr.) 1 % 40 27 72 -



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 70


Client Sample ID 0990_BORE11_170429

0990_QC1GW_170428

0990_QC2GW_170428

0990_QCSGW_170428






N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA) 0.05 ug/L < 0.05 < 0.05 < 0.05 -

D5-N-EtFOSA (surr.) 1 % 31 23 64 -

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol(N-MeFOSE) 0.05 ug/L < 0.05 < 0.05 < 0.05 -

D7-N-MeFOSE (surr.) 1 % 35 27 68 -

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE) 0.05 ug/L < 0.05 < 0.05 < 0.05 -

D9-N-EtFOSE (surr.) 1 % 41 29 58 -

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA) 0.05 ug/L < 0.05 < 0.05 < 0.05 -

D5-N-EtFOSAA (surr.) 1 % 35 31 81 -

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA) 0.05 ug/L < 0.05 < 0.05 < 0.05 -

D3-N-MeFOSAA (surr.) 1 % 42 41 92 -


Perfluorobutanesulfonic acid (PFBS) 0.01 ug/L < 0.01 N090.06 N090.04 -

13C3-PFBS (surr.) 1 % 105 104 109 -

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L < 0.01 N090.06 N090.04 -

Perfluorohexanesulfonic acid (PFHxS) 0.01 ug/L N090.02 N090.39 N090.42 -

18O2-PFHxS (surr.) 1 % 93 84 98 -

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L < 0.01 0.03 N090.01 -

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N090.10 N091.0 N090.25 -

13C8-PFOS (surr.) 1 % 62 51 95 -

Perfluorodecanesulfonic acid (PFDS) 0.01 ug/L < 0.01 < 0.01 < 0.01 -


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2 FTS) 0.01 ug/L < 0.01 < 0.01 < 0.01 -

13C2-4:2 FTS (surr.) 1 % 136 116 127 -

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) 0.05 ug/L < 0.05 0.10 < 0.05 -

13C2-6:2 FTS (surr.) 1 % 121 99 98 -

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) 0.01 ug/L < 0.01 < 0.01 < 0.01 -

13C2-8:2 FTS (surr.) 1 % 55 55 121 -

1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2FTS) 0.01 ug/L < 0.01 < 0.01 < 0.01 -

Conductivity (at 25°C) 1 uS/cm 510 - - -

pH 0.1 pH Units 7.8 - - -

Client Sample ID 0990_QC9GW_170429

0990_QC13GW_170430

0990_QC18GW_170501

0990_75COLLINS-BORE_170428



Date Sampled Apr 29, 2017 Apr 30, 2017 May 01, 2017 Apr 28, 2017


PFOS/PFOA/6:2FTS

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 -

Perfluorooctanoic acid (PFOA) 0.01 ug/L < 0.01 < 0.01 < 0.01 -

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) 0.05 ug/L < 0.05 < 0.05 < 0.05 -

13C8-PFOS (surr.) 1 % 93 104 104 -

13C8-PFOA (surr.) 1 % 103 106 101 -

13C2-6:2 FTS (surr.) 1 % 78 98 66 -



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 70



0990_QC13GW_170430

0990_QC18GW_170501







Perfluorobutanoic acid (PFBA) 0.05 ug/L - - - < 0.05

13C4-PFBA (surr.) 1 % - - - 120

Perfluoropentanoic acid (PFPeA) 0.01 ug/L - - - N090.02

13C5-PFPeA (surr.) 1 % - - - 117

Perfluorohexanoic acid (PFHxA) 0.01 ug/L - - - N090.12

13C5-PFHxA (surr.) 1 % - - - 109

Perfluoroheptanoic acid (PFHpA) 0.01 ug/L - - - N090.02

13C4-PFHpA (surr.) 1 % - - - 108

Perfluorooctanoic acid (PFOA) 0.01 ug/L - - - N090.04

13C8-PFOA (surr.) 1 % - - - 108

Perfluorononanoic acid (PFNA) 0.01 ug/L - - - < 0.01

13C5-PFNA (surr.) 1 % - - - 109

Perfluorodecanoic acid (PFDA) 0.01 ug/L - - - < 0.01

13C6-PFDA (surr.) 1 % - - - 80

Perfluoroundecanoic acid (PFUnA) 0.01 ug/L - - - < 0.01

13C2-PFUnDA (surr.) 1 % - - - 55

Perfluorododecanoic acid (PFDoA) 0.01 ug/L - - - < 0.01

13C2-PFDoDA (surr.) 1 % - - - 40

Perfluorotridecanoic acid (PFTrDA) 0.01 ug/L - - - < 0.01

Perfluorotetradecanoic acid (PFTeDA) 0.01 ug/L - - - < 0.01

13C2-PFTeDA (surr.) 1 % - - - 18


Perfluorooctane sulfonamide (FOSA) 0.05 ug/L - - - < 0.05

13C8-FOSA (surr.) 1 % - - - 79

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA) 0.05 ug/L - - - < 0.05

D3-N-MeFOSA (surr.) 1 % - - - 56

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA) 0.05 ug/L - - - < 0.05

D5-N-EtFOSA (surr.) 1 % - - - 56

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol(N-MeFOSE) 0.05 ug/L - - - < 0.05

D7-N-MeFOSE (surr.) 1 % - - - 57

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE) 0.05 ug/L - - - < 0.05

D9-N-EtFOSE (surr.) 1 % - - - 50

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA) 0.05 ug/L - - - < 0.05

D5-N-EtFOSAA (surr.) 1 % - - - 65

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA) 0.05 ug/L - - - < 0.05

D3-N-MeFOSAA (surr.) 1 % - - - 69


Perfluorobutanesulfonic acid (PFBS) 0.01 ug/L - - - N090.11

13C3-PFBS (surr.) 1 % - - - 113

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L - - - N090.11

Perfluorohexanesulfonic acid (PFHxS) 0.01 ug/L - - - N090.74

18O2-PFHxS (surr.) 1 % - - - 101

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L - - - N090.05

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L - - - N091.5

13C8-PFOS (surr.) 1 % - - - 86

Perfluorodecanesulfonic acid (PFDS) 0.01 ug/L - - - < 0.01



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 70


emma.delborrello

Rectangle


0990_QC13GW_170430

0990_QC18GW_170501







1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2 FTS) 0.01 ug/L - - - < 0.01

13C2-4:2 FTS (surr.) 1 % - - - 120

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) 0.05 ug/L - - - < 0.05

13C2-6:2 FTS (surr.) 1 % - - - 88

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) 0.01 ug/L - - - < 0.01

13C2-8:2 FTS (surr.) 1 % - - - 80

1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2FTS) 0.01 ug/L - - - < 0.01

Client Sample ID0990_PRIVATEBORE001_170428

0990_QC6_17/04/28

0990_QC14_17/04/30

0990_SW04_17/04/30





PFOS/PFOA/6:2FTS

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L - < 0.01 < 0.01 -

Perfluorooctanoic acid (PFOA) 0.01 ug/L - < 0.01 < 0.01 -

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) 0.05 ug/L - < 0.05 < 0.05 -

13C8-PFOS (surr.) 1 % - 81 82 -

13C8-PFOA (surr.) 1 % - 101 112 -

13C2-6:2 FTS (surr.) 1 % - 81 76 -


Perfluorobutanoic acid (PFBA) 0.05 ug/L < 0.05 - - < 0.05

13C4-PFBA (surr.) 1 % 128 - - 118

Perfluoropentanoic acid (PFPeA) 0.01 ug/L N090.03 - - < 0.01

13C5-PFPeA (surr.) 1 % 135 - - 107

Perfluorohexanoic acid (PFHxA) 0.01 ug/L N090.15 - - < 0.01

13C5-PFHxA (surr.) 1 % 128 - - 106

Perfluoroheptanoic acid (PFHpA) 0.01 ug/L N090.02 - - < 0.01

13C4-PFHpA (surr.) 1 % 126 - - 102

Perfluorooctanoic acid (PFOA) 0.01 ug/L N090.05 - - < 0.01

13C8-PFOA (surr.) 1 % 126 - - 98

Perfluorononanoic acid (PFNA) 0.01 ug/L < 0.01 - - < 0.01

13C5-PFNA (surr.) 1 % 109 - - 92

Perfluorodecanoic acid (PFDA) 0.01 ug/L < 0.01 - - < 0.01

13C6-PFDA (surr.) 1 % 89 - - 78

Perfluoroundecanoic acid (PFUnA) 0.01 ug/L < 0.01 - - < 0.01

13C2-PFUnDA (surr.) 1 % 89 - - 68

Perfluorododecanoic acid (PFDoA) 0.01 ug/L < 0.01 - - < 0.01

13C2-PFDoDA (surr.) 1 % 95 - - 60

Perfluorotridecanoic acid (PFTrDA) 0.01 ug/L < 0.01 - - < 0.01

Perfluorotetradecanoic acid (PFTeDA) 0.01 ug/L < 0.01 - - < 0.01

13C2-PFTeDA (surr.) 1 % 88 - - 43



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 70


emma.delborrello

Rectangle


0990_QC6_17/04/28

0990_QC14_17/04/30

0990_SW04_17/04/30






Perfluorooctane sulfonamide (FOSA) 0.05 ug/L < 0.05 - - < 0.05

13C8-FOSA (surr.) 1 % 93 - - 73

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA) 0.05 ug/L < 0.05 - - < 0.05

D3-N-MeFOSA (surr.) 1 % 96 - - 54

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA) 0.05 ug/L < 0.05 - - < 0.05

D5-N-EtFOSA (surr.) 1 % 91 - - 52

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol(N-MeFOSE) 0.05 ug/L < 0.05 - - < 0.05

D7-N-MeFOSE (surr.) 1 % 83 - - 48

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE) 0.05 ug/L < 0.05 - - < 0.05

D9-N-EtFOSE (surr.) 1 % 79 - - 48

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA) 0.05 ug/L < 0.05 - - < 0.05

D5-N-EtFOSAA (surr.) 1 % 71 - - 65

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA) 0.05 ug/L < 0.05 - - < 0.05

D3-N-MeFOSAA (surr.) 1 % 73 - - 70


Perfluorobutanesulfonic acid (PFBS) 0.01 ug/L N090.14 - - < 0.01

13C3-PFBS (surr.) 1 % 140 - - 110

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L N090.15 - - < 0.01

Perfluorohexanesulfonic acid (PFHxS) 0.01 ug/L N090.95 - - N090.01

18O2-PFHxS (surr.) 1 % 121 - - 99

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L N090.07 - - < 0.01

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N091.9 - - 0.02

13C8-PFOS (surr.) 1 % 91 - - 78

Perfluorodecanesulfonic acid (PFDS) 0.01 ug/L < 0.01 - - < 0.01


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2 FTS) 0.01 ug/L < 0.01 - - < 0.01

13C2-4:2 FTS (surr.) 1 % 165 - - 131

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) 0.05 ug/L < 0.05 - - < 0.05

13C2-6:2 FTS (surr.) 1 % 114 - - 95

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) 0.01 ug/L < 0.01 - - < 0.01

13C2-8:2 FTS (surr.) 1 % 102 - - 92

1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2FTS) 0.01 ug/L < 0.01 - - < 0.01



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 12 of 70


Client Sample ID 0990_SW05_17/04/30

0990_SW06_17/04/30

0990_SW07_17/05/01

0990_SW09_17/05/01



Date Sampled Apr 30, 2017 Apr 30, 2017 May 01, 2017 May 01, 2017



Perfluorobutanoic acid (PFBA) 0.05 ug/L < 0.05 < 0.05 < 0.05 < 0.05

13C4-PFBA (surr.) 1 % 118 116 122 114

Perfluoropentanoic acid (PFPeA) 0.01 ug/L < 0.01 < 0.01 < 0.01 N090.05

13C5-PFPeA (surr.) 1 % 108 105 110 104

Perfluorohexanoic acid (PFHxA) 0.01 ug/L < 0.01 < 0.01 < 0.01 N090.21

13C5-PFHxA (surr.) 1 % 104 103 107 103

Perfluoroheptanoic acid (PFHpA) 0.01 ug/L < 0.01 < 0.01 < 0.01 N090.03

13C4-PFHpA (surr.) 1 % 104 103 106 95

Perfluorooctanoic acid (PFOA) 0.01 ug/L < 0.01 < 0.01 < 0.01 N090.07

13C8-PFOA (surr.) 1 % 102 101 103 81


13C5-PFNA (surr.) 1 % 95 89 94 65


13C6-PFDA (surr.) 1 % 77 72 78 47


13C2-PFUnDA (surr.) 1 % 64 61 64 39


13C2-PFDoDA (surr.) 1 % 63 56 58 36



13C2-PFTeDA (surr.) 1 % 44 33 40 25



13C8-FOSA (surr.) 1 % 75 70 73 40


D3-N-MeFOSA (surr.) 1 % 78 62 51 35


D5-N-EtFOSA (surr.) 1 % 80 55 40 30


D7-N-MeFOSE (surr.) 1 % 54 48 45 28


D9-N-EtFOSE (surr.) 1 % 57 46 46 29


D5-N-EtFOSAA (surr.) 1 % 63 58 62 30


D3-N-MeFOSAA (surr.) 1 % 66 61 68 32


Perfluorobutanesulfonic acid (PFBS) 0.01 ug/L < 0.01 < 0.01 < 0.01 N090.14

13C3-PFBS (surr.) 1 % 111 111 113 111

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L < 0.01 < 0.01 < 0.01 N090.12


18O2-PFHxS (surr.) 1 % 99 98 101 86

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L < 0.01 < 0.01 < 0.01 N090.08


13C8-PFOS (surr.) 1 % 79 73 78 47




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 13 of 70



0990_SW06_17/04/30

0990_SW07_17/05/01

0990_SW09_17/05/01







13C2-4:2 FTS (surr.) 1 % 131 126 127 126


13C2-6:2 FTS (surr.) 1 % 97 94 92 77


13C2-8:2 FTS (surr.) 1 % 85 83 85 53


Conductivity (at 25°C) 1 uS/cm - 700 - 820

pH 0.1 pH Units - 7.9 - 7.5


0990_SW16_17/05/01

0990_SW23_17/05/01

0990_SW27_17/05/01



Date Sampled May 01, 2017 May 01, 2017 May 01, 2017 May 01, 2017




13C4-PFBA (surr.) 1 % 121 123 122 112

Perfluoropentanoic acid (PFPeA) 0.01 ug/L N090.03 N090.03 0.02 0.04

13C5-PFPeA (surr.) 1 % 113 111 131 123


13C5-PFHxA (surr.) 1 % 108 108 121 119


13C4-PFHpA (surr.) 1 % 107 107 115 113


13C8-PFOA (surr.) 1 % 110 105 104 103


13C5-PFNA (surr.) 1 % 98 100 93 99


13C6-PFDA (surr.) 1 % 80 78 77 82


13C2-PFUnDA (surr.) 1 % 69 67 68 72


13C2-PFDoDA (surr.) 1 % 63 59 68 67



13C2-PFTeDA (surr.) 1 % 41 40 78 68



13C8-FOSA (surr.) 1 % 72 76 59 62


D3-N-MeFOSA (surr.) 1 % 55 66 59 53


D5-N-EtFOSA (surr.) 1 % 44 54 59 61



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 14 of 70



0990_SW16_17/05/01

0990_SW23_17/05/01

0990_SW27_17/05/01







D7-N-MeFOSE (surr.) 1 % 51 53 47 45


D9-N-EtFOSE (surr.) 1 % 51 53 49 46


D5-N-EtFOSAA (surr.) 1 % 66 68 72 72


D3-N-MeFOSAA (surr.) 1 % 73 68 74 75



13C3-PFBS (surr.) 1 % 115 116 128 125



18O2-PFHxS (surr.) 1 % 99 99 99 98



13C8-PFOS (surr.) 1 % 75 80 67 72




13C2-4:2 FTS (surr.) 1 % 125 137 178 181


13C2-6:2 FTS (surr.) 1 % 87 102 122 128


13C2-8:2 FTS (surr.) 1 % 84 93 112 130


Conductivity (at 25°C) 1 uS/cm - - - 620

pH 0.1 pH Units - - - 8.3


0990_SW29_17/05/01

0990_SW31_17/05/01

0990_SW32_17/05/01







13C4-PFBA (surr.) 1 % 113 118 120 118

Perfluoropentanoic acid (PFPeA) 0.01 ug/L 0.03 < 0.01 < 0.01 < 0.01

13C5-PFPeA (surr.) 1 % 113 133 132 126

Perfluorohexanoic acid (PFHxA) 0.01 ug/L N090.11 < 0.01 < 0.01 < 0.01

13C5-PFHxA (surr.) 1 % 111 127 129 127




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 15 of 70



0990_SW29_17/05/01

0990_SW31_17/05/01

0990_SW32_17/05/01






13C4-PFHpA (surr.) 1 % 113 119 119 117

Perfluorooctanoic acid (PFOA) 0.01 ug/L N090.03 < 0.01 < 0.01 < 0.01

13C8-PFOA (surr.) 1 % 105 113 109 109


13C5-PFNA (surr.) 1 % 105 97 98 98


13C6-PFDA (surr.) 1 % 82 83 75 75


13C2-PFUnDA (surr.) 1 % 71 72 63 67


13C2-PFDoDA (surr.) 1 % 66 70 66 69



13C2-PFTeDA (surr.) 1 % 66 81 84 81



13C8-FOSA (surr.) 1 % 78 61 65 61


D3-N-MeFOSA (surr.) 1 % 70 60 75 59


D5-N-EtFOSA (surr.) 1 % 80 59 83 65


D7-N-MeFOSE (surr.) 1 % 53 46 66 47


D9-N-EtFOSE (surr.) 1 % 57 48 62 47


D5-N-EtFOSAA (surr.) 1 % 68 76 69 69


D3-N-MeFOSAA (surr.) 1 % 76 82 70 74


Perfluorobutanesulfonic acid (PFBS) 0.01 ug/L N090.07 < 0.01 < 0.01 < 0.01

13C3-PFBS (surr.) 1 % 115 133 132 130

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L N090.06 < 0.01 < 0.01 < 0.01

Perfluorohexanesulfonic acid (PFHxS) 0.01 ug/L N090.41 < 0.01 < 0.01 < 0.01

18O2-PFHxS (surr.) 1 % 101 108 108 109


Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N090.38 < 0.01 < 0.01 < 0.01

13C8-PFOS (surr.) 1 % 78 76 70 73




13C2-4:2 FTS (surr.) 1 % 153 197 198 191


13C2-6:2 FTS (surr.) 1 % 118 139 137 135




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 16 of 70



0990_SW29_17/05/01

0990_SW31_17/05/01

0990_SW32_17/05/01






13C2-8:2 FTS (surr.) 1 % 113 131 118 120


Conductivity (at 25°C) 1 uS/cm - - 660 690

pH 0.1 pH Units - - 8.4 8.4


0990_SW38_17/04/30

0990_SW39_17/04/30

0990_SW44_17/04/30







13C4-PFBA (surr.) 1 % 120 119 120 107

Perfluoropentanoic acid (PFPeA) 0.01 ug/L < 0.01 < 0.01 < 0.01 0.02

13C5-PFPeA (surr.) 1 % 139 135 129 127

Perfluorohexanoic acid (PFHxA) 0.01 ug/L < 0.01 < 0.01 < 0.01 N090.01

13C5-PFHxA (surr.) 1 % 129 129 132 118

Perfluoroheptanoic acid (PFHpA) 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

13C4-PFHpA (surr.) 1 % 121 121 125 112

Perfluorooctanoic acid (PFOA) 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

13C8-PFOA (surr.) 1 % 105 111 116 103


13C5-PFNA (surr.) 1 % 93 99 108 97


13C6-PFDA (surr.) 1 % 78 80 85 83


13C2-PFUnDA (surr.) 1 % 74 70 75 76


13C2-PFDoDA (surr.) 1 % 75 70 75 72



13C2-PFTeDA (surr.) 1 % 71 71 80 63



13C8-FOSA (surr.) 1 % 59 64 70 61


D3-N-MeFOSA (surr.) 1 % 57 66 69 60


D5-N-EtFOSA (surr.) 1 % 74 67 65 65


D7-N-MeFOSE (surr.) 1 % 49 53 61 44


D9-N-EtFOSE (surr.) 1 % 51 53 63 51



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 17 of 70



0990_SW38_17/04/30

0990_SW39_17/04/30

0990_SW44_17/04/30







D5-N-EtFOSAA (surr.) 1 % 75 76 77 86


D3-N-MeFOSAA (surr.) 1 % 77 76 83 91


Perfluorobutanesulfonic acid (PFBS) 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

13C3-PFBS (surr.) 1 % 132 133 135 122

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01


18O2-PFHxS (surr.) 1 % 103 108 112 103



13C8-PFOS (surr.) 1 % 72 73 78 78




13C2-4:2 FTS (surr.) 1 % 197 194 199 178


13C2-6:2 FTS (surr.) 1 % 131 132 139 127


13C2-8:2 FTS (surr.) 1 % 125 122 130 128



pH 0.1 pH Units 7.9 7.7 - 8.1


0990_SW49_17/04/30

0990_SW50_17/05/01

0990_SW51_17/05/01






Perfluorobutanoic acid (PFBA) 0.05 ug/L 0.06 0.09 < 0.05 < 0.05

13C4-PFBA (surr.) 1 % 93 124 119 119

Perfluoropentanoic acid (PFPeA) 0.01 ug/L 0.07 0.14 0.04 0.04

13C5-PFPeA (surr.) 1 % 97 126 133 129


13C5-PFHxA (surr.) 1 % 88 118 123 127


13C4-PFHpA (surr.) 1 % 85 121 119 125


13C8-PFOA (surr.) 1 % 77 113 109 114


13C5-PFNA (surr.) 1 % 68 108 100 105




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 18 of 70



0990_SW49_17/04/30

0990_SW50_17/05/01

0990_SW51_17/05/01






13C6-PFDA (surr.) 1 % 53 90 81 83


13C2-PFUnDA (surr.) 1 % 45 73 75 73


13C2-PFDoDA (surr.) 1 % 40 67 76 72



13C2-PFTeDA (surr.) 1 % 49 89 90 84



13C8-FOSA (surr.) 1 % 39 60 62 62


D3-N-MeFOSA (surr.) 1 % 42 67 72 68


D5-N-EtFOSA (surr.) 1 % 53 67 77 72


D7-N-MeFOSE (surr.) 1 % 29 44 49 47


D9-N-EtFOSE (surr.) 1 % 32 47 55 50


D5-N-EtFOSAA (surr.) 1 % 45 75 78 72


D3-N-MeFOSAA (surr.) 1 % 49 84 83 76



13C3-PFBS (surr.) 1 % 92 122 129 132



18O2-PFHxS (surr.) 1 % 72 100 103 107



13C8-PFOS (surr.) 1 % 48 76 72 69




13C2-4:2 FTS (surr.) 1 % 129 161 190 191


13C2-6:2 FTS (surr.) 1 % 84 118 132 139


13C2-8:2 FTS (surr.) 1 % 73 119 125 124


Conductivity (at 25°C) 1 uS/cm - - 650 -

pH 0.1 pH Units - - 7.8 -



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 19 of 70



0990_SW54_17/04/29

0990_SW56_17/0430

0990_SW57_17/04/30







13C4-PFBA (surr.) 1 % 121 128 95 118

Perfluoropentanoic acid (PFPeA) 0.01 ug/L 0.04 0.02 0.02 0.02

13C5-PFPeA (surr.) 1 % 133 128 86 134


13C5-PFHxA (surr.) 1 % 126 126 89 125


13C4-PFHpA (surr.) 1 % 122 121 84 123

Perfluorooctanoic acid (PFOA) 0.01 ug/L N090.04 0.01 N090.01 N090.01

13C8-PFOA (surr.) 1 % 113 109 73 113


13C5-PFNA (surr.) 1 % 106 94 63 105


13C6-PFDA (surr.) 1 % 78 77 52 79


13C2-PFUnDA (surr.) 1 % 69 68 44 66


13C2-PFDoDA (surr.) 1 % 69 69 42 67



13C2-PFTeDA (surr.) 1 % 86 83 53 103



13C8-FOSA (surr.) 1 % 66 60 41 62


D3-N-MeFOSA (surr.) 1 % 76 62 37 79


D5-N-EtFOSA (surr.) 1 % 92 55 44 96


D7-N-MeFOSE (surr.) 1 % 57 44 27 54


D9-N-EtFOSE (surr.) 1 % 64 51 30 58


D5-N-EtFOSAA (surr.) 1 % 70 65 44 73


D3-N-MeFOSAA (surr.) 1 % 75 64 46 77



13C3-PFBS (surr.) 1 % 131 129 90 131



18O2-PFHxS (surr.) 1 % 104 104 69 108



13C8-PFOS (surr.) 1 % 71 69 47 77




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 20 of 70



0990_SW54_17/04/29

0990_SW56_17/0430

0990_SW57_17/04/30







13C2-4:2 FTS (surr.) 1 % 189 173 112 189


13C2-6:2 FTS (surr.) 1 % 135 115 69 135


13C2-8:2 FTS (surr.) 1 % 117 102 62 117


Conductivity (at 25°C) 1 uS/cm - - 670 -

pH 0.1 pH Units - - 8.0 -


0990_SW59_17/04/30

0990_SW60_17/04/30

0990_SW61_17/04/30






Perfluorobutanoic acid (PFBA) 0.05 ug/L < 0.05 < 0.05 < 0.05 0.08

13C4-PFBA (surr.) 1 % 127 126 108 110


13C5-PFPeA (surr.) 1 % 115 117 110 102


13C5-PFHxA (surr.) 1 % 127 125 117 106

Perfluoroheptanoic acid (PFHpA) 0.01 ug/L < 0.01 < 0.01 0.01 N090.07

13C4-PFHpA (surr.) 1 % 127 132 122 107


13C8-PFOA (surr.) 1 % 116 125 112 95


13C5-PFNA (surr.) 1 % 103 105 102 77


13C6-PFDA (surr.) 1 % 75 69 73 57


13C2-PFUnDA (surr.) 1 % 64 55 61 46


13C2-PFDoDA (surr.) 1 % 62 53 62 45



13C2-PFTeDA (surr.) 1 % 63 54 64 61



13C8-FOSA (surr.) 1 % 74 66 62 40


D3-N-MeFOSA (surr.) 1 % 85 87 79 43


D5-N-EtFOSA (surr.) 1 % 100 97 83 55



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 21 of 70



0990_SW59_17/04/30

0990_SW60_17/04/30

0990_SW61_17/04/30







D7-N-MeFOSE (surr.) 1 % 61 52 58 29


D9-N-EtFOSE (surr.) 1 % 69 57 62 34


D5-N-EtFOSAA (surr.) 1 % 65 54 60 43


D3-N-MeFOSAA (surr.) 1 % 64 58 63 49



13C3-PFBS (surr.) 1 % 128 128 116 106



18O2-PFHxS (surr.) 1 % 111 113 101 87



13C8-PFOS (surr.) 1 % 69 65 66 50




13C2-4:2 FTS (surr.) 1 % 174 179 168 137


13C2-6:2 FTS (surr.) 1 % 125 137 126 92


13C2-8:2 FTS (surr.) 1 % 99 91 99 64



pH 0.1 pH Units 7.9 7.8 - 7.6


0990_SW64_17/04/30

0990_SW68_17/04/30

0990_SW74_17/04/29






Perfluorobutanoic acid (PFBA) 0.05 ug/L 0.12 0.11 < 0.05 < 0.05

13C4-PFBA (surr.) 1 % 93 112 114 104

Perfluoropentanoic acid (PFPeA) 0.01 ug/L N090.19 N090.18 < 0.01 N090.02

13C5-PFPeA (surr.) 1 % 90 108 113 115


13C5-PFHxA (surr.) 1 % 97 108 120 123

Perfluoroheptanoic acid (PFHpA) 0.01 ug/L N090.09 N090.08 < 0.01 < 0.01



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 22 of 70



0990_SW64_17/04/30

0990_SW68_17/04/30

0990_SW74_17/04/29






13C4-PFHpA (surr.) 1 % 100 111 116 116

Perfluorooctanoic acid (PFOA) 0.01 ug/L N090.19 N090.22 < 0.01 N090.01

13C8-PFOA (surr.) 1 % 84 97 97 96


13C5-PFNA (surr.) 1 % 74 86 65 75


13C6-PFDA (surr.) 1 % 58 67 50 57


13C2-PFUnDA (surr.) 1 % 45 58 43 46


13C2-PFDoDA (surr.) 1 % 42 57 47 50



13C2-PFTeDA (surr.) 1 % 38 72 51 60



13C8-FOSA (surr.) 1 % 37 45 36 43


D3-N-MeFOSA (surr.) 1 % 40 44 40 44


D5-N-EtFOSA (surr.) 1 % 39 45 50 58


D7-N-MeFOSE (surr.) 1 % 28 35 29 31


D9-N-EtFOSE (surr.) 1 % 32 38 34 35


D5-N-EtFOSAA (surr.) 1 % 51 63 46 45


D3-N-MeFOSAA (surr.) 1 % 56 64 51 51



13C3-PFBS (surr.) 1 % 102 114 123 121



18O2-PFHxS (surr.) 1 % 82 88 91 95

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L N090.10 N090.17 < 0.01 N090.01


13C8-PFOS (surr.) 1 % 49 63 43 50




13C2-4:2 FTS (surr.) 1 % 142 160 175 173


13C2-6:2 FTS (surr.) 1 % 92 107 105 107




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 23 of 70



0990_SW64_17/04/30

0990_SW68_17/04/30

0990_SW74_17/04/29






13C2-8:2 FTS (surr.) 1 % 75 94 72 75


Conductivity (at 25°C) 1 uS/cm - 520 - -

pH 0.1 pH Units - 8.2 - -


0990_QC10SW_17/04/30

0990_QC11SW_17/04/30

0990_QC15SW_17/05/01



Date Sampled May 01, 2017 Apr 30, 2017 Apr 30, 2017 May 01, 2017




13C4-PFBA (surr.) 1 % 88 103 114 107

Perfluoropentanoic acid (PFPeA) 0.01 ug/L < 0.01 N090.16 N090.02 N090.04

13C5-PFPeA (surr.) 1 % 91 112 117 105

Perfluorohexanoic acid (PFHxA) 0.01 ug/L < 0.01 N090.44 N090.04 N090.11

13C5-PFHxA (surr.) 1 % 100 119 126 114

Perfluoroheptanoic acid (PFHpA) 0.01 ug/L < 0.01 N090.07 < 0.01 N090.02

13C4-PFHpA (surr.) 1 % 97 121 115 109

Perfluorooctanoic acid (PFOA) 0.01 ug/L < 0.01 N090.16 N090.01 N090.04

13C8-PFOA (surr.) 1 % 80 115 101 97


13C5-PFNA (surr.) 1 % 68 109 91 85


13C6-PFDA (surr.) 1 % 56 73 63 53


13C2-PFUnDA (surr.) 1 % 45 59 50 43


13C2-PFDoDA (surr.) 1 % 41 59 52 46



13C2-PFTeDA (surr.) 1 % 34 62 64 55



13C8-FOSA (surr.) 1 % 43 66 58 55


D3-N-MeFOSA (surr.) 1 % 42 82 68 64


D5-N-EtFOSA (surr.) 1 % 42 80 86 67


D7-N-MeFOSE (surr.) 1 % 34 66 53 54


D9-N-EtFOSE (surr.) 1 % 36 64 54 54



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 24 of 70



0990_QC10SW_17/04/30

0990_QC11SW_17/04/30

0990_QC15SW_17/05/01



Date Sampled May 01, 2017 Apr 30, 2017 Apr 30, 2017 May 01, 2017




D5-N-EtFOSAA (surr.) 1 % 48 57 51 45


D3-N-MeFOSAA (surr.) 1 % 54 60 52 50


Perfluorobutanesulfonic acid (PFBS) 0.01 ug/L < 0.01 N090.19 N090.03 N090.06

13C3-PFBS (surr.) 1 % 105 119 126 114

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L < 0.01 N090.16 N090.03 N090.06

Perfluorohexanesulfonic acid (PFHxS) 0.01 ug/L < 0.01 N091.4 N090.20 N090.45

18O2-PFHxS (surr.) 1 % 82 94 95 89

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L < 0.01 N090.08 N090.01 N090.03


13C8-PFOS (surr.) 1 % 52 75 59 51




13C2-4:2 FTS (surr.) 1 % 143 169 172 149


13C2-6:2 FTS (surr.) 1 % 89 131 110 101


13C2-8:2 FTS (surr.) 1 % 73 100 79 70


Conductivity (at 25°C) 1 uS/cm - - 680 690

pH 0.1 pH Units - - 8.0 7.8


0990_NT0049MW02_170428

0990_NT0367MW01_170428

0990_NT0077MW01_170428



Date Sampled May 01, 2017 Apr 28, 2017 Apr 28, 2017 Apr 28, 2017




13C4-PFBA (surr.) 1 % 112 121 108 110

Perfluoropentanoic acid (PFPeA) 0.01 ug/L N090.03 0.06 < 0.01 N090.02

13C5-PFPeA (surr.) 1 % 119 126 122 118

Perfluorohexanoic acid (PFHxA) 0.01 ug/L N090.10 N090.06 < 0.01 N090.03

13C5-PFHxA (surr.) 1 % 120 127 128 123

Perfluoroheptanoic acid (PFHpA) 0.01 ug/L N090.02 N090.03 < 0.01 N090.01

13C4-PFHpA (surr.) 1 % 114 126 125 125

Perfluorooctanoic acid (PFOA) 0.01 ug/L N090.03 N090.02 < 0.01 N090.02

13C8-PFOA (surr.) 1 % 102 119 111 117


13C5-PFNA (surr.) 1 % 91 119 99 114




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 25 of 70



0990_NT0049MW02_170428

0990_NT0367MW01_170428

0990_NT0077MW01_170428



Date Sampled May 01, 2017 Apr 28, 2017 Apr 28, 2017 Apr 28, 2017



13C6-PFDA (surr.) 1 % 66 110 82 107


13C2-PFUnDA (surr.) 1 % 57 93 82 107


13C2-PFDoDA (surr.) 1 % 56 65 60 65



13C2-PFTeDA (surr.) 1 % 61 72 69 117



13C8-FOSA (surr.) 1 % 59 75 52 63


D3-N-MeFOSA (surr.) 1 % 66 86 59 80


D5-N-EtFOSA (surr.) 1 % 73 104 68 111


D7-N-MeFOSE (surr.) 1 % 57 71 36 50


D9-N-EtFOSE (surr.) 1 % 53 70 38 61


D5-N-EtFOSAA (surr.) 1 % 60 78 65 92


D3-N-MeFOSAA (surr.) 1 % 62 124 105 133


Perfluorobutanesulfonic acid (PFBS) 0.01 ug/L N090.06 N090.01 < 0.01 N090.03

13C3-PFBS (surr.) 1 % 121 126 123 124

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L N090.05 N090.01 < 0.01 N090.03


18O2-PFHxS (surr.) 1 % 92 111 105 108

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L N090.03 < 0.01 < 0.01 N090.02


13C8-PFOS (surr.) 1 % 63 94 73 88




13C2-4:2 FTS (surr.) 1 % 171 179 172 181


13C2-6:2 FTS (surr.) 1 % 115 131 120 130


13C2-8:2 FTS (surr.) 1 % 92 151 112 156



pH 0.1 pH Units 8.2 - 7.0 7.1



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 26 of 70



0990_077MW03_170428

0990_NT0046MW01_170429

0990_NT0046MW03_170429






Perfluorobutanoic acid (PFBA) 0.05 ug/L < 0.05 < 0.05 0.11 < 0.05

13C4-PFBA (surr.) 1 % 117 107 104 105

Perfluoropentanoic acid (PFPeA) 0.01 ug/L N090.02 N090.02 N090.23 < 0.01

13C5-PFPeA (surr.) 1 % 120 109 98 92


13C5-PFHxA (surr.) 1 % 126 124 98 103

Perfluoroheptanoic acid (PFHpA) 0.01 ug/L < 0.01 < 0.01 N090.04 < 0.01

13C4-PFHpA (surr.) 1 % 127 125 103 102

Perfluorooctanoic acid (PFOA) 0.01 ug/L N090.01 N090.01 N090.05 < 0.01

13C8-PFOA (surr.) 1 % 113 117 94 98


13C5-PFNA (surr.) 1 % 109 119 88 98


13C6-PFDA (surr.) 1 % 105 108 78 90


13C2-PFUnDA (surr.) 1 % 97 102 67 61


13C2-PFDoDA (surr.) 1 % 64 73 55 50



13C2-PFTeDA (surr.) 1 % 95 72 56 65



13C8-FOSA (surr.) 1 % 64 70 49 61


D3-N-MeFOSA (surr.) 1 % 77 84 46 68


D5-N-EtFOSA (surr.) 1 % 87 100 51 73


D7-N-MeFOSE (surr.) 1 % 53 56 34 56


D9-N-EtFOSE (surr.) 1 % 63 66 40 58


D5-N-EtFOSAA (surr.) 1 % 79 89 72 57


D3-N-MeFOSAA (surr.) 1 % 123 136 73 66


Perfluorobutanesulfonic acid (PFBS) 0.01 ug/L N090.04 N090.03 N090.48 < 0.01

13C3-PFBS (surr.) 1 % 126 122 105 105

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L 0.03 N090.02 N090.25 < 0.01


18O2-PFHxS (surr.) 1 % 106 108 89 99

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L N090.01 N090.01 N090.04 < 0.01


13C8-PFOS (surr.) 1 % 85 95 69 81




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 27 of 70



0990_077MW03_170428

0990_NT0046MW01_170429

0990_NT0046MW03_170429







13C2-4:2 FTS (surr.) 1 % 176 171 152 139


13C2-6:2 FTS (surr.) 1 % 126 134 108 113


13C2-8:2 FTS (surr.) 1 % 144 157 107 121



pH 0.1 pH Units 7.1 7.0 - 7.5


0990_NT0050MW01_170429

0990_054MW02_170428

R160990_064MW01_170429






Perfluorobutanoic acid (PFBA) 0.05 ug/L 2.5 < 0.05 < 0.05 12

13C4-PFBA (surr.) 1 % 75 98 106 131

Perfluoropentanoic acid (PFPeA) 0.01 ug/L N093.9 < 0.01 < 0.01 N0915

13C5-PFPeA (surr.) 1 % 66 104 111 112

Perfluorohexanoic acid (PFHxA) 0.01 ug/L N0917 < 0.01 < 0.01 N0926

13C5-PFHxA (surr.) 1 % 99 111 120 121

Perfluoroheptanoic acid (PFHpA) 0.01 ug/L N092.3 < 0.01 < 0.01 N0911

13C4-PFHpA (surr.) 1 % 69 111 117 123

Perfluorooctanoic acid (PFOA) 0.01 ug/L N095.4 < 0.01 < 0.01 N0923

13C8-PFOA (surr.) 1 % 95 101 113 120

Perfluorononanoic acid (PFNA) 0.01 ug/L N090.09 < 0.01 < 0.01 3.1

13C5-PFNA (surr.) 1 % 68 97 101 121

Perfluorodecanoic acid (PFDA) 0.01 ug/L < 0.01 < 0.01 < 0.01 0.71

13C6-PFDA (surr.) 1 % 43 90 93 110


13C2-PFUnDA (surr.) 1 % 50 90 84 115


13C2-PFDoDA (surr.) 1 % 45 67 68 109



13C2-PFTeDA (surr.) 1 % 48 127 97 66



13C8-FOSA (surr.) 1 % 38 53 55 113


D3-N-MeFOSA (surr.) 1 % 43 58 55 93


D5-N-EtFOSA (surr.) 1 % 48 74 80 100



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 28 of 70



0990_NT0050MW01_170429

0990_054MW02_170428

R160990_064MW01_170429







D7-N-MeFOSE (surr.) 1 % 31 44 43 95


D9-N-EtFOSE (surr.) 1 % 30 51 46 92


D5-N-EtFOSAA (surr.) 1 % 50 95 74 113


D3-N-MeFOSAA (surr.) 1 % 52 121 92 107


Perfluorobutanesulfonic acid (PFBS) 0.01 ug/L N096.1 < 0.01 N090.02 13

13C3-PFBS (surr.) 1 % 109 113 125 136

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L N095.6 < 0.01 N090.01 N098.5

Perfluorohexanesulfonic acid (PFHxS) 0.01 ug/L N0934 < 0.01 N090.05 N0970

18O2-PFHxS (surr.) 1 % 97 101 109 121

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L N093.0 < 0.01 < 0.01 N0912

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N09110 N090.08 N090.05 N09660

13C8-PFOS (surr.) 1 % 91 76 77 85




13C2-4:2 FTS (surr.) 1 % 95 158 170 129

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) 0.05 ug/L 0.17 < 0.05 < 0.05 0.41

13C2-6:2 FTS (surr.) 1 % 78 127 126 117

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) 0.01 ug/L 0.08 < 0.01 < 0.01 25

13C2-8:2 FTS (surr.) 1 % 67 142 130 127



pH 0.1 pH Units 7.5 - 7.0 7.2

Client Sample IDR160990_064MW02_170429

0990_064MW04_170429

0990_064MW05_170429

0990_064MW06_170429






Perfluorobutanoic acid (PFBA) 0.05 ug/L 48 < 0.05 < 0.05 0.05

13C4-PFBA (surr.) 1 % 115 100 90 137

Perfluoropentanoic acid (PFPeA) 0.01 ug/L N09120 < 0.01 N090.01 N090.06

13C5-PFPeA (surr.) 1 % 93 111 91 140

Perfluorohexanoic acid (PFHxA) 0.01 ug/L N09370 N090.01 N090.02 N090.29

13C5-PFHxA (surr.) 1 % 114 117 90 155

Perfluoroheptanoic acid (PFHpA) 0.01 ug/L N0963 < 0.01 < 0.01 N090.04



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 29 of 70



0990_064MW04_170429

0990_064MW05_170429

0990_064MW06_170429






13C4-PFHpA (surr.) 1 % 101 113 92 155

Perfluorooctanoic acid (PFOA) 0.01 ug/L N09160 < 0.01 < 0.01 N090.09

13C8-PFOA (surr.) 1 % 95 101 86 143

Perfluorononanoic acid (PFNA) 0.01 ug/L N095.4 < 0.01 < 0.01 < 0.01

13C5-PFNA (surr.) 1 % 111 96 87 145


13C6-PFDA (surr.) 1 % 65 87 78 136


13C2-PFUnDA (surr.) 1 % 103 76 75 124


13C2-PFDoDA (surr.) 1 % 90 66 69 100



13C2-PFTeDA (surr.) 1 % 56 114 44 65



13C8-FOSA (surr.) 1 % 103 54 47 100


D3-N-MeFOSA (surr.) 1 % 73 68 48 99


D5-N-EtFOSA (surr.) 1 % 67 79 51 123


D7-N-MeFOSE (surr.) 1 % 73 45 34 76


D9-N-EtFOSE (surr.) 1 % 68 51 35 66


D5-N-EtFOSAA (surr.) 1 % 103 76 96 96


D3-N-MeFOSAA (surr.) 1 % 98 77 97 100


Perfluorobutanesulfonic acid (PFBS) 0.01 ug/L 130 N090.41 N090.17 0.20

13C3-PFBS (surr.) 1 % 102 120 93 152

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L N09100 N090.26 N090.07 N090.17

Perfluorohexanesulfonic acid (PFHxS) 0.01 ug/L N09650 N090.82 N090.75 N090.96

18O2-PFHxS (surr.) 1 % 110 99 80 140

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L N0938 N090.01 < 0.01 N090.05

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N093600 N090.28 N090.06 N090.22

13C8-PFOS (surr.) 1 % 124 78 66 133




13C2-4:2 FTS (surr.) 1 % 72 167 129 174

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) 0.05 ug/L 3.9 < 0.05 < 0.05 < 0.05

13C2-6:2 FTS (surr.) 1 % 86 120 107 127

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) 0.01 ug/L 0.74 < 0.01 < 0.01 < 0.01



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 30 of 70



0990_064MW04_170429

0990_064MW05_170429

0990_064MW06_170429






13C2-8:2 FTS (surr.) 1 % 95 128 116 123


Conductivity (at 25°C) 1 uS/cm 480 - - -

pH 0.1 pH Units 7.2 - - -


0990_SW53_170429

Sample Matrix Water Water

Eurofins | mgt Sample No. M17-My03538 M17-My03539

Date Sampled Apr 29, 2017 Apr 29, 2017



Perfluorobutanoic acid (PFBA) 0.05 ug/L 0.18 < 0.05

13C4-PFBA (surr.) 1 % 104 113

Perfluoropentanoic acid (PFPeA) 0.01 ug/L N090.25 < 0.01

13C5-PFPeA (surr.) 1 % 114 105

Perfluorohexanoic acid (PFHxA) 0.01 ug/L N091.1 N090.01

13C5-PFHxA (surr.) 1 % 102 119

Perfluoroheptanoic acid (PFHpA) 0.01 ug/L N090.09 < 0.01

13C4-PFHpA (surr.) 1 % 108 105

Perfluorooctanoic acid (PFOA) 0.01 ug/L N090.15 < 0.01

13C8-PFOA (surr.) 1 % 88 84

Perfluorononanoic acid (PFNA) 0.01 ug/L < 0.01 < 0.01

13C5-PFNA (surr.) 1 % 82 68

Perfluorodecanoic acid (PFDA) 0.01 ug/L < 0.01 < 0.01

13C6-PFDA (surr.) 1 % 76 55

Perfluoroundecanoic acid (PFUnA) 0.01 ug/L < 0.01 < 0.01

13C2-PFUnDA (surr.) 1 % 77 49

Perfluorododecanoic acid (PFDoA) 0.01 ug/L < 0.01 < 0.01

13C2-PFDoDA (surr.) 1 % 54 50

Perfluorotridecanoic acid (PFTrDA) 0.01 ug/L < 0.01 < 0.01

Perfluorotetradecanoic acid (PFTeDA) 0.01 ug/L < 0.01 < 0.01

13C2-PFTeDA (surr.) 1 % 104 67


Perfluorooctane sulfonamide (FOSA) 0.05 ug/L < 0.05 < 0.05

13C8-FOSA (surr.) 1 % 47 38

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA) 0.05 ug/L < 0.05 < 0.05

D3-N-MeFOSA (surr.) 1 % 66 43

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA) 0.05 ug/L < 0.05 < 0.05

D5-N-EtFOSA (surr.) 1 % 70 72

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol(N-MeFOSE) 0.05 ug/L < 0.05 < 0.05

D7-N-MeFOSE (surr.) 1 % 47 34

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE) 0.05 ug/L < 0.05 < 0.05

D9-N-EtFOSE (surr.) 1 % 49 33



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 31 of 70



0990_SW53_170429


Eurofins | mgt Sample No. M17-My03538 M17-My03539

Date Sampled Apr 29, 2017 Apr 29, 2017



N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA) 0.05 ug/L < 0.05 < 0.05

D5-N-EtFOSAA (surr.) 1 % 78 51

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA) 0.05 ug/L < 0.05 < 0.05

D3-N-MeFOSAA (surr.) 1 % 108 49


Perfluorobutanesulfonic acid (PFBS) 0.01 ug/L N090.65 N090.01

13C3-PFBS (surr.) 1 % 112 123

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L N090.45 < 0.01

Perfluorohexanesulfonic acid (PFHxS) 0.01 ug/L N094.3 N090.06

18O2-PFHxS (surr.) 1 % 107 87

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L N090.14 < 0.01

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N093.8 N090.07

13C8-PFOS (surr.) 1 % 69 48

Perfluorodecanesulfonic acid (PFDS) 0.01 ug/L < 0.01 < 0.01


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2 FTS) 0.01 ug/L < 0.01 < 0.01

13C2-4:2 FTS (surr.) 1 % 172 157

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) 0.05 ug/L < 0.05 < 0.05

13C2-6:2 FTS (surr.) 1 % 119 94

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) 0.01 ug/L 0.02 < 0.01

13C2-8:2 FTS (surr.) 1 % 124 73

1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2FTS) 0.01 ug/L < 0.01 < 0.01

Conductivity (at 25°C) 1 uS/cm 200 790

pH 0.1 pH Units 7.5 7.3



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 32 of 70





PFOS/PFOA/6:2FTS Brisbane May 03, 2017 14 Day

- Method: LTM-ORG-2100 Analysis of PFCs in environmental samples by LC-MS/MS

Conductivity (at 25°C) Brisbane May 08, 2017 28 Day

- Method: LTM-INO-4030

pH Brisbane May 08, 2017 0 Day

- Method: LTM-GEN-7090 pH in water by ISE












ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 33 of 70


.Company Name: Coffey Environments Pty Ltd VIC Order No.: Received: May 3, 2017 10:00 AMAddress: 3G Marine Pde Report #: 544592 Due: May 10, 2017

Abbotsford Phone: 03 8413 6900 Priority: 5 DayVIC 3067 Fax: Contact Name: Chris Molloy



Sample Detail

Conductivity (at 25°C

)

HO

LD

pH PF

OS

/PF

OA

/6:2FT

S

Per- and P


ubstances(P

FA

Ss)



Brisbane Laboratory - NATA Site # 20794 X X X X X


External Laboratory


Matrix LAB ID

1 0990_053MW01_170427

Apr 28, 2017 Water M17-My03446 X X X

2 0990_053MW06_170428

Apr 28, 2017 Water M17-My03448 X X X

3 0990_070MW01_170428

Apr 28, 2017 Water M17-My03449 X

4 0990_BCPMW01_170428

Apr 28, 2017 Water M17-My03450 X X X

5 0990_BCRUMW01_170428

Apr 28, 2017 Water M17-My03451 X X X

6 0990_BORE06 Apr 28, 2017 Water M17-My03452 X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 34 of 70


Company Name: Coffey Environments Pty Ltd VIC Order No.: Received: May 3, 2017 10:00 AMAddress: 3G Marine Pde Report #: 544592 Due: May 10, 2017




Sample Detail


)

HO

LD

pH PF

OS

/PF

OA

/6:2FT

S

Per- and P


ubstances(P

FA

Ss)





_170428

7 0990_BORE05_170428

Apr 28, 2017 Water M17-My03453 X X X

8 0990_NT0073MW02_170428

Apr 28, 2017 Water M17-My03454X X X

9 0990_NT0050MW02_170429


10 0990_NT0065MW02_170428

Apr 28, 2017 Water M17-My03456X

11 0990_NT0065MW04_170428









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 35 of 70






Sample Detail


)

HO

LD

pH PF

OS

/PF

OA

/6:2FT

S

Per- and P


ubstances(P

FA

Ss)





12 0990_NT0269MW01_170428


13 0990_NT0269MW02_170428


14 0990_BORE24_170428

Apr 28, 2017 Water M17-My03460 X

15 0990_NT0048MW1_170428

Apr 28, 2017 Water M17-My03461 X X X

16 0990_NT0064MW11_170429


17 0990_NT0064MW12_17042

Apr 29, 2017 Water M17-My03463X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 36 of 70






Sample Detail


)

HO

LD

pH PF

OS

/PF

OA

/6:2FT

S

Per- and P


ubstances(P

FA

Ss)





9

18 0990_NT0064MW13_170429


19 0990_NT0064MW14_170429

Apr 29, 2017 Water M17-My03465X

20 0990_BORE10_170429

Apr 29, 2017 Water M17-My03466 X X X

21 0990_BORE11_170429

Apr 29, 2017 Water M17-My03467 X X X

22 0990_QC1GW_170428

Apr 28, 2017 Water M17-My03468 X

23 0990_QC2GW_170428

Apr 28, 2017 Water M17-My03469 X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 37 of 70






Sample Detail


)

HO

LD

pH PF

OS

/PF

OA

/6:2FT

S

Per- and P


ubstances(P

FA

Ss)





24 0990_QCSGW_170428

Apr 28, 2017 Water M17-My03473 X

25 0990_QC9GW_170429

Apr 29, 2017 Water M17-My03474 X

26 0990_QC13GW_170430

Apr 30, 2017 Water M17-My03475 X

27 0990_QC18GW_170501

May 01, 2017 Water M17-My03476 X

28 0990_75COLLINS-BORE_170428

Apr 28, 2017 Water M17-My03477X

29 0990_PRIVATE BORE001_170428

Apr 28, 2017 Water M17-My03478X

30 0990_QC6_17 Apr 28, 2017 Water M17-My03479 X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 38 of 70


emma.delborrello

Rectangle





Sample Detail


)

HO

LD

pH PF

OS

/PF

OA

/6:2FT

S

Per- and P


ubstances(P

FA

Ss)





/04/28

31 0990_QC14_17/04/30

Apr 30, 2017 Water M17-My03480 X

32 0990_SW04_17/04/30

Apr 30, 2017 Water M17-My03481 X

33 0990_SW05_17/04/30

Apr 30, 2017 Water M17-My03482 X

34 0990_SW06_17/04/30

Apr 30, 2017 Water M17-My03483 X X X

35 0990_SW07_17/05/01

May 01, 2017 Water M17-My03484 X

36 0990_SW09_17/05/01

May 01, 2017 Water M17-My03485 X X X

37 0990_SW14_1 May 01, 2017 Water M17-My03486 X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 39 of 70






Sample Detail


)

HO

LD

pH PF

OS

/PF

OA

/6:2FT

S

Per- and P


ubstances(P

FA

Ss)





7/05/01

38 0990_SW16_17/05/01

May 01, 2017 Water M17-My03487 X

39 0990_SW23_17/05/01

May 01, 2017 Water M17-My03488 X

40 0990_SW27_17/05/01

May 01, 2017 Water M17-My03489 X X X

41 0990_SW28_17/05/01

May 01, 2017 Water M17-My03490 X

42 0990_SW29_17/05/01

May 01, 2017 Water M17-My03491 X

43 0990_SW31_17/05/01

May 01, 2017 Water M17-My03492 X X X

44 0990_SW32_1 May 01, 2017 Water M17-My03493 X X X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 40 of 70






Sample Detail


)

HO

LD

pH PF

OS

/PF

OA

/6:2FT

S

Per- and P


ubstances(P

FA

Ss)





7/05/01

45 0990_SW37_17/04/30

Apr 30, 2017 Water M17-My03494 X X X

46 0990_SW38_17/04/30

Apr 30, 2017 Water M17-My03495 X X X

47 0990_SW39_17/04/30

Apr 30, 2017 Water M17-My03496 X

48 0990_SW44_17/04/30

Apr 30, 2017 Water M17-My03497 X X X

49 0990_SW46_17/04/30

Apr 30, 2017 Water M17-My03498 X

50 0990_SW49_17/04/30

Apr 30, 2017 Water M17-My03499 X

51 0990_SW50_1 May 01, 2017 Water M17-My03500 X X X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 41 of 70






Sample Detail


)

HO

LD

pH PF

OS

/PF

OA

/6:2FT

S

Per- and P


ubstances(P

FA

Ss)





7/05/01

52 0990_SW51_17/05/01

May 01, 2017 Water M17-My03501 X

53 0990_SW52_17/04/30

Apr 30, 2017 Water M17-My03502 X

54 0990_SW54_17/04/29

Apr 29, 2017 Water M17-My03503 X

55 0990_SW56_17/0430

Apr 30, 2017 Water M17-My03504 X X X

56 0990_SW57_17/04/30

Apr 30, 2017 Water M17-My03505 X

57 0990_SW58_17/04/30

Apr 30, 2017 Water M17-My03506 X X X

58 0990_SW59_1 Apr 30, 2017 Water M17-My03507 X X X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 42 of 70






Sample Detail


)

HO

LD

pH PF

OS

/PF

OA

/6:2FT

S

Per- and P


ubstances(P

FA

Ss)





7/04/30

59 0990_SW60_17/04/30

Apr 30, 2017 Water M17-My03508 X

60 0990_SW61_17/04/30

Apr 30, 2017 Water M17-My03509 X X X

61 0990_SW62_17/04/30

Apr 30, 2017 Water M17-My03510 X

62 0990_SW64_17/04/30

Apr 30, 2017 Water M17-My03511 X X X

63 0990_SW68_17/04/30

Apr 30, 2017 Water M17-My03512 X

64 0990_SW74_17/04/29

Apr 29, 2017 Water M17-My03513 X

65 0990_SW81_1 May 01, 2017 Water M17-My03514 X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 43 of 70






Sample Detail


)

HO

LD

pH PF

OS

/PF

OA

/6:2FT

S

Per- and P


ubstances(P

FA

Ss)





7/05/01

66 0990_QC10SW_17/04/30

Apr 30, 2017 Water M17-My03515 X

67 0990_QC11SW_17/04/30

Apr 30, 2017 Water M17-My03517 X X X

68 0990_QC15SW_17/05/01

May 01, 2017 Water M17-My03519 X X X

69 0990_SW21_17/05/01

May 01, 2017 Water M17-My03522 X X X

70 0990_NT0049MW02_170428

Apr 28, 2017 Water M17-My03523X

71 0990_NT0367MW01_170428









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 44 of 70






Sample Detail


)

HO

LD

pH PF

OS

/PF

OA

/6:2FT

S

Per- and P


ubstances(P

FA

Ss)





72 0990_NT0077MW01_170428


73 0990_077MW01_170428

Apr 28, 2017 Water M17-My03526 X X X

74 0990_077MW03_170428

Apr 28, 2017 Water M17-My03527 X X X

75 0990_NT0046MW01_170429

Apr 29, 2017 Water M17-My03528X

76 0990_NT0046MW03_170429


77 0990_NT0065MW03_17042









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 45 of 70






Sample Detail


)

HO

LD

pH PF

OS

/PF

OA

/6:2FT

S

Per- and P


ubstances(P

FA

Ss)





8

78 0990_NT0050MW01_170429

Apr 29, 2017 Water M17-My03531X

79 0990_054MW02_170428

Apr 28, 2017 Water M17-My03532 X X X

80 0990_064MW01_170429

Apr 29, 2017 Water M17-My03533 X X X

81 0990_064MW02_170429

Apr 29, 2017 Water M17-My03534 X X X

82 0990_064MW04_170429

Apr 29, 2017 Water M17-My03535 X

83 0990_064MW05_170429

Apr 29, 2017 Water M17-My03536 X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 46 of 70






Sample Detail


)

HO

LD

pH PF

OS

/PF

OA

/6:2FT

S

Per- and P


ubstances(P

FA

Ss)





84 0990_064MW06_170429

Apr 29, 2017 Water M17-My03537 X

85 0990_NT0064MW10_170429


86 0990_SW53_170429

Apr 29, 2017 Water M17-My03539 X X X

87 0990_053MWA_170428

Apr 29, 2017 Water M17-My03698 X









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 47 of 70



General

Holding Times

Units

Terms




request.





6. Samples were analysed on an 'as received' basis. 7. This report replaces any interim results previously issued.



Receipt Advice.




mg/kg: milligrams per Kilogram mg/l: milligrams per litre

ug/l: micrograms per litre ppm: Parts per million


org/100ml: Organisms per 100 millilitres NTU: Nephelometric Turbidity Units






LCS Laboratory Control Sample - reported as percent recovery

CRM Certified Reference Material - reported as percent recovery













NCP Non-Client Parent - QC performed on samples not pertaining to this report, QC is representative of the sequence or batch that client samples were analysed within























ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 48 of 70




PassLimits

QualifyingCode

Method Blank

PFOS/PFOA/6:2FTS




Method Blank













Method Blank









Method Blank








Method Blank






LCS - % Recovery

PFOS/PFOA/6:2FTS




LCS - % Recovery







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 49 of 70



PassLimits

QualifyingCode









LCS - % Recovery









LCS - % Recovery








LCS - % Recovery







LimitsPass

LimitsQualifying

Code

Spike - % Recovery

PFOS/PFOA/6:2FTS Result 1

Perfluorooctanesulfonic acid(PFOS) M17-My03451 CP % 100 50-150 Pass

Perfluorooctanoic acid (PFOA) M17-My03451 CP % 110 50-150 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-My03451 CP % 87 50-150 Pass

Spike - % Recovery


Perfluorobutanoic acid (PFBA) M17-My03451 CP % 112 50-150 Pass

Perfluoropentanoic acid (PFPeA) M17-My03451 CP % 109 50-150 Pass

Perfluorohexanoic acid (PFHxA) M17-My03451 CP % 111 50-150 Pass

Perfluoroheptanoic acid (PFHpA) M17-My03451 CP % 102 50-150 Pass

Perfluorononanoic acid (PFNA) M17-My03451 CP % 105 50-150 Pass

Perfluorodecanoic acid (PFDA) M17-My03451 CP % 109 50-150 Pass

Perfluoroundecanoic acid (PFUnA) M17-My03451 CP % 101 50-150 Pass

Perfluorododecanoic acid (PFDoA) M17-My03451 CP % 104 50-150 Pass

Perfluorotridecanoic acid (PFTrDA) M17-My03451 CP % 103 50-150 Pass

Perfluorotetradecanoic acid(PFTeDA) M17-My03451 CP % 107 50-150 Pass

Spike - % Recovery



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 50 of 70



LimitsPass

LimitsQualifying

Code


Perfluorooctane sulfonamide(FOSA) M17-My03451 CP % 98 50-150 Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) M17-My03451 CP % 123 50-150 Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) M17-My03451 CP % 99 50-150 Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) M17-My03451 CP % 89 50-150 Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) M17-My03451 CP % 105 50-150 Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-My03451 CP % 112 50-150 Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-My03451 CP % 91 50-150 Pass

Spike - % Recovery


Perfluorobutanesulfonic acid(PFBS) M17-My03451 CP % 92 50-150 Pass

Perfluoropentanesulfonic acid(PFPeS) M17-My03451 CP % 102 50-150 Pass

Perfluorohexanesulfonic acid(PFHxS) M17-My03451 CP % 101 50-150 Pass

Perfluoroheptanesulfonic acid(PFHpS) M17-My03451 CP % 109 50-150 Pass

Perfluorodecanesulfonic acid(PFDS) M17-My03451 CP % 86 50-150 Pass

Spike - % Recovery


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-My03451 CP % 93 50-150 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-My03451 CP % 102 50-150 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) M17-My03451 CP % 82 50-150 Pass

Spike - % Recovery





Spike - % Recovery












Spike - % Recovery



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 51 of 70



LimitsPass

LimitsQualifying

Code









Spike - % Recovery







Spike - % Recovery





Spike - % Recovery





Spike - % Recovery












Spike - % Recovery



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 52 of 70



LimitsPass

LimitsQualifying

Code









Spike - % Recovery







Spike - % Recovery





Spike - % Recovery





Spike - % Recovery












Spike - % Recovery



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 53 of 70



LimitsPass

LimitsQualifying

Code









Spike - % Recovery







Spike - % Recovery





Spike - % Recovery





Spike - % Recovery












Spike - % Recovery



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 54 of 70



LimitsPass

LimitsQualifying

Code









Spike - % Recovery







Spike - % Recovery





Spike - % Recovery





Spike - % Recovery












Spike - % Recovery



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 55 of 70



LimitsPass

LimitsQualifying

Code









Spike - % Recovery







Spike - % Recovery





Spike - % Recovery





Spike - % Recovery












Spike - % Recovery



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 56 of 70



LimitsPass

LimitsQualifying

Code









Spike - % Recovery







Spike - % Recovery





Spike - % Recovery





Spike - % Recovery












Spike - % Recovery



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 57 of 70



LimitsPass

LimitsQualifying

Code









Spike - % Recovery







Spike - % Recovery





Spike - % Recovery





Spike - % Recovery












Spike - % Recovery



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 58 of 70



LimitsPass

LimitsQualifying

Code









Spike - % Recovery







Spike - % Recovery






LimitsPass

LimitsQualifying

Code

Duplicate


Conductivity (at 25°C) M17-My03446 CP uS/cm 1000 970 6.4 30% Pass

pH M17-My03446 CP pH Units 6.9 6.9 pass 30% Pass

Duplicate

PFOS/PFOA/6:2FTS Result 1 Result 2 RPD

Perfluorooctanesulfonic acid(PFOS) M17-My03449 CP ug/L 0.07 0.09 15 30% Pass

Perfluorooctanoic acid (PFOA) M17-My03449 CP ug/L 0.01 0.01 2.0 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-My03449 CP ug/L < 0.05 < 0.05 <1 30% Pass

Duplicate


Perfluorobutanoic acid (PFBA) M17-My03449 CP ug/L < 0.05 < 0.05 <1 30% Pass

Perfluoropentanoic acid (PFPeA) M17-My03449 CP ug/L 0.02 0.02 3.0 30% Pass

Perfluorohexanoic acid (PFHxA) M17-My03449 CP ug/L 0.09 0.09 3.0 30% Pass

Perfluoroheptanoic acid (PFHpA) M17-My03449 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorononanoic acid (PFNA) M17-My03449 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanoic acid (PFDA) M17-My03449 CP ug/L < 0.01 < 0.01 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 59 of 70


Duplicate


Perfluoroundecanoic acid (PFUnA) M17-My03449 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorododecanoic acid (PFDoA) M17-My03449 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) M17-My03449 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) M17-My03449 CP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


Perfluorooctane sulfonamide(FOSA) M17-My03449 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) M17-My03449 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) M17-My03449 CP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) M17-My03449 CP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) M17-My03449 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-My03449 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-My03449 CP ug/L < 0.05 < 0.05 <1 30% Pass

Duplicate


Perfluorobutanesulfonic acid(PFBS) M17-My03449 CP ug/L 0.08 0.08 3.0 30% Pass

Perfluoropentanesulfonic acid(PFPeS) M17-My03449 CP ug/L 0.05 0.05 3.0 30% Pass

Perfluorohexanesulfonic acid(PFHxS) M17-My03449 CP ug/L 0.18 0.17 3.0 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) M17-My03449 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanesulfonic acid(PFDS) M17-My03449 CP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-My03449 CP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-My03449 CP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) M17-My03449 CP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


Perfluorooctanesulfonic acid(PFOS) M17-My03454 CP ug/L 0.03 0.03 6.0 30% Pass

Perfluorooctanoic acid (PFOA) M17-My03454 CP ug/L < 0.01 < 0.01 <1 30% Pass


Duplicate



Perfluorohexanoic acid (PFHxA) M17-My03454 CP ug/L < 0.01 < 0.01 <1 30% Pass







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 60 of 70


Duplicate





Duplicate









Duplicate


Perfluorobutanesulfonic acid(PFBS) M17-My03454 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoropentanesulfonic acid(PFPeS) M17-My03454 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanesulfonic acid(PFHxS) M17-My03454 CP ug/L < 0.01 < 0.01 <1 30% Pass



Duplicate





Duplicate


Conductivity (at 25°C) M17-My03461 CP uS/cm 330 340 3.6 30% Pass


Duplicate







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 61 of 70


Duplicate












Duplicate









Duplicate



Perfluoropentanesulfonic acid(PFPeS) M17-My03469 CP ug/L 0.04 0.04 <1 30% Pass


Perfluoroheptanesulfonic acid(PFHpS) M17-My03469 CP ug/L 0.01 0.01 <1 30% Pass


Duplicate





Duplicate


Perfluorooctanesulfonic acid(PFOS) M17-My03479 CP ug/L < 0.01 < 0.01 <1 30% Pass





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 62 of 70


Duplicate



Perfluoropentanoic acid (PFPeA) M17-My03479 CP ug/L < 0.01 < 0.01 <1 30% Pass









Duplicate









Duplicate







Duplicate





Duplicate







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 63 of 70


Duplicate





Perfluoroheptanoic acid (PFHpA) M17-My03488 CP ug/L 0.02 0.02 1.0 30% Pass







Duplicate









Duplicate





Perfluoroheptanesulfonic acid(PFHpS) M17-My03488 CP ug/L 0.03 0.03 9.0 30% Pass


Duplicate





Duplicate


Conductivity (at 25°C) M17-My03494 CP uS/cm 710 710 <1 30% Pass




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 64 of 70


Duplicate



Perfluorooctanoic acid (PFOA) M17-My03503 CP ug/L 0.01 < 0.01 5.0 30% Pass


Duplicate



Perfluoropentanoic acid (PFPeA) M17-My03503 CP ug/L 0.02 0.02 <1 30% Pass









Duplicate









Duplicate







Duplicate







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 65 of 70


Duplicate





Duplicate












Duplicate









Duplicate




Perfluorohexanesulfonic acid(PFHxS) M17-My03506 CP ug/L 0.19 0.19 <1 30% Pass



Duplicate







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 66 of 70


Duplicate




Duplicate



Perfluorooctanoic acid (PFOA) M17-My03522 CP ug/L 0.03 0.03 <1 30% Pass


Duplicate












Duplicate









Duplicate





Perfluoroheptanesulfonic acid(PFHpS) M17-My03522 CP ug/L 0.03 0.03 13 30% Pass




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 67 of 70


Duplicate





Duplicate





Duplicate












Duplicate









Duplicate









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 68 of 70


Duplicate





Duplicate






ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 69 of 70


Comments










N11


R16 The LORs have been raised due to the high concentration of one or more analytes

Authorised By


Jonathon Angell Senior Analyst-Inorganic (QLD)


Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 70 of 70





3G Marine Pde

Abbotsford

VIC 3067


Report 544592-W-V2




Client Sample ID0990_75COLLINS-BORE_170428

Sample Matrix Water

Eurofins | mgt Sample No. M17-My03477





Perfluoropentanoic acid (PFPeA) 0.01 ug/L N090.02

Perfluorohexanoic acid (PFHxA) 0.01 ug/L N090.12

Perfluoroheptanoic acid (PFHpA) 0.01 ug/L N090.02

Perfluorooctanoic acid (PFOA) 0.01 ug/L N090.04







13C4-PFBA (surr.) 1 % 120

13C5-PFPeA (surr.) 1 % 117

13C5-PFHxA (surr.) 1 % 109

13C4-PFHpA (surr.) 1 % 108

13C8-PFOA (surr.) 1 % 108

13C5-PFNA (surr.) 1 % 109

13C6-PFDA (surr.) 1 % 80












13C8-FOSA (surr.) 1 % 79





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 27




emma.delborrello

Rectangle

Client Sample ID0990_75COLLINS-BORE_170428

Sample Matrix Water











Perfluorobutanesulfonic acid (PFBS) 0.01 ug/L N090.11


Perfluorohexanesulfonic acid (PFHxS) 0.01 ug/L N090.74




13C3-PFBS (surr.) 1 % 113

18O2-PFHxS (surr.) 1 % 101

13C8-PFOS (surr.) 1 % 86






13C2-4:2 FTS (surr.) 1 % 120

13C2-6:2 FTS (surr.) 1 % 88

13C2-8:2 FTS (surr.) 1 % 80




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 27


emma.delborrello

Rectangle
















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 27



General

Holding Times

Units

Terms




request.










Receipt Advice.



















































ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 27




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






LCS - % Recovery













LCS - % Recovery





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 27



PassLimits

QualifyingCode








LCS - % Recovery








LCS - % Recovery







LimitsPass

LimitsQualifying

Code

Spike - % Recovery













Spike - % Recovery









Spike - % Recovery





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 27



LimitsPass

LimitsQualifying

Code







Spike - % Recovery






Spike - % Recovery













Spike - % Recovery









Spike - % Recovery






ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 27



LimitsPass

LimitsQualifying

Code






Spike - % Recovery






Spike - % Recovery













Spike - % Recovery









Spike - % Recovery







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 27



LimitsPass

LimitsQualifying

Code





Spike - % Recovery






Spike - % Recovery


Perfluorobutanoic acid (PFBA) S17-My04377 NCP % 110 50-150 Pass

Perfluoropentanoic acid (PFPeA) S17-My04377 NCP % 123 50-150 Pass

Perfluorohexanoic acid (PFHxA) S17-My04377 NCP % 106 50-150 Pass

Perfluoroheptanoic acid (PFHpA) S17-My04377 NCP % 110 50-150 Pass

Perfluorooctanoic acid (PFOA) S17-My04377 NCP % 115 50-150 Pass

Perfluorononanoic acid (PFNA) S17-My04377 NCP % 110 50-150 Pass

Perfluorodecanoic acid (PFDA) S17-My04377 NCP % 108 50-150 Pass

Perfluoroundecanoic acid (PFUnA) S17-My04377 NCP % 106 50-150 Pass

Perfluorododecanoic acid (PFDoA) S17-My04377 NCP % 106 50-150 Pass

Perfluorotridecanoic acid (PFTrDA) S17-My04377 NCP % 135 50-150 Pass

Perfluorotetradecanoic acid(PFTeDA) S17-My04377 NCP % 101 50-150 Pass

Spike - % Recovery


Perfluorooctane sulfonamide(FOSA) S17-My04377 NCP % 116 50-150 Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) S17-My04377 NCP % 111 50-150 Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) S17-My04377 NCP % 100 50-150 Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) S17-My04377 NCP % 117 50-150 Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) S17-My04377 NCP % 96 50-150 Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) S17-My04377 NCP % 109 50-150 Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) S17-My04377 NCP % 109 50-150 Pass

Spike - % Recovery


Perfluorobutanesulfonic acid(PFBS) S17-My04377 NCP % 111 50-150 Pass

Perfluoropentanesulfonic acid(PFPeS) S17-My04377 NCP % 118 50-150 Pass

Perfluorohexanesulfonic acid(PFHxS) S17-My04377 NCP % 108 50-150 Pass




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 27



LimitsPass

LimitsQualifying

Code

Perfluoroheptanesulfonic acid(PFHpS) S17-My04377 NCP % 109 50-150 Pass

Perfluorooctanesulfonic acid(PFOS) S17-My04377 NCP % 110 50-150 Pass

Perfluorodecanesulfonic acid(PFDS) S17-My04377 NCP % 89 50-150 Pass

Spike - % Recovery


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) S17-My04377 NCP % 111 50-150 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) S17-My04377 NCP % 107 50-150 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) S17-My04377 NCP % 91 50-150 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) S17-My04377 NCP % 71 50-150 Pass

Spike - % Recovery













Spike - % Recovery









Spike - % Recovery









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 27



LimitsPass

LimitsQualifying

Code



Spike - % Recovery






Spike - % Recovery













Spike - % Recovery









Spike - % Recovery










ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 27



LimitsPass

LimitsQualifying

Code


Spike - % Recovery






Spike - % Recovery













Spike - % Recovery









Spike - % Recovery








Spike - % Recovery




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 12 of 27



LimitsPass

LimitsQualifying

Code






Spike - % Recovery













Spike - % Recovery









Spike - % Recovery








Spike - % Recovery





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 13 of 27



LimitsPass

LimitsQualifying

Code





Spike - % Recovery













Spike - % Recovery









Spike - % Recovery








Spike - % Recovery





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 14 of 27



LimitsPass

LimitsQualifying

Code





Spike - % Recovery













Spike - % Recovery









Spike - % Recovery








Spike - % Recovery





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 15 of 27



LimitsPass

LimitsQualifying

Code






LimitsPass

LimitsQualifying

Code

Duplicate













Duplicate









Duplicate











ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 16 of 27


Duplicate






Duplicate












Duplicate









Duplicate











ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 17 of 27


Duplicate






Duplicate













Duplicate









Duplicate











ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 18 of 27


Duplicate






Duplicate


Perfluorobutanoic acid (PFBA) S17-My04378 NCP ug/L < 0.05 < 0.05 <1 30% Pass

Perfluoropentanoic acid (PFPeA) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanoic acid (PFHxA) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanoic acid (PFHpA) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanoic acid (PFOA) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorononanoic acid (PFNA) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanoic acid (PFDA) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroundecanoic acid (PFUnA) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorododecanoic acid (PFDoA) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


Perfluorooctane sulfonamide(FOSA) S17-My04378 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) S17-My04378 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) S17-My04378 NCP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) S17-My04378 NCP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) S17-My04378 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) S17-My04378 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) S17-My04378 NCP ug/L < 0.05 < 0.05 <1 30% Pass

Duplicate


Perfluorobutanesulfonic acid(PFBS) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoropentanesulfonic acid(PFPeS) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanesulfonic acid(PFHxS) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanesulfonic acid(PFOS) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanesulfonic acid(PFDS) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 19 of 27


Duplicate


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) S17-My04378 NCP ug/L < 0.05 < 0.05 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate













Duplicate









Duplicate











ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 20 of 27


Duplicate






Duplicate













Duplicate









Duplicate











ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 21 of 27


Duplicate






Duplicate













Duplicate









Duplicate











ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 22 of 27


Duplicate






Duplicate













Duplicate









Duplicate











ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 23 of 27


Duplicate






Duplicate













Duplicate









Duplicate











ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 24 of 27


Duplicate






Duplicate













Duplicate









Duplicate











ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 25 of 27


Duplicate









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 26 of 27


Comments

V2- Split report










N11



Authorised By




Glenn Jackson








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 27 of 27





3G Marine Pde

Abbotsford

VIC 3067


Report 544592-W-V3





Sample Matrix Water






Perfluoropentanoic acid (PFPeA) 0.01 ug/L N090.03

Perfluorohexanoic acid (PFHxA) 0.01 ug/L N090.15

Perfluoroheptanoic acid (PFHpA) 0.01 ug/L N090.02

Perfluorooctanoic acid (PFOA) 0.01 ug/L N090.05







13C4-PFBA (surr.) 1 % 128

13C5-PFPeA (surr.) 1 % 135

13C5-PFHxA (surr.) 1 % 128

13C4-PFHpA (surr.) 1 % 126

13C8-PFOA (surr.) 1 % 126

13C5-PFNA (surr.) 1 % 109

13C6-PFDA (surr.) 1 % 89












13C8-FOSA (surr.) 1 % 93





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 29





Sample Matrix Water











Perfluorobutanesulfonic acid (PFBS) 0.01 ug/L N090.14


Perfluorohexanesulfonic acid (PFHxS) 0.01 ug/L N090.95




13C3-PFBS (surr.) 1 % 140

18O2-PFHxS (surr.) 1 % 121

13C8-PFOS (surr.) 1 % 91






13C2-4:2 FTS (surr.) 1 % 165

13C2-6:2 FTS (surr.) 1 % 114

13C2-8:2 FTS (surr.) 1 % 102




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 29

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 29



General

Holding Times

Units

Terms




request.










Receipt Advice.



















































ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 29




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






LCS - % Recovery













LCS - % Recovery





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 29



PassLimits

QualifyingCode








LCS - % Recovery








LCS - % Recovery







LimitsPass

LimitsQualifying

Code

Spike - % Recovery













Spike - % Recovery









Spike - % Recovery





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 29



LimitsPass

LimitsQualifying

Code







Spike - % Recovery






Spike - % Recovery













Spike - % Recovery









Spike - % Recovery






ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 29



LimitsPass

LimitsQualifying

Code






Spike - % Recovery






Spike - % Recovery













Spike - % Recovery









Spike - % Recovery







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 29



LimitsPass

LimitsQualifying

Code





Spike - % Recovery






Spike - % Recovery













Spike - % Recovery









Spike - % Recovery








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 29



LimitsPass

LimitsQualifying

Code




Spike - % Recovery






Spike - % Recovery













Spike - % Recovery









Spike - % Recovery









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 29



LimitsPass

LimitsQualifying

Code



Spike - % Recovery






Spike - % Recovery













Spike - % Recovery









Spike - % Recovery










ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 29



LimitsPass

LimitsQualifying

Code


Spike - % Recovery






Spike - % Recovery













Spike - % Recovery









Spike - % Recovery








Spike - % Recovery




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 12 of 29



LimitsPass

LimitsQualifying

Code






Spike - % Recovery













Spike - % Recovery









Spike - % Recovery








Spike - % Recovery





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 13 of 29



LimitsPass

LimitsQualifying

Code





Spike - % Recovery













Spike - % Recovery









Spike - % Recovery








Spike - % Recovery





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 14 of 29



LimitsPass

LimitsQualifying

Code





Spike - % Recovery













Spike - % Recovery









Spike - % Recovery








Spike - % Recovery





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 15 of 29



LimitsPass

LimitsQualifying

Code





Spike - % Recovery













Spike - % Recovery









Spike - % Recovery








Spike - % Recovery





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 16 of 29



LimitsPass

LimitsQualifying

Code






LimitsPass

LimitsQualifying

Code

Duplicate













Duplicate









Duplicate











ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 17 of 29


Duplicate






Duplicate












Duplicate









Duplicate











ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 18 of 29


Duplicate






Duplicate













Duplicate









Duplicate











ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 19 of 29


Duplicate






Duplicate


Perfluorobutanoic acid (PFBA) S17-My04378 NCP ug/L < 0.05 < 0.05 <1 30% Pass

Perfluoropentanoic acid (PFPeA) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanoic acid (PFHxA) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanoic acid (PFHpA) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanoic acid (PFOA) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorononanoic acid (PFNA) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanoic acid (PFDA) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroundecanoic acid (PFUnA) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorododecanoic acid (PFDoA) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


Perfluorooctane sulfonamide(FOSA) S17-My04378 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) S17-My04378 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) S17-My04378 NCP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) S17-My04378 NCP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) S17-My04378 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) S17-My04378 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) S17-My04378 NCP ug/L < 0.05 < 0.05 <1 30% Pass

Duplicate


Perfluorobutanesulfonic acid(PFBS) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoropentanesulfonic acid(PFPeS) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanesulfonic acid(PFHxS) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanesulfonic acid(PFOS) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanesulfonic acid(PFDS) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 20 of 29


Duplicate


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) S17-My04378 NCP ug/L < 0.05 < 0.05 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) S17-My04378 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


Perfluorobutanoic acid (PFBA) S17-My04378 NCP ug/L < 0.05 ** 5.0 30% Pass

Perfluoropentanoic acid (PFPeA) S17-My04378 NCP ug/L < 0.01 ** 1.0 30% Pass

Perfluorohexanoic acid (PFHxA) S17-My04378 NCP ug/L < 0.01 ** 14 30% Pass

Perfluoroheptanoic acid (PFHpA) S17-My04378 NCP ug/L < 0.01 ** <1 30% Pass

Perfluorooctanoic acid (PFOA) S17-My04378 NCP ug/L < 0.01 ** <1 30% Pass

Perfluorononanoic acid (PFNA) S17-My04378 NCP ug/L < 0.01 ** <1 30% Pass

Perfluorodecanoic acid (PFDA) S17-My04378 NCP ug/L < 0.01 ** <1 30% Pass

Perfluoroundecanoic acid (PFUnA) S17-My04378 NCP ug/L < 0.01 ** <1 30% Pass

Perfluorododecanoic acid (PFDoA) S17-My04378 NCP ug/L < 0.01 ** <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) S17-My04378 NCP ug/L < 0.01 ** <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) S17-My04378 NCP ug/L < 0.01 ** <1 30% Pass

Duplicate


Perfluorooctane sulfonamide(FOSA) S17-My04378 NCP ug/L < 0.05 ** <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) S17-My04378 NCP ug/L < 0.05 ** <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) S17-My04378 NCP ug/L < 0.05 ** <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) S17-My04378 NCP ug/L < 0.05 ** <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) S17-My04378 NCP ug/L < 0.05 ** <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) S17-My04378 NCP ug/L < 0.05 ** <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) S17-My04378 NCP ug/L < 0.05 ** <1 30% Pass

Duplicate


Perfluorobutanesulfonic acid(PFBS) S17-My04378 NCP ug/L < 0.01 ** <1 30% Pass

Perfluoropentanesulfonic acid(PFPeS) S17-My04378 NCP ug/L < 0.01 ** <1 30% Pass

Perfluorohexanesulfonic acid(PFHxS) S17-My04378 NCP ug/L < 0.01 ** <1 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) S17-My04378 NCP ug/L < 0.01 ** <1 30% Pass

Perfluorooctanesulfonic acid(PFOS) S17-My04378 NCP ug/L < 0.01 ** 22 30% Pass

Perfluorodecanesulfonic acid(PFDS) S17-My04378 NCP ug/L < 0.01 ** <1 30% Pass




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 21 of 29


Duplicate


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) S17-My04378 NCP ug/L < 0.01 ** <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) S17-My04378 NCP ug/L < 0.05 ** 21 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) S17-My04378 NCP ug/L < 0.01 ** <1 30% Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) S17-My04378 NCP ug/L < 0.01 ** <1 30% Pass

Duplicate













Duplicate









Duplicate











ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 22 of 29


Duplicate






Duplicate













Duplicate









Duplicate











ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 23 of 29


Duplicate






Duplicate













Duplicate









Duplicate











ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 24 of 29


Duplicate






Duplicate













Duplicate









Duplicate











ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 25 of 29


Duplicate






Duplicate













Duplicate









Duplicate











ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 26 of 29


Duplicate






Duplicate













Duplicate









Duplicate











ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 27 of 29


Duplicate









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 28 of 29


Comments

V3- Split report










N11



Authorised By




Glenn Jackson








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 29 of 29





3G Marine Pde

Abbotsford

VIC 3067


Report 546502-W




Client Sample ID0990_TDL220COLLINRD -BORE

0990_TDL220COLLINRD -TANK1

0990_TDL220COLLINRD -TAP1

0990_TDL1661STUART BORE







Perfluoropentanoic acid (PFPeA) 0.01 ug/L N090.04 N090.04 N090.03 < 0.01


Perfluoroheptanoic acid (PFHpA) 0.01 ug/L N090.03 N090.03 N090.02 < 0.01

Perfluorooctanoic acid (PFOA) 0.01 ug/L N090.07 N090.07 N090.05 < 0.01







13C4-PFBA (surr.) 1 % 91 100 96 83

13C5-PFPeA (surr.) 1 % 114 122 115 103

13C5-PFHxA (surr.) 1 % 117 118 120 113

13C4-PFHpA (surr.) 1 % 136 137 141 123

13C8-PFOA (surr.) 1 % 118 124 125 110

13C5-PFNA (surr.) 1 % 109 124 138 102

13C6-PFDA (surr.) 1 % 53 61 69 65

13C2-PFUnDA (surr.) 1 % 52 63 60 45

13C2-PFDoDA (surr.) 1 % 47 53 64 49

13C2-PFTeDA (surr.) 1 % 22 20 23 26









13C8-FOSA (surr.) 1 % 73 87 86 59

D3-N-MeFOSA (surr.) 1 % 40 53 63 26



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 11




emma.delborrello

Rectangle

emma.delborrello

Rectangle

emma.delborrello

Rectangle

emma.delborrello

Rectangle

Client Sample ID0990_TDL220COLLINRD -BORE

0990_TDL220COLLINRD -TANK1

0990_TDL220COLLINRD -TAP1

0990_TDL1661STUART BORE






D5-N-EtFOSA (surr.) 1 % 30 42 52 22

D7-N-MeFOSE (surr.) 1 % 37 39 48 20

D9-N-EtFOSE (surr.) 1 % 35 40 46 25

D5-N-EtFOSAA (surr.) 1 % 55 58 63 44

D3-N-MeFOSAA (surr.) 1 % 56 59 69 47


Perfluorobutanesulfonic acid (PFBS) 0.01 ug/L 0.14 0.14 0.10 < 0.01

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L N090.14 0.13 N090.11 < 0.01


Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L N090.08 N090.08 N090.05 < 0.01

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N092.8 N093.1 N092.0 < 0.01


13C3-PFBS (surr.) 1 % 115 115 119 130

18O2-PFHxS (surr.) 1 % 80 84 86 123

13C8-PFOS (surr.) 1 % 64 65 78 97






13C2-4:2 FTS (surr.) 1 % 241 235 243 177

13C2-6:2 FTS (surr.) 1 % 163 171 176 133

13C2-8:2 FTS (surr.) 1 % 85 93 98 78



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 11


emma.delborrello

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emma.delborrello

Rectangle

emma.delborrello

Rectangle

emma.delborrello

Rectangle















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 11


.Company Name: Coffey Environments Pty Ltd VIC Order No.: Received: May 16, 2017 12:32 PMAddress: 3G Marine Pde Report #: 546502 Due: May 23, 2017




Sample Detail

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_TDL220COLLINRD -BORE

May 12, 2017 Water M17-My16593X

2 0990_TDL220COLLINRD -TANK1

May 12, 2017 Water M17-My16594X

3 0990_TDL220COLLINRD -TAP1

May 12, 2017 Water M17-My16595X

4 0990_TDL1661STUARTBORE

May 12, 2017 Water M17-My16596X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 11


emma.delborrello

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emma.delborrello

Rectangle

emma.delborrello

Rectangle

emma.delborrello

Rectangle

Company Name: Coffey Environments Pty Ltd VIC Order No.: Received: May 16, 2017 12:32 PMAddress: 3G Marine Pde Report #: 546502 Due: May 23, 2017




Sample Detail

Per- and P


ubstances(P

FA

Ss)





Test Counts 4








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 11



General

Holding Times

Units

Terms




request.










Receipt Advice.


















































ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 11




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






LCS - % Recovery













LCS - % Recovery




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 11



PassLimits

QualifyingCode








LCS - % Recovery








LCS - % Recovery







LimitsPass

LimitsQualifying

Code

Spike - % Recovery













Spike - % Recovery









Spike - % Recovery




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 11



LimitsPass

LimitsQualifying

Code







Spike - % Recovery







LimitsPass

LimitsQualifying

Code

Duplicate













Duplicate











ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 11


Duplicate








Duplicate








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 11


Comments










N11


Authorised By



Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 11





3G Marine Pde

Abbotsford

VIC 3067


Report 546502-W-V2




Client Sample ID0990_TDL220COLLINSRD -BORE

0990_TDL220COLLINSRD -TANK1

0990_TDL220COLLINSRD -TAP1


Eurofins | mgt Sample No. M17-My16593 M17-My16594 M17-My16595

Date Sampled May 12, 2017 May 12, 2017 May 12, 2017



Perfluorobutanoic acid (PFBA) 0.05 ug/L < 0.05 < 0.05 < 0.05

Perfluoropentanoic acid (PFPeA) 0.01 ug/L N090.04 N090.04 N090.03

Perfluorohexanoic acid (PFHxA) 0.01 ug/L N090.21 N090.22 N090.16

Perfluoroheptanoic acid (PFHpA) 0.01 ug/L N090.03 N090.03 N090.02

Perfluorooctanoic acid (PFOA) 0.01 ug/L N090.07 N090.07 N090.05

Perfluorononanoic acid (PFNA) 0.01 ug/L < 0.01 < 0.01 < 0.01

Perfluorodecanoic acid (PFDA) 0.01 ug/L < 0.01 < 0.01 < 0.01

Perfluoroundecanoic acid (PFUnA) 0.01 ug/L < 0.01 < 0.01 < 0.01

Perfluorododecanoic acid (PFDoA) 0.01 ug/L < 0.01 < 0.01 < 0.01


Perfluorotetradecanoic acid (PFTeDA) 0.01 ug/L < 0.01 < 0.01 < 0.01

13C4-PFBA (surr.) 1 % 91 100 96

13C5-PFPeA (surr.) 1 % 114 122 115

13C5-PFHxA (surr.) 1 % 117 118 120

13C4-PFHpA (surr.) 1 % 136 137 141

13C8-PFOA (surr.) 1 % 118 124 125

13C5-PFNA (surr.) 1 % 109 124 138

13C6-PFDA (surr.) 1 % 53 61 69

13C2-PFUnDA (surr.) 1 % 52 63 60

13C2-PFDoDA (surr.) 1 % 47 53 64

13C2-PFTeDA (surr.) 1 % 22 20 23


Perfluorooctane sulfonamide (FOSA) 0.05 ug/L < 0.05 < 0.05 < 0.05

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA) 0.05 ug/L < 0.05 < 0.05 < 0.05

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA) 0.05 ug/L < 0.05 < 0.05 < 0.05

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol(N-MeFOSE) 0.05 ug/L < 0.05 < 0.05 < 0.05

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE) 0.05 ug/L < 0.05 < 0.05 < 0.05

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA) 0.05 ug/L < 0.05 < 0.05 < 0.05

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA) 0.05 ug/L < 0.05 < 0.05 < 0.05

13C8-FOSA (surr.) 1 % 73 87 86

D3-N-MeFOSA (surr.) 1 % 40 53 63




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 9




emma.delborrello

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emma.delborrello

Rectangle

emma.delborrello

Rectangle

Client Sample ID0990_TDL220COLLINSRD -BORE

0990_TDL220COLLINSRD -TANK1

0990_TDL220COLLINSRD -TAP1


Eurofins | mgt Sample No. M17-My16593 M17-My16594 M17-My16595

Date Sampled May 12, 2017 May 12, 2017 May 12, 2017



D5-N-EtFOSA (surr.) 1 % 30 42 52

D7-N-MeFOSE (surr.) 1 % 37 39 48

D9-N-EtFOSE (surr.) 1 % 35 40 46

D5-N-EtFOSAA (surr.) 1 % 55 58 63

D3-N-MeFOSAA (surr.) 1 % 56 59 69


Perfluorobutanesulfonic acid (PFBS) 0.01 ug/L 0.14 0.14 0.10

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L N090.14 0.13 N090.11

Perfluorohexanesulfonic acid (PFHxS) 0.01 ug/L N091.4 N091.5 N091.1

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L N090.08 N090.08 N090.05

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N092.8 N093.1 N092.0


13C3-PFBS (surr.) 1 % 115 115 119

18O2-PFHxS (surr.) 1 % 80 84 86

13C8-PFOS (surr.) 1 % 64 65 78


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2 FTS) 0.01 ug/L < 0.01 < 0.01 < 0.01

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) 0.05 ug/L < 0.05 < 0.05 < 0.05

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) 0.01 ug/L < 0.01 < 0.01 < 0.01


13C2-4:2 FTS (surr.) 1 % 241 235 243

13C2-6:2 FTS (surr.) 1 % 163 171 176

13C2-8:2 FTS (surr.) 1 % 85 93 98




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

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ABN : 50 005 085 521 Telephone: +61 3 8564 5000

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General

Holding Times

Units

Terms




request.










Receipt Advice.



















































ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 9




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






LCS - % Recovery













LCS - % Recovery





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

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PassLimits

QualifyingCode








LCS - % Recovery








LCS - % Recovery







LimitsPass

LimitsQualifying

Code

Spike - % Recovery













Spike - % Recovery









Spike - % Recovery





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

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LimitsPass

LimitsQualifying

Code







Spike - % Recovery







LimitsPass

LimitsQualifying

Code

Duplicate













Duplicate












ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 9


Duplicate








Duplicate









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 9


Comments

Split Report










N11


Authorised By



Glenn Jackson








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 9





3G Marine Pde

Abbotsford

VIC 3067


Report 546502-W-V3




Client Sample ID 0990_TDL1661STUART BORE

Sample Matrix Water


Date Sampled May 12, 2017














13C4-PFBA (surr.) 1 % 83

13C5-PFPeA (surr.) 1 % 103

13C5-PFHxA (surr.) 1 % 113

13C4-PFHpA (surr.) 1 % 123

13C8-PFOA (surr.) 1 % 110

13C5-PFNA (surr.) 1 % 102

13C6-PFDA (surr.) 1 % 65












13C8-FOSA (surr.) 1 % 59






ABN : 50 005 085 521 Telephone: +61 3 8564 5000

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Client Sample ID 0990_TDL1661STUART BORE

Sample Matrix Water


Date Sampled May 12, 2017














13C3-PFBS (surr.) 1 % 130

18O2-PFHxS (surr.) 1 % 123

13C8-PFOS (surr.) 1 % 97






13C2-4:2 FTS (surr.) 1 % 177

13C2-6:2 FTS (surr.) 1 % 133

13C2-8:2 FTS (surr.) 1 % 78




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

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ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 11



General

Holding Times

Units

Terms




request.










Receipt Advice.



















































ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 11




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






LCS - % Recovery













LCS - % Recovery





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 11



PassLimits

QualifyingCode








LCS - % Recovery








LCS - % Recovery







LimitsPass

LimitsQualifying

Code

Spike - % Recovery













Spike - % Recovery









Spike - % Recovery





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 11



LimitsPass

LimitsQualifying

Code







Spike - % Recovery






Spike - % Recovery


Perfluorobutanoic acid (PFBA) M17-My16662 NCP % 106 50-150 Pass

Perfluoropentanoic acid (PFPeA) B17-My17853 NCP % 105 50-150 Pass

Perfluorohexanoic acid (PFHxA) M17-My16662 NCP % 108 50-150 Pass

Perfluoroheptanoic acid (PFHpA) M17-My16662 NCP % 113 50-150 Pass

Perfluorooctanoic acid (PFOA) M17-My16662 NCP % 109 50-150 Pass

Perfluorononanoic acid (PFNA) M17-My16662 NCP % 112 50-150 Pass

Perfluorodecanoic acid (PFDA) M17-My16662 NCP % 118 50-150 Pass

Perfluoroundecanoic acid (PFUnA) M17-My16662 NCP % 100 50-150 Pass

Perfluorododecanoic acid (PFDoA) M17-My16662 NCP % 106 50-150 Pass

Perfluorotridecanoic acid (PFTrDA) M17-My16662 NCP % 149 50-150 Pass

Perfluorotetradecanoic acid(PFTeDA) M17-My16662 NCP % 121 50-150 Pass

Spike - % Recovery


Perfluorooctane sulfonamide(FOSA) M17-My16662 NCP % 105 50-150 Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) M17-My16662 NCP % 107 50-150 Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) M17-My16662 NCP % 128 50-150 Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) M17-My16662 NCP % 109 50-150 Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) M17-My16662 NCP % 116 50-150 Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-My16662 NCP % 104 50-150 Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-My16662 NCP % 112 50-150 Pass

Spike - % Recovery


Perfluorobutanesulfonic acid(PFBS) M17-My16662 NCP % 97 50-150 Pass




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 11



LimitsPass

LimitsQualifying

Code

Perfluoropentanesulfonic acid(PFPeS) M17-My16662 NCP % 100 50-150 Pass

Perfluorohexanesulfonic acid(PFHxS) M17-My16662 NCP % 111 50-150 Pass

Perfluoroheptanesulfonic acid(PFHpS) M17-My16662 NCP % 103 50-150 Pass

Perfluorooctanesulfonic acid(PFOS) M17-My16662 NCP % 110 50-150 Pass

Perfluorodecanesulfonic acid(PFDS) M17-My16662 NCP % 91 50-150 Pass

Spike - % Recovery


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-My16662 NCP % 118 50-150 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-My16662 NCP % 116 50-150 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-My16662 NCP % 107 50-150 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) M17-My16662 NCP % 148 50-150 Pass


LimitsPass

LimitsQualifying

Code

Duplicate













Duplicate












ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 11


Duplicate








Duplicate






Duplicate


Perfluorobutanoic acid (PFBA) M17-My16661 NCP ug/L < 0.05 < 0.05 <1 30% Pass

Perfluoropentanoic acid (PFPeA) B17-My17855 NCP ug/L 0.58 0.77 28 30% Pass

Perfluorohexanoic acid (PFHxA) M17-My16661 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanoic acid (PFHpA) M17-My16661 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanoic acid (PFOA) M17-My16661 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorononanoic acid (PFNA) M17-My16661 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanoic acid (PFDA) M17-My16661 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroundecanoic acid (PFUnA) M17-My16661 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorododecanoic acid (PFDoA) M17-My16661 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) M17-My16661 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) M17-My16661 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


Perfluorooctane sulfonamide(FOSA) M17-My16661 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) M17-My16661 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) M17-My16661 NCP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) M17-My16661 NCP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) M17-My16661 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-My16661 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-My16661 NCP ug/L < 0.05 < 0.05 <1 30% Pass




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 11


Duplicate


Perfluorobutanesulfonic acid(PFBS) M17-My16661 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoropentanesulfonic acid(PFPeS) M17-My16661 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanesulfonic acid(PFHxS) M17-My16661 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) M17-My16661 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanesulfonic acid(PFOS) M17-My16661 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanesulfonic acid(PFDS) M17-My16661 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-My16661 NCP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-My16661 NCP ug/L < 0.05 < 0.05 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-My16661 NCP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) M17-My16661 NCP ug/L < 0.01 < 0.01 <1 30% Pass




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 11


Comments

Split Report










N11


Authorised By



Glenn Jackson








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 11





3G Marine Pde

Abbotsford

VIC 3067


Report 552653-W



Received Date Jul 03, 2017

Client Sample ID

0990_5694STUARTHWY_BORE_170629

0990_5694STUARTHWY_TANK_170629


Eurofins | mgt Sample No. M17-Jl01774 M17-Jl01775

Date Sampled Jun 29, 2017 Jun 29, 2017



Perfluorobutanoic acid (PFBA) 0.05 ug/L < 0.05 < 0.05

Perfluoropentanoic acid (PFPeA) 0.01 ug/L < 0.01 < 0.01

Perfluorohexanoic acid (PFHxA) 0.01 ug/L < 0.01 < 0.01

Perfluoroheptanoic acid (PFHpA) 0.01 ug/L < 0.01 < 0.01

Perfluorooctanoic acid (PFOA) 0.01 ug/L < 0.01 < 0.01

Perfluorononanoic acid (PFNA) 0.01 ug/L < 0.01 < 0.01

Perfluorodecanoic acid (PFDA) 0.01 ug/L < 0.01 < 0.01

Perfluoroundecanoic acid (PFUnA) 0.01 ug/L < 0.01 < 0.01

Perfluorododecanoic acid (PFDoA) 0.01 ug/L < 0.01 < 0.01


Perfluorotetradecanoic acid (PFTeDA) 0.01 ug/L < 0.01 < 0.01

13C4-PFBA (surr.) 1 % 95 96

13C5-PFPeA (surr.) 1 % 80 81

13C5-PFHxA (surr.) 1 % 93 93

13C4-PFHpA (surr.) 1 % 104 106

13C8-PFOA (surr.) 1 % 108 109

13C5-PFNA (surr.) 1 % 103 104

13C6-PFDA (surr.) 1 % 90 92

13C2-PFUnDA (surr.) 1 % 70 93

13C2-PFDoDA (surr.) 1 % 60 81

13C2-PFTeDA (surr.) 1 % 21 31


Perfluorooctane sulfonamide (FOSA) 0.05 ug/L < 0.05 < 0.05

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA) 0.05 ug/L < 0.05 < 0.05

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA) 0.05 ug/L < 0.05 < 0.05

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol(N-MeFOSE) 0.05 ug/L < 0.05 < 0.05

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE) 0.05 ug/L < 0.05 < 0.05

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA) 0.05 ug/L < 0.05 < 0.05

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA) 0.05 ug/L < 0.05 < 0.05

13C8-FOSA (surr.) 1 % 130 116


Date Reported: Jul 10, 2017


ABN : 50 005 085 521 Telephone: +61 3 8564 5000

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Client Sample ID

0990_5694STUARTHWY_BORE_170629

0990_5694STUARTHWY_TANK_170629


Eurofins | mgt Sample No. M17-Jl01774 M17-Jl01775

Date Sampled Jun 29, 2017 Jun 29, 2017









Perfluorobutanesulfonic acid (PFBS) 0.01 ug/L < 0.01 < 0.01

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L < 0.01 < 0.01

Perfluorohexanesulfonic acid (PFHxS) 0.01 ug/L < 0.01 < 0.01

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L < 0.01 < 0.01

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L < 0.01 < 0.01


13C3-PFBS (surr.) 1 % 104 103

18O2-PFHxS (surr.) 1 % 109 112

13C8-PFOS (surr.) 1 % 83 86


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2 FTS) 0.01 ug/L < 0.01 < 0.01

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) 0.05 ug/L < 0.05 < 0.05

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) 0.01 ug/L < 0.01 < 0.01


13C2-4:2 FTS (surr.) 1 % 118 113

13C2-6:2 FTS (surr.) 1 % 129 141

13C2-8:2 FTS (surr.) 1 % 86 96



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

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Perfluoroalkyl carboxylic acids (PFCAs) Brisbane Jul 07, 2017 14 Day


Perfluoroalkane sulfonamides (PFASAs) Brisbane Jul 07, 2017 14 Day


Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates (PFSAs) Brisbane Jul 07, 2017 14 Day


n:2 Fluorotelomer sulfonic acids Brisbane Jul 07, 2017 14 Day




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 10


.Company Name: Coffey Environments Pty Ltd VIC Order No.: Received: Jul 3, 2017 8:56 AMAddress: 3G Marine Pde Report #: 552653 Due: Jul 10, 2017




Sample Detail

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_5694STUARTHWY_BORE_170629

Jun 29, 2017 Water M17-Jl01774X

2 0990_5694STUARTHWY_TANK_170629

Jun 29, 2017 Water M17-Jl01775X

Test Counts 2






Date Reported:Jul 10, 2017


ABN : 50 005 085 521 Telephone: +61 3 8564 5000

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General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 10




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






LCS - % Recovery













LCS - % Recovery




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 10



PassLimits

QualifyingCode








LCS - % Recovery








LCS - % Recovery







LimitsPass

LimitsQualifying

Code

Spike - % Recovery


Perfluorobutanoic acid (PFBA) M17-Jl01776 NCP % 99 50-150 Pass

Perfluoropentanoic acid (PFPeA) M17-Jl01776 NCP % 105 50-150 Pass

Perfluorohexanoic acid (PFHxA) M17-Jl01776 NCP % 116 50-150 Pass

Perfluoroheptanoic acid (PFHpA) M17-Jl01776 NCP % 100 50-150 Pass

Perfluorooctanoic acid (PFOA) M17-Jl01776 NCP % 109 50-150 Pass

Perfluorononanoic acid (PFNA) M17-Jl01776 NCP % 110 50-150 Pass

Perfluorodecanoic acid (PFDA) M17-Jl01776 NCP % 109 50-150 Pass

Perfluoroundecanoic acid (PFUnA) M17-Jl01776 NCP % 101 50-150 Pass

Perfluorododecanoic acid (PFDoA) M17-Jl01776 NCP % 134 50-150 Pass

Perfluorotridecanoic acid (PFTrDA) M17-Jl01776 NCP % 54 50-150 Pass

Perfluorotetradecanoic acid(PFTeDA) M17-Jl01776 NCP % 104 50-150 Pass

Spike - % Recovery


Perfluorooctane sulfonamide(FOSA) M17-Jl01776 NCP % 103 50-150 Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) M17-Jl01776 NCP % 113 50-150 Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) M17-Jl01776 NCP % 110 50-150 Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) M17-Jl01776 NCP % 110 50-150 Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) M17-Jl01776 NCP % 101 50-150 Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-Jl01776 NCP % 101 50-150 Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-Jl01776 NCP % 101 50-150 Pass

Spike - % Recovery




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 10



LimitsPass

LimitsQualifying

Code

Perfluorobutanesulfonic acid(PFBS) M17-Jl01776 NCP % 97 50-150 Pass

Perfluoropentanesulfonic acid(PFPeS) M17-Jl01776 NCP % 94 50-150 Pass

Perfluorohexanesulfonic acid(PFHxS) M17-Jl01776 NCP % 88 50-150 Pass

Perfluoroheptanesulfonic acid(PFHpS) M17-Jl01776 NCP % 97 50-150 Pass

Perfluorooctanesulfonic acid(PFOS) M17-Jl01776 NCP % 94 50-150 Pass

Perfluorodecanesulfonic acid(PFDS) M17-Jl01776 NCP % 82 50-150 Pass

Spike - % Recovery


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-Jl01776 NCP % 97 50-150 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-Jl01776 NCP % 100 50-150 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-Jl01776 NCP % 109 50-150 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) M17-Jl01776 NCP % 52 50-150 Pass


LimitsPass

LimitsQualifying

Code

Duplicate


Perfluorobutanoic acid (PFBA) M17-Jl01774 CP ug/L < 0.05 < 0.05 <1 30% Pass

Perfluoropentanoic acid (PFPeA) M17-Jl01774 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanoic acid (PFHxA) M17-Jl01774 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanoic acid (PFHpA) M17-Jl01774 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanoic acid (PFOA) M17-Jl01774 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorononanoic acid (PFNA) M17-Jl01774 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanoic acid (PFDA) M17-Jl01774 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroundecanoic acid (PFUnA) M17-Jl01774 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorododecanoic acid (PFDoA) M17-Jl01774 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) M17-Jl01774 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) M17-Jl01774 CP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


Perfluorooctane sulfonamide(FOSA) M17-Jl01774 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) M17-Jl01774 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) M17-Jl01774 CP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) M17-Jl01774 CP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) M17-Jl01774 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-Jl01774 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-Jl01774 CP ug/L < 0.05 < 0.05 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 10


Duplicate


Perfluorobutanesulfonic acid(PFBS) M17-Jl01774 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoropentanesulfonic acid(PFPeS) M17-Jl01774 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanesulfonic acid(PFHxS) M17-Jl01774 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) M17-Jl01774 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanesulfonic acid(PFOS) M17-Jl01774 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanesulfonic acid(PFDS) M17-Jl01774 CP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-Jl01774 CP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-Jl01774 CP ug/L < 0.05 < 0.05 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-Jl01774 CP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) M17-Jl01774 CP ug/L < 0.01 < 0.01 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 10


Comments

Some surrogate recoveries were recorded in excess of the QC limit designated in QSM 5.1 of 50-150%. Since no positive results were reportedfor any PFAS compounds for any of the Samples in this case no data was affected.









Code Description

N11


Authorised By



Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 10





3G Marine Pde

Abbotsford

VIC 3067


Report 552657-W



Received Date Jul 03, 2017

Client Sample ID0990_MANBULLOO_BORE_170627

Sample Matrix Water

Eurofins | mgt Sample No. M17-Jl01784

Date Sampled Jun 27, 2017














13C4-PFBA (surr.) 1 % 99


13C5-PFHxA (surr.) 1 % 114

13C4-PFHpA (surr.) 1 % 121

13C8-PFOA (surr.) 1 % 120

13C5-PFNA (surr.) 1 % 109

13C6-PFDA (surr.) 1 % 87



13C2-PFTeDA (surr.) 1 % INT









13C8-FOSA (surr.) 1 % 128




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 10




emma.delborrello

Rectangle

Client Sample ID0990_MANBULLOO_BORE_170627

Sample Matrix Water

Eurofins | mgt Sample No. M17-Jl01784

Date Sampled Jun 27, 2017















13C3-PFBS (surr.) 1 % 118

18O2-PFHxS (surr.) 1 % 128

13C8-PFOS (surr.) 1 % 83






13C2-4:2 FTS (surr.) 1 % 162

13C2-6:2 FTS (surr.) 1 % 145

13C2-8:2 FTS (surr.) 1 % 92



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 10


emma.delborrello

Rectangle





Perfluoroalkyl carboxylic acids (PFCAs) Brisbane Jul 07, 2017 14 Day


Perfluoroalkane sulfonamides (PFASAs) Brisbane Jul 07, 2017 14 Day


Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates (PFSAs) Brisbane Jul 07, 2017 14 Day


n:2 Fluorotelomer sulfonic acids Brisbane Jul 07, 2017 14 Day




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 10


.Company Name: Coffey Environments Pty Ltd VIC Order No.: Received: Jul 3, 2017 8:56 AMAddress: 3G Marine Pde Report #: 552657 Due: Jul 10, 2017




Sample Detail

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_MANBULLOO_BORE_170627

Jun 27, 2017 Water M17-Jl01784X

Test Counts 1






Date Reported:Jul 10, 2017


ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 10


emma.delborrello

Rectangle


General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 10




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






LCS - % Recovery













LCS - % Recovery




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 10



PassLimits

QualifyingCode








LCS - % Recovery








LCS - % Recovery







LimitsPass

LimitsQualifying

Code

Spike - % Recovery


Perfluorobutanoic acid (PFBA) M17-Jl01781 NCP % 92 50-150 Pass

Perfluoropentanoic acid (PFPeA) M17-Jl01781 NCP % 100 50-150 Pass

Perfluorohexanoic acid (PFHxA) M17-Jl01781 NCP % 104 50-150 Pass

Perfluoroheptanoic acid (PFHpA) M17-Jl01781 NCP % 94 50-150 Pass

Perfluorooctanoic acid (PFOA) M17-Jl01781 NCP % 100 50-150 Pass

Perfluorononanoic acid (PFNA) M17-Jl01781 NCP % 102 50-150 Pass

Perfluorodecanoic acid (PFDA) M17-Jl01781 NCP % 101 50-150 Pass

Perfluoroundecanoic acid (PFUnA) M17-Jl01781 NCP % 98 50-150 Pass

Perfluorododecanoic acid (PFDoA) M17-Jl01781 NCP % 108 50-150 Pass

Perfluorotridecanoic acid (PFTrDA) M17-Jl01781 NCP % 64 50-150 Pass

Perfluorotetradecanoic acid(PFTeDA) M17-Jl01781 NCP % 108 50-150 Pass

Spike - % Recovery


Perfluorooctane sulfonamide(FOSA) M17-Jl01781 NCP % 94 50-150 Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) M17-Jl01781 NCP % 106 50-150 Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) M17-Jl01781 NCP % 96 50-150 Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) M17-Jl01781 NCP % 112 50-150 Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) M17-Jl01781 NCP % 98 50-150 Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-Jl01781 NCP % 100 50-150 Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-Jl01781 NCP % 92 50-150 Pass

Spike - % Recovery




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 10



LimitsPass

LimitsQualifying

Code

Perfluorobutanesulfonic acid(PFBS) M17-Jl01781 NCP % 91 50-150 Pass

Perfluoropentanesulfonic acid(PFPeS) M17-Jl01781 NCP % 89 50-150 Pass

Perfluorohexanesulfonic acid(PFHxS) M17-Jl01781 NCP % 88 50-150 Pass

Perfluoroheptanesulfonic acid(PFHpS) M17-Jl01781 NCP % 88 50-150 Pass

Perfluorooctanesulfonic acid(PFOS) M17-Jl01781 NCP % 87 50-150 Pass

Perfluorodecanesulfonic acid(PFDS) M17-Jl01781 NCP % 83 50-150 Pass

Spike - % Recovery


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-Jl01781 NCP % 91 50-150 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-Jl01781 NCP % 92 50-150 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-Jl01781 NCP % 103 50-150 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) M17-Jl01781 NCP % 56 50-150 Pass


LimitsPass

LimitsQualifying

Code

Duplicate


Perfluorobutanoic acid (PFBA) M17-Jl01779 NCP ug/L < 0.05 < 0.05 <1 30% Pass

Perfluoropentanoic acid (PFPeA) M17-Jl01779 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanoic acid (PFHxA) M17-Jl01779 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanoic acid (PFHpA) M17-Jl01779 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanoic acid (PFOA) M17-Jl01779 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorononanoic acid (PFNA) M17-Jl01779 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanoic acid (PFDA) M17-Jl01779 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroundecanoic acid (PFUnA) M17-Jl01779 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorododecanoic acid (PFDoA) M17-Jl01779 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) M17-Jl01779 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) M17-Jl01779 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


Perfluorooctane sulfonamide(FOSA) M17-Jl01779 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) M17-Jl01779 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) M17-Jl01779 NCP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) M17-Jl01779 NCP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) M17-Jl01779 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-Jl01779 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-Jl01779 NCP ug/L < 0.05 < 0.05 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 10


Duplicate


Perfluorobutanesulfonic acid(PFBS) M17-Jl01779 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoropentanesulfonic acid(PFPeS) M17-Jl01779 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanesulfonic acid(PFHxS) M17-Jl01779 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) M17-Jl01779 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanesulfonic acid(PFOS) M17-Jl01779 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanesulfonic acid(PFDS) M17-Jl01779 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-Jl01779 NCP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-Jl01779 NCP ug/L < 0.05 < 0.05 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-Jl01779 NCP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) M17-Jl01779 NCP ug/L < 0.01 < 0.01 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 10


Comments

Some surrogate recoveries were recorded in excess of the QC limit designated in QSM 5.1 of 50-150%. Since no positive results were reportedfor any PFAS compounds for any of the Samples in this case no data was affected.









Code Description

N11


Authorised By



Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 10





3G Marine Pde

Abbotsford

VIC 3067


Report 558274-W



Received Date Aug 10, 2017


Sample Matrix Water

Eurofins | mgt Sample No. M17-Au14518





Perfluoropentanoic acid (PFPeA)N11 0.01 ug/L N090.05


Perfluoroheptanoic acid (PFHpA)N11 0.01 ug/L N090.03

Perfluorooctanoic acid (PFOA)N11 0.01 ug/L N090.05



Perfluoroundecanoic acid (PFUnA)N11 0.01 ug/L 0.01


Perfluorotridecanoic acid (PFTrDA) 0.01 ug/L 0.01

Perfluorotetradecanoic acid (PFTeDA)N11 0.01 ug/L 0.01

13C4-PFBA (surr.) 1 % 64




13C8-PFOA (surr.) 1 % 93

13C5-PFNA (surr.) 1 % 85

13C6-PFDA (surr.) 1 % 67












13C8-FOSA (surr.) 1 % 80


Date Reported: Aug 21, 2017


ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 11





Sample Matrix Water

















13C3-PFBS (surr.) 1 % 106

18O2-PFHxS (surr.) 1 % 102

13C8-PFOS (surr.) 1 % 79




1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS)N11 0.01 ug/L 0.06


13C2-4:2 FTS (surr.) 1 % 86

13C2-6:2 FTS (surr.) 1 % 105

13C2-8:2 FTS (surr.) 1 % 82

PFASs Summations







Chloride 1 mg/L 17






Alkali Metals

Calcium 0.5 mg/L 82



Sodium 0.5 mg/L 4.3



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 11






Perfluoroalkyl carboxylic acids (PFCAs) Brisbane Aug 17, 2017 14 Day


Perfluoroalkane sulfonamides (PFASAs) Brisbane Aug 17, 2017 14 Day


Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates (PFSAs) Brisbane Aug 17, 2017 14 Day


n:2 Fluorotelomer sulfonic acids Brisbane Aug 17, 2017 14 Day



Ammonia (as N) Melbourne Aug 12, 2017 28 Day


Chloride Melbourne Aug 12, 2017 28 Day


Nitrate (as N) Melbourne Aug 12, 2017 7 Day


Sulphate (as SO4) Melbourne Aug 12, 2017 28 Day


Alkalinity (speciated) Melbourne Aug 12, 2017 14 Day


Alkali Metals Melbourne Aug 12, 2017 180 Day




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 11


.Company Name: Coffey Environments Pty Ltd VIC Order No.: Received: Aug 10, 2017 1:42 PMAddress: 3G Marine Pde Report #: 558274 Due: Aug 17, 2017




Sample Detail

Eurofins | m

gt Suite B

11

Per- and P


ubstances(P

FA

Ss)

Melbourne Laboratory - NATA Site # 1254 & 14271 X




External Laboratory


Matrix LAB ID

1 0090_PB008_170804

Aug 04, 2017 Water M17-Au14518 X X

Test Counts 1 1






Date Reported:Aug 21, 2017


ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 11



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 11




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank





Method Blank




Method Blank

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 11



PassLimits

QualifyingCode

LCS - % Recovery













LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery





LCS - % Recovery



LCS - % Recovery

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 11



LimitsPass

LimitsQualifying

Code

Spike - % Recovery


Perfluorobutanoic acid (PFBA) B17-Au17420 NCP % 107 50-150 Pass

Perfluoropentanoic acid (PFPeA) B17-Au17420 NCP % 107 50-150 Pass

Perfluorohexanoic acid (PFHxA) B17-Au17420 NCP % 105 50-150 Pass

Perfluoroheptanoic acid (PFHpA) B17-Au17420 NCP % 108 50-150 Pass

Perfluorooctanoic acid (PFOA) B17-Au17420 NCP % 106 50-150 Pass

Perfluorononanoic acid (PFNA) B17-Au17420 NCP % 107 50-150 Pass

Perfluorodecanoic acid (PFDA) B17-Au17420 NCP % 105 50-150 Pass

Perfluoroundecanoic acid (PFUnA) B17-Au17420 NCP % 101 50-150 Pass

Perfluorododecanoic acid (PFDoA) B17-Au17420 NCP % 111 50-150 Pass

Perfluorotridecanoic acid (PFTrDA) B17-Au17420 NCP % 109 50-150 Pass

Perfluorotetradecanoic acid(PFTeDA) B17-Au17420 NCP % 106 50-150 Pass

Spike - % Recovery


Perfluorooctane sulfonamide(FOSA) B17-Au17420 NCP % 101 50-150 Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) B17-Au17420 NCP % 106 50-150 Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) B17-Au17420 NCP % 97 50-150 Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) B17-Au17420 NCP % 102 50-150 Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) B17-Au17420 NCP % 105 50-150 Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) B17-Au17420 NCP % 106 50-150 Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) B17-Au17420 NCP % 102 50-150 Pass

Spike - % Recovery


Perfluorobutanesulfonic acid(PFBS) B17-Au17420 NCP % 106 50-150 Pass

Perfluoropentanesulfonic acid(PFPeS) B17-Au17420 NCP % 107 50-150 Pass

Perfluorohexanesulfonic acid(PFHxS) B17-Au17420 NCP % 108 50-150 Pass

Perfluoroheptanesulfonic acid(PFHpS) B17-Au17420 NCP % 111 50-150 Pass

Perfluorooctanesulfonic acid(PFOS) B17-Au17420 NCP % 105 50-150 Pass

Perfluorodecanesulfonic acid(PFDS) B17-Au17420 NCP % 109 50-150 Pass

Spike - % Recovery


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) B17-Au17420 NCP % 107 50-150 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) B17-Au17420 NCP % 104 50-150 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) B17-Au17420 NCP % 95 50-150 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) B17-Au17420 NCP % 92 50-150 Pass

Spike - % Recovery

Result 1



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 11



LimitsPass

LimitsQualifying

Code

Ammonia (as N) M17-Au14069 NCP % 98 70-130 Pass

Chloride M17-Au13603 NCP % 111 70-130 Pass

Nitrate (as N) M17-Au14069 NCP % 97 70-130 Pass

Sulphate (as SO4) M17-Au13068 NCP % 89 70-130 Pass

Spike - % Recovery


Carbonate Alkalinity (as CaCO3) M17-Au14373 NCP % 96 70-130 Pass

Spike - % Recovery


Calcium M17-Au15549 NCP % 109 70-130 Pass

Magnesium M17-Au16383 NCP % 127 70-130 Pass

Potassium M17-Au15549 NCP % 95 70-130 Pass

Sodium M17-Au16383 NCP % 126 70-130 Pass


LimitsPass

LimitsQualifying

Code

Duplicate


Perfluorobutanoic acid (PFBA) M17-Au14798 NCP ug/L < 0.05 < 0.05 <1 30% Pass

Perfluoropentanoic acid (PFPeA) M17-Au14798 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanoic acid (PFHxA) M17-Au14798 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanoic acid (PFHpA) M17-Au14798 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanoic acid (PFOA) M17-Au14798 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorononanoic acid (PFNA) M17-Au14798 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanoic acid (PFDA) M17-Au14798 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroundecanoic acid (PFUnA) M17-Au14798 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorododecanoic acid (PFDoA) M17-Au14798 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) M17-Au14798 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) M17-Au14798 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


Perfluorooctane sulfonamide(FOSA) M17-Au14798 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) M17-Au14798 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) M17-Au14798 NCP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) M17-Au14798 NCP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) M17-Au14798 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-Au14798 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-Au14798 NCP ug/L < 0.05 < 0.05 <1 30% Pass

Duplicate


Perfluorobutanesulfonic acid(PFBS) M17-Au14798 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoropentanesulfonic acid(PFPeS) M17-Au14798 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanesulfonic acid(PFHxS) M17-Au14798 NCP ug/L 0.01 0.01 1.0 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) M17-Au14798 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanesulfonic acid(PFOS) M17-Au14798 NCP ug/L 0.03 0.02 5.0 30% Pass

Perfluorodecanesulfonic acid(PFDS) M17-Au14798 NCP ug/L < 0.01 < 0.01 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 11


Duplicate


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-Au14798 NCP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-Au14798 NCP ug/L < 0.05 < 0.05 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-Au14798 NCP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) M17-Au14798 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


Ammonia (as N) M17-Au16344 NCP mg/L < 0.01 < 0.01 <1 30% Pass

Chloride M17-Au13227 NCP mg/L 220 220 1.9 30% Pass

Nitrate (as N) M17-Au16344 NCP mg/L 0.03 0.03 10 30% Pass

Sulphate (as SO4) M17-Au14976 NCP mg/L 18 18 <1 30% Pass

Duplicate


Bicarbonate Alkalinity (as CaCO3) M17-Au14329 NCP mg/L 65 65 1.0 30% Pass

Carbonate Alkalinity (as CaCO3) M17-Au14329 NCP mg/L < 10 < 10 <1 30% Pass

Duplicate


Calcium M17-Au14518 CP mg/L 82 78 5.0 30% Pass

Magnesium M17-Au14518 CP mg/L 36 35 1.0 30% Pass

Potassium M17-Au14518 CP mg/L 1.9 1.9 1.0 30% Pass

Sodium M17-Au14518 CP mg/L 4.3 4.2 3.0 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 11


Comments










N11


Authorised By





Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 11






Abbotsford

VIC 3067

Attention: Jeni Young

Report 559645-W





Sample Matrix Water
















13C4-PFBA (surr.) 1 % 92



13C4-PFHpA (surr.) 1 % 102

13C8-PFOA (surr.) 1 % 105

13C5-PFNA (surr.) 1 % 86

13C6-PFDA (surr.) 1 % 62












13C8-FOSA (surr.) 1 % 21

D3-N-MeFOSA (surr.) 1 % INT

Date Reported: Sep 01, 2017


ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 11





Sample Matrix Water






D7-N-MeFOSE (surr.) 1 % INT

D9-N-EtFOSE (surr.) 1 % INT

D5-N-EtFOSAA (surr.) 1 % INT









13C3-PFBS (surr.) 1 % 106

18O2-PFHxS (surr.) 1 % 123

13C8-PFOS (surr.) 1 % 104






13C2-4:2 FTS (surr.) 1 % 114

13C2-6:2 FTS (surr.) 1 % 89

13C2-8:2 FTS (surr.) 1 % 48

PFASs Summations






Ammonia (as N) 0.01 mg/L 0.01

Chloride 1 mg/L 14






Alkali Metals

Calcium 0.5 mg/L 100



Sodium 0.5 mg/L 4.8



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 11





























ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 11


.Company Name: Coffey Environments Pty Ltd VIC Order No.: Received: Aug 22, 2017 12:00 AMAddress: 3G Marine Pde Report #: 559645 Due: Aug 29, 2017

Abbotsford Phone: 03 8413 6900 Priority: 5 DayVIC 3067 Fax: Contact Name: Jeni Young



Sample Detail

Eurofins | m

gt Suite B

11

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_PB026_170816

Aug 16, 2017 Water M17-Au25650 X X

Test Counts 1 1






Date Reported:Sep 01, 2017


ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 11



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 11




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank





Method Blank




Method Blank

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 11



PassLimits

QualifyingCode

LCS - % Recovery













LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery





LCS - % Recovery



LCS - % Recovery

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 11



LimitsPass

LimitsQualifying

Code

Spike - % Recovery


Perfluorobutanoic acid (PFBA) M17-Au25648 NCP % 114 50-150 Pass

Perfluoropentanoic acid (PFPeA) M17-Au25648 NCP % 143 50-150 Pass

Perfluorohexanoic acid (PFHxA) M17-Au25648 NCP % 97 50-150 Pass

Perfluoroheptanoic acid (PFHpA) M17-Au25648 NCP % 120 50-150 Pass

Perfluorooctanoic acid (PFOA) M17-Au25648 NCP % 111 50-150 Pass

Perfluorononanoic acid (PFNA) M17-Au25648 NCP % 142 50-150 Pass

Perfluorodecanoic acid (PFDA) M17-Au25648 NCP % 117 50-150 Pass

Perfluoroundecanoic acid (PFUnA) M17-Au25648 NCP % 108 50-150 Pass

Perfluorododecanoic acid (PFDoA) M17-Au25648 NCP % 133 50-150 Pass

Perfluorotridecanoic acid (PFTrDA) M17-Au25648 NCP % 136 50-150 Pass

Perfluorotetradecanoic acid(PFTeDA) M17-Au25648 NCP % 137 50-150 Pass

Spike - % Recovery


Perfluorooctane sulfonamide(FOSA) M17-Au25648 NCP % 100 50-150 Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) M17-Au25648 NCP % 134 50-150 Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) M17-Au25648 NCP % 104 50-150 Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) M17-Au25648 NCP % 105 50-150 Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) M17-Au25648 NCP % 116 50-150 Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-Au25648 NCP % 120 50-150 Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-Au25648 NCP % 101 50-150 Pass

Spike - % Recovery


Perfluorobutanesulfonic acid(PFBS) M17-Au25648 NCP % 108 50-150 Pass

Perfluoropentanesulfonic acid(PFPeS) M17-Au25648 NCP % 76 50-150 Pass

Perfluorohexanesulfonic acid(PFHxS) M17-Au25648 NCP % 111 50-150 Pass

Perfluoroheptanesulfonic acid(PFHpS) M17-Au25648 NCP % 141 50-150 Pass

Perfluorooctanesulfonic acid(PFOS) M17-Au25648 NCP % 107 50-150 Pass

Perfluorodecanesulfonic acid(PFDS) M17-Au25648 NCP % 115 50-150 Pass

Spike - % Recovery


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-Au25648 NCP % 102 50-150 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-Au25648 NCP % 91 50-150 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-Au25648 NCP % 134 50-150 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) M17-Au25648 NCP % 117 50-150 Pass

Spike - % Recovery

Result 1



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 11



LimitsPass

LimitsQualifying

Code


Chloride P17-Au25697 NCP % 122 70-130 Pass



Spike - % Recovery


Bicarbonate Alkalinity (as CaCO3) M17-Au25112 NCP % 90 70-130 Pass

Spike - % Recovery


Calcium P17-Au25694 NCP % 122 70-130 Pass


Sodium P17-Au25694 NCP % 113 70-130 Pass


LimitsPass

LimitsQualifying

Code

Duplicate













Duplicate









Duplicate




Perfluorohexanesulfonic acid(PFHxS) M17-Au26495 NCP ug/L < 0.01 < 0.01 <1 30% Pass


Perfluorooctanesulfonic acid(PFOS) M17-Au26495 NCP ug/L < 0.01 < 0.01 <1 30% Pass




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 11


Duplicate






Duplicate


Ammonia (as N) M17-Au25819 NCP mg/L 58 55 5.0 30% Pass

Chloride M17-Au25254 NCP mg/L 180 180 <1 30% Pass

Nitrate (as N) M17-Au25819 NCP mg/L < 0.4 < 0.4 <1 30% Pass

Sulphate (as SO4) M17-Au25652 NCP mg/L < 5 < 5 <1 30% Pass

Duplicate




Duplicate


Calcium M17-Au25118 NCP mg/L < 0.5 < 0.5 <1 30% Pass

Magnesium M17-Au25118 NCP mg/L < 0.5 < 0.5 <1 30% Pass

Potassium M17-Au25118 NCP mg/L < 0.5 < 0.5 <1 30% Pass

Sodium M17-Au25118 NCP mg/L < 0.5 < 0.5 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 11


Comments










N11


Authorised By





Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 11






Abbotsford

VIC 3067

Attention: Sarah Richards

Report 559646-W





Sample Matrix Water
















13C4-PFBA (surr.) 1 % 95


13C5-PFHxA (surr.) 1 % 103

13C4-PFHpA (surr.) 1 % 116

13C8-PFOA (surr.) 1 % 116

13C5-PFNA (surr.) 1 % 100

13C6-PFDA (surr.) 1 % 58












13C8-FOSA (surr.) 1 % 30




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 11





Sample Matrix Water











Perfluorobutanesulfonic acid (PFBS)N11 0.01 ug/L N090.09






13C3-PFBS (surr.) 1 % 98


13C8-PFOS (surr.) 1 % 82






13C2-4:2 FTS (surr.) 1 % 107

13C2-6:2 FTS (surr.) 1 % 85

13C2-8:2 FTS (surr.) 1 % 48

PFASs Summations







Chloride 1 mg/L 16






Alkali Metals




Sodium 0.5 mg/L 6.7



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 11





























ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 11



Abbotsford Phone: 03 8413 6900 Priority: 5 DayVIC 3067 Fax: Contact Name: Sarah Richards



Sample Detail

Eurofins | m

gt Suite B

11

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_PB025_170815

Aug 15, 2017 Water M17-Au25651 X X

Test Counts 1 1








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 11



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 11




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank





Method Blank




Method Blank

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 11



PassLimits

QualifyingCode

LCS - % Recovery













LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery





LCS - % Recovery



LCS - % Recovery

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 11



LimitsPass

LimitsQualifying

Code

Spike - % Recovery













Spike - % Recovery









Spike - % Recovery








Spike - % Recovery






Spike - % Recovery

Result 1



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 11



LimitsPass

LimitsQualifying

Code





Spike - % Recovery



Spike - % Recovery






LimitsPass

LimitsQualifying

Code

Duplicate













Duplicate









Duplicate










ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 11


Duplicate






Duplicate






Duplicate




Duplicate








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 11


Comments










N11


Authorised By





Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 11






Abbotsford

VIC 3067


Report 559647-W





Sample Matrix Water
















13C4-PFBA (surr.) 1 % 105


13C5-PFHxA (surr.) 1 % 116

13C4-PFHpA (surr.) 1 % 125

13C8-PFOA (surr.) 1 % 135

13C5-PFNA (surr.) 1 % 119

13C6-PFDA (surr.) 1 % 76












13C8-FOSA (surr.) 1 % 54




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 11





Sample Matrix Water

















13C3-PFBS (surr.) 1 % 100

18O2-PFHxS (surr.) 1 % 105

13C8-PFOS (surr.) 1 % 94






13C2-4:2 FTS (surr.) 1 % 123

13C2-6:2 FTS (surr.) 1 % 88

13C2-8:2 FTS (surr.) 1 % 55

PFASs Summations







Chloride 1 mg/L 17






Alkali Metals




Sodium 0.5 mg/L 4.8



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 11





























ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 11






Sample Detail

Eurofins | m

gt Suite B

11

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_PB024_170815

Aug 15, 2017 Water M17-Au25652 X X

Test Counts 1 1








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 11



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 11




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank





Method Blank




Method Blank

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 11



PassLimits

QualifyingCode

LCS - % Recovery













LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery





LCS - % Recovery



LCS - % Recovery

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 11



LimitsPass

LimitsQualifying

Code

Spike - % Recovery













Spike - % Recovery









Spike - % Recovery








Spike - % Recovery






Spike - % Recovery

Result 1



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 11



LimitsPass

LimitsQualifying

Code





Spike - % Recovery



Spike - % Recovery






LimitsPass

LimitsQualifying

Code

Duplicate













Duplicate









Duplicate










ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 11


Duplicate






Duplicate



Chloride M17-Au25652 CP mg/L 17 18 8.3 30% Pass


Sulphate (as SO4) M17-Au25652 CP mg/L < 5 < 5 <1 30% Pass

Duplicate




Duplicate








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 11


Comments










N11


Authorised By





Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 11






Abbotsford

VIC 3067


Report 559648-W




Client Sample ID 0990_PB021_170814-1

0990_PB021_170814-2


Eurofins | mgt Sample No. M17-Au25653 M17-Au32402

Date Sampled Aug 14, 2017 Aug 14, 2017



Perfluorobutanoic acid (PFBA)N11 0.05 ug/L < 0.05 < 0.05

Perfluoropentanoic acid (PFPeA)N11 0.01 ug/L < 0.01 < 0.01

Perfluorohexanoic acid (PFHxA)N11 0.01 ug/L < 0.01 < 0.01

Perfluoroheptanoic acid (PFHpA)N11 0.01 ug/L < 0.01 < 0.01

Perfluorooctanoic acid (PFOA)N11 0.01 ug/L < 0.01 < 0.01

Perfluorononanoic acid (PFNA)N11 0.01 ug/L < 0.01 < 0.01

Perfluorodecanoic acid (PFDA)N11 0.01 ug/L < 0.01 < 0.01

Perfluoroundecanoic acid (PFUnA)N11 0.01 ug/L < 0.01 < 0.01

Perfluorododecanoic acid (PFDoA)N11 0.01 ug/L < 0.01 < 0.01


Perfluorotetradecanoic acid (PFTeDA)N11 0.01 ug/L < 0.01 < 0.01

13C4-PFBA (surr.) 1 % 95 123

13C5-PFPeA (surr.) 1 % 70 131

13C5-PFHxA (surr.) 1 % 109 139

13C4-PFHpA (surr.) 1 % 121 124

13C8-PFOA (surr.) 1 % 120 120

13C5-PFNA (surr.) 1 % 104 105

13C6-PFDA (surr.) 1 % 69 83

13C2-PFUnDA (surr.) 1 % 67 69

13C2-PFDoDA (surr.) 1 % 61 71

13C2-PFTeDA (surr.) 1 % 58 64


Perfluorooctane sulfonamide (FOSA)N11 0.05 ug/L < 0.05 < 0.05

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA)N11 0.05 ug/L < 0.05 < 0.05

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA)N11 0.05 ug/L < 0.05 < 0.05

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol(N-MeFOSE)N11 0.05 ug/L < 0.05 < 0.05

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE)N11 0.05 ug/L < 0.05 < 0.05

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA)N11 0.05 ug/L < 0.05 < 0.05

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA)N11 0.05 ug/L < 0.05 < 0.05

13C8-FOSA (surr.) 1 % 43 85




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 11





0990_PB021_170814-2






D5-N-EtFOSA (surr.) 1 % INT 55






Perfluorobutanesulfonic acid (PFBS)N11 0.01 ug/L < 0.01 < 0.01


Perfluorohexanesulfonic acid (PFHxS)N11 0.01 ug/L < 0.01 < 0.01




13C3-PFBS (surr.) 1 % 105 109

18O2-PFHxS (surr.) 1 % 121 103

13C8-PFOS (surr.) 1 % 104 96


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS)N11 0.01 ug/L < 0.01 < 0.01

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS)N11 0.05 ug/L < 0.05 < 0.05

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS)N11 0.01 ug/L < 0.01 < 0.01


13C2-4:2 FTS (surr.) 1 % 112 130

13C2-6:2 FTS (surr.) 1 % 84 101

13C2-8:2 FTS (surr.) 1 % 51 80

PFASs Summations

Sum (PFHxS + PFOS) 0.01 ug/L < 0.01 < 0.01

Sum of US EPA PFAS (PFOS + PFOA) 0.01 ug/L < 0.01 < 0.01

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 0.01 ug/L < 0.01 < 0.01

Sum of WA DER PFAS (n=10) 0.05 ug/L < 0.05 < 0.05

Sum of PFASs (n=28) 0.1 ug/L < 0.1 < 0.1

Ammonia (as N) 0.01 mg/L 0.02 0.02

Chloride 1 mg/L 12 16

Nitrate (as N) 0.02 mg/L 0.25 0.29

Sulphate (as SO4) 5 mg/L < 5 < 5


Bicarbonate Alkalinity (as CaCO3) 20 mg/L 530 430

Carbonate Alkalinity (as CaCO3) 10 mg/L < 10 < 10

Alkali Metals

Calcium 0.5 mg/L 68 < 0.5

Magnesium 0.5 mg/L 41 < 0.5

Potassium 0.5 mg/L 2.1 < 0.5

Sodium 0.5 mg/L 24 170



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 11





























ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 11






Sample Detail

Eurofins | m

gt Suite B

11

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_PB021_170814-1

Aug 14, 2017 Water M17-Au25653 X X

2 0990_PB021_170814-2

Aug 14, 2017 Water M17-Au32402 X X

Test Counts 2 2








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 11



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 11




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank





Method Blank




Method Blank

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 11



PassLimits

QualifyingCode

LCS - % Recovery













LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery





LCS - % Recovery



LCS - % Recovery

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 11



LimitsPass

LimitsQualifying

Code

Spike - % Recovery













Spike - % Recovery









Spike - % Recovery








Spike - % Recovery






Spike - % Recovery

Result 1



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 11



LimitsPass

LimitsQualifying

Code





Spike - % Recovery



Spike - % Recovery





Spike - % Recovery




LimitsPass

LimitsQualifying

Code

Duplicate













Duplicate









Duplicate








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 11


Duplicate




Duplicate






Duplicate






Duplicate




Duplicate



Magnesium M17-Au25108 NCP mg/L 1400 < 0.5 <1 30% Pass





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 11


Comments









Code Description

N11


Authorised By





Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 11






Abbotsford

VIC 3067


Report 559650-W





Sample Matrix Water
















13C4-PFBA (surr.) 1 % 85




13C8-PFOA (surr.) 1 % 97

13C5-PFNA (surr.) 1 % 87

13C6-PFDA (surr.) 1 % 56












13C8-FOSA (surr.) 1 % 31




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 11





Sample Matrix Water

















13C3-PFBS (surr.) 1 % 97


13C8-PFOS (surr.) 1 % 79






13C2-4:2 FTS (surr.) 1 % 107

13C2-6:2 FTS (surr.) 1 % 78

13C2-8:2 FTS (surr.) 1 % 45

PFASs Summations







Chloride 1 mg/L 13






Alkali Metals




Sodium 0.5 mg/L 5.5



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 11





























ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 11






Sample Detail

Eurofins | m

gt Suite B

11

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_PB023_170815

Aug 15, 2017 Water M17-Au25657 X X

Test Counts 1 1








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 11



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 11




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank





Method Blank




Method Blank

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 11



PassLimits

QualifyingCode

LCS - % Recovery













LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery





LCS - % Recovery



LCS - % Recovery

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 11



LimitsPass

LimitsQualifying

Code

Spike - % Recovery













Spike - % Recovery









Spike - % Recovery








Spike - % Recovery






Spike - % Recovery

Result 1



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 11



LimitsPass

LimitsQualifying

Code





Spike - % Recovery



Spike - % Recovery






LimitsPass

LimitsQualifying

Code

Duplicate













Duplicate









Duplicate










ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 11


Duplicate






Duplicate






Duplicate




Duplicate








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 11


Comments










N11


Authorised By





Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 11






Abbotsford

VIC 3067


Report 559652-W





Sample Matrix Water
















13C4-PFBA (surr.) 1 % 96


13C5-PFHxA (surr.) 1 % 116

13C4-PFHpA (surr.) 1 % 127

13C8-PFOA (surr.) 1 % 125

13C5-PFNA (surr.) 1 % 97

13C6-PFDA (surr.) 1 % 64












13C8-FOSA (surr.) 1 % 85




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 11





Sample Matrix Water









D3-N-MeFOSAA (surr.) 1 % INT








13C3-PFBS (surr.) 1 % 104

18O2-PFHxS (surr.) 1 % 119

13C8-PFOS (surr.) 1 % 90






13C2-4:2 FTS (surr.) 1 % 108

13C2-6:2 FTS (surr.) 1 % 86

13C2-8:2 FTS (surr.) 1 % 40

PFASs Summations







Chloride 1 mg/L 15






Alkali Metals

Calcium 0.5 mg/L 92



Sodium 0.5 mg/L 21



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 11





























ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 11






Sample Detail

Eurofins | m

gt Suite B

11

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_PB022_170814

Aug 14, 2017 Water M17-Au25658 X X

Test Counts 1 1








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 11



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 11




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank





Method Blank




Method Blank

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 11



PassLimits

QualifyingCode

LCS - % Recovery













LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery





LCS - % Recovery



LCS - % Recovery

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 11



LimitsPass

LimitsQualifying

Code

Spike - % Recovery













Spike - % Recovery









Spike - % Recovery








Spike - % Recovery






Spike - % Recovery

Result 1



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 11



LimitsPass

LimitsQualifying

Code





Spike - % Recovery



Spike - % Recovery






LimitsPass

LimitsQualifying

Code

Duplicate



Perfluoropentanoic acid (PFPeA) M17-Au26590 NCP ug/L 0.03 0.03 4.0 30% Pass

Perfluorohexanoic acid (PFHxA) M17-Au26590 NCP ug/L 0.08 0.09 <1 30% Pass

Perfluoroheptanoic acid (PFHpA) M17-Au26590 NCP ug/L 0.02 0.01 2.0 30% Pass

Perfluorooctanoic acid (PFOA) M17-Au26590 NCP ug/L 0.03 0.03 6.0 30% Pass







Duplicate









Duplicate


Perfluorobutanesulfonic acid(PFBS) M17-Au26590 NCP ug/L 0.08 0.08 1.0 30% Pass

Perfluoropentanesulfonic acid(PFPeS) M17-Au26590 NCP ug/L 0.07 0.07 2.0 30% Pass


Perfluoroheptanesulfonic acid(PFHpS) M17-Au26590 NCP ug/L 0.08 0.08 4.0 30% Pass





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 11


Duplicate






Duplicate



Chloride M17-Au25254 NCP mg/L 180 180 <1 30% Pass



Duplicate




Duplicate








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 11


Comments









Code Description

N11


Authorised By





Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 11






Abbotsford

VIC 3067


Report 559662-W





Sample Matrix Water
















13C4-PFBA (surr.) 1 % 102


13C5-PFHxA (surr.) 1 % 117

13C4-PFHpA (surr.) 1 % 133

13C8-PFOA (surr.) 1 % 125

13C5-PFNA (surr.) 1 % 114

13C6-PFDA (surr.) 1 % 73












13C8-FOSA (surr.) 1 % 36




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 11





Sample Matrix Water

















13C3-PFBS (surr.) 1 % 104

18O2-PFHxS (surr.) 1 % 119

13C8-PFOS (surr.) 1 % 113






13C2-4:2 FTS (surr.) 1 % 110

13C2-6:2 FTS (surr.) 1 % 80

13C2-8:2 FTS (surr.) 1 % 47

PFASs Summations







Chloride 1 mg/L 15






Alkali Metals

Calcium 0.5 mg/L 89



Sodium 0.5 mg/L 6.7



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 11





























ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 11






Sample Detail

Eurofins | m

gt Suite B

11

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_PB020_170814

Aug 14, 2017 Water M17-Au25698 X X

Test Counts 1 1








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 11



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 11




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank





Method Blank




Method Blank

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 11



PassLimits

QualifyingCode

LCS - % Recovery













LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery





LCS - % Recovery



LCS - % Recovery

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 11



LimitsPass

LimitsQualifying

Code

Spike - % Recovery













Spike - % Recovery









Spike - % Recovery








Spike - % Recovery






Spike - % Recovery

Result 1



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 11



LimitsPass

LimitsQualifying

Code





Spike - % Recovery



Spike - % Recovery






LimitsPass

LimitsQualifying

Code

Duplicate



Perfluoropentanoic acid (PFPeA) M17-Au26590 NCP ug/L 0.03 0.03 4.0 30% Pass

Perfluorohexanoic acid (PFHxA) M17-Au26590 NCP ug/L 0.08 0.09 <1 30% Pass

Perfluoroheptanoic acid (PFHpA) M17-Au26590 NCP ug/L 0.02 0.01 2.0 30% Pass

Perfluorooctanoic acid (PFOA) M17-Au26590 NCP ug/L 0.03 0.03 6.0 30% Pass







Duplicate









Duplicate


Perfluorobutanesulfonic acid(PFBS) M17-Au26590 NCP ug/L 0.08 0.08 1.0 30% Pass

Perfluoropentanesulfonic acid(PFPeS) M17-Au26590 NCP ug/L 0.07 0.07 2.0 30% Pass


Perfluoroheptanesulfonic acid(PFHpS) M17-Au26590 NCP ug/L 0.08 0.08 4.0 30% Pass





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 11


Duplicate






Duplicate






Duplicate




Duplicate








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 11


Comments









Code Description

N11


Authorised By





Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 11





3G Marine Pde

Abbotsford

VIC 3067


Report 559770-W




Client Sample ID 0990_PB007_1_170802-1

0990_PB007_2_170802


Eurofins | mgt Sample No. B17-Au26301 B17-Au26302





Perfluoropentanoic acid (PFPeA)N11 0.01 ug/L N090.02 N090.02

Perfluorohexanoic acid (PFHxA)N11 0.01 ug/L N090.09 N090.09

Perfluoroheptanoic acid (PFHpA)N11 0.01 ug/L N090.01 N090.01

Perfluorooctanoic acid (PFOA)N11 0.01 ug/L N090.03 N090.03







13C4-PFBA (surr.) 1 % 147 145

13C5-PFPeA (surr.) 1 % 121 128

13C5-PFHxA (surr.) 1 % 134 129

13C4-PFHpA (surr.) 1 % 154 146

13C8-PFOA (surr.) 1 % 185 147

13C5-PFNA (surr.) 1 % 153 145

13C6-PFDA (surr.) 1 % 87 82

13C2-PFUnDA (surr.) 1 % 72 76

13C2-PFDoDA (surr.) 1 % 64 64

13C2-PFTeDA (surr.) 1 % 32 28









13C8-FOSA (surr.) 1 % 96 93




ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 1 of 11




Client Sample ID 0990_PB007_1_170802-1

0990_PB007_2_170802


Eurofins | mgt Sample No. B17-Au26301 B17-Au26302










Perfluorobutanesulfonic acid (PFBS)N11 0.01 ug/L N090.07 N090.07

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L N090.08 N090.09

Perfluorohexanesulfonic acid (PFHxS)N11 0.01 ug/L N090.56 N090.69

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L N090.04 N090.04

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N091.1 N091.1


13C3-PFBS (surr.) 1 % 136 134

18O2-PFHxS (surr.) 1 % 113 105

13C8-PFOS (surr.) 1 % 82 119






13C2-4:2 FTS (surr.) 1 % 164 131

13C2-6:2 FTS (surr.) 1 % 127 115

13C2-8:2 FTS (surr.) 1 % 86 86

PFASs Summations

Sum (PFHxS + PFOS) 0.01 ug/L 1.66 1.79

Sum of US EPA PFAS (PFOS + PFOA) 0.01 ug/L 1.13 1.13

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 0.01 ug/L 1.69 1.82

Sum of WA DER PFAS (n=10) 0.05 ug/L 1.88 2.01

Sum of PFASs (n=28) 0.1 ug/L 2 2.14

Ammonia (as N) 0.01 mg/L < 0.01 -

Bicarbonate Alkalinity (as CaCO3) 20 mg/L 510 -

Chloride 1 mg/L 15 -

Nitrate (as N) 0.02 mg/L 0.22 -

Sulphate (as SO4) 5 mg/L < 5 -


Carbonate Alkalinity (as CaCO3) 10 mg/L < 10 -

Alkali Metals

Calcium 0.5 mg/L 110 -

Magnesium 0.5 mg/L 39 -

Potassium 0.5 mg/L 1.8 -

Sodium 0.5 mg/L 4.7 -



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 2 of 11

















Bicarbonate Alkalinity (as CaCO3) Melbourne Aug 24, 2017 14 Day














ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 3 of 11






Sample Detail

Eurofins | m

gt Suite B

11

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_PB007_1_170802-1

Aug 02, 2017 Water B17-Au26301 X X

2 0990_PB007_2_170802

Aug 02, 2017 Water B17-Au26302 X

Test Counts 1 2








ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 4 of 11



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 5 of 11




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank






Method Blank



Method Blank

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 6 of 11



PassLimits

QualifyingCode

LCS - % Recovery













LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery





LCS - % Recovery



LCS - % Recovery

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 7 of 11



LimitsPass

LimitsQualifying

Code

Spike - % Recovery













Spike - % Recovery









Spike - % Recovery








Spike - % Recovery






Spike - % Recovery

Result 1



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 8 of 11



LimitsPass

LimitsQualifying

Code




Sulphate (as SO4) B17-Au26301 CP % 115 70-130 Pass

Spike - % Recovery



Spike - % Recovery






LimitsPass

LimitsQualifying

Code

Duplicate


Perfluorobutanoic acid (PFBA) B17-Au26315 NCP ug/L < 0.05 < 0.05 <1 30% Pass

Perfluoropentanoic acid (PFPeA) B17-Au26315 NCP ug/L 0.03 0.03 2.0 30% Pass

Perfluorohexanoic acid (PFHxA) B17-Au26315 NCP ug/L 0.12 0.12 1.0 30% Pass

Perfluoroheptanoic acid (PFHpA) B17-Au26315 NCP ug/L 0.02 0.02 4.0 30% Pass

Perfluorooctanoic acid (PFOA) B17-Au26315 NCP ug/L 0.04 0.04 1.0 30% Pass

Perfluorononanoic acid (PFNA) B17-Au26315 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanoic acid (PFDA) B17-Au26315 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroundecanoic acid (PFUnA) B17-Au26315 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorododecanoic acid (PFDoA) B17-Au26315 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) B17-Au26315 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) B17-Au26315 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


Perfluorooctane sulfonamide(FOSA) B17-Au26315 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) B17-Au26315 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) B17-Au26315 NCP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) B17-Au26315 NCP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) B17-Au26315 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) B17-Au26315 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) B17-Au26315 NCP ug/L < 0.05 < 0.05 <1 30% Pass

Duplicate


Perfluorobutanesulfonic acid(PFBS) B17-Au26315 NCP ug/L 0.09 0.09 1.0 30% Pass

Perfluoropentanesulfonic acid(PFPeS) B17-Au26315 NCP ug/L 0.11 0.11 5.0 30% Pass

Perfluorohexanesulfonic acid(PFHxS) B17-Au26315 NCP ug/L 0.85 0.84 1.0 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) B17-Au26315 NCP ug/L 0.05 0.05 1.0 30% Pass

Perfluorooctanesulfonic acid(PFOS) B17-Au26321 NCP ug/L 0.05 0.05 5.0 30% Pass

Perfluorodecanesulfonic acid(PFDS) B17-Au26315 NCP ug/L < 0.01 < 0.01 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 9 of 11


Duplicate


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) B17-Au26315 NCP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) B17-Au26315 NCP ug/L < 0.05 < 0.05 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) B17-Au26315 NCP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) B17-Au26315 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate



Bicarbonate Alkalinity (as CaCO3) B17-Au26301 CP mg/L 510 470 8.0 30% Pass

Chloride B17-Au26315 NCP mg/L 14 14 2.5 30% Pass


Sulphate (as SO4) B17-Au26315 NCP mg/L < 5 < 5 <1 30% Pass

Duplicate


Carbonate Alkalinity (as CaCO3) B17-Au26301 CP mg/L < 10 < 10 <1 30% Pass

Duplicate


Calcium M17-Au26270 NCP mg/L 18 19 2.0 30% Pass

Magnesium M17-Au26270 NCP mg/L 21 21 2.0 30% Pass

Potassium M17-Au26270 NCP mg/L 3.9 3.8 2.0 30% Pass

Sodium M17-Au26270 NCP mg/L 140 140 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 10 of 11


Comments










N11


Authorised By





Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 11 of 11





3G Marine Pde

Abbotsford

VIC 3067


Report 559774-W




Client Sample ID 0990_PB006_1_170802

Sample Matrix Water

Eurofins | mgt Sample No. B17-Au26315















13C4-PFBA (surr.) 1 % 137

13C5-PFPeA (surr.) 1 % 126

13C5-PFHxA (surr.) 1 % 133

13C4-PFHpA (surr.) 1 % 153

13C8-PFOA (surr.) 1 % 144

13C5-PFNA (surr.) 1 % 134

13C6-PFDA (surr.) 1 % 78












13C8-FOSA (surr.) 1 % 93




ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 1 of 11





Sample Matrix Water

Eurofins | mgt Sample No. B17-Au26315
















13C3-PFBS (surr.) 1 % 134

18O2-PFHxS (surr.) 1 % 102

13C8-PFOS (surr.) 1 % 88






13C2-4:2 FTS (surr.) 1 % 159

13C2-6:2 FTS (surr.) 1 % 132

13C2-8:2 FTS (surr.) 1 % 80

PFASs Summations







Chloride 1 mg/L 14






Alkali Metals




Sodium 0.5 mg/L 4.9



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 2 of 11





























ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 3 of 11






Sample Detail

Eurofins | m

gt Suite B

11

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_PB006_1_170802

Aug 02, 2017 Water B17-Au26315 X X

Test Counts 1 1








ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 4 of 11



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 5 of 11




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank





Method Blank




Method Blank

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 6 of 11



PassLimits

QualifyingCode

LCS - % Recovery













LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery





LCS - % Recovery



LCS - % Recovery

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 7 of 11



LimitsPass

LimitsQualifying

Code

Spike - % Recovery













Spike - % Recovery









Spike - % Recovery








Spike - % Recovery






Spike - % Recovery

Result 1



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 8 of 11



LimitsPass

LimitsQualifying

Code




Sulphate (as SO4) B17-Au26301 NCP % 115 70-130 Pass

Spike - % Recovery



Spike - % Recovery






LimitsPass

LimitsQualifying

Code

Duplicate


Perfluorobutanoic acid (PFBA) B17-Au26321 NCP ug/L < 0.05 < 0.05 <1 30% Pass

Perfluoropentanoic acid (PFPeA) B17-Au26321 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanoic acid (PFHxA) B17-Au26321 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanoic acid (PFHpA) B17-Au26321 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanoic acid (PFOA) B17-Au26321 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorononanoic acid (PFNA) B17-Au26321 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanoic acid (PFDA) B17-Au26321 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroundecanoic acid (PFUnA) B17-Au26321 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorododecanoic acid (PFDoA) B17-Au26321 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) B17-Au26321 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) B17-Au26321 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


Perfluorooctane sulfonamide(FOSA) B17-Au26321 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) B17-Au26321 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) B17-Au26321 NCP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) B17-Au26321 NCP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) B17-Au26321 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) B17-Au26321 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) B17-Au26321 NCP ug/L < 0.05 < 0.05 <1 30% Pass

Duplicate


Perfluorobutanesulfonic acid(PFBS) B17-Au26321 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoropentanesulfonic acid(PFPeS) B17-Au26321 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanesulfonic acid(PFHxS) B17-Au26321 NCP ug/L 0.03 0.02 6.0 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) B17-Au26321 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanesulfonic acid(PFOS) B17-Au26321 NCP ug/L 0.05 0.05 5.0 30% Pass

Perfluorodecanesulfonic acid(PFDS) B17-Au26321 NCP ug/L < 0.01 < 0.01 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 9 of 11


Duplicate


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) B17-Au26321 NCP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) B17-Au26321 NCP ug/L < 0.05 < 0.05 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) B17-Au26321 NCP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) B17-Au26321 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate



Chloride B17-Au26315 CP mg/L 14 14 2.5 30% Pass


Sulphate (as SO4) B17-Au26315 CP mg/L < 5 < 5 <1 30% Pass

Duplicate


Bicarbonate Alkalinity (as CaCO3) B17-Au26301 NCP mg/L 510 470 8.0 30% Pass

Carbonate Alkalinity (as CaCO3) B17-Au26301 NCP mg/L < 10 < 10 <1 30% Pass

Duplicate








ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 10 of 11


Comments










N11


Authorised By





Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 11 of 11





3G Marine Pde

Abbotsford

VIC 3067


Report 559777-W





0990_PB005_2_170801

0990_PB005_3_170801


Eurofins | mgt Sample No. B17-Au26320 B17-Au26321 B17-Au26322

Date Sampled Aug 02, 2017 Aug 02, 2017 Aug 02, 2017














13C4-PFBA (surr.) 1 % 154 149 111

13C5-PFPeA (surr.) 1 % 132 124 96

13C5-PFHxA (surr.) 1 % 139 137 128

13C4-PFHpA (surr.) 1 % 154 154 147

13C8-PFOA (surr.) 1 % 175 189 170

13C5-PFNA (surr.) 1 % 147 139 133

13C6-PFDA (surr.) 1 % 88 95 95

13C2-PFUnDA (surr.) 1 % 64 74 74

13C2-PFDoDA (surr.) 1 % 51 69 65

13C2-PFTeDA (surr.) 1 % 24 33 30









13C8-FOSA (surr.) 1 % 97 97 86

D3-N-MeFOSA (surr.) 1 % 53 61 54



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 1 of 11





0990_PB005_2_170801

0990_PB005_3_170801


Eurofins | mgt Sample No. B17-Au26320 B17-Au26321 B17-Au26322




D5-N-EtFOSA (surr.) 1 % 38 46 41

D7-N-MeFOSE (surr.) 1 % 44 48 43

D9-N-EtFOSE (surr.) 1 % 46 51 48

D5-N-EtFOSAA (surr.) 1 % 49 46 48

D3-N-MeFOSAA (surr.) 1 % 55 57 57




Perfluorohexanesulfonic acid (PFHxS)N11 0.01 ug/L N090.03 N090.03 N090.03


Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N090.06 N090.05 N090.04


13C3-PFBS (surr.) 1 % 143 141 131

18O2-PFHxS (surr.) 1 % 140 144 135

13C8-PFOS (surr.) 1 % 101 102 99






13C2-4:2 FTS (surr.) 1 % 148 153 139

13C2-6:2 FTS (surr.) 1 % 116 122 129

13C2-8:2 FTS (surr.) 1 % 73 78 94

PFASs Summations

Sum (PFHxS + PFOS) 0.01 ug/L 0.09 0.08 0.07

Sum of US EPA PFAS (PFOS + PFOA) 0.01 ug/L 0.06 0.05 0.04

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 0.01 ug/L 0.09 0.08 0.07

Sum of WA DER PFAS (n=10) 0.05 ug/L 0.09 0.08 0.07

Sum of PFASs (n=28) 0.1 ug/L < 0.1 < 0.1 < 0.1

Ammonia (as N) 0.01 mg/L < 0.01 - -

Chloride 1 mg/L 13 - -

Nitrate (as N) 0.02 mg/L 0.18 - -

Sulphate (as SO4) 5 mg/L < 5 - -


Bicarbonate Alkalinity (as CaCO3) 20 mg/L 420 - -

Carbonate Alkalinity (as CaCO3) 10 mg/L < 10 - -

Alkali Metals

Calcium 0.5 mg/L 91 - -

Magnesium 0.5 mg/L 38 - -

Potassium 0.5 mg/L 1.4 - -

Sodium 0.5 mg/L 3.2 - -



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 2 of 11





























ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 3 of 11






Sample Detail

Eurofins | m

gt Suite B

11

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_PB005_1_170801

Aug 02, 2017 Water B17-Au26320 X X

2 0990_PB005_2_170801

Aug 02, 2017 Water B17-Au26321 X

3 0990_PB005_3_170801

Aug 02, 2017 Water B17-Au26322 X

Test Counts 1 3








ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 4 of 11



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 5 of 11




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank





Method Blank




Method Blank

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 6 of 11



PassLimits

QualifyingCode

LCS - % Recovery













LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery





LCS - % Recovery



LCS - % Recovery

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 7 of 11



LimitsPass

LimitsQualifying

Code

Spike - % Recovery

Result 1




Sulphate (as SO4) B17-Au26301 NCP % 115 70-130 Pass

Spike - % Recovery



Spike - % Recovery





Spike - % Recovery


Perfluorobutanoic acid (PFBA) B17-Au26322 CP % 112 50-150 Pass

Perfluoropentanoic acid (PFPeA) B17-Au26322 CP % 119 50-150 Pass

Perfluorohexanoic acid (PFHxA) B17-Au26322 CP % 98 50-150 Pass

Perfluoroheptanoic acid (PFHpA) B17-Au26322 CP % 105 50-150 Pass

Perfluorooctanoic acid (PFOA) B17-Au26322 CP % 113 50-150 Pass

Perfluorononanoic acid (PFNA) B17-Au26322 CP % 114 50-150 Pass

Perfluorodecanoic acid (PFDA) B17-Au26322 CP % 96 50-150 Pass

Perfluoroundecanoic acid (PFUnA) B17-Au26322 CP % 108 50-150 Pass

Perfluorododecanoic acid (PFDoA) B17-Au26322 CP % 110 50-150 Pass

Perfluorotridecanoic acid (PFTrDA) B17-Au26322 CP % 87 50-150 Pass

Perfluorotetradecanoic acid(PFTeDA) B17-Au26322 CP % 129 50-150 Pass

Spike - % Recovery


Perfluorooctane sulfonamide(FOSA) B17-Au26322 CP % 111 50-150 Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) B17-Au26322 CP % 104 50-150 Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) B17-Au26322 CP % 96 50-150 Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) B17-Au26322 CP % 109 50-150 Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) B17-Au26322 CP % 106 50-150 Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) B17-Au26322 CP % 118 50-150 Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) B17-Au26322 CP % 109 50-150 Pass

Spike - % Recovery


Perfluorobutanesulfonic acid(PFBS) B17-Au26322 CP % 89 50-150 Pass

Perfluoropentanesulfonic acid(PFPeS) B17-Au26322 CP % 115 50-150 Pass

Perfluorohexanesulfonic acid(PFHxS) B17-Au26322 CP % 102 50-150 Pass

Perfluoroheptanesulfonic acid(PFHpS) B17-Au26322 CP % 99 50-150 Pass

Perfluorooctanesulfonic acid(PFOS) B17-Au26322 CP % 103 50-150 Pass

Perfluorodecanesulfonic acid(PFDS) B17-Au26322 CP % 123 50-150 Pass



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 8 of 11



LimitsPass

LimitsQualifying

Code

Spike - % Recovery


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) B17-Au26322 CP % 113 50-150 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) B17-Au26322 CP % 114 50-150 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) B17-Au26322 CP % 92 50-150 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) B17-Au26322 CP % 127 50-150 Pass


LimitsPass

LimitsQualifying

Code

Duplicate



Chloride B17-Au26315 NCP mg/L 14 14 2.5 30% Pass


Sulphate (as SO4) B17-Au26315 NCP mg/L < 5 < 5 <1 30% Pass

Duplicate


Bicarbonate Alkalinity (as CaCO3) B17-Au26301 NCP mg/L 510 470 8.0 30% Pass

Carbonate Alkalinity (as CaCO3) B17-Au26301 NCP mg/L < 10 < 10 <1 30% Pass

Duplicate






Duplicate


Perfluorobutanoic acid (PFBA) B17-Au26321 CP ug/L < 0.05 < 0.05 <1 30% Pass

Perfluoropentanoic acid (PFPeA) B17-Au26321 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanoic acid (PFHxA) B17-Au26321 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanoic acid (PFHpA) B17-Au26321 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanoic acid (PFOA) B17-Au26321 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorononanoic acid (PFNA) B17-Au26321 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanoic acid (PFDA) B17-Au26321 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroundecanoic acid (PFUnA) B17-Au26321 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorododecanoic acid (PFDoA) B17-Au26321 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) B17-Au26321 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) B17-Au26321 CP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


Perfluorooctane sulfonamide(FOSA) B17-Au26321 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) B17-Au26321 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) B17-Au26321 CP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) B17-Au26321 CP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) B17-Au26321 CP ug/L < 0.05 < 0.05 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 9 of 11


Duplicate


N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) B17-Au26321 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) B17-Au26321 CP ug/L < 0.05 < 0.05 <1 30% Pass

Duplicate


Perfluorobutanesulfonic acid(PFBS) B17-Au26321 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoropentanesulfonic acid(PFPeS) B17-Au26321 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanesulfonic acid(PFHxS) B17-Au26321 CP ug/L 0.03 0.02 6.0 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) B17-Au26321 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanesulfonic acid(PFOS) B17-Au26321 CP ug/L 0.05 0.05 5.0 30% Pass

Perfluorodecanesulfonic acid(PFDS) B17-Au26321 CP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) B17-Au26321 CP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) B17-Au26321 CP ug/L < 0.05 < 0.05 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) B17-Au26321 CP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) B17-Au26321 CP ug/L < 0.01 < 0.01 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 10 of 11


Comments










N11


Authorised By





Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 11 of 11






Abbotsford

VIC 3067


Report 559790-W




Client Sample ID 0990_QCMW148_170814

0990_QCMW161_170814

0990_QCBH149_170815

0990_QCMW163_170816


Eurofins | mgt Sample No. M17-Au26488 M17-Au26489 M17-Au26490 M17-Au26491

Date Sampled Aug 14, 2017 Aug 14, 2017 Aug 15, 2017 Aug 16, 2017


Total Recoverable Hydrocarbons - 1999 NEPM Fractions

TRH C6-C9 0.02 mg/L < 0.02 < 0.02 < 0.02 -

TRH C10-C14 0.05 mg/L < 0.05 < 0.05 < 0.05 -

TRH C15-C28 0.1 mg/L < 0.1 < 0.1 < 0.1 -

TRH C29-C36 0.1 mg/L < 0.1 < 0.1 < 0.1 -

TRH C10-36 (Total) 0.1 mg/L < 0.1 < 0.1 < 0.1 -

BTEX

Benzene 0.001 mg/L < 0.001 < 0.001 < 0.001 -

Toluene 0.001 mg/L < 0.001 < 0.001 < 0.001 -

Ethylbenzene 0.001 mg/L < 0.001 < 0.001 < 0.001 -

m&p-Xylenes 0.002 mg/L < 0.002 < 0.002 < 0.002 -

o-Xylene 0.001 mg/L < 0.001 < 0.001 < 0.001 -

Xylenes - Total 0.003 mg/L < 0.003 < 0.003 < 0.003 -

4-Bromofluorobenzene (surr.) 1 % 70 52 73 -


NaphthaleneN02 0.01 mg/L < 0.01 < 0.01 < 0.01 -

TRH C6-C10 less BTEX (F1)N04 0.02 mg/L < 0.02 < 0.02 < 0.02 -

TRH C6-C10 0.02 mg/L < 0.02 < 0.02 < 0.02 -

TRH >C10-C16 0.05 mg/L < 0.05 < 0.05 < 0.05 -

TRH >C10-C16 less Naphthalene (F2)N01 0.05 mg/L < 0.05 < 0.05 < 0.05 -

TRH >C16-C34 0.1 mg/L < 0.1 < 0.1 < 0.1 -

TRH >C34-C40 0.1 mg/L < 0.1 < 0.1 < 0.1 -

Polycyclic Aromatic Hydrocarbons

Acenaphthene 0.001 mg/L < 0.001 < 0.001 < 0.001 -

Acenaphthylene 0.001 mg/L < 0.001 < 0.001 < 0.001 -

Anthracene 0.001 mg/L < 0.001 < 0.001 < 0.001 -

Benz(a)anthracene 0.001 mg/L < 0.001 < 0.001 < 0.001 -

Benzo(a)pyrene 0.001 mg/L < 0.001 < 0.001 < 0.001 -

Benzo(b&j)fluorantheneN07 0.001 mg/L < 0.001 < 0.001 < 0.001 -

Benzo(g.h.i)perylene 0.001 mg/L < 0.001 < 0.001 < 0.001 -

Benzo(k)fluoranthene 0.001 mg/L < 0.001 < 0.001 < 0.001 -

Chrysene 0.001 mg/L < 0.001 < 0.001 < 0.001 -

Dibenz(a.h)anthracene 0.001 mg/L < 0.001 < 0.001 < 0.001 -

Fluoranthene 0.001 mg/L < 0.001 < 0.001 < 0.001 -

Fluorene 0.001 mg/L < 0.001 < 0.001 < 0.001 -

Indeno(1.2.3-cd)pyrene 0.001 mg/L < 0.001 < 0.001 < 0.001 -



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 24





0990_QCMW161_170814

0990_QCBH149_170815

0990_QCMW163_170816






Naphthalene 0.001 mg/L < 0.001 < 0.001 < 0.001 -

Phenanthrene 0.001 mg/L < 0.001 < 0.001 < 0.001 -

Pyrene 0.001 mg/L < 0.001 < 0.001 < 0.001 -

Total PAH* 0.001 mg/L < 0.001 < 0.001 < 0.001 -

2-Fluorobiphenyl (surr.) 1 % 104 98 135 -

p-Terphenyl-d14 (surr.) 1 % 81 97 127 -


Perfluorobutanoic acid (PFBA)N11 0.05 ug/L < 0.05 < 0.05 < 0.05 < 0.05

Perfluoropentanoic acid (PFPeA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

Perfluorohexanoic acid (PFHxA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

Perfluoroheptanoic acid (PFHpA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

Perfluorooctanoic acid (PFOA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

Perfluorononanoic acid (PFNA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

Perfluorodecanoic acid (PFDA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

Perfluoroundecanoic acid (PFUnA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

Perfluorododecanoic acid (PFDoA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01


Perfluorotetradecanoic acid (PFTeDA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

13C4-PFBA (surr.) 1 % 91 92 95 72

13C5-PFPeA (surr.) 1 % 73 69 72 51

13C5-PFHxA (surr.) 1 % 104 95 102 73

13C4-PFHpA (surr.) 1 % 106 96 102 75

13C8-PFOA (surr.) 1 % 120 94 114 76

13C5-PFNA (surr.) 1 % 102 84 112 74

13C6-PFDA (surr.) 1 % 98 63 85 60

13C2-PFUnDA (surr.) 1 % 115 67 88 65

13C2-PFDoDA (surr.) 1 % 96 57 72 56

13C2-PFTeDA (surr.) 1 % 83 58 75 66


Perfluorooctane sulfonamide (FOSA)N11 0.05 ug/L < 0.05 < 0.05 < 0.05 < 0.05

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA)N11 0.05 ug/L < 0.05 < 0.05 < 0.05 < 0.05

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA)N11 0.05 ug/L < 0.05 < 0.05 < 0.05 < 0.05

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol(N-MeFOSE)N11 0.05 ug/L < 0.05 < 0.05 < 0.05 < 0.05

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE)N11 0.05 ug/L < 0.05 < 0.05 < 0.05 < 0.05

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA)N11 0.05 ug/L < 0.05 < 0.05 < 0.05 < 0.05

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA)N11 0.05 ug/L < 0.05 < 0.05 < 0.05 < 0.05

13C8-FOSA (surr.) 1 % 44 45 30 26

D3-N-MeFOSA (surr.) 1 % 13 INT INT INT

D5-N-EtFOSA (surr.) 1 % INT INT INT INT

D7-N-MeFOSE (surr.) 1 % 20 15 13 INT

D9-N-EtFOSE (surr.) 1 % 23 16 15 INT

D5-N-EtFOSAA (surr.) 1 % 26 20 25 13

D3-N-MeFOSAA (surr.) 1 % 38 24 34 18



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 24



0990_QCMW161_170814

0990_QCBH149_170815

0990_QCMW163_170816






Perfluorobutanesulfonic acid (PFBS)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01


Perfluorohexanesulfonic acid (PFHxS)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01


Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01


13C3-PFBS (surr.) 1 % 108 109 107 107

18O2-PFHxS (surr.) 1 % 128 129 125 125

13C8-PFOS (surr.) 1 % 143 136 136 120


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS)N11 0.05 ug/L < 0.05 < 0.05 < 0.05 < 0.05

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01


13C2-4:2 FTS (surr.) 1 % 129 119 127 122

13C2-6:2 FTS (surr.) 1 % 107 101 101 97

13C2-8:2 FTS (surr.) 1 % 101 68 73 62

PFASs Summations

Sum (PFHxS + PFOS) 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

Sum of US EPA PFAS (PFOS + PFOA) 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

Sum of WA DER PFAS (n=10) 0.05 ug/L < 0.05 < 0.05 < 0.05 < 0.05

Sum of PFASs (n=28) 0.1 ug/L < 0.1 < 0.1 < 0.1 < 0.1

Heavy Metals

Aluminium 0.05 mg/L < 0.05 - < 0.05 -

Aluminium (filtered) 0.05 mg/L - < 0.05 - -

Arsenic 0.001 mg/L < 0.001 - < 0.001 -

Arsenic (filtered) 0.001 mg/L - < 0.001 - -

Cadmium 0.0002 mg/L < 0.0002 - < 0.0002 -

Cadmium (filtered) 0.0002 mg/L - < 0.0002 - -

Chromium 0.001 mg/L < 0.001 - < 0.001 -

Chromium (filtered) 0.001 mg/L - < 0.001 - -

Copper 0.001 mg/L < 0.001 - < 0.001 -

Copper (filtered) 0.001 mg/L - < 0.001 - -

Iron 0.05 mg/L < 0.05 - < 0.05 -

Iron (filtered) 0.05 mg/L - < 0.05 - -

Lead 0.001 mg/L < 0.001 - < 0.001 -

Lead (filtered) 0.001 mg/L - < 0.001 - -

Manganese 0.005 mg/L < 0.005 - < 0.005 -

Manganese (filtered) 0.005 mg/L - < 0.005 - -

Mercury 0.0001 mg/L < 0.0001 - < 0.0001 -

Mercury (filtered) 0.0001 mg/L - < 0.0001 - -

Nickel 0.001 mg/L < 0.001 - < 0.001 -

Nickel (filtered) 0.001 mg/L - < 0.001 - -

Zinc 0.005 mg/L < 0.005 - < 0.005 -

Zinc (filtered) 0.005 mg/L - < 0.005 - -



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 24



Sample Matrix Water





TRH C6-C9 0.02 mg/L < 0.02

TRH C10-C14 0.05 mg/L < 0.05

TRH C15-C28 0.1 mg/L < 0.1

TRH C29-C36 0.1 mg/L < 0.1

TRH C10-36 (Total) 0.1 mg/L < 0.1

BTEX

Benzene 0.001 mg/L < 0.001

Toluene 0.001 mg/L < 0.001

Ethylbenzene 0.001 mg/L < 0.001

m&p-Xylenes 0.002 mg/L < 0.002

o-Xylene 0.001 mg/L < 0.001

Xylenes - Total 0.003 mg/L < 0.003

4-Bromofluorobenzene (surr.) 1 % 74


NaphthaleneN02 0.01 mg/L < 0.01

TRH C6-C10 less BTEX (F1)N04 0.02 mg/L < 0.02

TRH C6-C10 0.02 mg/L < 0.02

TRH >C10-C16 0.05 mg/L < 0.05

TRH >C10-C16 less Naphthalene (F2)N01 0.05 mg/L < 0.05

TRH >C16-C34 0.1 mg/L < 0.1

TRH >C34-C40 0.1 mg/L < 0.1


Acenaphthene 0.001 mg/L < 0.001

Acenaphthylene 0.001 mg/L < 0.001

Anthracene 0.001 mg/L < 0.001

Benz(a)anthracene 0.001 mg/L < 0.001

Benzo(a)pyrene 0.001 mg/L < 0.001

Benzo(b&j)fluorantheneN07 0.001 mg/L < 0.001

Benzo(g.h.i)perylene 0.001 mg/L < 0.001

Benzo(k)fluoranthene 0.001 mg/L < 0.001

Chrysene 0.001 mg/L < 0.001

Dibenz(a.h)anthracene 0.001 mg/L < 0.001

Fluoranthene 0.001 mg/L < 0.001

Fluorene 0.001 mg/L < 0.001

Indeno(1.2.3-cd)pyrene 0.001 mg/L < 0.001

Naphthalene 0.001 mg/L < 0.001

Phenanthrene 0.001 mg/L < 0.001

Pyrene 0.001 mg/L < 0.001

Total PAH* 0.001 mg/L < 0.001

2-Fluorobiphenyl (surr.) 1 % 97

p-Terphenyl-d14 (surr.) 1 % 92










ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 24



Sample Matrix Water










13C4-PFBA (surr.) 1 % 89



13C4-PFHpA (surr.) 1 % 100

13C8-PFOA (surr.) 1 % 96

13C5-PFNA (surr.) 1 % 85

13C6-PFDA (surr.) 1 % 64












13C8-FOSA (surr.) 1 % 43














13C3-PFBS (surr.) 1 % 106

18O2-PFHxS (surr.) 1 % 122

13C8-PFOS (surr.) 1 % 113



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 24



Sample Matrix Water









13C2-4:2 FTS (surr.) 1 % 118

13C2-6:2 FTS (surr.) 1 % 95

13C2-8:2 FTS (surr.) 1 % 58

PFASs Summations






Heavy Metals

Aluminium 0.05 mg/L < 0.05

Arsenic 0.001 mg/L < 0.001

Cadmium 0.0002 mg/L < 0.0002

Chromium 0.001 mg/L < 0.001

Copper 0.001 mg/L < 0.001

Iron 0.05 mg/L < 0.05

Lead 0.001 mg/L < 0.001

Manganese 0.005 mg/L < 0.005

Mercury 0.0001 mg/L < 0.0001

Nickel 0.001 mg/L < 0.001

Zinc 0.005 mg/L < 0.005



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 24





Total Recoverable Hydrocarbons - 1999 NEPM Fractions Melbourne Aug 25, 2017 7 Day

- Method: LTM-ORG-2010 TRH C6-C36


- Method: TRH C6-C40 - LTM-ORG-2010



BTEX and Naphthalene

BTEX Melbourne Aug 24, 2017 14 Day


Polycyclic Aromatic Hydrocarbons Melbourne Aug 25, 2017 7 Day

- Method: LTM-ORG-2130 PAH and Phenols in Water by GCMS

Heavy Metals Melbourne Aug 24, 2017 180 Day

- Method: LTM-MET-3040 Metals in Waters by ICP-MS

Heavy Metals (filtered) Melbourne Aug 24, 2017 180 Day

- Method: LTM-MET-3040 Metals in Waters by ICP-MS

Mercury (filtered) Melbourne Aug 24, 2017 28 Day

- Method: USEPA 7470/1 Mercury












ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 24


.Company Name: Coffey Environments Pty Ltd VIC Order No.: Received: Aug 21, 2017 9:43 AMAddress: Level 1, 436 Johnston Street Report #: 559790 Due: Aug 28, 2017




Sample Detail

Alum

inium

Alum

inium (filtered)

Arsenic

Arsenic (filtered)

Cadm

ium

Cadm

ium (filtered)

Chrom

ium

Chrom

ium (filtered)

Copper

Copper (filtered)

HO

LD

Iron

Iron (filtered)

Lead

Lead (filtered)

Manganese

Manganese (filtered)

Mercury

Mercury (filtered)

Nickel

Nickel (filtered)

Zinc

Zinc (filtered)

Polycyclic A

romatic H

ydrocarbons

Organochlorine P

esticides

Organophosphorus P

esticides

Acid H

erbicides

BT

EX

and Naphthalene

Volatile O

rganics

Moisture S

et

Sem

ivolatile Organics

Total R

ecoverable Hydrocarbons

Per- and P


ubstances

1.4-Dioxane

Melbourne Laboratory - NATA Site # 1254 & 14271 X X X X X X X X X X X X X X X X X X X X X X X X X X X X X X X X

Sydney Laboratory - NATA Site # 18217 X



External Laboratory


Matrix LAB ID

1 0990_MW122_7.0_170814

Aug 14, 2017 Soil M17-Au26485 X X X X X X X X X X X X X

2 0990_MW120_5.0_170814


3 0990_MW120_19.0_170814


4 0990_QCMW148_170814

Aug 14, 2017 Water M17-Au26488 X X X X X X X X X X X X X X X

5 0990_QCMW161_170814


6 0990_QCBH1 Aug 15, 2017 Water M17-Au26490 X X X X X X X X X X X X X X X








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Page 8 of 24


Company Name: Coffey Environments Pty Ltd VIC Order No.: Received: Aug 21, 2017 9:43 AMAddress: Level 1, 436 Johnston Street Report #: 559790 Due: Aug 28, 2017




Sample Detail

Alum

inium

Alum

inium (filtered)

Arsenic

Arsenic (filtered)

Cadm

ium

Cadm

ium (filtered)

Chrom

ium

Chrom

ium (filtered)

Copper

Copper (filtered)

HO

LD

Iron

Iron (filtered)

Lead

Lead (filtered)

Manganese


Mercury

Mercury (filtered)

Nickel

Nickel (filtered)

Zinc

Zinc (filtered)

Polycyclic A

romatic H

ydrocarbons

Organochlorine P

esticides

Organophosphorus P

esticides

Acid H

erbicides

BT

EX

and Naphthalene

Volatile O

rganics

Moisture S

et

Sem

ivolatile Organics

Total R


Per- and P


ubstances

1.4-Dioxane





49_170815

7 0990_QCMW163_170816

Aug 16, 2017 Water M17-Au26491 X

8 0990_QCMW164_170816

Aug 16, 2017 Water M17-Au26492 X

9 0990_MW126_0.0_170816


10 0990_QCMW181_170816


11 0990_QCMW182_170816


12 0990_MW120_3.0_170814

Aug 14, 2017 Soil M17-Au26496 X

13 0990_MW120 Aug 14, 2017 Soil M17-Au26497 X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 24






Sample Detail

Alum

inium

Alum

inium (filtered)

Arsenic

Arsenic (filtered)

Cadm

ium

Cadm

ium (filtered)

Chrom

ium

Chrom

ium (filtered)

Copper

Copper (filtered)

HO

LD

Iron

Iron (filtered)

Lead

Lead (filtered)

Manganese


Mercury

Mercury (filtered)

Nickel

Nickel (filtered)

Zinc

Zinc (filtered)

Polycyclic A

romatic H

ydrocarbons

Organochlorine P

esticides

Organophosphorus P

esticides

Acid H

erbicides

BT

EX

and Naphthalene

Volatile O

rganics

Moisture S

et

Sem

ivolatile Organics

Total R


Per- and P


ubstances

1.4-Dioxane





_14.0_170814

14 0990_MW130_0.0_170816

Aug 16, 2017 Soil M17-Au26498 X

15 0990_MW130_0.2_170816

Aug 16, 2017 Soil M17-Au26499 X

16 0990_MW130_0.5_170816

Aug 16, 2017 Soil M17-Au26500 X

17 0990_MW130_1.0_170816

Aug 16, 2017 Soil M17-Au26501 X

18 0990_MW131_0.0_170816

Aug 16, 2017 Soil M17-Au26502 X

19 0990_MW131_0.2_170816

Aug 16, 2017 Soil M17-Au26503 X

20 0990_MW131 Aug 16, 2017 Soil M17-Au26504 X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 24






Sample Detail

Alum

inium

Alum

inium (filtered)

Arsenic

Arsenic (filtered)

Cadm

ium

Cadm

ium (filtered)

Chrom

ium

Chrom

ium (filtered)

Copper

Copper (filtered)

HO

LD

Iron

Iron (filtered)

Lead

Lead (filtered)

Manganese


Mercury

Mercury (filtered)

Nickel

Nickel (filtered)

Zinc

Zinc (filtered)

Polycyclic A

romatic H

ydrocarbons

Organochlorine P

esticides

Organophosphorus P

esticides

Acid H

erbicides

BT

EX

and Naphthalene

Volatile O

rganics

Moisture S

et

Sem

ivolatile Organics

Total R


Per- and P


ubstances

1.4-Dioxane





_0.5_170816

21 0990_MW131_1.0_170816

Aug 16, 2017 Soil M17-Au26505 X

22 0990_QCMW165_170816

Aug 16, 2017 Soil M17-Au26506 X

23 0990_QCMW165A_170816

Aug 16, 2017 Soil M17-Au26507 X

24 0990_QCMW130_9.0_170816

Aug 16, 2017 Soil M17-Au26508X

25 0990_QCMW166_170816

Aug 16, 2017 Soil M17-Au26509 X

26 0990_SS166_170815









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 24






Sample Detail

Alum

inium

Alum

inium (filtered)

Arsenic

Arsenic (filtered)

Cadm

ium

Cadm

ium (filtered)

Chrom

ium

Chrom

ium (filtered)

Copper

Copper (filtered)

HO

LD

Iron

Iron (filtered)

Lead

Lead (filtered)

Manganese


Mercury

Mercury (filtered)

Nickel

Nickel (filtered)

Zinc

Zinc (filtered)

Polycyclic A

romatic H

ydrocarbons

Organochlorine P

esticides

Organophosphorus P

esticides

Acid H

erbicides

BT

EX

and Naphthalene

Volatile O

rganics

Moisture S

et

Sem

ivolatile Organics

Total R


Per- and P


ubstances

1.4-Dioxane





27 0990_QCSS180_170815


28 0990_BH192_0.0_170815


29 0990_BH192_0.2_170815

Aug 15, 2017 Soil M17-Au26517 X

30 0990_BH192_0.5_170815


31 0990_BH193_0.0_170815

Aug 15, 2017 Soil M17-Au26519 X X X X X X X X X X X X X X X X X X X X X X

32 0990_BH193_0.2_170815

Aug 15, 2017 Soil M17-Au26520 X

33 0990_BH193_0.5_170815









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 12 of 24






Sample Detail

Alum

inium

Alum

inium (filtered)

Arsenic

Arsenic (filtered)

Cadm

ium

Cadm

ium (filtered)

Chrom

ium

Chrom

ium (filtered)

Copper

Copper (filtered)

HO

LD

Iron

Iron (filtered)

Lead

Lead (filtered)

Manganese


Mercury

Mercury (filtered)

Nickel

Nickel (filtered)

Zinc

Zinc (filtered)

Polycyclic A

romatic H

ydrocarbons

Organochlorine P

esticides

Organophosphorus P

esticides

Acid H

erbicides

BT

EX

and Naphthalene

Volatile O

rganics

Moisture S

et

Sem

ivolatile Organics

Total R


Per- and P


ubstances

1.4-Dioxane





Test Counts 14 1 14 1 14 1 14 1 14 1 16 14 1 14 1 14 1 14 1 14 1 14 1 5 1 1 1 5 1 11 1 5 17 1








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Page 13 of 24



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















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Page 14 of 24




PassLimits

QualifyingCode

Method Blank


TRH C6-C9 mg/L < 0.02 0.02 Pass

TRH C10-C14 mg/L < 0.05 0.05 Pass

TRH C15-C28 mg/L < 0.1 0.1 Pass

TRH C29-C36 mg/L < 0.1 0.1 Pass

Method Blank

BTEX

Benzene mg/L < 0.001 0.001 Pass

Toluene mg/L < 0.001 0.001 Pass

Ethylbenzene mg/L < 0.001 0.001 Pass

m&p-Xylenes mg/L < 0.002 0.002 Pass

o-Xylene mg/L < 0.001 0.001 Pass

Xylenes - Total mg/L < 0.003 0.003 Pass

Method Blank


Naphthalene mg/L < 0.01 0.01 Pass

TRH C6-C10 mg/L < 0.02 0.02 Pass

TRH >C10-C16 mg/L < 0.05 0.05 Pass

TRH >C16-C34 mg/L < 0.1 0.1 Pass

TRH >C34-C40 mg/L < 0.1 0.1 Pass

Method Blank


Acenaphthene mg/L < 0.001 0.001 Pass

Acenaphthylene mg/L < 0.001 0.001 Pass

Anthracene mg/L < 0.001 0.001 Pass

Benz(a)anthracene mg/L < 0.001 0.001 Pass

Benzo(a)pyrene mg/L < 0.001 0.001 Pass

Benzo(b&j)fluoranthene mg/L < 0.001 0.001 Pass

Benzo(g.h.i)perylene mg/L < 0.001 0.001 Pass

Benzo(k)fluoranthene mg/L < 0.001 0.001 Pass

Chrysene mg/L < 0.001 0.001 Pass

Dibenz(a.h)anthracene mg/L < 0.001 0.001 Pass

Fluoranthene mg/L < 0.001 0.001 Pass

Fluorene mg/L < 0.001 0.001 Pass

Indeno(1.2.3-cd)pyrene mg/L < 0.001 0.001 Pass

Naphthalene mg/L < 0.001 0.001 Pass

Phenanthrene mg/L < 0.001 0.001 Pass

Pyrene mg/L < 0.001 0.001 Pass

Method Blank















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Page 15 of 24



PassLimits

QualifyingCode

Method Blank









Method Blank








Method Blank






Method Blank

Heavy Metals

Aluminium mg/L < 0.05 0.05 Pass

Aluminium (filtered) mg/L < 0.05 0.05 Pass

Arsenic mg/L < 0.001 0.001 Pass

Arsenic (filtered) mg/L < 0.001 0.001 Pass

Cadmium mg/L < 0.0002 0.0002 Pass

Cadmium (filtered) mg/L < 0.0002 0.0002 Pass

Chromium mg/L < 0.001 0.001 Pass

Chromium (filtered) mg/L < 0.001 0.001 Pass

Copper mg/L < 0.001 0.001 Pass

Copper (filtered) mg/L < 0.001 0.001 Pass

Iron mg/L < 0.05 0.05 Pass

Iron (filtered) mg/L < 0.05 0.05 Pass

Lead mg/L < 0.001 0.001 Pass

Lead (filtered) mg/L < 0.001 0.001 Pass

Manganese mg/L < 0.005 0.005 Pass

Manganese (filtered) mg/L < 0.005 0.005 Pass

Mercury mg/L < 0.0001 0.0001 Pass

Mercury (filtered) mg/L < 0.0001 0.0001 Pass

Nickel mg/L < 0.001 0.001 Pass

Nickel (filtered) mg/L < 0.001 0.001 Pass

Zinc mg/L < 0.005 0.005 Pass

Zinc (filtered) mg/L < 0.005 0.005 Pass

LCS - % Recovery


TRH C6-C9 % 83 70-130 Pass

TRH C10-C14 % 86 70-130 Pass

LCS - % Recovery

BTEX

Benzene % 115 70-130 Pass



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Page 16 of 24



PassLimits

QualifyingCode

Toluene % 103 70-130 Pass

Ethylbenzene % 103 70-130 Pass

m&p-Xylenes % 101 70-130 Pass

Xylenes - Total % 102 70-130 Pass

LCS - % Recovery


Naphthalene % 91 70-130 Pass

TRH C6-C10 % 83 70-130 Pass

TRH >C10-C16 % 91 70-130 Pass

LCS - % Recovery


Acenaphthene % 125 70-130 Pass

Acenaphthylene % 108 70-130 Pass

Anthracene % 115 70-130 Pass

Benz(a)anthracene % 122 70-130 Pass

Benzo(a)pyrene % 118 70-130 Pass

Benzo(b&j)fluoranthene % 125 70-130 Pass

Benzo(g.h.i)perylene % 117 70-130 Pass

Benzo(k)fluoranthene % 129 70-130 Pass

Chrysene % 117 70-130 Pass

Dibenz(a.h)anthracene % 112 70-130 Pass

Fluoranthene % 120 70-130 Pass

Fluorene % 129 70-130 Pass

Indeno(1.2.3-cd)pyrene % 122 70-130 Pass


Phenanthrene % 115 70-130 Pass

Pyrene % 114 70-130 Pass

LCS - % Recovery













LCS - % Recovery









LCS - % Recovery







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Page 17 of 24



PassLimits

QualifyingCode




LCS - % Recovery






LCS - % Recovery

Heavy Metals

Aluminium % 118 80-120 Pass

Aluminium (filtered) % 118 80-120 Pass

Arsenic % 103 80-120 Pass

Arsenic (filtered) % 103 80-120 Pass

Cadmium % 100 80-120 Pass

Cadmium (filtered) % 100 80-120 Pass

Chromium % 101 80-120 Pass

Chromium (filtered) % 101 80-120 Pass

Copper % 99 80-120 Pass

Copper (filtered) % 99 80-120 Pass

Iron % 108 80-120 Pass

Iron (filtered) % 108 80-120 Pass

Lead % 100 80-120 Pass

Lead (filtered) % 100 80-120 Pass

Manganese % 107 80-120 Pass

Manganese (filtered) % 107 80-120 Pass

Mercury % 96 75-125 Pass

Mercury (filtered) % 96 70-130 Pass

Nickel % 99 80-120 Pass

Nickel (filtered) % 99 80-120 Pass

Zinc % 102 80-120 Pass

Zinc (filtered) % 102 80-120 Pass


LimitsPass

LimitsQualifying

Code

Spike - % Recovery

Total Recoverable Hydrocarbons - 1999 NEPM Fractions Result 1

TRH C6-C9 M17-Au25289 NCP % 76 70-130 Pass

TRH C10-C14 B17-Au26129 NCP % 118 70-130 Pass

Spike - % Recovery

BTEX Result 1

Benzene M17-Au25289 NCP % 105 70-130 Pass

Toluene M17-Au25289 NCP % 98 70-130 Pass

Ethylbenzene M17-Au25289 NCP % 96 70-130 Pass

m&p-Xylenes M17-Au25289 NCP % 100 70-130 Pass

o-Xylene M17-Au25289 NCP % 93 70-130 Pass

Xylenes - Total M17-Au25289 NCP % 98 70-130 Pass

Spike - % Recovery


Naphthalene M17-Au25289 NCP % 74 70-130 Pass


TRH >C10-C16 B17-Au26129 NCP % 125 70-130 Pass

Spike - % Recovery

Heavy Metals Result 1

Aluminium Z17-Au25837 NCP % 105 75-125 Pass



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Page 18 of 24



LimitsPass

LimitsQualifying

Code

Arsenic Z17-Au25837 NCP % 108 75-125 Pass

Cadmium Z17-Au25837 NCP % 102 75-125 Pass

Chromium Z17-Au25837 NCP % 103 75-125 Pass

Copper Z17-Au25837 NCP % 102 75-125 Pass

Iron Z17-Au25837 NCP % 103 75-125 Pass

Lead Z17-Au25837 NCP % 103 75-125 Pass

Manganese Z17-Au25837 NCP % 104 75-125 Pass

Mercury Z17-Au25837 NCP % 90 70-130 Pass

Nickel Z17-Au25837 NCP % 103 75-125 Pass

Zinc Z17-Au25837 NCP % 107 75-125 Pass

Spike - % Recovery


Aluminium (filtered) M17-Au26270 NCP % 97 75-125 Pass

Arsenic (filtered) M17-Au26270 NCP % 103 70-130 Pass

Cadmium (filtered) M17-Au26270 NCP % 100 70-130 Pass

Chromium (filtered) M17-Au26270 NCP % 92 70-130 Pass

Copper (filtered) M17-Au26270 NCP % 97 70-130 Pass

Iron (filtered) M17-Au26270 NCP % 100 70-130 Pass

Lead (filtered) M17-Au26270 NCP % 98 70-130 Pass

Manganese (filtered) M17-Au26270 NCP % 101 70-130 Pass

Mercury (filtered) M17-Au26270 NCP % 99 70-130 Pass

Nickel (filtered) M17-Au26270 NCP % 95 70-130 Pass

Zinc (filtered) M17-Au26270 NCP % 98 70-130 Pass

Spike - % Recovery

Polycyclic Aromatic Hydrocarbons Result 1

Acenaphthene M17-Au26490 CP % 106 70-130 Pass

Acenaphthylene M17-Au26490 CP % 96 70-130 Pass

Anthracene M17-Au26490 CP % 103 70-130 Pass

Benz(a)anthracene M17-Au26490 CP % 107 70-130 Pass

Benzo(a)pyrene M17-Au26490 CP % 126 70-130 Pass

Benzo(b&j)fluoranthene M17-Au26490 CP % 97 70-130 Pass

Benzo(g.h.i)perylene M17-Au26490 CP % 115 70-130 Pass

Benzo(k)fluoranthene M17-Au26490 CP % 122 70-130 Pass

Chrysene M17-Au26490 CP % 99 70-130 Pass

Dibenz(a.h)anthracene M17-Au26490 CP % 115 70-130 Pass

Fluoranthene M17-Au26490 CP % 104 70-130 Pass

Fluorene M17-Au26490 CP % 108 70-130 Pass

Indeno(1.2.3-cd)pyrene M17-Au26490 CP % 120 70-130 Pass

Naphthalene M17-Au26490 CP % 98 70-130 Pass

Phenanthrene M17-Au26490 CP % 92 70-130 Pass

Pyrene M17-Au26490 CP % 100 70-130 Pass

Spike - % Recovery


Perfluorobutanoic acid (PFBA) M17-Au26490 CP % 114 50-150 Pass

Perfluoropentanoic acid (PFPeA) M17-Au26490 CP % 137 50-150 Pass

Perfluorohexanoic acid (PFHxA) M17-Au26490 CP % 99 50-150 Pass

Perfluoroheptanoic acid (PFHpA) M17-Au26490 CP % 120 50-150 Pass

Perfluorooctanoic acid (PFOA) M17-Au26490 CP % 110 50-150 Pass

Perfluorononanoic acid (PFNA) M17-Au26490 CP % 140 50-150 Pass

Perfluorodecanoic acid (PFDA) M17-Au26490 CP % 116 50-150 Pass

Perfluoroundecanoic acid (PFUnA) M17-Au26490 CP % 105 50-150 Pass

Perfluorododecanoic acid (PFDoA) M17-Au26490 CP % 127 50-150 Pass

Perfluorotridecanoic acid (PFTrDA) M17-Au26490 CP % 128 50-150 Pass

Perfluorotetradecanoic acid(PFTeDA) M17-Au26490 CP % 128 50-150 Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 19 of 24



LimitsPass

LimitsQualifying

Code

Spike - % Recovery


Perfluorooctane sulfonamide(FOSA) M17-Au26490 CP % 94 50-150 Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) M17-Au26490 CP % 126 50-150 Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) M17-Au26490 CP % 117 50-150 Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) M17-Au26490 CP % 96 50-150 Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) M17-Au26490 CP % 100 50-150 Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-Au26490 CP % 115 50-150 Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-Au26490 CP % 100 50-150 Pass

Spike - % Recovery


Perfluorobutanesulfonic acid(PFBS) M17-Au26490 CP % 110 50-150 Pass

Perfluoropentanesulfonic acid(PFPeS) M17-Au26490 CP % 78 50-150 Pass

Perfluorohexanesulfonic acid(PFHxS) M17-Au26490 CP % 111 50-150 Pass

Perfluoroheptanesulfonic acid(PFHpS) M17-Au26490 CP % 113 50-150 Pass

Perfluorooctanesulfonic acid(PFOS) M17-Au26490 CP % 102 50-150 Pass

Perfluorodecanesulfonic acid(PFDS) M17-Au26490 CP % 113 50-150 Pass

Spike - % Recovery


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-Au26490 CP % 101 50-150 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-Au26490 CP % 90 50-150 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-Au26490 CP % 124 50-150 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) M17-Au26490 CP % 124 50-150 Pass


LimitsPass

LimitsQualifying

Code

Duplicate

Total Recoverable Hydrocarbons - 1999 NEPM Fractions Result 1 Result 2 RPD

TRH C6-C9 M17-Au23804 NCP mg/L < 0.02 < 0.02 <1 30% Pass

Duplicate

BTEX Result 1 Result 2 RPD

Benzene M17-Au23804 NCP mg/L < 0.001 < 0.001 <1 30% Pass

Toluene M17-Au23804 NCP mg/L < 0.001 < 0.001 <1 30% Pass

Ethylbenzene M17-Au23804 NCP mg/L < 0.001 < 0.001 <1 30% Pass

m&p-Xylenes M17-Au23804 NCP mg/L < 0.002 < 0.002 <1 30% Pass

o-Xylene M17-Au23804 NCP mg/L < 0.001 < 0.001 <1 30% Pass

Xylenes - Total M17-Au23804 NCP mg/L < 0.003 < 0.003 <1 30% Pass

Duplicate


Naphthalene M17-Au23804 NCP mg/L < 0.01 < 0.01 <1 30% Pass

TRH C6-C10 M17-Au23804 NCP mg/L < 0.02 < 0.02 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 20 of 24


Duplicate


Perfluorobutanoic acid (PFBA) M17-Au26488 CP ug/L < 0.05 < 0.05 <1 30% Pass

Perfluoropentanoic acid (PFPeA) M17-Au26488 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanoic acid (PFHxA) M17-Au26488 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanoic acid (PFHpA) M17-Au26488 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanoic acid (PFOA) M17-Au26488 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorononanoic acid (PFNA) M17-Au26488 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanoic acid (PFDA) M17-Au26488 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroundecanoic acid (PFUnA) M17-Au26488 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorododecanoic acid (PFDoA) M17-Au26488 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) M17-Au26488 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) M17-Au26488 CP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


Perfluorooctane sulfonamide(FOSA) M17-Au26488 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) M17-Au26488 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) M17-Au26488 CP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) M17-Au26488 CP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) M17-Au26488 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-Au26488 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-Au26488 CP ug/L < 0.05 < 0.05 <1 30% Pass

Duplicate


Perfluorobutanesulfonic acid(PFBS) M17-Au26488 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoropentanesulfonic acid(PFPeS) M17-Au26488 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanesulfonic acid(PFHxS) M17-Au26488 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) M17-Au26488 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanesulfonic acid(PFOS) M17-Au26488 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanesulfonic acid(PFDS) M17-Au26488 CP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-Au26488 CP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-Au26488 CP ug/L < 0.05 < 0.05 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-Au26488 CP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) M17-Au26488 CP ug/L < 0.01 < 0.01 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 21 of 24


Duplicate

Heavy Metals Result 1 Result 2 RPD

Aluminium Z17-Au25837 NCP mg/L < 0.05 < 0.05 <1 30% Pass

Arsenic Z17-Au25837 NCP mg/L < 0.001 < 0.001 <1 30% Pass

Cadmium Z17-Au25837 NCP mg/L < 0.0002 < 0.0002 <1 30% Pass

Chromium Z17-Au25837 NCP mg/L < 0.001 < 0.001 <1 30% Pass

Copper Z17-Au25837 NCP mg/L < 0.001 < 0.001 <1 30% Pass

Iron Z17-Au25837 NCP mg/L < 0.05 < 0.05 <1 30% Pass

Lead Z17-Au25837 NCP mg/L < 0.001 < 0.001 <1 30% Pass

Manganese Z17-Au25837 NCP mg/L 0.068 0.061 10 30% Pass

Mercury Z17-Au25837 NCP mg/L < 0.0001 < 0.0001 <1 30% Pass

Nickel Z17-Au25837 NCP mg/L 0.002 0.002 10 30% Pass

Zinc Z17-Au25837 NCP mg/L 0.009 0.011 20 30% Pass

Duplicate


TRH C10-C14 M17-Au26489 CP mg/L < 0.05 < 0.05 <1 30% Pass



Duplicate


TRH >C10-C16 M17-Au26489 CP mg/L < 0.05 < 0.05 <1 30% Pass



Duplicate

Polycyclic Aromatic Hydrocarbons Result 1 Result 2 RPD

Acenaphthene M17-Au26489 CP mg/L < 0.001 < 0.001 <1 30% Pass

Acenaphthylene M17-Au26489 CP mg/L < 0.001 < 0.001 <1 30% Pass

Anthracene M17-Au26489 CP mg/L < 0.001 < 0.001 <1 30% Pass

Benz(a)anthracene M17-Au26489 CP mg/L < 0.001 < 0.001 <1 30% Pass

Benzo(a)pyrene M17-Au26489 CP mg/L < 0.001 < 0.001 <1 30% Pass

Benzo(b&j)fluoranthene M17-Au26489 CP mg/L < 0.001 < 0.001 <1 30% Pass

Benzo(g.h.i)perylene M17-Au26489 CP mg/L < 0.001 < 0.001 <1 30% Pass

Benzo(k)fluoranthene M17-Au26489 CP mg/L < 0.001 < 0.001 <1 30% Pass

Chrysene M17-Au26489 CP mg/L < 0.001 < 0.001 <1 30% Pass

Dibenz(a.h)anthracene M17-Au26489 CP mg/L < 0.001 < 0.001 <1 30% Pass

Fluoranthene M17-Au26489 CP mg/L < 0.001 < 0.001 <1 30% Pass

Fluorene M17-Au26489 CP mg/L < 0.001 < 0.001 <1 30% Pass

Indeno(1.2.3-cd)pyrene M17-Au26489 CP mg/L < 0.001 < 0.001 <1 30% Pass

Naphthalene M17-Au26489 CP mg/L < 0.001 < 0.001 <1 30% Pass

Phenanthrene M17-Au26489 CP mg/L < 0.001 < 0.001 <1 30% Pass

Pyrene M17-Au26489 CP mg/L < 0.001 < 0.001 <1 30% Pass

Duplicate


Aluminium (filtered) M17-Au26270 NCP mg/L < 0.05 < 0.05 <1 30% Pass

Arsenic (filtered) M17-Au26270 NCP mg/L 0.001 0.001 <1 30% Pass

Cadmium (filtered) M17-Au26270 NCP mg/L < 0.0002 < 0.0002 <1 30% Pass

Chromium (filtered) M17-Au26270 NCP mg/L 0.077 0.073 5.0 30% Pass

Copper (filtered) M17-Au26270 NCP mg/L 0.003 0.003 1.0 30% Pass

Iron (filtered) M17-Au26270 NCP mg/L < 0.05 < 0.05 <1 30% Pass

Lead (filtered) M17-Au26270 NCP mg/L < 0.001 < 0.001 <1 30% Pass

Manganese (filtered) M17-Au26270 NCP mg/L < 0.005 < 0.005 <1 30% Pass

Mercury (filtered) M17-Au26270 NCP mg/L < 0.0001 < 0.0001 <1 30% Pass

Nickel (filtered) M17-Au26270 NCP mg/L 0.003 0.003 10 30% Pass

Zinc (filtered) M17-Au26270 NCP mg/L 0.029 0.027 5.0 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 22 of 24


Duplicate













Duplicate









Duplicate








Duplicate








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 23 of 24


Comments









Code Description

N01F2 is determined by arithmetically subtracting the "naphthalene" value from the ">C10-C16" value. The naphthalene value used in this calculation is obtained from volatiles(Purge & Trap analysis).

N02

Where we have reported both volatile (P&T GCMS) and semivolatile (GCMS) naphthalene data, results may not be identical. Provided correct sample handling protocols havebeen followed, any observed differences in results are likely to be due to procedural differences within each methodology. Results determined by both techniques have passedall QAQC acceptance criteria, and are entirely technically valid.

N04F1 is determined by arithmetically subtracting the "Total BTEX" value from the "C6-C10" value. The "Total BTEX" value is obtained by summing the concentrations of BTEXanalytes. The "C6-C10" value is obtained by quantitating against a standard of mixed aromatic/aliphatic analytes.

N07Please note:- These two PAH isomers closely co-elute using the most contemporary analytical methods and both the reported concentration (and the TEQ) apply specifically tothe total of the two co-eluting PAHs

N11


Authorised By



Alex Petridis Senior Analyst-Organic (VIC)

Harry Bacalis Senior Analyst-Volatile (VIC)


Joseph Edouard Senior Analyst-Organic (VIC)

Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 24 of 24






Abbotsford

VIC 3067


Report 559812-S




Client Sample ID 0990_MW129_0.1_170818

0990_MW129_0.5_170818

0990_QCMW184_170818

0990_QCMW175_170819

Sample Matrix Soil Soil Soil Soil





TRH C6-C9 20 mg/kg - < 20 - -

TRH C10-C14 20 mg/kg - < 20 - -

TRH C15-C28 50 mg/kg - < 50 - -

TRH C29-C36 50 mg/kg - < 50 - -

TRH C10-36 (Total) 50 mg/kg - < 50 - -

BTEX

Benzene 0.1 mg/kg - < 0.1 - -

Toluene 0.1 mg/kg - < 0.1 - -

Ethylbenzene 0.1 mg/kg - < 0.1 - -

m&p-Xylenes 0.2 mg/kg - < 0.2 - -

o-Xylene 0.1 mg/kg - < 0.1 - -

Xylenes - Total 0.3 mg/kg - < 0.3 - -

4-Bromofluorobenzene (surr.) 1 % - 83 - -

Volatile Organics

1.1-Dichloroethane 0.5 mg/kg - < 0.5 - < 0.5

1.1-Dichloroethene 0.5 mg/kg - < 0.5 - < 0.5

1.1.1-Trichloroethane 0.5 mg/kg - < 0.5 - < 0.5

1.1.1.2-Tetrachloroethane 0.5 mg/kg - < 0.5 - < 0.5

1.1.2-Trichloroethane 0.5 mg/kg - < 0.5 - < 0.5

1.1.2.2-Tetrachloroethane 0.5 mg/kg - < 0.5 - < 0.5

1.2-Dibromoethane 0.5 mg/kg - < 0.5 - < 0.5

1.2-Dichlorobenzene 0.5 mg/kg - < 0.5 - < 0.5

1.2-Dichloroethane 0.5 mg/kg - < 0.5 - < 0.5

1.2-Dichloropropane 0.5 mg/kg - < 0.5 - < 0.5

1.2.3-Trichloropropane 0.5 mg/kg - < 0.5 - < 0.5

1.2.4-Trimethylbenzene 0.5 mg/kg - < 0.5 - < 0.5


1.3-Dichloropropane 0.5 mg/kg - < 0.5 - < 0.5

1.3.5-Trimethylbenzene 0.5 mg/kg - < 0.5 - < 0.5


2-Butanone (MEK) 0.5 mg/kg - < 0.5 - < 0.5

2-Propanone (Acetone) 0.5 mg/kg - < 0.5 - < 0.5

4-Chlorotoluene 0.5 mg/kg - < 0.5 - < 0.5

4-Methyl-2-pentanone (MIBK) 0.5 mg/kg - < 0.5 - < 0.5

Allyl chloride 0.5 mg/kg - < 0.5 - < 0.5



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Page 1 of 35

Report Number: 559812-S




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0990_QCMW184_170818

0990_QCMW175_170819





Volatile Organics

Benzene 0.1 mg/kg - < 0.1 - < 0.1

Bromobenzene 0.5 mg/kg - < 0.5 - < 0.5

Bromochloromethane 0.5 mg/kg - < 0.5 - < 0.5

Bromodichloromethane 0.5 mg/kg - < 0.5 - < 0.5

Bromoform 0.5 mg/kg - < 0.5 - < 0.5

Bromomethane 0.5 mg/kg - < 0.5 - < 0.5

Carbon disulfide 0.5 mg/kg - < 0.5 - < 0.5

Carbon Tetrachloride 0.5 mg/kg - < 0.5 - < 0.5

Chlorobenzene 0.5 mg/kg - < 0.5 - < 0.5

Chloroethane 0.5 mg/kg - < 0.5 - < 0.5

Chloroform 0.5 mg/kg - < 0.5 - < 0.5

Chloromethane 0.5 mg/kg - < 0.5 - < 0.5

cis-1.2-Dichloroethene 0.5 mg/kg - < 0.5 - < 0.5

cis-1.3-Dichloropropene 0.5 mg/kg - < 0.5 - < 0.5

Dibromochloromethane 0.5 mg/kg - < 0.5 - < 0.5

Dibromomethane 0.5 mg/kg - < 0.5 - < 0.5

Dichlorodifluoromethane 0.5 mg/kg - < 0.5 - < 0.5

Ethylbenzene 0.1 mg/kg - < 0.1 - < 0.1

Iodomethane 0.5 mg/kg - < 0.5 - < 0.5

Isopropyl benzene (Cumene) 0.5 mg/kg - < 0.5 - < 0.5

m&p-Xylenes 0.2 mg/kg - < 0.2 - < 0.2

Methylene Chloride 0.5 mg/kg - < 0.5 - < 0.5

o-Xylene 0.1 mg/kg - < 0.1 - < 0.1

Styrene 0.5 mg/kg - < 0.5 - < 0.5

Tetrachloroethene 0.5 mg/kg - < 0.5 - < 0.5

Toluene 0.1 mg/kg - < 0.1 - < 0.1

trans-1.2-Dichloroethene 0.5 mg/kg - < 0.5 - < 0.5

trans-1.3-Dichloropropene 0.5 mg/kg - < 0.5 - < 0.5

Trichloroethene 0.5 mg/kg - < 0.5 - < 0.5

Trichlorofluoromethane 0.5 mg/kg - < 0.5 - < 0.5

Vinyl chloride 0.5 mg/kg - < 0.5 - < 0.5

Xylenes - Total 0.3 mg/kg - < 0.3 - < 0.3

Vic EPA IWRG 621 Chlorinated hydrocarbons (Total)* 0.5 mg/kg - < 0.5 - < 0.5

Vic EPA IWRG 621 Other chlorinated hydrocarbons(Total)* 0.5 mg/kg - < 0.5 - < 0.5

4-Bromofluorobenzene (surr.) 1 % - 83 - 81

Fluorobenzene (surr.) 1 % - 123 - 86


NaphthaleneN02 0.5 mg/kg - < 0.5 - -

TRH C6-C10 less BTEX (F1)N04 20 mg/kg - < 20 - -

TRH C6-C10 20 mg/kg - < 20 - -

TRH >C10-C16 50 mg/kg - < 50 - -

TRH >C10-C16 less Naphthalene (F2)N01 50 mg/kg - < 50 - -

TRH >C16-C34 100 mg/kg - < 100 - -

TRH >C34-C40 100 mg/kg - < 100 - -



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Semivolatile Organics

2-Methyl-4.6-dinitrophenol 5 mg/kg - < 5 - < 5

Benzo(a)pyrene TEQ (lower bound) * 0.5 mg/kg - < 0.5 - < 0.5

Benzo(a)pyrene TEQ (medium bound) * 0.5 mg/kg - 0.6 - 0.6

Benzo(a)pyrene TEQ (upper bound) * 0.5 mg/kg - 1.2 - 1.2

1-Chloronaphthalene 0.5 mg/kg - < 0.5 - < 0.5

1-Naphthylamine 0.5 mg/kg - < 0.5 - < 0.5


1.2.3-Trichlorobenzene 0.5 mg/kg - < 0.5 - < 0.5

1.2.3.4-Tetrachlorobenzene 0.5 mg/kg - < 0.5 - < 0.5







2-Chloronaphthalene 0.5 mg/kg - < 0.5 - < 0.5

2-Chlorophenol 0.5 mg/kg - < 0.5 - < 0.5

2-Methylnaphthalene 0.5 mg/kg - < 0.5 - < 0.5

2-Methylphenol (o-Cresol) 0.2 mg/kg - < 0.2 - < 0.2

2-Naphthylamine 0.5 mg/kg - < 0.5 - < 0.5

2-Nitroaniline 0.5 mg/kg - < 0.5 - < 0.5

2-Nitrophenol 1.0 mg/kg - < 1 - < 1

2-Picoline 0.5 mg/kg - < 0.5 - < 0.5

2.3.4.6-Tetrachlorophenol 0.5 mg/kg - < 0.5 - < 0.5

2.4-Dichlorophenol 0.5 mg/kg - < 0.5 - < 0.5

2.4-Dimethylphenol 0.5 mg/kg - < 0.5 - < 0.5

2.4-Dinitrophenol 5 mg/kg - < 5 - < 5

2.4-Dinitrotoluene 0.5 mg/kg - < 0.5 - < 0.5

2.4.5-Trichlorophenol 1.0 mg/kg - < 1 - < 1

2.4.6-Trichlorophenol 1.0 mg/kg - < 1 - < 1

2.6-Dichlorophenol 0.5 mg/kg - < 0.5 - < 0.5

2.6-Dinitrotoluene 0.5 mg/kg - < 0.5 - < 0.5

3&4-Methylphenol (m&p-Cresol) 0.4 mg/kg - < 0.4 - < 0.4

3-Methylcholanthrene 0.5 mg/kg - < 0.5 - < 0.5

3.3'-Dichlorobenzidine 0.5 mg/kg - < 0.5 - < 0.5

4-Aminobiphenyl 0.5 mg/kg - < 0.5 - < 0.5

4-Bromophenyl phenyl ether 0.5 mg/kg - < 0.5 - < 0.5

4-Chloro-3-methylphenol 1.0 mg/kg - < 1 - < 1

4-Chlorophenyl phenyl ether 0.5 mg/kg - < 0.5 - < 0.5

4-Nitrophenol 5 mg/kg - < 5 - < 5

4.4'-DDD 0.5 mg/kg - < 0.5 - < 0.5

4.4'-DDE 0.5 mg/kg - < 0.5 - < 0.5

4.4'-DDT 0.5 mg/kg - < 0.5 - < 0.5

7.12-Dimethylbenz(a)anthracene 0.5 mg/kg - < 0.5 - < 0.5

a-BHC 0.5 mg/kg - < 0.5 - < 0.5

Acenaphthene 0.5 mg/kg - < 0.5 - < 0.5

Acenaphthylene 0.5 mg/kg - < 0.5 - < 0.5

Acetophenone 0.5 mg/kg - < 0.5 - < 0.5

Aldrin 0.5 mg/kg - < 0.5 - < 0.5



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Aniline 0.5 mg/kg - < 0.5 - < 0.5

Anthracene 0.5 mg/kg - < 0.5 - < 0.5

b-BHC 0.5 mg/kg - < 0.5 - < 0.5

Benz(a)anthracene 0.5 mg/kg - < 0.5 - < 0.5

Benzo(a)pyrene 0.5 mg/kg - < 0.5 - < 0.5

Benzo(b&j)fluorantheneN07 0.5 mg/kg - < 0.5 - < 0.5

Benzo(g.h.i)perylene 0.5 mg/kg - < 0.5 - < 0.5

Benzo(k)fluoranthene 0.5 mg/kg - < 0.5 - < 0.5

Benzyl chloride 0.5 mg/kg - < 0.5 - < 0.5

Bis(2-chloroethoxy)methane 0.5 mg/kg - < 0.5 - < 0.5

Bis(2-chloroisopropyl)ether 0.5 mg/kg - < 0.5 - < 0.5

Bis(2-ethylhexyl)phthalate 0.5 mg/kg - < 0.5 - < 0.5

Butyl benzyl phthalate 0.5 mg/kg - < 0.5 - < 0.5

Chrysene 0.5 mg/kg - < 0.5 - < 0.5

d-BHC 0.5 mg/kg - < 0.5 - < 0.5

Di-n-butyl phthalate 0.5 mg/kg - < 0.5 - < 0.5

Di-n-octyl phthalate 0.5 mg/kg - < 0.5 - < 0.5

Dibenz(a.h)anthracene 0.5 mg/kg - < 0.5 - < 0.5

Dibenz(a.j)acridine 0.5 mg/kg - < 0.5 - < 0.5

Dibenzofuran 0.5 mg/kg - < 0.5 - < 0.5

Dieldrin 0.5 mg/kg - < 0.5 - < 0.5

Diethyl phthalate 0.5 mg/kg - < 0.5 - < 0.5

Dimethyl phthalate 0.5 mg/kg - < 0.5 - < 0.5

Dimethylaminoazobenzene 0.5 mg/kg - < 0.5 - < 0.5

Diphenylamine 0.5 mg/kg - < 0.5 - < 0.5

Endosulfan I 0.5 mg/kg - < 0.5 - < 0.5

Endosulfan II 0.5 mg/kg - < 0.5 - < 0.5

Endosulfan sulphate 0.5 mg/kg - < 0.5 - < 0.5

Endrin 0.5 mg/kg - < 0.5 - < 0.5

Endrin aldehyde 0.5 mg/kg - < 0.5 - < 0.5

Endrin ketone 0.5 mg/kg - < 0.5 - < 0.5

Fluoranthene 0.5 mg/kg - < 0.5 - < 0.5

Fluorene 0.5 mg/kg - < 0.5 - < 0.5

g-BHC (Lindane) 0.5 mg/kg - < 0.5 - < 0.5

Heptachlor 0.5 mg/kg - < 0.5 - < 0.5

Heptachlor epoxide 0.5 mg/kg - < 0.5 - < 0.5

Hexachlorobenzene 0.5 mg/kg - < 0.5 - < 0.5

Hexachlorobutadiene 0.5 mg/kg - < 0.5 - < 0.5

Hexachlorocyclopentadiene 0.5 mg/kg - < 0.5 - < 0.5

Hexachloroethane 0.5 mg/kg - < 0.5 - < 0.5

Indeno(1.2.3-cd)pyrene 0.5 mg/kg - < 0.5 - < 0.5

Methoxychlor 0.5 mg/kg - < 0.5 - < 0.5

N-Nitrosodibutylamine 0.5 mg/kg - < 0.5 - < 0.5

N-Nitrosodipropylamine 0.5 mg/kg - < 0.5 - < 0.5

N-Nitrosopiperidine 0.5 mg/kg - < 0.5 - < 0.5

Naphthalene 0.5 mg/kg - < 0.5 - < 0.5

Nitrobenzene 0.5 mg/kg - < 0.5 - < 0.5

Pentachlorobenzene 0.5 mg/kg - < 0.5 - < 0.5

Pentachloronitrobenzene 0.5 mg/kg - < 0.5 - < 0.5



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Page 4 of 35



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Pentachlorophenol 1.0 mg/kg - < 1 - < 1

Phenanthrene 0.5 mg/kg - < 0.5 - < 0.5

Phenol 0.5 mg/kg - < 0.5 - < 0.5

Pronamide 0.5 mg/kg - < 0.5 - < 0.5

Pyrene 0.5 mg/kg - < 0.5 - < 0.5

Trifluralin 0.5 mg/kg - < 0.5 - < 0.5

Phenol-d6 (surr.) 1 % - 81 - 82

Nitrobenzene-d5 (surr.) 1 % - 90 - 93

2-Fluorobiphenyl (surr.) 1 % - 104 - 109

2.4.6-Tribromophenol (surr.) 1 % - 31 - 36


Perfluorobutanoic acid (PFBA)N11 5 ug/kg 13 < 5 10 < 5

Perfluoropentanoic acid (PFPeA)N11 5 ug/kg 24 9.2 20 < 5

Perfluorohexanoic acid (PFHxA)N11 5 ug/kg N0996 N0932 N0987 N0938

Perfluoroheptanoic acid (PFHpA)N11 5 ug/kg N0931 N0927 N0930 N097.4

Perfluorooctanoic acid (PFOA)N11 5 ug/kg N0956 N0994 N0956 N0911

Perfluorononanoic acid (PFNA)N11 5 ug/kg < 5 < 5 < 5 < 5

Perfluorodecanoic acid (PFDA)N11 5 ug/kg < 5 < 5 < 5 < 5

Perfluoroundecanoic acid (PFUnA)N11 5 ug/kg < 5 < 5 < 5 < 5

Perfluorododecanoic acid (PFDoA)N11 5 ug/kg < 5 < 5 < 5 < 5

Perfluorotridecanoic acid (PFTrDA) 5 ug/kg < 5 < 5 < 5 < 5

Perfluorotetradecanoic acid (PFTeDA)N11 5 ug/kg < 5 < 5 < 5 < 5

13C4-PFBA (surr.) 1 % 114 117 118 115

13C5-PFPeA (surr.) 1 % 105 107 106 103

13C5-PFHxA (surr.) 1 % 112 120 116 115

13C4-PFHpA (surr.) 1 % 109 113 112 112

13C8-PFOA (surr.) 1 % 104 103 106 102

13C5-PFNA (surr.) 1 % 111 112 115 126

13C6-PFDA (surr.) 1 % 97 91 96 108

13C2-PFUnDA (surr.) 1 % 112 114 117 109

13C2-PFDoDA (surr.) 1 % 114 120 119 113

13C2-PFTeDA (surr.) 1 % 133 132 138 114


Perfluorooctane sulfonamide (FOSA)N11 5 ug/kg N0918 < 5 N0918 < 5

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA)N11 5 ug/kg < 5 < 5 < 5 < 5

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA)N11 5 ug/kg < 5 < 5 < 5 < 5

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol(N-MeFOSE)N11 5 ug/kg < 5 < 5 < 5 < 5

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE)N11 5 ug/kg < 5 < 5 < 5 < 5

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA)N11 10 ug/kg < 10 < 10 < 10 < 10

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA)N11 10 ug/kg < 10 < 10 < 10 < 10

13C8-FOSA (surr.) 1 % 80 81 82 75

D3-N-MeFOSA (surr.) 1 % 133 135 141 120

D5-N-EtFOSA (surr.) 1 % 101 100 102 92

D7-N-MeFOSE (surr.) 1 % 120 123 130 113

D9-N-EtFOSE (surr.) 1 % 126 124 127 112



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Page 5 of 35



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D5-N-EtFOSAA (surr.) 1 % 145 142 149 140

D3-N-MeFOSAA (surr.) 1 % 156 155 155 158


Perfluorobutanesulfonic acid (PFBS)N11 5 ug/kg 16 5.2 15 39

Perfluoropentanesulfonic acid (PFPeS) 5 ug/kg 23 11 22 32

Perfluorohexanesulfonic acid (PFHxS)N11 5 ug/kg N09180 N09170 N09170 N09320

Perfluoroheptanesulfonic acid (PFHpS) 5 ug/kg N0925 N0965 N0926 < 5

Perfluorooctanesulfonic acid (PFOS)N11 5 ug/kg N091700 N091300 N091800 N0934

Perfluorodecanesulfonic acid (PFDS) 5 ug/kg < 5 < 5 < 5 < 5

13C3-PFBS (surr.) 1 % 110 110 111 111

18O2-PFHxS (surr.) 1 % 103 106 106 101

13C8-PFOS (surr.) 1 % 103 86 110 99


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS)N11 5 ug/kg < 5 < 5 < 5 < 5

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS)N11 10 ug/kg < 10 19 < 10 < 10

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS)N11 5 ug/kg 6.3 < 5 < 5 < 5

1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2FTS) 5 ug/kg < 5 < 5 < 5 < 5

13C2-4:2 FTS (surr.) 1 % 114 116 117 121

13C2-6:2 FTS (surr.) 1 % 106 108 108 115

13C2-8:2 FTS (surr.) 1 % 122 121 126 131

PFASs Summations

Sum (PFHxS + PFOS) 5 ug/kg 1880 1470 1970 354

Sum of US EPA PFAS (PFOS + PFOA) 5 ug/kg 1756 1394 1856 45

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 5 ug/kg 1936 1564 2026 365

Sum of WA DER PFAS (n=10) 10 ug/kg 2122.3 1656.4 2188 449.4

Sum of PFASs (n=28) 50 ug/kg 2188.3 1732.4 2254 481.4

1.4-Dioxane

1.4-Dioxane 10 ug/kg - < 10 - < 10

1.4-Dioxane-d8 (surr.) 1 % - 86 - 78

Heavy Metals

Arsenic 2 mg/kg 2.9 15 5.7 6.7

Cadmium 0.4 mg/kg < 0.4 < 0.4 < 0.4 < 0.4

Chromium 5 mg/kg 25 140 47 52

Copper 5 mg/kg 6.6 8.2 6.2 17

Lead 5 mg/kg 5.9 20 9.3 20

Mercury 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1

Nickel 5 mg/kg 6.5 < 5 6.9 14

Zinc 5 mg/kg 8.3 < 5 8.5 13

% Moisture 1 % 3.6 6.0 4.0 21



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0990_MW128_1.0_170819

0990_MW129_1.0_170818





Volatile Organics

1.1-Dichloroethane 0.5 mg/kg < 0.5 - - -

1.1-Dichloroethene 0.5 mg/kg < 0.5 - - -

1.1.1-Trichloroethane 0.5 mg/kg < 0.5 - - -

1.1.1.2-Tetrachloroethane 0.5 mg/kg < 0.5 - - -

1.1.2-Trichloroethane 0.5 mg/kg < 0.5 - - -

1.1.2.2-Tetrachloroethane 0.5 mg/kg < 0.5 - - -

1.2-Dibromoethane 0.5 mg/kg < 0.5 - - -

1.2-Dichlorobenzene 0.5 mg/kg < 0.5 - - -

1.2-Dichloroethane 0.5 mg/kg < 0.5 - - -

1.2-Dichloropropane 0.5 mg/kg < 0.5 - - -

1.2.3-Trichloropropane 0.5 mg/kg < 0.5 - - -

1.2.4-Trimethylbenzene 0.5 mg/kg < 0.5 - - -


1.3-Dichloropropane 0.5 mg/kg < 0.5 - - -

1.3.5-Trimethylbenzene 0.5 mg/kg < 0.5 - - -


2-Butanone (MEK) 0.5 mg/kg < 0.5 - - -

2-Propanone (Acetone) 0.5 mg/kg < 0.5 - - -

4-Chlorotoluene 0.5 mg/kg < 0.5 - - -

4-Methyl-2-pentanone (MIBK) 0.5 mg/kg < 0.5 - - -

Allyl chloride 0.5 mg/kg < 0.5 - - -

Benzene 0.1 mg/kg < 0.1 - - -

Bromobenzene 0.5 mg/kg < 0.5 - - -

Bromochloromethane 0.5 mg/kg < 0.5 - - -

Bromodichloromethane 0.5 mg/kg < 0.5 - - -

Bromoform 0.5 mg/kg < 0.5 - - -

Bromomethane 0.5 mg/kg < 0.5 - - -

Carbon disulfide 0.5 mg/kg < 0.5 - - -

Carbon Tetrachloride 0.5 mg/kg < 0.5 - - -

Chlorobenzene 0.5 mg/kg < 0.5 - - -

Chloroethane 0.5 mg/kg < 0.5 - - -

Chloroform 0.5 mg/kg < 0.5 - - -

Chloromethane 0.5 mg/kg < 0.5 - - -

cis-1.2-Dichloroethene 0.5 mg/kg < 0.5 - - -

cis-1.3-Dichloropropene 0.5 mg/kg < 0.5 - - -

Dibromochloromethane 0.5 mg/kg < 0.5 - - -

Dibromomethane 0.5 mg/kg < 0.5 - - -

Dichlorodifluoromethane 0.5 mg/kg < 0.5 - - -

Ethylbenzene 0.1 mg/kg < 0.1 - - -

Iodomethane 0.5 mg/kg < 0.5 - - -

Isopropyl benzene (Cumene) 0.5 mg/kg < 0.5 - - -

m&p-Xylenes 0.2 mg/kg < 0.2 - - -

Methylene Chloride 0.5 mg/kg < 0.5 - - -

o-Xylene 0.1 mg/kg < 0.1 - - -

Styrene 0.5 mg/kg < 0.5 - - -

Tetrachloroethene 0.5 mg/kg < 0.5 - - -

Toluene 0.1 mg/kg < 0.1 - - -

trans-1.2-Dichloroethene 0.5 mg/kg < 0.5 - - -

trans-1.3-Dichloropropene 0.5 mg/kg < 0.5 - - -



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 35



0990_MW128_0.5_170819

0990_MW128_1.0_170819

0990_MW129_1.0_170818





Volatile Organics

Trichloroethene 0.5 mg/kg < 0.5 - - -

Trichlorofluoromethane 0.5 mg/kg < 0.5 - - -

Vinyl chloride 0.5 mg/kg < 0.5 - - -

Xylenes - Total 0.3 mg/kg < 0.3 - - -

Vic EPA IWRG 621 Chlorinated hydrocarbons (Total)* 0.5 mg/kg < 0.5 - - -

Vic EPA IWRG 621 Other chlorinated hydrocarbons(Total)* 0.5 mg/kg < 0.5 - - -

4-Bromofluorobenzene (surr.) 1 % 64 - - -

Fluorobenzene (surr.) 1 % 78 - - -


2-Methyl-4.6-dinitrophenol 5 mg/kg < 5 - - -

Benzo(a)pyrene TEQ (lower bound) * 0.5 mg/kg < 0.5 - - -

Benzo(a)pyrene TEQ (medium bound) * 0.5 mg/kg 0.6 - - -

Benzo(a)pyrene TEQ (upper bound) * 0.5 mg/kg 1.2 - - -

1-Chloronaphthalene 0.5 mg/kg < 0.5 - - -

1-Naphthylamine 0.5 mg/kg < 0.5 - - -


1.2.3-Trichlorobenzene 0.5 mg/kg < 0.5 - - -

1.2.3.4-Tetrachlorobenzene 0.5 mg/kg < 0.5 - - -







2-Chloronaphthalene 0.5 mg/kg < 0.5 - - -

2-Chlorophenol 0.5 mg/kg < 0.5 - - -

2-Methylnaphthalene 0.5 mg/kg < 0.5 - - -

2-Methylphenol (o-Cresol) 0.2 mg/kg < 0.2 - - -

2-Naphthylamine 0.5 mg/kg < 0.5 - - -

2-Nitroaniline 0.5 mg/kg < 0.5 - - -

2-Nitrophenol 1.0 mg/kg < 1 - - -

2-Picoline 0.5 mg/kg < 0.5 - - -

2.3.4.6-Tetrachlorophenol 0.5 mg/kg < 0.5 - - -

2.4-Dichlorophenol 0.5 mg/kg < 0.5 - - -

2.4-Dimethylphenol 0.5 mg/kg < 0.5 - - -

2.4-Dinitrophenol 5 mg/kg < 5 - - -

2.4-Dinitrotoluene 0.5 mg/kg < 0.5 - - -

2.4.5-Trichlorophenol 1.0 mg/kg < 1 - - -

2.4.6-Trichlorophenol 1.0 mg/kg < 1 - - -

2.6-Dichlorophenol 0.5 mg/kg < 0.5 - - -

2.6-Dinitrotoluene 0.5 mg/kg < 0.5 - - -

3&4-Methylphenol (m&p-Cresol) 0.4 mg/kg < 0.4 - - -

3-Methylcholanthrene 0.5 mg/kg < 0.5 - - -

3.3'-Dichlorobenzidine 0.5 mg/kg < 0.5 - - -

4-Aminobiphenyl 0.5 mg/kg < 0.5 - - -

4-Bromophenyl phenyl ether 0.5 mg/kg < 0.5 - - -

4-Chloro-3-methylphenol 1.0 mg/kg < 1 - - -

4-Chlorophenyl phenyl ether 0.5 mg/kg < 0.5 - - -



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 35



0990_MW128_0.5_170819

0990_MW128_1.0_170819

0990_MW129_1.0_170818






4-Nitrophenol 5 mg/kg < 5 - - -

4.4'-DDD 0.5 mg/kg < 0.5 - - -

4.4'-DDE 0.5 mg/kg < 0.5 - - -

4.4'-DDT 0.5 mg/kg < 0.5 - - -

7.12-Dimethylbenz(a)anthracene 0.5 mg/kg < 0.5 - - -

a-BHC 0.5 mg/kg < 0.5 - - -

Acenaphthene 0.5 mg/kg < 0.5 - - -

Acenaphthylene 0.5 mg/kg < 0.5 - - -

Acetophenone 0.5 mg/kg < 0.5 - - -

Aldrin 0.5 mg/kg < 0.5 - - -

Aniline 0.5 mg/kg < 0.5 - - -

Anthracene 0.5 mg/kg < 0.5 - - -

b-BHC 0.5 mg/kg < 0.5 - - -

Benz(a)anthracene 0.5 mg/kg < 0.5 - - -

Benzo(a)pyrene 0.5 mg/kg < 0.5 - - -

Benzo(b&j)fluorantheneN07 0.5 mg/kg < 0.5 - - -

Benzo(g.h.i)perylene 0.5 mg/kg < 0.5 - - -

Benzo(k)fluoranthene 0.5 mg/kg < 0.5 - - -

Benzyl chloride 0.5 mg/kg < 0.5 - - -

Bis(2-chloroethoxy)methane 0.5 mg/kg < 0.5 - - -

Bis(2-chloroisopropyl)ether 0.5 mg/kg < 0.5 - - -

Bis(2-ethylhexyl)phthalate 0.5 mg/kg < 0.5 - - -

Butyl benzyl phthalate 0.5 mg/kg < 0.5 - - -

Chrysene 0.5 mg/kg < 0.5 - - -

d-BHC 0.5 mg/kg < 0.5 - - -

Di-n-butyl phthalate 0.5 mg/kg < 0.5 - - -

Di-n-octyl phthalate 0.5 mg/kg < 0.5 - - -

Dibenz(a.h)anthracene 0.5 mg/kg < 0.5 - - -

Dibenz(a.j)acridine 0.5 mg/kg < 0.5 - - -

Dibenzofuran 0.5 mg/kg < 0.5 - - -

Dieldrin 0.5 mg/kg < 0.5 - - -

Diethyl phthalate 0.5 mg/kg < 0.5 - - -

Dimethyl phthalate 0.5 mg/kg < 0.5 - - -

Dimethylaminoazobenzene 0.5 mg/kg < 0.5 - - -

Diphenylamine 0.5 mg/kg < 0.5 - - -

Endosulfan I 0.5 mg/kg < 0.5 - - -

Endosulfan II 0.5 mg/kg < 0.5 - - -

Endosulfan sulphate 0.5 mg/kg < 0.5 - - -

Endrin 0.5 mg/kg < 0.5 - - -

Endrin aldehyde 0.5 mg/kg < 0.5 - - -

Endrin ketone 0.5 mg/kg < 0.5 - - -

Fluoranthene 0.5 mg/kg < 0.5 - - -

Fluorene 0.5 mg/kg < 0.5 - - -

g-BHC (Lindane) 0.5 mg/kg < 0.5 - - -

Heptachlor 0.5 mg/kg < 0.5 - - -

Heptachlor epoxide 0.5 mg/kg < 0.5 - - -

Hexachlorobenzene 0.5 mg/kg < 0.5 - - -

Hexachlorobutadiene 0.5 mg/kg < 0.5 - - -

Hexachlorocyclopentadiene 0.5 mg/kg < 0.5 - - -



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 35



0990_MW128_0.5_170819

0990_MW128_1.0_170819

0990_MW129_1.0_170818






Hexachloroethane 0.5 mg/kg < 0.5 - - -

Indeno(1.2.3-cd)pyrene 0.5 mg/kg < 0.5 - - -

Methoxychlor 0.5 mg/kg < 0.5 - - -

N-Nitrosodibutylamine 0.5 mg/kg < 0.5 - - -

N-Nitrosodipropylamine 0.5 mg/kg < 0.5 - - -

N-Nitrosopiperidine 0.5 mg/kg < 0.5 - - -

Naphthalene 0.5 mg/kg < 0.5 - - -

Nitrobenzene 0.5 mg/kg < 0.5 - - -

Pentachlorobenzene 0.5 mg/kg < 0.5 - - -

Pentachloronitrobenzene 0.5 mg/kg < 0.5 - - -

Pentachlorophenol 1.0 mg/kg < 1 - - -

Phenanthrene 0.5 mg/kg < 0.5 - - -

Phenol 0.5 mg/kg < 0.5 - - -

Pronamide 0.5 mg/kg < 0.5 - - -

Pyrene 0.5 mg/kg < 0.5 - - -

Trifluralin 0.5 mg/kg < 0.5 - - -

Phenol-d6 (surr.) 1 % 78 - - -

Nitrobenzene-d5 (surr.) 1 % 93 - - -

2-Fluorobiphenyl (surr.) 1 % 111 - - -

2.4.6-Tribromophenol (surr.) 1 % 46 - - -


Perfluorobutanoic acid (PFBA)N11 5 ug/kg < 5 < 5 < 5 6.3

Perfluoropentanoic acid (PFPeA)N11 5 ug/kg < 5 < 5 < 5 14

Perfluorohexanoic acid (PFHxA)N11 5 ug/kg N0920 < 5 < 5 N0952

Perfluoroheptanoic acid (PFHpA)N11 5 ug/kg < 5 < 5 < 5 N0930

Perfluorooctanoic acid (PFOA)N11 5 ug/kg N096.4 < 5 < 5 N09140

Perfluorononanoic acid (PFNA)N11 5 ug/kg < 5 < 5 < 5 < 5

Perfluorodecanoic acid (PFDA)N11 5 ug/kg < 5 < 5 < 5 < 5

Perfluoroundecanoic acid (PFUnA)N11 5 ug/kg < 5 < 5 < 5 < 5

Perfluorododecanoic acid (PFDoA)N11 5 ug/kg < 5 < 5 < 5 < 5

Perfluorotridecanoic acid (PFTrDA) 5 ug/kg < 5 < 5 < 5 < 5

Perfluorotetradecanoic acid (PFTeDA)N11 5 ug/kg < 5 < 5 < 5 < 5

13C4-PFBA (surr.) 1 % 116 126 123 129

13C5-PFPeA (surr.) 1 % 113 119 133 134

13C5-PFHxA (surr.) 1 % 120 131 128 127

13C4-PFHpA (surr.) 1 % 113 119 116 118

13C8-PFOA (surr.) 1 % 100 115 112 102

13C5-PFNA (surr.) 1 % 109 116 112 116

13C6-PFDA (surr.) 1 % 110 116 117 99

13C2-PFUnDA (surr.) 1 % 111 113 107 110

13C2-PFDoDA (surr.) 1 % 108 124 121 123

13C2-PFTeDA (surr.) 1 % 123 132 130 135


Perfluorooctane sulfonamide (FOSA)N11 5 ug/kg < 5 < 5 < 5 < 5

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA)N11 5 ug/kg < 5 < 5 < 5 < 5

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA)N11 5 ug/kg < 5 < 5 < 5 < 5

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol(N-MeFOSE)N11 5 ug/kg < 5 < 5 < 5 < 5



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 35



0990_MW128_0.5_170819

0990_MW128_1.0_170819

0990_MW129_1.0_170818






2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE)N11 5 ug/kg < 5 < 5 < 5 < 5

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA)N11 10 ug/kg < 10 < 10 < 10 < 10

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA)N11 10 ug/kg < 10 < 10 < 10 < 10

13C8-FOSA (surr.) 1 % 83 79 75 77

D3-N-MeFOSA (surr.) 1 % 132 142 137 142

D5-N-EtFOSA (surr.) 1 % 94 100 94 94

D7-N-MeFOSE (surr.) 1 % 118 149 148 161

D9-N-EtFOSE (surr.) 1 % 112 138 137 143

D5-N-EtFOSAA (surr.) 1 % 132 142 148 160

D3-N-MeFOSAA (surr.) 1 % 149 159 168 177


Perfluorobutanesulfonic acid (PFBS)N11 5 ug/kg 21 < 5 < 5 10

Perfluoropentanesulfonic acid (PFPeS) 5 ug/kg 17 < 5 < 5 10

Perfluorohexanesulfonic acid (PFHxS)N11 5 ug/kg N09160 < 5 < 5 N09290

Perfluoroheptanesulfonic acid (PFHpS) 5 ug/kg < 5 < 5 < 5 12

Perfluorooctanesulfonic acid (PFOS)N11 5 ug/kg N0923 N0953 N0929 N092200

Perfluorodecanesulfonic acid (PFDS) 5 ug/kg < 5 < 5 < 5 < 5

13C3-PFBS (surr.) 1 % 112 118 118 120

18O2-PFHxS (surr.) 1 % 106 117 112 111

13C8-PFOS (surr.) 1 % 102 109 104 67


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS)N11 5 ug/kg < 5 < 5 < 5 < 5

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS)N11 10 ug/kg < 10 < 10 < 10 15

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS)N11 5 ug/kg < 5 < 5 < 5 < 5

1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2FTS) 5 ug/kg < 5 < 5 < 5 < 5

13C2-4:2 FTS (surr.) 1 % 119 124 124 124

13C2-6:2 FTS (surr.) 1 % 118 103 106 116

13C2-8:2 FTS (surr.) 1 % 125 134 133 140

PFASs Summations

Sum (PFHxS + PFOS) 5 ug/kg 183 53 29 2490

Sum of US EPA PFAS (PFOS + PFOA) 5 ug/kg 29.4 53 29 2340

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 5 ug/kg 189.4 53 29 2630

Sum of WA DER PFAS (n=10) 10 ug/kg 230.4 53 29 2757.3

Sum of PFASs (n=28) 50 ug/kg 247.4 53 < 50 2779.3

1.4-Dioxane

1.4-Dioxane 10 ug/kg < 10 - - -

1.4-Dioxane-d8 (surr.) 1 % 85 - - -

Heavy Metals

Arsenic 2 mg/kg 4.9 15 5.0 5.3

Cadmium 0.4 mg/kg < 0.4 < 0.4 < 0.4 < 0.4

Chromium 5 mg/kg 41 55 37 47

Copper 5 mg/kg 14 21 12 7.3

Lead 5 mg/kg 20 50 31 7.8

Mercury 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 35



0990_MW128_0.5_170819

0990_MW128_1.0_170819

0990_MW129_1.0_170818





Heavy Metals

Nickel 5 mg/kg 12 17 10 8.6

Zinc 5 mg/kg 45 6.9 6.5 < 5

% Moisture 1 % 3.0 12 21 7.5



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 12 of 35






- Method: LTM-ORG-2010 TRH C6-C36





BTEX and Naphthalene

BTEX Melbourne Aug 24, 2017 14 Day


Volatile Organics Melbourne Aug 24, 2017 7 Days

- Method: LTM-ORG-2150 VOCs in Soils Liquid and other Aqueous Matrices

Semivolatile Organics Melbourne Aug 24, 2017 14 Day

- Method: USEPA 8270 Semivolatile Organics

Metals M8 Sydney Aug 24, 2017 28 Day

- Method: LTM-MET-3040_R0 TOTAL AND DISSOLVED METALS AND MERCURY IN WATERS BY ICP-MS










% Moisture Melbourne Aug 24, 2017 14 Day

- Method: LTM-GEN-7080 Moisture



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 13 of 35


.Company Name: Coffey Environments Pty Ltd VIC Order No.: Received: Aug 22, 2017 9:52 PMAddress: Level 1, 436 Johnston Street Report #: 559812 Due: Aug 30, 2017




Sample Detail

Chloride

HO

LD

Sulphate (as S

O4)

Total A

lkalinity (as CaC

O3)

Alkali M

etals

Metals M

8

BT

EX

and Naphthalene

Volatile O

rganics

Moisture S

et

Sem

ivolatile Organics

Total R


Per- and P


ubstances(P

FA

Ss)

1.4-Dioxane

Melbourne Laboratory - NATA Site # 1254 & 14271 X X X X X X X X X X

Sydney Laboratory - NATA Site # 18217 X X



External Laboratory


Matrix LAB ID

1 0990_PB027_170817

Aug 17, 2017 Water M17-Au26590 X X X X X

2 0990_PB028_1_170817


3 0990_PB028_2_170817


4 0990_QCMW167_170817

Aug 17, 2017 Water M17-Au26593 X

5 0990_QCMW183_170817

Aug 17, 2017 Water M17-Au26594 X

6 0990_PB29_1 Aug 18, 2017 Water M17-Au26595 X X X X X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 14 of 35


Company Name: Coffey Environments Pty Ltd VIC Order No.: Received: Aug 22, 2017 9:52 PMAddress: Level 1, 436 Johnston Street Report #: 559812 Due: Aug 30, 2017




Sample Detail

Chloride

HO

LD

Sulphate (as S

O4)

Total A

lkalinity (as CaC

O3)

Alkali M

etals

Metals M

8

BT

EX

and Naphthalene

Volatile O

rganics

Moisture S

et

Sem

ivolatile Organics

Total R


Per- and P


ubstances(P

FA

Ss)

1.4-Dioxane





70818

7 0990_MW129_0.1_170818

Aug 18, 2017 Soil M17-Au26596 X X X

8 0990_MW129_0.5_170818

Aug 18, 2017 Soil M17-Au26597 X X X X X X X X

9 0990_QCMW185_170818

Aug 18, 2017 Water M17-Au26598 X

10 0990_QCMW184_170818

Aug 18, 2017 Soil M17-Au26599 X X X

11 0990_QCMW168_170818

Aug 18, 2017 Water M17-Au26600 X

12 0990_QCMW175_170819

Aug 19, 2017 Soil M17-Au26601 X X X X X X

13 0990_QCMW1 Aug 19, 2017 Water M17-Au26602 X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 15 of 35






Sample Detail

Chloride

HO

LD

Sulphate (as S

O4)

Total A

lkalinity (as CaC

O3)

Alkali M

etals

Metals M

8

BT

EX

and Naphthalene

Volatile O

rganics

Moisture S

et

Sem

ivolatile Organics

Total R


Per- and P


ubstances(P

FA

Ss)

1.4-Dioxane





76_170819

14 0990_MW128_0.0_170819


15 0990_MW128_0.5_170819

Aug 19, 2017 Soil M17-Au26604 X X X

16 0990_MW128_1.0_170819

Aug 19, 2017 Soil M17-Au26605 X X X

17 0990_QCMW190_170819

Aug 19, 2017 Water M17-Au26606 X

18 0990_MW126_11.2_170817

Aug 17, 2017 Soil M17-Au26607 X

19 0990_MW139_0.0_170817

Aug 17, 2017 Soil M17-Au26608 X

20 0990_MW139 Aug 17, 2017 Soil M17-Au26609 X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 16 of 35






Sample Detail

Chloride

HO

LD

Sulphate (as S

O4)

Total A

lkalinity (as CaC

O3)

Alkali M

etals

Metals M

8

BT

EX

and Naphthalene

Volatile O

rganics

Moisture S

et

Sem

ivolatile Organics

Total R


Per- and P


ubstances(P

FA

Ss)

1.4-Dioxane





_0.2_170817

21 0990_MW139_0.5_170817

Aug 17, 2017 Soil M17-Au26610 X

22 0990_MW139_1.0_170817

Aug 17, 2017 Soil M17-Au26611 X

23 0990_QCMW174_170818

Aug 18, 2017 Water M17-Au26612 X

24 0990_MW129_0.7_170818

Aug 18, 2017 Soil M17-Au26613 X

25 0990_QCMW184A_170818

Aug 18, 2017 Soil M17-Au26614 X

26 0990_MW139_10.0_170818

Aug 18, 2017 Soil M17-Au26615 X

27 0990_MW128 Aug 19, 2017 Soil M17-Au26616 X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 17 of 35






Sample Detail

Chloride

HO

LD

Sulphate (as S

O4)

Total A

lkalinity (as CaC

O3)

Alkali M

etals

Metals M

8

BT

EX

and Naphthalene

Volatile O

rganics

Moisture S

et

Sem

ivolatile Organics

Total R


Per- and P


ubstances(P

FA

Ss)

1.4-Dioxane





_0.2_170819

28 0990_MW140_0.0_170819

Aug 19, 2017 Soil M17-Au26617 X

29 0990_MW140_0.2_170819

Aug 19, 2017 Soil M17-Au26618 X

30 0990_MW140_0.5_170819

Aug 19, 2017 Soil M17-Au26619 X

31 0990_MW140_1.0_170819

Aug 19, 2017 Soil M17-Au26620 X

32 0990_QCMW169_170819

Aug 19, 2017 Soil M17-Au26621 X

33 0990_QCMW169A_170819

Aug 19, 2017 Soil M17-Au26622 X

34 0990_MW129 Aug 18, 2017 Soil M17-Au26623 X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 18 of 35






Sample Detail

Chloride

HO

LD

Sulphate (as S

O4)

Total A

lkalinity (as CaC

O3)

Alkali M

etals

Metals M

8

BT

EX

and Naphthalene

Volatile O

rganics

Moisture S

et

Sem

ivolatile Organics

Total R


Per- and P


ubstances(P

FA

Ss)

1.4-Dioxane





_3.8_170818

35 0990_MW129_1.0_170818

Aug 18, 2017 Soil M17-Au26625 X X X

Test Counts 4 17 4 4 4 8 1 3 8 3 1 18 3








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 19 of 35



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 20 of 35




PassLimits

QualifyingCode

Method Blank


TRH C6-C9 mg/kg < 20 20 Pass




Method Blank

BTEX

Benzene mg/kg < 0.1 0.1 Pass

Toluene mg/kg < 0.1 0.1 Pass

Ethylbenzene mg/kg < 0.1 0.1 Pass

m&p-Xylenes mg/kg < 0.2 0.2 Pass

o-Xylene mg/kg < 0.1 0.1 Pass

Xylenes - Total mg/kg < 0.3 0.3 Pass

Method Blank

Volatile Organics

1.1-Dichloroethane mg/kg < 0.5 0.5 Pass

1.1-Dichloroethene mg/kg < 0.5 0.5 Pass

1.1.1-Trichloroethane mg/kg < 0.5 0.5 Pass

1.1.1.2-Tetrachloroethane mg/kg < 0.5 0.5 Pass

1.1.2-Trichloroethane mg/kg < 0.5 0.5 Pass

1.1.2.2-Tetrachloroethane mg/kg < 0.5 0.5 Pass

1.2-Dibromoethane mg/kg < 0.5 0.5 Pass

1.2-Dichlorobenzene mg/kg < 0.5 0.5 Pass

1.2-Dichloroethane mg/kg < 0.5 0.5 Pass

1.2-Dichloropropane mg/kg < 0.5 0.5 Pass

1.2.3-Trichloropropane mg/kg < 0.5 0.5 Pass

1.2.4-Trimethylbenzene mg/kg < 0.5 0.5 Pass


1.3-Dichloropropane mg/kg < 0.5 0.5 Pass

1.3.5-Trimethylbenzene mg/kg < 0.5 0.5 Pass


2-Butanone (MEK) mg/kg < 0.5 0.5 Pass

2-Propanone (Acetone) mg/kg < 0.5 0.5 Pass

4-Chlorotoluene mg/kg < 0.5 0.5 Pass

4-Methyl-2-pentanone (MIBK) mg/kg < 0.5 0.5 Pass

Allyl chloride mg/kg < 0.5 0.5 Pass

Bromobenzene mg/kg < 0.5 0.5 Pass

Bromochloromethane mg/kg < 0.5 0.5 Pass

Bromodichloromethane mg/kg < 0.5 0.5 Pass

Bromoform mg/kg < 0.5 0.5 Pass

Bromomethane mg/kg < 0.5 0.5 Pass

Carbon disulfide mg/kg < 0.5 0.5 Pass

Carbon Tetrachloride mg/kg < 0.5 0.5 Pass

Chlorobenzene mg/kg < 0.5 0.5 Pass

Chloroethane mg/kg < 0.5 0.5 Pass

Chloroform mg/kg < 0.5 0.5 Pass

Chloromethane mg/kg < 0.5 0.5 Pass

cis-1.2-Dichloroethene mg/kg < 0.5 0.5 Pass

cis-1.3-Dichloropropene mg/kg < 0.5 0.5 Pass

Dibromochloromethane mg/kg < 0.5 0.5 Pass

Dibromomethane mg/kg < 0.5 0.5 Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 21 of 35



PassLimits

QualifyingCode

Dichlorodifluoromethane mg/kg < 0.5 0.5 Pass

Iodomethane mg/kg < 0.5 0.5 Pass

Isopropyl benzene (Cumene) mg/kg < 0.5 0.5 Pass

Methylene Chloride mg/kg < 0.5 0.5 Pass

Styrene mg/kg < 0.5 0.5 Pass

Tetrachloroethene mg/kg < 0.5 0.5 Pass

trans-1.2-Dichloroethene mg/kg < 0.5 0.5 Pass

trans-1.3-Dichloropropene mg/kg < 0.5 0.5 Pass

Trichloroethene mg/kg < 0.5 0.5 Pass

Trichlorofluoromethane mg/kg < 0.5 0.5 Pass

Vinyl chloride mg/kg < 0.5 0.5 Pass

Method Blank


Naphthalene mg/kg < 0.5 0.5 Pass


TRH >C10-C16 mg/kg < 50 50 Pass

TRH >C16-C34 mg/kg < 100 100 Pass

TRH >C34-C40 mg/kg < 100 100 Pass

Method Blank


2-Methyl-4.6-dinitrophenol mg/kg < 5 5 Pass

1-Naphthylamine mg/kg < 0.5 0.5 Pass


1.2.3-Trichlorobenzene mg/kg < 0.5 0.5 Pass

1.2.3.4-Tetrachlorobenzene mg/kg < 0.5 0.5 Pass







2-Chloronaphthalene mg/kg < 0.5 0.5 Pass

2-Chlorophenol mg/kg < 0.5 0.5 Pass

2-Methylnaphthalene mg/kg < 0.5 0.5 Pass

2-Methylphenol (o-Cresol) mg/kg < 0.2 0.2 Pass

2-Naphthylamine mg/kg < 0.5 0.5 Pass

2-Nitroaniline mg/kg < 0.5 0.5 Pass

2-Nitrophenol mg/kg < 1 1.0 Pass

2-Picoline mg/kg < 0.5 0.5 Pass

2.3.4.6-Tetrachlorophenol mg/kg < 0.5 0.5 Pass

2.4-Dichlorophenol mg/kg < 0.5 0.5 Pass

2.4-Dimethylphenol mg/kg < 0.5 0.5 Pass

2.4-Dinitrophenol mg/kg < 5 5 Pass

2.4.5-Trichlorophenol mg/kg < 1 1.0 Pass

2.4.6-Trichlorophenol mg/kg < 1 1.0 Pass

2.6-Dichlorophenol mg/kg < 0.5 0.5 Pass

2.6-Dinitrotoluene mg/kg < 0.5 0.5 Pass

3&4-Methylphenol (m&p-Cresol) mg/kg < 0.4 0.4 Pass

3-Methylcholanthrene mg/kg < 0.5 0.5 Pass

3.3'-Dichlorobenzidine mg/kg < 0.5 0.5 Pass

4-Aminobiphenyl mg/kg < 0.5 0.5 Pass

4-Bromophenyl phenyl ether mg/kg < 0.5 0.5 Pass

4-Chloro-3-methylphenol mg/kg < 1 1.0 Pass

4-Chlorophenyl phenyl ether mg/kg < 0.5 0.5 Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 22 of 35



PassLimits

QualifyingCode

4-Nitrophenol mg/kg < 5 5 Pass

4.4'-DDD mg/kg < 0.5 0.5 Pass

4.4'-DDE mg/kg < 0.5 0.5 Pass

4.4'-DDT mg/kg < 0.5 0.5 Pass

7.12-Dimethylbenz(a)anthracene mg/kg < 0.5 0.5 Pass

a-BHC mg/kg < 0.5 0.5 Pass

Acenaphthene mg/kg < 0.5 0.5 Pass

Acenaphthylene mg/kg < 0.5 0.5 Pass

Acetophenone mg/kg < 0.5 0.5 Pass

Aldrin mg/kg < 0.5 0.5 Pass

Aniline mg/kg < 0.5 0.5 Pass

Anthracene mg/kg < 0.5 0.5 Pass

b-BHC mg/kg < 0.5 0.5 Pass

Benz(a)anthracene mg/kg < 0.5 0.5 Pass

Benzo(a)pyrene mg/kg < 0.5 0.5 Pass

Benzo(b&j)fluoranthene mg/kg < 0.5 0.5 Pass

Benzo(g.h.i)perylene mg/kg < 0.5 0.5 Pass

Benzo(k)fluoranthene mg/kg < 0.5 0.5 Pass

Benzyl chloride mg/kg < 0.5 0.5 Pass

Bis(2-chloroethoxy)methane mg/kg < 0.5 0.5 Pass

Bis(2-chloroisopropyl)ether mg/kg < 0.5 0.5 Pass

Bis(2-ethylhexyl)phthalate mg/kg < 0.5 0.5 Pass

Butyl benzyl phthalate mg/kg < 0.5 0.5 Pass

Chrysene mg/kg < 0.5 0.5 Pass

d-BHC mg/kg < 0.5 0.5 Pass

Di-n-butyl phthalate mg/kg < 0.5 0.5 Pass

Di-n-octyl phthalate mg/kg < 0.5 0.5 Pass

Dibenz(a.h)anthracene mg/kg < 0.5 0.5 Pass

Dibenz(a.j)acridine mg/kg < 0.5 0.5 Pass

Dibenzofuran mg/kg < 0.5 0.5 Pass

Dieldrin mg/kg < 0.5 0.5 Pass

Diethyl phthalate mg/kg < 0.5 0.5 Pass

Dimethyl phthalate mg/kg < 0.5 0.5 Pass

Dimethylaminoazobenzene mg/kg < 0.5 0.5 Pass

Diphenylamine mg/kg < 0.5 0.5 Pass

Endosulfan I mg/kg < 0.5 0.5 Pass

Endosulfan II mg/kg < 0.5 0.5 Pass

Endosulfan sulphate mg/kg < 0.5 0.5 Pass

Endrin mg/kg < 0.5 0.5 Pass

Endrin aldehyde mg/kg < 0.5 0.5 Pass

Endrin ketone mg/kg < 0.5 0.5 Pass

Fluoranthene mg/kg < 0.5 0.5 Pass

Fluorene mg/kg < 0.5 0.5 Pass

g-BHC (Lindane) mg/kg < 0.5 0.5 Pass

Heptachlor mg/kg < 0.5 0.5 Pass

Heptachlor epoxide mg/kg < 0.5 0.5 Pass

Hexachlorobenzene mg/kg < 0.5 0.5 Pass

Hexachlorobutadiene mg/kg < 0.5 0.5 Pass

Hexachlorocyclopentadiene mg/kg < 0.5 0.5 Pass

Hexachloroethane mg/kg < 0.5 0.5 Pass

Indeno(1.2.3-cd)pyrene mg/kg < 0.5 0.5 Pass

Methoxychlor mg/kg < 0.5 0.5 Pass

N-Nitrosodibutylamine mg/kg < 0.5 0.5 Pass

N-Nitrosodipropylamine mg/kg < 0.5 0.5 Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 23 of 35



PassLimits

QualifyingCode

N-Nitrosopiperidine mg/kg < 0.5 0.5 Pass

Naphthalene mg/kg < 0.5 0.5 Pass

Nitrobenzene mg/kg < 0.5 0.5 Pass

Pentachlorobenzene mg/kg < 0.5 0.5 Pass

Pentachloronitrobenzene mg/kg < 0.5 0.5 Pass

Pentachlorophenol mg/kg < 1 1.0 Pass

Phenanthrene mg/kg < 0.5 0.5 Pass

Phenol mg/kg < 0.5 0.5 Pass

Pronamide mg/kg < 0.5 0.5 Pass

Pyrene mg/kg < 0.5 0.5 Pass

Trifluralin mg/kg < 0.5 0.5 Pass

Method Blank


Perfluorobutanoic acid (PFBA) ug/kg < 5 5 Pass

Perfluoropentanoic acid (PFPeA) ug/kg < 5 5 Pass

Perfluorohexanoic acid (PFHxA) ug/kg < 5 5 Pass

Perfluoroheptanoic acid (PFHpA) ug/kg < 5 5 Pass

Perfluorooctanoic acid (PFOA) ug/kg < 5 5 Pass

Perfluorononanoic acid (PFNA) ug/kg < 5 5 Pass

Perfluorodecanoic acid (PFDA) ug/kg < 5 5 Pass

Perfluoroundecanoic acid (PFUnA) ug/kg < 5 5 Pass

Perfluorododecanoic acid (PFDoA) ug/kg < 5 5 Pass

Perfluorotridecanoic acid (PFTrDA) ug/kg < 5 5 Pass

Perfluorotetradecanoic acid (PFTeDA) ug/kg < 5 5 Pass

Method Blank


Perfluorooctane sulfonamide (FOSA) ug/kg < 5 5 Pass

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA) ug/kg < 5 5 Pass

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA) ug/kg < 5 5 Pass

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol (N-MeFOSE) ug/kg < 5 5 Pass

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE) ug/kg < 5 5 Pass

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA) ug/kg < 10 10 Pass

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA) ug/kg < 10 10 Pass

Method Blank


Perfluorobutanesulfonic acid (PFBS) ug/kg < 5 5 Pass

Perfluoropentanesulfonic acid (PFPeS) ug/kg < 5 5 Pass

Perfluorohexanesulfonic acid (PFHxS) ug/kg < 5 5 Pass

Perfluoroheptanesulfonic acid (PFHpS) ug/kg < 5 5 Pass

Perfluorooctanesulfonic acid (PFOS) ug/kg < 5 5 Pass

Perfluorodecanesulfonic acid (PFDS) ug/kg < 5 5 Pass

Method Blank


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2 FTS) ug/kg < 5 5 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) ug/kg < 10 10 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) ug/kg < 5 5 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2 FTS) ug/kg < 5 5 Pass

Method Blank

1.4-Dioxane

1.4-Dioxane ug/kg < 10 10 Pass

Method Blank

Heavy Metals

Arsenic mg/kg < 2 2 Pass

Cadmium mg/kg < 0.4 0.4 Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 24 of 35



PassLimits

QualifyingCode

Chromium mg/kg < 5 5 Pass

Copper mg/kg < 5 5 Pass

Lead mg/kg < 5 5 Pass

Mercury mg/kg < 0.1 0.1 Pass

Nickel mg/kg < 5 5 Pass

Zinc mg/kg < 5 5 Pass

LCS - % Recovery


TRH C6-C9 % 106 70-130 Pass

TRH C10-C14 % 78 70-130 Pass

LCS - % Recovery

BTEX

Benzene % 94 70-130 Pass

Toluene % 86 70-130 Pass

Ethylbenzene % 85 70-130 Pass

m&p-Xylenes % 122 70-130 Pass

Xylenes - Total % 116 70-130 Pass

LCS - % Recovery

Volatile Organics

1.1-Dichloroethene % 74 70-130 Pass

1.1.1-Trichloroethane % 111 70-130 Pass

1.2-Dichlorobenzene % 90 70-130 Pass

1.2-Dichloroethane % 102 70-130 Pass

Trichloroethene % 87 70-130 Pass

LCS - % Recovery



TRH C6-C10 % 101 70-130 Pass

TRH >C10-C16 % 79 70-130 Pass

LCS - % Recovery


1.2.4-Trichlorobenzene % 109 70-130 Pass

1.4-Dichlorobenzene % 102 70-130 Pass

2-Chlorophenol % 108 30-130 Pass

2.4-Dinitrotoluene % 86 70-130 Pass

4-Chloro-3-methylphenol % 105 30-130 Pass

Acenaphthene % 97 70-130 Pass

N-Nitrosodipropylamine % 80 70-130 Pass

Phenol % 107 30-130 Pass

Pyrene % 105 70-130 Pass

LCS - % Recovery













LCS - % Recovery



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 25 of 35



PassLimits

QualifyingCode









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery

1.4-Dioxane

1.4-Dioxane % 123 70-130 Pass

LCS - % Recovery

Heavy Metals

Arsenic % 95 70-130 Pass

Cadmium % 96 70-130 Pass

Chromium % 110 70-130 Pass

Copper % 112 70-130 Pass

Lead % 100 70-130 Pass

Mercury % 107 70-130 Pass

Nickel % 109 70-130 Pass

Zinc % 107 70-130 Pass


LimitsPass

LimitsQualifying

Code

Spike - % Recovery













Spike - % Recovery




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 26 of 35



LimitsPass

LimitsQualifying

Code








Spike - % Recovery







Spike - % Recovery






Spike - % Recovery




Spike - % Recovery

BTEX Result 1

Benzene M17-Au30136 NCP % 104 70-130 Pass

Toluene M17-Au30136 NCP % 99 70-130 Pass

Ethylbenzene M17-Au30136 NCP % 89 70-130 Pass

m&p-Xylenes M17-Au30136 NCP % 129 70-130 Pass

o-Xylene M17-Au30136 NCP % 107 70-130 Pass

Xylenes - Total M17-Au30136 NCP % 121 70-130 Pass

Spike - % Recovery

Volatile Organics Result 1

1.1-Dichloroethene M17-Au30136 NCP % 98 70-130 Pass

1.2-Dichlorobenzene M17-Au30136 NCP % 109 70-130 Pass

1.2-Dichloroethane M17-Au30136 NCP % 109 70-130 Pass

Trichloroethene M17-Au30136 NCP % 118 70-130 Pass

Spike - % Recovery




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 27 of 35



LimitsPass

LimitsQualifying

Code

Naphthalene M17-Au30136 NCP % 104 70-130 Pass


TRH >C10-C16 M17-Au29576 NCP % 83 70-130 Pass

Spike - % Recovery

Semivolatile Organics Result 1

1.2.4-Trichlorobenzene M17-Au25089 NCP % 108 70-130 Pass

1.4-Dichlorobenzene M17-Au25089 NCP % 102 70-130 Pass

2.4-Dinitrophenol M17-Au28241 NCP % 59 30-130 Pass

2.4-Dinitrotoluene M17-Au29145 NCP % 93 70-130 Pass

3&4-Methylphenol (m&p-Cresol) M17-Au25281 NCP % 34 30-130 Pass

4-Nitrophenol M17-Au28241 NCP % 31 30-130 Pass

N-Nitrosodipropylamine M17-Au25089 NCP % 72 70-130 Pass

Spike - % Recovery


Arsenic M17-Au26597 CP % 115 70-130 Pass

Cadmium M17-Au26597 CP % 117 70-130 Pass

Chromium M17-Au26597 CP % 85 70-130 Pass

Copper M17-Au26597 CP % 112 70-130 Pass

Lead M17-Au26597 CP % 107 70-130 Pass

Mercury M17-Au26597 CP % 105 70-130 Pass

Nickel M17-Au26597 CP % 111 70-130 Pass

Zinc M17-Au26597 CP % 114 70-130 Pass

Spike - % Recovery

Semivolatile Organics Result 1

2-Methyl-4.6-dinitrophenol M17-Au26601 CP % 72 30-130 Pass

2-Chlorophenol M17-Au26601 CP % 97 30-130 Pass

2-Methylphenol (o-Cresol) M17-Au26601 CP % 84 30-130 Pass

2-Nitrophenol M17-Au26601 CP % 86 30-130 Pass

2.4-Dichlorophenol M17-Au26601 CP % 89 30-130 Pass

2.4-Dimethylphenol M17-Au26601 CP % 103 30-130 Pass

2.4.5-Trichlorophenol M17-Au26601 CP % 120 30-130 Pass

2.4.6-Trichlorophenol M17-Au26601 CP % 76 30-130 Pass

2.6-Dichlorophenol M17-Au26601 CP % 106 30-130 Pass

4-Chloro-3-methylphenol M17-Au26601 CP % 104 30-130 Pass

Acenaphthene M17-Au26601 CP % 81 70-130 Pass

Acenaphthylene M17-Au26601 CP % 106 70-130 Pass

Anthracene M17-Au26601 CP % 92 70-130 Pass

Benz(a)anthracene M17-Au26601 CP % 84 70-130 Pass

Benzo(a)pyrene M17-Au26601 CP % 93 70-130 Pass

Benzo(b&j)fluoranthene M17-Au26601 CP % 111 70-130 Pass

Benzo(g.h.i)perylene M17-Au26601 CP % 65 70-130 Fail Q08

Benzo(k)fluoranthene M17-Au26601 CP % 86 70-130 Pass

Chrysene M17-Au26601 CP % 75 70-130 Pass

Dibenz(a.h)anthracene M17-Au26601 CP % 72 70-130 Pass

Fluoranthene M17-Au26601 CP % 98 70-130 Pass

Fluorene M17-Au26601 CP % 80 70-130 Pass

Indeno(1.2.3-cd)pyrene M17-Au26601 CP % 81 70-130 Pass

Naphthalene M17-Au26601 CP % 88 70-130 Pass

Pentachlorophenol M17-Au26601 CP % 33 30-130 Pass

Phenanthrene M17-Au26601 CP % 91 70-130 Pass

Phenol M17-Au26601 CP % 93 30-130 Pass

Pyrene M17-Au26601 CP % 96 70-130 Pass

Spike - % Recovery




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 28 of 35



LimitsPass

LimitsQualifying

Code


Spike - % Recovery

1.4-Dioxane Result 1

1.4-Dioxane M17-Au26601 CP % 121 70-130 Pass


LimitsPass

LimitsQualifying

Code

Duplicate


% Moisture M17-Au26726 NCP % 27 27 1.0 30% Pass

Duplicate


TRH C6-C9 M17-Au25140 NCP mg/kg < 20 < 20 <1 30% Pass




Duplicate

BTEX Result 1 Result 2 RPD

Benzene M17-Au25140 NCP mg/kg < 0.1 < 0.1 <1 30% Pass

Toluene M17-Au25140 NCP mg/kg < 0.1 < 0.1 <1 30% Pass

Ethylbenzene M17-Au25140 NCP mg/kg < 0.1 < 0.1 <1 30% Pass

m&p-Xylenes M17-Au25140 NCP mg/kg < 0.2 < 0.2 <1 30% Pass

o-Xylene M17-Au25140 NCP mg/kg < 0.1 < 0.1 <1 30% Pass

Xylenes - Total M17-Au25140 NCP mg/kg < 0.3 < 0.3 <1 30% Pass

Duplicate

Volatile Organics Result 1 Result 2 RPD

1.1-Dichloroethane M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

1.1-Dichloroethene M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

1.1.1-Trichloroethane M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

1.1.1.2-Tetrachloroethane M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

1.1.2-Trichloroethane M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

1.1.2.2-Tetrachloroethane M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

1.2-Dibromoethane M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

1.2-Dichlorobenzene M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

1.2-Dichloroethane M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

1.2-Dichloropropane M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

1.2.3-Trichloropropane M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

1.2.4-Trimethylbenzene M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass


1.3-Dichloropropane M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

1.3.5-Trimethylbenzene M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass


2-Butanone (MEK) M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

2-Propanone (Acetone) M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

4-Chlorotoluene M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

4-Methyl-2-pentanone (MIBK) M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Allyl chloride M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Bromobenzene M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Bromochloromethane M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Bromodichloromethane M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Bromoform M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Bromomethane M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Carbon disulfide M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Carbon Tetrachloride M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Chlorobenzene M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 29 of 35


Duplicate

Volatile Organics Result 1 Result 2 RPD

Chloroethane M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Chloroform M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Chloromethane M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

cis-1.2-Dichloroethene M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

cis-1.3-Dichloropropene M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Dibromochloromethane M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Dibromomethane M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Dichlorodifluoromethane M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Iodomethane M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Isopropyl benzene (Cumene) M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Methylene Chloride M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Styrene M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Tetrachloroethene M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

trans-1.2-Dichloroethene M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

trans-1.3-Dichloropropene M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Trichloroethene M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Trichlorofluoromethane M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Vinyl chloride M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Duplicate


Naphthalene M17-Au25140 NCP mg/kg < 0.5 < 0.5 <1 30% Pass


TRH >C10-C16 M17-Au24954 NCP mg/kg < 50 < 50 <1 30% Pass



Duplicate

Semivolatile Organics Result 1 Result 2 RPD

2-Methyl-4.6-dinitrophenol M17-Au25088 NCP mg/kg < 5 < 5 <1 30% Pass

1-Chloronaphthalene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

1-Naphthylamine M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass


1.2.3-Trichlorobenzene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

1.2.3.4-Tetrachlorobenzene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass







2-Chloronaphthalene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

2-Chlorophenol M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

2-Methylnaphthalene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

2-Methylphenol (o-Cresol) M17-Au25088 NCP mg/kg < 0.2 < 0.2 <1 30% Pass

2-Naphthylamine M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

2-Nitroaniline M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

2-Nitrophenol M17-Au25088 NCP mg/kg < 1 < 1 <1 30% Pass

2-Picoline M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

2.3.4.6-Tetrachlorophenol M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

2.4-Dichlorophenol M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

2.4-Dimethylphenol M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

2.4-Dinitrophenol M17-Au25088 NCP mg/kg < 5 < 5 <1 30% Pass

2.4-Dinitrotoluene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

2.4.5-Trichlorophenol M17-Au25088 NCP mg/kg < 1 < 1 <1 30% Pass

2.4.6-Trichlorophenol M17-Au25088 NCP mg/kg < 1 < 1 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 30 of 35


Duplicate


2.6-Dichlorophenol M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

2.6-Dinitrotoluene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

3&4-Methylphenol (m&p-Cresol) M17-Au25088 NCP mg/kg < 0.4 < 0.4 <1 30% Pass

3-Methylcholanthrene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

3.3'-Dichlorobenzidine M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

4-Aminobiphenyl M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

4-Bromophenyl phenyl ether M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

4-Chloro-3-methylphenol M17-Au25088 NCP mg/kg < 1 < 1 <1 30% Pass

4-Chlorophenyl phenyl ether M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

4-Nitrophenol M17-Au25088 NCP mg/kg < 5 < 5 <1 30% Pass

4.4'-DDD M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

4.4'-DDE M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

4.4'-DDT M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

7.12-Dimethylbenz(a)anthracene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

a-BHC M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Acenaphthene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Acenaphthylene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Acetophenone M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Aldrin M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Aniline M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Anthracene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

b-BHC M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Benz(a)anthracene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Benzo(a)pyrene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Benzo(b&j)fluoranthene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Benzo(g.h.i)perylene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Benzo(k)fluoranthene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Benzyl chloride M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Bis(2-chloroethoxy)methane M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Bis(2-chloroisopropyl)ether M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Bis(2-ethylhexyl)phthalate M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Butyl benzyl phthalate M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Chrysene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

d-BHC M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Di-n-butyl phthalate M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Di-n-octyl phthalate M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Dibenz(a.h)anthracene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Dibenz(a.j)acridine M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Dibenzofuran M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Dieldrin M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Diethyl phthalate M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Dimethyl phthalate M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Dimethylaminoazobenzene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Diphenylamine M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Endosulfan I M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Endosulfan II M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Endosulfan sulphate M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Endrin M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Endrin aldehyde M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Endrin ketone M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Fluoranthene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Fluorene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

g-BHC (Lindane) M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Heptachlor M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 31 of 35


Duplicate


Heptachlor epoxide M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Hexachlorobenzene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Hexachlorobutadiene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Hexachlorocyclopentadiene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Hexachloroethane M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Indeno(1.2.3-cd)pyrene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Methoxychlor M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

N-Nitrosodibutylamine M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

N-Nitrosodipropylamine M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

N-Nitrosopiperidine M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Naphthalene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Nitrobenzene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Pentachlorobenzene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Pentachloronitrobenzene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Pentachlorophenol M17-Au25088 NCP mg/kg < 1 < 1 <1 30% Pass

Phenanthrene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Phenol M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Pronamide M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Pyrene M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Trifluralin M17-Au25088 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Duplicate


Arsenic M17-Au26597 CP mg/kg 15 14 11 30% Pass

Cadmium M17-Au26597 CP mg/kg < 0.4 < 0.4 <1 30% Pass

Chromium M17-Au26597 CP mg/kg 140 120 13 30% Pass

Copper M17-Au26597 CP mg/kg 8.2 7.2 13 30% Pass

Lead M17-Au26597 CP mg/kg 20 18 12 30% Pass

Mercury M17-Au26597 CP mg/kg < 0.1 < 0.1 <1 30% Pass

Nickel M17-Au26597 CP mg/kg < 5 < 5 <1 30% Pass

Zinc M17-Au26597 CP mg/kg < 5 < 5 <1 30% Pass

Duplicate


Perfluorobutanoic acid (PFBA) M17-Au26603 CP ug/kg < 5 < 5 <1 30% Pass

Perfluoropentanoic acid (PFPeA) M17-Au26603 CP ug/kg < 5 < 5 <1 30% Pass

Perfluorohexanoic acid (PFHxA) M17-Au26603 CP ug/kg 20 21 4.0 30% Pass

Perfluoroheptanoic acid (PFHpA) M17-Au26603 CP ug/kg < 5 < 5 <1 30% Pass

Perfluorooctanoic acid (PFOA) M17-Au26603 CP ug/kg 6.4 6.6 3.0 30% Pass

Perfluorononanoic acid (PFNA) M17-Au26603 CP ug/kg < 5 < 5 <1 30% Pass

Perfluorodecanoic acid (PFDA) M17-Au26603 CP ug/kg < 5 < 5 <1 30% Pass

Perfluoroundecanoic acid (PFUnA) M17-Au26603 CP ug/kg < 5 < 5 <1 30% Pass

Perfluorododecanoic acid (PFDoA) M17-Au26603 CP ug/kg < 5 < 5 <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) M17-Au26603 CP ug/kg < 5 < 5 <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) M17-Au26603 CP ug/kg < 5 < 5 <1 30% Pass

Duplicate


Perfluorooctane sulfonamide(FOSA) M17-Au26603 CP ug/kg < 5 < 5 <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) M17-Au26603 CP ug/kg < 5 < 5 <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) M17-Au26603 CP ug/kg < 5 < 5 <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) M17-Au26603 CP ug/kg < 5 < 5 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 32 of 35


Duplicate


2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) M17-Au26603 CP ug/kg < 5 < 5 <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-Au26603 CP ug/kg < 10 < 10 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-Au26603 CP ug/kg < 10 < 10 <1 30% Pass

Duplicate


Perfluorobutanesulfonic acid(PFBS) M17-Au26603 CP ug/kg 21 24 11 30% Pass

Perfluoropentanesulfonic acid(PFPeS) M17-Au26603 CP ug/kg 17 17 <1 30% Pass

Perfluorohexanesulfonic acid(PFHxS) M17-Au26603 CP ug/kg 160 160 5.0 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) M17-Au26603 CP ug/kg < 5 < 5 <1 30% Pass

Perfluorooctanesulfonic acid(PFOS) M17-Au26603 CP ug/kg 23 23 <1 30% Pass

Perfluorodecanesulfonic acid(PFDS) M17-Au26603 CP ug/kg < 5 < 5 <1 30% Pass

Duplicate


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-Au26603 CP ug/kg < 5 < 5 <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-Au26603 CP ug/kg < 10 < 10 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-Au26603 CP ug/kg < 5 < 5 <1 30% Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) M17-Au26603 CP ug/kg < 5 < 5 <1 30% Pass

Duplicate

1.4-Dioxane Result 1 Result 2 RPD

1.4-Dioxane M17-Au26603 CP ug/kg < 10 < 10 <1 30% Pass

Duplicate


Perfluorobutanoic acid (PFBA) M17-Au26604 CP ug/kg < 5 < 5 <1 30% Pass

Perfluoropentanoic acid (PFPeA) M17-Au26604 CP ug/kg < 5 < 5 <1 30% Pass

Perfluorohexanoic acid (PFHxA) M17-Au26604 CP ug/kg < 5 < 5 <1 30% Pass

Perfluoroheptanoic acid (PFHpA) M17-Au26604 CP ug/kg < 5 < 5 <1 30% Pass

Perfluorooctanoic acid (PFOA) M17-Au26604 CP ug/kg < 5 < 5 <1 30% Pass

Perfluorononanoic acid (PFNA) M17-Au26604 CP ug/kg < 5 < 5 <1 30% Pass

Perfluorodecanoic acid (PFDA) M17-Au26604 CP ug/kg < 5 < 5 <1 30% Pass

Perfluoroundecanoic acid (PFUnA) M17-Au26604 CP ug/kg < 5 < 5 <1 30% Pass

Perfluorododecanoic acid (PFDoA) M17-Au26604 CP ug/kg < 5 < 5 <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) M17-Au26604 CP ug/kg < 5 < 5 <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) M17-Au26604 CP ug/kg < 5 < 5 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 33 of 35


Duplicate


Perfluorooctane sulfonamide(FOSA) M17-Au26604 CP ug/kg < 5 < 5 <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) M17-Au26604 CP ug/kg < 5 < 5 <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) M17-Au26604 CP ug/kg < 5 < 5 <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) M17-Au26604 CP ug/kg < 5 < 5 <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) M17-Au26604 CP ug/kg < 5 < 5 <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-Au26604 CP ug/kg < 10 < 10 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-Au26604 CP ug/kg < 10 < 10 <1 30% Pass

Duplicate


Perfluorobutanesulfonic acid(PFBS) M17-Au26604 CP ug/kg < 5 < 5 <1 30% Pass

Perfluoropentanesulfonic acid(PFPeS) M17-Au26604 CP ug/kg < 5 < 5 <1 30% Pass

Perfluorohexanesulfonic acid(PFHxS) M17-Au26604 CP ug/kg < 5 < 5 <1 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) M17-Au26604 CP ug/kg < 5 < 5 <1 30% Pass

Perfluorooctanesulfonic acid(PFOS) M17-Au26604 CP ug/kg 53 50 6.0 30% Pass

Perfluorodecanesulfonic acid(PFDS) M17-Au26604 CP ug/kg < 5 < 5 <1 30% Pass

Duplicate


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-Au26604 CP ug/kg < 5 < 5 <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-Au26604 CP ug/kg < 10 < 10 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-Au26604 CP ug/kg < 5 < 5 <1 30% Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) M17-Au26604 CP ug/kg < 5 < 5 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 34 of 35


Comments









Code Description

N01F2 is determined by arithmetically subtracting the "naphthalene" value from the ">C10-C16" value. The naphthalene value used in this calculation is obtained from volatiles(Purge & Trap analysis).

N02

Where we have reported both volatile (P&T GCMS) and semivolatile (GCMS) naphthalene data, results may not be identical. Provided correct sample handling protocols havebeen followed, any observed differences in results are likely to be due to procedural differences within each methodology. Results determined by both techniques have passedall QAQC acceptance criteria, and are entirely technically valid.

N04F1 is determined by arithmetically subtracting the "Total BTEX" value from the "C6-C10" value. The "Total BTEX" value is obtained by summing the concentrations of BTEXanalytes. The "C6-C10" value is obtained by quantitating against a standard of mixed aromatic/aliphatic analytes.

N07Please note:- These two PAH isomers closely co-elute using the most contemporary analytical methods and both the reported concentration (and the TEQ) apply specifically tothe total of the two co-eluting PAHs

N09 Quantification of linear and branched isomers has been conducted as a single total response using the relative response factor for the corresponding linear/branched standard.

N11



Authorised By



Alex Petridis Senior Analyst-Organic (VIC)

Harry Bacalis Senior Analyst-Volatile (VIC)



Joseph Edouard Senior Analyst-Organic (VIC)

Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 35 of 35






Abbotsford

VIC 3067


Report 559812-W





0990_PB028_1_170817

0990_PB028_2_170817

0990_QCMW167_170817







Perfluoropentanoic acid (PFPeA)N11 0.01 ug/L N090.03 < 0.01 < 0.01 < 0.01

Perfluorohexanoic acid (PFHxA)N11 0.01 ug/L N090.08 < 0.01 < 0.01 < 0.01

Perfluoroheptanoic acid (PFHpA)N11 0.01 ug/L N090.02 < 0.01 < 0.01 < 0.01

Perfluorooctanoic acid (PFOA)N11 0.01 ug/L N090.03 < 0.01 < 0.01 < 0.01







13C4-PFBA (surr.) 1 % 104 106 107 86

13C5-PFPeA (surr.) 1 % 78 84 83 66

13C5-PFHxA (surr.) 1 % 107 118 118 84

13C4-PFHpA (surr.) 1 % 116 126 123 82

13C8-PFOA (surr.) 1 % 112 123 124 87

13C5-PFNA (surr.) 1 % 101 103 97 82

13C6-PFDA (surr.) 1 % 59 70 68 65

13C2-PFUnDA (surr.) 1 % 69 70 73 63

13C2-PFDoDA (surr.) 1 % 64 66 69 56

13C2-PFTeDA (surr.) 1 % 66 68 74 48









13C8-FOSA (surr.) 1 % 35 46 62 36

D3-N-MeFOSA (surr.) 1 % INT 10 12 INT



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 22





0990_PB028_1_170817

0990_PB028_2_170817

0990_QCMW167_170817






D5-N-EtFOSA (surr.) 1 % INT INT 11 INT

D7-N-MeFOSE (surr.) 1 % INT 17 19 13

D9-N-EtFOSE (surr.) 1 % INT 17 19 13

D5-N-EtFOSAA (surr.) 1 % 13 10 10 20

D3-N-MeFOSAA (surr.) 1 % 16 13 13 25


Perfluorobutanesulfonic acid (PFBS)N11 0.01 ug/L 0.08 < 0.01 < 0.01 < 0.01

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L N090.07 < 0.01 < 0.01 < 0.01

Perfluorohexanesulfonic acid (PFHxS)N11 0.01 ug/L N090.63 < 0.01 < 0.01 < 0.01


Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N090.81 < 0.01 < 0.01 < 0.01


13C3-PFBS (surr.) 1 % 97 102 103 104

18O2-PFHxS (surr.) 1 % 89 117 120 121

13C8-PFOS (surr.) 1 % 78 100 100 114






13C2-4:2 FTS (surr.) 1 % 121 124 122 132

13C2-6:2 FTS (surr.) 1 % 115 124 113 126

13C2-8:2 FTS (surr.) 1 % 41 48 48 58

PFASs Summations

Sum (PFHxS + PFOS) 0.01 ug/L 1.44 < 0.01 < 0.01 < 0.01

Sum of US EPA PFAS (PFOS + PFOA) 0.01 ug/L 0.84 < 0.01 < 0.01 < 0.01

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 0.01 ug/L 1.47 < 0.01 < 0.01 < 0.01

Sum of WA DER PFAS (n=10) 0.05 ug/L 1.68 < 0.05 < 0.05 < 0.05

Sum of PFASs (n=28) 0.1 ug/L 1.83 < 0.1 < 0.1 < 0.1

Chloride 1 mg/L 11 13 15 -

Sulphate (as SO4) 5 mg/L < 5 < 5 < 5 -


Total Alkalinity (as CaCO3) 20 mg/L 480 570 500 -

Alkali Metals

Calcium 0.5 mg/L 38 34 41 -

Magnesium 0.5 mg/L 32 44 47 -

Potassium 0.5 mg/L 7.2 2.0 1.8 -

Sodium 0.5 mg/L 56 46 36 -



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 22



0990_PB29_170818

0990_QCMW185_170818

0990_QCMW168_170818







Perfluoropentanoic acid (PFPeA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

Perfluorohexanoic acid (PFHxA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

Perfluoroheptanoic acid (PFHpA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

Perfluorooctanoic acid (PFOA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01







13C4-PFBA (surr.) 1 % 108 92 40 54

13C5-PFPeA (surr.) 1 % 85 77 30 40

13C5-PFHxA (surr.) 1 % 115 106 38 50

13C4-PFHpA (surr.) 1 % 117 118 44 50

13C8-PFOA (surr.) 1 % 115 118 60 55

13C5-PFNA (surr.) 1 % 103 108 61 53

13C6-PFDA (surr.) 1 % 77 74 57 42

13C2-PFUnDA (surr.) 1 % 76 69 66 48

13C2-PFDoDA (surr.) 1 % 63 66 64 49

13C2-PFTeDA (surr.) 1 % 52 66 62 42









13C8-FOSA (surr.) 1 % 31 65 17 20

D3-N-MeFOSA (surr.) 1 % INT 15 INT INT

D5-N-EtFOSA (surr.) 1 % INT 13 INT INT

D7-N-MeFOSE (surr.) 1 % 12 24 INT INT

D9-N-EtFOSE (surr.) 1 % 12 23 INT INT

D5-N-EtFOSAA (surr.) 1 % 22 11 13 11

D3-N-MeFOSAA (surr.) 1 % 31 13 18 13


Perfluorobutanesulfonic acid (PFBS)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01


Perfluorohexanesulfonic acid (PFHxS)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01


Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01


13C3-PFBS (surr.) 1 % 102 104 100 99

18O2-PFHxS (surr.) 1 % 120 122 118 114

13C8-PFOS (surr.) 1 % 122 112 123 105



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 22



0990_PB29_170818

0990_QCMW185_170818

0990_QCMW168_170818










13C2-4:2 FTS (surr.) 1 % 126 114 128 115

13C2-6:2 FTS (surr.) 1 % 121 112 132 111

13C2-8:2 FTS (surr.) 1 % 63 51 72 59

PFASs Summations

Sum (PFHxS + PFOS) 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

Sum of US EPA PFAS (PFOS + PFOA) 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

Sum of WA DER PFAS (n=10) 0.05 ug/L < 0.05 < 0.05 < 0.05 < 0.05

Sum of PFASs (n=28) 0.1 ug/L < 0.1 < 0.1 < 0.1 < 0.1

Chloride 1 mg/L - 13 - -

Sulphate (as SO4) 5 mg/L - < 5 - -


Total Alkalinity (as CaCO3) 20 mg/L - 390 - -

Alkali Metals

Calcium 0.5 mg/L - 90 - -

Magnesium 0.5 mg/L - 37 - -

Potassium 0.5 mg/L - 2.8 - -

Sodium 0.5 mg/L - 7.5 - -


0990_QCMW190_170819

















13C4-PFBA (surr.) 1 % 54 71

13C5-PFPeA (surr.) 1 % 42 60

13C5-PFHxA (surr.) 1 % 51 80

13C4-PFHpA (surr.) 1 % 51 82



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 22



0990_QCMW190_170819






13C8-PFOA (surr.) 1 % 53 84

13C5-PFNA (surr.) 1 % 54 76

13C6-PFDA (surr.) 1 % 47 60

13C2-PFUnDA (surr.) 1 % 55 65

13C2-PFDoDA (surr.) 1 % 55 56

13C2-PFTeDA (surr.) 1 % 52 45









13C8-FOSA (surr.) 1 % 24 54

D3-N-MeFOSA (surr.) 1 % INT 11


D7-N-MeFOSE (surr.) 1 % INT 20

D9-N-EtFOSE (surr.) 1 % INT 19










13C3-PFBS (surr.) 1 % 100 101

18O2-PFHxS (surr.) 1 % 117 117

13C8-PFOS (surr.) 1 % 107 121






13C2-4:2 FTS (surr.) 1 % 112 110

13C2-6:2 FTS (surr.) 1 % 111 112

13C2-8:2 FTS (surr.) 1 % 57 64



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 22



0990_QCMW190_170819





PFASs Summations





Sum of PFASs (n=28) 0.1 ug/L < 0.1 < 0.1



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 22
























ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 22






Sample Detail

Chloride

HO

LD

Sulphate (as S

O4)

Total A

lkalinity (as CaC

O3)

Alkali M

etals

Metals M

8

BT

EX

and Naphthalene

Volatile O

rganics

Moisture S

et

Sem

ivolatile Organics

Total R


Per- and P


ubstances(P

FA

Ss)

1.4-Dioxane





External Laboratory


Matrix LAB ID

1 0990_PB027_170817


2 0990_PB028_1_170817


3 0990_PB028_2_170817


4 0990_QCMW167_170817

Aug 17, 2017 Water M17-Au26593 X

5 0990_QCMW183_170817

Aug 17, 2017 Water M17-Au26594 X

6 0990_PB29_1 Aug 18, 2017 Water M17-Au26595 X X X X X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 22






Sample Detail

Chloride

HO

LD

Sulphate (as S

O4)

Total A

lkalinity (as CaC

O3)

Alkali M

etals

Metals M

8

BT

EX

and Naphthalene

Volatile O

rganics

Moisture S

et

Sem

ivolatile Organics

Total R


Per- and P


ubstances(P

FA

Ss)

1.4-Dioxane





70818

7 0990_MW129_0.1_170818

Aug 18, 2017 Soil M17-Au26596 X X X

8 0990_MW129_0.5_170818

Aug 18, 2017 Soil M17-Au26597 X X X X X X X X

9 0990_QCMW185_170818

Aug 18, 2017 Water M17-Au26598 X

10 0990_QCMW184_170818

Aug 18, 2017 Soil M17-Au26599 X X X

11 0990_QCMW168_170818

Aug 18, 2017 Water M17-Au26600 X

12 0990_QCMW175_170819


13 0990_QCMW1 Aug 19, 2017 Water M17-Au26602 X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 22






Sample Detail

Chloride

HO

LD

Sulphate (as S

O4)

Total A

lkalinity (as CaC

O3)

Alkali M

etals

Metals M

8

BT

EX

and Naphthalene

Volatile O

rganics

Moisture S

et

Sem

ivolatile Organics

Total R


Per- and P


ubstances(P

FA

Ss)

1.4-Dioxane





76_170819

14 0990_MW128_0.0_170819


15 0990_MW128_0.5_170819

Aug 19, 2017 Soil M17-Au26604 X X X

16 0990_MW128_1.0_170819

Aug 19, 2017 Soil M17-Au26605 X X X

17 0990_QCMW190_170819

Aug 19, 2017 Water M17-Au26606 X

18 0990_MW126_11.2_170817

Aug 17, 2017 Soil M17-Au26607 X

19 0990_MW139_0.0_170817

Aug 17, 2017 Soil M17-Au26608 X

20 0990_MW139 Aug 17, 2017 Soil M17-Au26609 X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 22






Sample Detail

Chloride

HO

LD

Sulphate (as S

O4)

Total A

lkalinity (as CaC

O3)

Alkali M

etals

Metals M

8

BT

EX

and Naphthalene

Volatile O

rganics

Moisture S

et

Sem

ivolatile Organics

Total R


Per- and P


ubstances(P

FA

Ss)

1.4-Dioxane





_0.2_170817

21 0990_MW139_0.5_170817

Aug 17, 2017 Soil M17-Au26610 X

22 0990_MW139_1.0_170817

Aug 17, 2017 Soil M17-Au26611 X

23 0990_QCMW174_170818

Aug 18, 2017 Water M17-Au26612 X

24 0990_MW129_0.7_170818

Aug 18, 2017 Soil M17-Au26613 X

25 0990_QCMW184A_170818

Aug 18, 2017 Soil M17-Au26614 X

26 0990_MW139_10.0_170818

Aug 18, 2017 Soil M17-Au26615 X

27 0990_MW128 Aug 19, 2017 Soil M17-Au26616 X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 22






Sample Detail

Chloride

HO

LD

Sulphate (as S

O4)

Total A

lkalinity (as CaC

O3)

Alkali M

etals

Metals M

8

BT

EX

and Naphthalene

Volatile O

rganics

Moisture S

et

Sem

ivolatile Organics

Total R


Per- and P


ubstances(P

FA

Ss)

1.4-Dioxane





_0.2_170819

28 0990_MW140_0.0_170819

Aug 19, 2017 Soil M17-Au26617 X

29 0990_MW140_0.2_170819

Aug 19, 2017 Soil M17-Au26618 X

30 0990_MW140_0.5_170819

Aug 19, 2017 Soil M17-Au26619 X

31 0990_MW140_1.0_170819

Aug 19, 2017 Soil M17-Au26620 X

32 0990_QCMW169_170819

Aug 19, 2017 Soil M17-Au26621 X

33 0990_QCMW169A_170819

Aug 19, 2017 Soil M17-Au26622 X

34 0990_MW129 Aug 18, 2017 Soil M17-Au26623 X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 12 of 22






Sample Detail

Chloride

HO

LD

Sulphate (as S

O4)

Total A

lkalinity (as CaC

O3)

Alkali M

etals

Metals M

8

BT

EX

and Naphthalene

Volatile O

rganics

Moisture S

et

Sem

ivolatile Organics

Total R


Per- and P


ubstances(P

FA

Ss)

1.4-Dioxane





_3.8_170818

35 0990_MW129_1.0_170818

Aug 18, 2017 Soil M17-Au26625 X X X

Test Counts 4 17 4 4 4 8 1 3 8 3 1 18 3








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 13 of 22



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 14 of 22




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank



Method Blank



Method Blank

Alkali Metals





LCS - % Recovery





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 15 of 22



PassLimits

QualifyingCode











LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery



LCS - % Recovery



LCS - % Recovery

Alkali Metals






LimitsPass

LimitsQualifying

Code

Spike - % Recovery

Result 1



Spike - % Recovery


Calcium M17-Au27410 NCP % 152 70-130 Fail Q08



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 16 of 22



LimitsPass

LimitsQualifying

Code

Magnesium M17-Au27410 NCP % 139 70-130 Fail Q08



Spike - % Recovery













Spike - % Recovery









Spike - % Recovery








Spike - % Recovery







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 17 of 22



LimitsPass

LimitsQualifying

Code


Spike - % Recovery













Spike - % Recovery









Spike - % Recovery








Spike - % Recovery








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 18 of 22



LimitsPass

LimitsQualifying

Code

Duplicate



Perfluoropentanoic acid (PFPeA) M17-Au26590 CP ug/L 0.03 0.03 4.0 30% Pass

Perfluorohexanoic acid (PFHxA) M17-Au26590 CP ug/L 0.08 0.09 <1 30% Pass

Perfluoroheptanoic acid (PFHpA) M17-Au26590 CP ug/L 0.02 0.01 2.0 30% Pass

Perfluorooctanoic acid (PFOA) M17-Au26590 CP ug/L 0.03 0.03 6.0 30% Pass







Duplicate









Duplicate


Perfluorobutanesulfonic acid(PFBS) M17-Au26590 CP ug/L 0.08 0.08 1.0 30% Pass

Perfluoropentanesulfonic acid(PFPeS) M17-Au26590 CP ug/L 0.07 0.07 2.0 30% Pass

Perfluorohexanesulfonic acid(PFHxS) M17-Au26590 CP ug/L 0.63 0.64 2.0 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) M17-Au26590 CP ug/L 0.08 0.08 4.0 30% Pass

Perfluorooctanesulfonic acid(PFOS) M17-Au26590 CP ug/L 0.81 0.76 6.0 30% Pass


Duplicate








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 19 of 22


Duplicate



Sulphate (as SO4) M17-Au27408 NCP mg/L 1900 1800 7.0 30% Pass

Duplicate


Total Alkalinity (as CaCO3) P17-Au26801 NCP mg/L 61 63 3.0 30% Pass

Duplicate




Potassium M17-Au27410 NCP mg/L 720 770 6.0 30% Pass

Sodium M17-Au27410 NCP mg/L 360 380 6.0 30% Pass

Duplicate













Duplicate









Duplicate










ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 20 of 22


Duplicate








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 21 of 22


Comments










N11



Authorised By





Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 22 of 22






Abbotsford

VIC 3067


Report 559812-W-V2





Sample Matrix Water
















13C4-PFBA (surr.) 1 % 104


13C5-PFHxA (surr.) 1 % 107

13C4-PFHpA (surr.) 1 % 116

13C8-PFOA (surr.) 1 % 112

13C5-PFNA (surr.) 1 % 101

13C6-PFDA (surr.) 1 % 59












13C8-FOSA (surr.) 1 % 35


First Reported: Sep 01, 2017



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 13





Sample Matrix Water

















13C3-PFBS (surr.) 1 % 97


13C8-PFOS (surr.) 1 % 78






13C2-4:2 FTS (surr.) 1 % 121

13C2-6:2 FTS (surr.) 1 % 115

13C2-8:2 FTS (surr.) 1 % 41

PFASs Summations






Chloride 1 mg/L 11




Alkali Metals

Calcium 0.5 mg/L 38



Sodium 0.5 mg/L 56




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 13

























ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 13



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.


















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 13




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank



Method Blank



Method Blank

Alkali Metals





LCS - % Recovery






ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 13



PassLimits

QualifyingCode











LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery



LCS - % Recovery



LCS - % Recovery

Alkali Metals






LimitsPass

LimitsQualifying

Code

Spike - % Recovery










ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 13



LimitsPass

LimitsQualifying

Code







Spike - % Recovery









Spike - % Recovery








Spike - % Recovery






Spike - % Recovery

Result 1



Spike - % Recovery








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 13



LimitsPass

LimitsQualifying

Code


Spike - % Recovery













Spike - % Recovery









Spike - % Recovery








Spike - % Recovery






Spike - % Recovery




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 13



LimitsPass

LimitsQualifying

Code













Spike - % Recovery









Spike - % Recovery








Spike - % Recovery









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 13



LimitsPass

LimitsQualifying

Code

Duplicate













Duplicate









Duplicate








Duplicate









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 13


Duplicate




Duplicate



Duplicate






Duplicate













Duplicate









Duplicate











ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 13


Duplicate









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 12 of 13


Comments










N11



Authorised By





Glenn Jackson








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 13 of 13






Abbotsford

VIC 3067


Report 559812-W-V3





0990_PB028_2_170817

















13C4-PFBA (surr.) 1 % 106 107

13C5-PFPeA (surr.) 1 % 84 83

13C5-PFHxA (surr.) 1 % 118 118

13C4-PFHpA (surr.) 1 % 126 123

13C8-PFOA (surr.) 1 % 123 124

13C5-PFNA (surr.) 1 % 103 97

13C6-PFDA (surr.) 1 % 70 68

13C2-PFUnDA (surr.) 1 % 70 73

13C2-PFDoDA (surr.) 1 % 66 69

13C2-PFTeDA (surr.) 1 % 68 74









13C8-FOSA (surr.) 1 % 46 62





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 14





0990_PB028_2_170817


















13C3-PFBS (surr.) 1 % 102 103

18O2-PFHxS (surr.) 1 % 117 120

13C8-PFOS (surr.) 1 % 100 100






13C2-4:2 FTS (surr.) 1 % 124 122

13C2-6:2 FTS (surr.) 1 % 124 113

13C2-8:2 FTS (surr.) 1 % 48 48

PFASs Summations





Sum of PFASs (n=28) 0.1 ug/L < 0.1 < 0.1

Chloride 1 mg/L 13 15



Total Alkalinity (as CaCO3) 20 mg/L 570 500

Alkali Metals

Calcium 0.5 mg/L 34 41

Magnesium 0.5 mg/L 44 47

Potassium 0.5 mg/L 2.0 1.8





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 14

























ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 14



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.


















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 14




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank



Method Blank



Method Blank

Alkali Metals





LCS - % Recovery






ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 14



PassLimits

QualifyingCode











LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery



LCS - % Recovery



LCS - % Recovery

Alkali Metals






LimitsPass

LimitsQualifying

Code

Spike - % Recovery










ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 14



LimitsPass

LimitsQualifying

Code







Spike - % Recovery









Spike - % Recovery








Spike - % Recovery






Spike - % Recovery

Result 1



Spike - % Recovery








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 14



LimitsPass

LimitsQualifying

Code


Spike - % Recovery

Result 1



Spike - % Recovery






Spike - % Recovery













Spike - % Recovery









Spike - % Recovery








Spike - % Recovery




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 14



LimitsPass

LimitsQualifying

Code






Spike - % Recovery













Spike - % Recovery









Spike - % Recovery








Spike - % Recovery





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 14



LimitsPass

LimitsQualifying

Code






LimitsPass

LimitsQualifying

Code

Duplicate













Duplicate









Duplicate











ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 14


Duplicate






Duplicate




Duplicate



Duplicate






Duplicate













Duplicate












ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 14


Duplicate








Duplicate






Duplicate


Chloride M17-Au26832 NCP mg/L 15000 ** 3.2 30% Pass

Sulphate (as SO4) M17-Au27408 NCP mg/L 1900 ** 7.0 30% Pass

Duplicate


Total Alkalinity (as CaCO3) P17-Au26801 NCP mg/L 61 ** 3.0 30% Pass

Duplicate


Calcium M17-Au27410 NCP mg/L 97 ** 7.0 30% Pass

Magnesium M17-Au27410 NCP mg/L 110 ** 7.0 30% Pass

Potassium M17-Au27865 NCP mg/L 2.9 2.9 <1 30% Pass

Sodium M17-Au27410 NCP mg/L 360 ** 6.0 30% Pass

Duplicate
















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 12 of 14


Duplicate









Duplicate








Duplicate









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 13 of 14


Comments

V2- Report split

V3- Report split










N11



Authorised By





Glenn Jackson








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 14 of 14






Abbotsford

VIC 3067


Report 559812-W-V4





Sample Matrix Water
















13C4-PFBA (surr.) 1 % 92


13C5-PFHxA (surr.) 1 % 106

13C4-PFHpA (surr.) 1 % 118

13C8-PFOA (surr.) 1 % 118

13C5-PFNA (surr.) 1 % 108

13C6-PFDA (surr.) 1 % 74












13C8-FOSA (surr.) 1 % 65





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 17





Sample Matrix Water

















13C3-PFBS (surr.) 1 % 104

18O2-PFHxS (surr.) 1 % 122

13C8-PFOS (surr.) 1 % 112






13C2-4:2 FTS (surr.) 1 % 114

13C2-6:2 FTS (surr.) 1 % 112

13C2-8:2 FTS (surr.) 1 % 51

PFASs Summations






Chloride 1 mg/L 13




Alkali Metals

Calcium 0.5 mg/L 90



Sodium 0.5 mg/L 7.5




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 17

























ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 17



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.


















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 17




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank



Method Blank



Method Blank

Alkali Metals





LCS - % Recovery






ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 17



PassLimits

QualifyingCode











LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery



LCS - % Recovery



LCS - % Recovery

Alkali Metals






LimitsPass

LimitsQualifying

Code

Spike - % Recovery










ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 17



LimitsPass

LimitsQualifying

Code







Spike - % Recovery









Spike - % Recovery








Spike - % Recovery






Spike - % Recovery

Result 1



Spike - % Recovery








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 17



LimitsPass

LimitsQualifying

Code


Spike - % Recovery

Result 1



Spike - % Recovery






Spike - % Recovery













Spike - % Recovery









Spike - % Recovery








Spike - % Recovery




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 17



LimitsPass

LimitsQualifying

Code






Spike - % Recovery













Spike - % Recovery









Spike - % Recovery








Spike - % Recovery





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 17



LimitsPass

LimitsQualifying

Code





Spike - % Recovery

Result 1



Spike - % Recovery






Spike - % Recovery













Spike - % Recovery









Spike - % Recovery







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 17



LimitsPass

LimitsQualifying

Code





Spike - % Recovery







LimitsPass

LimitsQualifying

Code

Duplicate













Duplicate












ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 17


Duplicate








Duplicate






Duplicate




Duplicate



Duplicate






Duplicate
















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 12 of 17


Duplicate









Duplicate








Duplicate






Duplicate




Duplicate



Duplicate


Calcium M17-Au27410 NCP mg/L 97 ** 7.0 30% Pass

Magnesium M17-Au27410 NCP mg/L 110 ** 7.0 30% Pass

Potassium M17-Au27865 NCP mg/L 2.9 2.9 <1 30% Pass

Sodium M17-Au27410 NCP mg/L 360 ** 6.0 30% Pass




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 13 of 17


Duplicate













Duplicate









Duplicate








Duplicate









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 14 of 17


Duplicate


Perfluorobutanoic acid (PFBA) M17-Au26495 NCP ug/L < 0.05 ** <1 30% Pass

Perfluoropentanoic acid (PFPeA) M17-Au26495 NCP ug/L < 0.01 ** <1 30% Pass

Perfluorohexanoic acid (PFHxA) M17-Au26495 NCP ug/L < 0.01 ** <1 30% Pass

Perfluoroheptanoic acid (PFHpA) M17-Au26495 NCP ug/L < 0.01 ** <1 30% Pass

Perfluorooctanoic acid (PFOA) M17-Au26495 NCP ug/L < 0.01 ** <1 30% Pass

Perfluorononanoic acid (PFNA) M17-Au26495 NCP ug/L < 0.01 ** <1 30% Pass

Perfluorodecanoic acid (PFDA) M17-Au26495 NCP ug/L < 0.01 ** <1 30% Pass

Perfluoroundecanoic acid (PFUnA) M17-Au26495 NCP ug/L < 0.01 ** <1 30% Pass

Perfluorododecanoic acid (PFDoA) M17-Au26495 NCP ug/L < 0.01 ** <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) M17-Au26495 NCP ug/L < 0.01 ** 200 30% Fail

Perfluorotetradecanoic acid(PFTeDA) M17-Au26495 NCP ug/L < 0.01 ** 200 30% Fail

Duplicate


Perfluorooctane sulfonamide(FOSA) M17-Au26495 NCP ug/L < 0.05 ** <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) M17-Au26495 NCP ug/L < 0.05 ** <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) M17-Au26495 NCP ug/L < 0.05 ** 200 30% Fail

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) M17-Au26495 NCP ug/L < 0.05 ** <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) M17-Au26495 NCP ug/L < 0.05 ** <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-Au26495 NCP ug/L < 0.05 ** <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-Au26495 NCP ug/L < 0.05 ** <1 30% Pass

Duplicate


Perfluorobutanesulfonic acid(PFBS) M17-Au26495 NCP ug/L < 0.01 ** <1 30% Pass

Perfluoropentanesulfonic acid(PFPeS) M17-Au26495 NCP ug/L < 0.01 ** <1 30% Pass

Perfluorohexanesulfonic acid(PFHxS) M17-Au26495 NCP ug/L < 0.01 ** <1 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) M17-Au26495 NCP ug/L < 0.01 ** <1 30% Pass

Perfluorooctanesulfonic acid(PFOS) M17-Au26495 NCP ug/L < 0.01 ** <1 30% Pass

Perfluorodecanesulfonic acid(PFDS) M17-Au26495 NCP ug/L < 0.01 ** <1 30% Pass

Duplicate


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-Au26495 NCP ug/L < 0.01 ** <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-Au26495 NCP ug/L < 0.05 ** 5.0 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-Au26495 NCP ug/L < 0.01 ** <1 30% Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) M17-Au26495 NCP ug/L < 0.01 ** <1 30% Pass

Duplicate







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 15 of 17


Duplicate



Duplicate



Magnesium M17-Au27865 NCP mg/L 3.3 3.4 3.0 30% Pass

Potassium M17-Au27865 NCP mg/L 2.9 ** <1 30% Pass

Sodium M17-Au28491 NCP mg/L 26 22 13 30% Pass




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 16 of 17


Comments

V2- Report split

V3- Report split

V4- Report split










N11



Authorised By





Glenn Jackson








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 17 of 17






Abbotsford

VIC 3067


Report 560521-W





0990_PB009_2_170808

0990_PB009_3_170808


Eurofins | mgt Sample No. M17-Au24017 M17-Au24018 M17-Au24019















13C4-PFBA (surr.) 1 % 109 107 113

13C5-PFPeA (surr.) 1 % 106 104 110

13C5-PFHxA (surr.) 1 % 123 121 125

13C4-PFHpA (surr.) 1 % 119 119 122

13C8-PFOA (surr.) 1 % 119 122 126

13C5-PFNA (surr.) 1 % 102 105 117

13C6-PFDA (surr.) 1 % 88 91 101

13C2-PFUnDA (surr.) 1 % 79 81 93

13C2-PFDoDA (surr.) 1 % 70 70 78

13C2-PFTeDA (surr.) 1 % 50 50 53









13C8-FOSA (surr.) 1 % 78 80 92

D3-N-MeFOSA (surr.) 1 % 47 44 61



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 11





0990_PB009_2_170808

0990_PB009_3_170808


Eurofins | mgt Sample No. M17-Au24017 M17-Au24018 M17-Au24019




D5-N-EtFOSA (surr.) 1 % 38 35 49

D7-N-MeFOSE (surr.) 1 % 58 58 71

D9-N-EtFOSE (surr.) 1 % 55 54 68

D5-N-EtFOSAA (surr.) 1 % 67 84 82

D3-N-MeFOSAA (surr.) 1 % 68 80 77




Perfluorohexanesulfonic acid (PFHxS)N11 0.01 ug/L N090.02 < 0.01 < 0.01


Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N090.04 < 0.01 < 0.01


13C3-PFBS (surr.) 1 % 118 118 122

18O2-PFHxS (surr.) 1 % 114 114 119

13C8-PFOS (surr.) 1 % 79 81 87






13C2-4:2 FTS (surr.) 1 % 144 138 146

13C2-6:2 FTS (surr.) 1 % 149 149 159

13C2-8:2 FTS (surr.) 1 % 112 110 122

PFASs Summations

Sum (PFHxS + PFOS) 0.01 ug/L 0.06 < 0.01 < 0.01

Sum of US EPA PFAS (PFOS + PFOA) 0.01 ug/L 0.04 < 0.01 < 0.01

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 0.01 ug/L 0.06 < 0.01 < 0.01

Sum of WA DER PFAS (n=10) 0.05 ug/L 0.06 < 0.05 < 0.05

Sum of PFASs (n=28) 0.1 ug/L < 0.1 < 0.1 < 0.1

Ammonia (as N) 0.01 mg/L < 0.01 - -

Chloride 1 mg/L 5.3 - -

Nitrate (as N) 0.02 mg/L 0.13 - -

Sulphate (as SO4) 5 mg/L < 5 - -


Bicarbonate Alkalinity (as CaCO3) 20 mg/L 450 - -

Carbonate Alkalinity (as CaCO3) 10 mg/L < 10 - -

Alkali Metals

Calcium 0.5 mg/L 34 - -

Magnesium 0.5 mg/L 31 - -

Potassium 0.5 mg/L 1.9 - -

Sodium 0.5 mg/L 3.7 - -



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 11





























ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 11


.Company Name: Coffey Environments Pty Ltd VIC Order No.: Received: Aug 11, 2017 10:10 AMAddress: Level 1, 436 Johnston Street Report #: 560521 Due: Sep 4, 2017




Sample Detail

Eurofins | m

gt Suite B

11

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_PB009_1_170808

Aug 08, 2017 Water M17-Au24017 X X

2 0990_PB009_2_170808

Aug 08, 2017 Water M17-Au24018 X

3 0990_PB009_3_170808

Aug 08, 2017 Water M17-Au24019 X

Test Counts 1 3








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 11



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 11




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank





Method Blank




Method Blank

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 11



PassLimits

QualifyingCode

LCS - % Recovery













LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery





LCS - % Recovery


Bicarbonate Alkalinity (as CaCO3) % 83 70-130 Pass


LCS - % Recovery

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 11



LimitsPass

LimitsQualifying

Code

Spike - % Recovery













Spike - % Recovery









Spike - % Recovery








Spike - % Recovery






Spike - % Recovery

Result 1



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 11



LimitsPass

LimitsQualifying

Code





Spike - % Recovery


Bicarbonate Alkalinity (as CaCO3) P17-Au30755 NCP % 78 70-130 Pass


Spike - % Recovery







LimitsPass

LimitsQualifying

Code

Duplicate



Chloride M17-Au24021 NCP mg/L 4.5 4.5 <1 30% Pass

Nitrate (as N) M17-Au24020 NCP mg/L 0.20 0.20 2.0 30% Pass

Sulphate (as SO4) S17-Au28753 NCP mg/L 1300 1300 1.4 30% Pass

Duplicate


Bicarbonate Alkalinity (as CaCO3) M17-Au30271 NCP mg/L < 20 < 20 <1 30% Pass


Duplicate


Calcium M17-Au24021 NCP mg/L 49 56 13 30% Pass

Magnesium M17-Au24021 NCP mg/L 29 34 15 30% Pass

Potassium M17-Au24021 NCP mg/L 1.7 1.5 11 30% Pass

Sodium M17-Au24021 NCP mg/L 3.1 2.9 4.0 30% Pass

Duplicate













Duplicate








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 11


Duplicate





Duplicate








Duplicate








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 11


Comments










N11



Authorised By





Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 11






Abbotsford

VIC 3067


Report 560524-W





Sample Matrix Water
















13C4-PFBA (surr.) 1 % 138

13C5-PFPeA (surr.) 1 % 126

13C5-PFHxA (surr.) 1 % 151

13C4-PFHpA (surr.) 1 % 149

13C8-PFOA (surr.) 1 % 152

13C5-PFNA (surr.) 1 % 130

13C6-PFDA (surr.) 1 % 110












13C8-FOSA (surr.) 1 % 101




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 11





Sample Matrix Water

















13C3-PFBS (surr.) 1 % 145

18O2-PFHxS (surr.) 1 % 143

13C8-PFOS (surr.) 1 % 100






13C2-4:2 FTS (surr.) 1 % 183

13C2-6:2 FTS (surr.) 1 % 188

13C2-8:2 FTS (surr.) 1 % 139

PFASs Summations







Chloride 1 mg/L 4.5






Alkali Metals

Calcium 0.5 mg/L 49



Sodium 0.5 mg/L 3.1



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 11





























ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 11






Sample Detail

Eurofins | m

gt Suite B

11

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_PB011_170808

Aug 08, 2017 Water M17-Au24021 X X

Test Counts 1 1








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 11



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 11




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank





Method Blank




Method Blank

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 11



PassLimits

QualifyingCode

LCS - % Recovery













LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery





LCS - % Recovery


Bicarbonate Alkalinity (as CaCO3) % 83 70-130 Pass


LCS - % Recovery

Alkali Metals







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 11



LimitsPass

LimitsQualifying

Code

Spike - % Recovery













Spike - % Recovery









Spike - % Recovery








Spike - % Recovery






Spike - % Recovery

Result 1



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 11



LimitsPass

LimitsQualifying

Code





Spike - % Recovery


Bicarbonate Alkalinity (as CaCO3) P17-Au30755 NCP % 78 70-130 Pass


Spike - % Recovery


Calcium M17-Au24021 CP % 138 70-130 Fail Q08

Magnesium M17-Au24021 CP % 109 70-130 Pass




LimitsPass

LimitsQualifying

Code

Duplicate













Duplicate









Duplicate








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 11


Duplicate




Duplicate






Duplicate



Chloride M17-Au24021 CP mg/L 4.5 4.5 <1 30% Pass

Nitrate (as N) M17-Au24020 NCP mg/L 0.20 0.20 2.0 30% Pass

Sulphate (as SO4) S17-Au28753 NCP mg/L 1300 1300 1.4 30% Pass

Duplicate


Bicarbonate Alkalinity (as CaCO3) M17-Au30271 NCP mg/L < 20 < 20 <1 30% Pass


Duplicate


Calcium M17-Au24021 CP mg/L 49 56 13 30% Pass

Magnesium M17-Au24021 CP mg/L 29 34 15 30% Pass

Potassium M17-Au24021 CP mg/L 1.7 1.5 11 30% Pass

Sodium M17-Au24021 CP mg/L 3.1 2.9 4.0 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 11


Comments










N11



Authorised By





Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 11






Abbotsford

VIC 3067


Report 560575-W





Sample Matrix Water
















13C4-PFBA (surr.) 1 % 78


13C5-PFHxA (surr.) 1 % 107

13C4-PFHpA (surr.) 1 % 116

13C8-PFOA (surr.) 1 % 118

13C5-PFNA (surr.) 1 % 104

13C6-PFDA (surr.) 1 % 73












13C8-FOSA (surr.) 1 % 63




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 11





Sample Matrix Water

















13C3-PFBS (surr.) 1 % 101

18O2-PFHxS (surr.) 1 % 104

13C8-PFOS (surr.) 1 % 81






13C2-4:2 FTS (surr.) 1 % 130

13C2-6:2 FTS (surr.) 1 % 120

13C2-8:2 FTS (surr.) 1 % 73

PFASs Summations






Chloride 1 mg/L 14




Alkali Metals

Calcium 0.5 mg/L 76



Sodium 0.5 mg/L 39



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 11






Perfluoroalkyl carboxylic acids (PFCAs) Brisbane Sep 07, 2017 14 Day


Perfluoroalkane sulfonamides (PFASAs) Brisbane Sep 07, 2017 14 Day


Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates (PFSAs) Brisbane Sep 07, 2017 14 Day


n:2 Fluorotelomer sulfonic acids Brisbane Sep 07, 2017 14 Day












ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 11


.Company Name: Coffey Environments Pty Ltd VIC Order No.: Received: Aug 28, 2017 5:46 PMAddress: Level 1, 436 Johnston Street Report #: 560575 Due: Sep 5, 2017




Sample Detail

Chloride

Sulphate (as S

O4)

Total A

lkalinity (as CaC

O3)

Alkali M

etals

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_PB012_170810










ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 11



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 11




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank



Method Blank



Method Blank

Alkali Metals





LCS - % Recovery





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 11



PassLimits

QualifyingCode











LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery



LCS - % Recovery



LCS - % Recovery

Alkali Metals






LimitsPass

LimitsQualifying

Code

Spike - % Recovery









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 11



LimitsPass

LimitsQualifying

Code







Spike - % Recovery









Spike - % Recovery








Spike - % Recovery






Spike - % Recovery

Result 1



Spike - % Recovery


Total Alkalinity (as CaCO3) M17-Au25715 NCP % 122 70-130 Pass

Spike - % Recovery




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 11



LimitsPass

LimitsQualifying

Code






LimitsPass

LimitsQualifying

Code

Duplicate













Duplicate









Duplicate










ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 11


Duplicate






Duplicate




Duplicate



Duplicate








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 11


Comments









Code Description

N11



Authorised By





Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 11






Abbotsford

VIC 3067


Report 560578-W





Sample Matrix Water
















13C4-PFBA (surr.) 1 % 78


13C5-PFHxA (surr.) 1 % 111

13C4-PFHpA (surr.) 1 % 121

13C8-PFOA (surr.) 1 % 128

13C5-PFNA (surr.) 1 % 102

13C6-PFDA (surr.) 1 % 76












13C8-FOSA (surr.) 1 % 66




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 11





Sample Matrix Water

















13C3-PFBS (surr.) 1 % 109

18O2-PFHxS (surr.) 1 % 103

13C8-PFOS (surr.) 1 % 84






13C2-4:2 FTS (surr.) 1 % 117

13C2-6:2 FTS (surr.) 1 % 106

13C2-8:2 FTS (surr.) 1 % 78

PFASs Summations






Chloride 1 mg/L 15




Alkali Metals

Calcium 0.5 mg/L 89



Sodium 0.5 mg/L 4.4



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 11
























ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 11






Sample Detail

CA

NC

ELLE

D

Chloride

Sulphate (as S

O4)

Total A

lkalinity (as CaC

O3)

Alkali M

etals

Per- and P


ubstances(P

FA

Ss)

Melbourne Laboratory - NATA Site # 1254 & 14271 X X X X X




External Laboratory


Matrix LAB ID

1 0990_PB013_170810-1


2 0990_PB013_170810-2

Aug 10, 2017 Water M17-Au32911 X

Test Counts 1 1 1 1 1 1








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 11



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 11




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank



Method Blank



Method Blank

Alkali Metals





LCS - % Recovery





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 11



PassLimits

QualifyingCode











LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery



LCS - % Recovery



LCS - % Recovery

Alkali Metals






LimitsPass

LimitsQualifying

Code

Spike - % Recovery









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 11



LimitsPass

LimitsQualifying

Code







Spike - % Recovery









Spike - % Recovery








Spike - % Recovery






Spike - % Recovery

Result 1

Chloride B17-Au35297 NCP % 130 70-130 Pass


Spike - % Recovery



Spike - % Recovery




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 11



LimitsPass

LimitsQualifying

Code

Calcium B17-Au35173 NCP % 115 70-130 Pass



Sodium B17-Au35173 NCP % 124 70-130 Pass


LimitsPass

LimitsQualifying

Code

Duplicate













Duplicate









Duplicate










ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 11


Duplicate






Duplicate




Duplicate


Total Alkalinity (as CaCO3) B17-Au35173 NCP mg/L < 20 < 20 <1 30% Pass

Duplicate


Calcium B17-Au35173 NCP mg/L 120 100 19 30% Pass

Magnesium B17-Au35173 NCP mg/L 100 100 1.0 30% Pass

Potassium B17-Au35173 NCP mg/L 2.3 2.3 2.0 30% Pass

Sodium B17-Au35173 NCP mg/L 260 260 1.0 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 11


Comments










N11


Authorised By





Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 11






Abbotsford

VIC 3067


Report 560580-W





Sample Matrix Water
















13C4-PFBA (surr.) 1 % 73


13C5-PFHxA (surr.) 1 % 107

13C4-PFHpA (surr.) 1 % 118

13C8-PFOA (surr.) 1 % 123

13C5-PFNA (surr.) 1 % 105

13C6-PFDA (surr.) 1 % 80












13C8-FOSA (surr.) 1 % 69




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 11





Sample Matrix Water













Perfluorohexanesulfonic acid (PFHxS)N11 0.01 ug/L 0.03




13C3-PFBS (surr.) 1 % 103

18O2-PFHxS (surr.) 1 % 105

13C8-PFOS (surr.) 1 % 89






13C2-4:2 FTS (surr.) 1 % 128

13C2-6:2 FTS (surr.) 1 % 115

13C2-8:2 FTS (surr.) 1 % 81

PFASs Summations






Chloride 1 mg/L 5.4




Alkali Metals

Calcium 0.5 mg/L 74



Sodium 0.5 mg/L 21



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 11
























ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 11






Sample Detail

Chloride

Sulphate (as S

O4)

Total A

lkalinity (as CaC

O3)

Alkali M

etals

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_PB014_170810










ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 11



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 11




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank



Method Blank



Method Blank

Alkali Metals





LCS - % Recovery





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 11



PassLimits

QualifyingCode











LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery



LCS - % Recovery



LCS - % Recovery

Alkali Metals






LimitsPass

LimitsQualifying

Code

Spike - % Recovery









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 11



LimitsPass

LimitsQualifying

Code







Spike - % Recovery









Spike - % Recovery








Spike - % Recovery






Spike - % Recovery

Result 1



Spike - % Recovery



Spike - % Recovery




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 11



LimitsPass

LimitsQualifying

Code






LimitsPass

LimitsQualifying

Code

Duplicate













Duplicate









Duplicate










ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 11


Duplicate






Duplicate




Duplicate



Duplicate








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 11


Comments










N11



Authorised By





Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 11






Abbotsford

VIC 3067


Report 560581-W





Sample Matrix Water




Chloride 1 mg/L 14




Alkali Metals

Calcium 0.5 mg/L 92



Sodium 0.5 mg/L 4.5



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 6

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 6






Sample Detail

Chloride

Sulphate (as S

O4)

Total A

lkalinity (as CaC

O3)

Alkali M

etals



Brisbane Laboratory - NATA Site # 20794


External Laboratory


Matrix LAB ID

1 0990_PB015_170811

Aug 11, 2017 Water M17-Au19874 X X X X

Test Counts 1 1 1 1








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 6



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 6




PassLimits

QualifyingCode

Method Blank



Method Blank



Method Blank

Alkali Metals





LCS - % Recovery



LCS - % Recovery

Alkali Metals






LimitsPass

LimitsQualifying

Code

Spike - % Recovery

Result 1



Spike - % Recovery







LimitsPass

LimitsQualifying

Code

Duplicate




Duplicate



Duplicate








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 6


Comments










Authorised By




Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 6






Abbotsford

VIC 3067


Report 560581-W-V2





Sample Matrix Water






Perfluoropentanoic acid (PFPeA)N11 0.01 ug/L 0.04

Perfluorohexanoic acid (PFHxA)N11 0.01 ug/L 0.17

Perfluoroheptanoic acid (PFHpA)N11 0.01 ug/L 0.03

Perfluorooctanoic acid (PFOA)N11 0.01 ug/L 0.05







13C4-PFBA (surr.) 1 % 52




13C8-PFOA (surr.) 1 % 71

13C5-PFNA (surr.) 1 % 67

13C6-PFDA (surr.) 1 % 51












13C8-FOSA (surr.) 1 % 25


First Reported: Aug 31, 2017



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 9





Sample Matrix Water












Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L 0.15

Perfluorohexanesulfonic acid (PFHxS)N11 0.01 ug/L 1.0

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L 0.06

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L 1.8


13C3-PFBS (surr.) 1 % 99


13C8-PFOS (surr.) 1 % 78






13C2-4:2 FTS (surr.) 1 % 117

13C2-6:2 FTS (surr.) 1 % 100

13C2-8:2 FTS (surr.) 1 % 66

PFASs Summations






Chloride 1 mg/L 14




Alkali Metals

Calcium 0.5 mg/L 92



Sodium 0.5 mg/L 4.5




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 9

























ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 9






Sample Detail

Chloride

Sulphate (as S

O4)

Total A

lkalinity (as CaC

O3)

Alkali M

etals



Brisbane Laboratory - NATA Site # 20794


External Laboratory


Matrix LAB ID

1 0990_PB015_170811

Aug 11, 2017 Water M17-Au19874 X X X X

Test Counts 1 1 1 1






First Reported:Aug 31, 2017



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 9



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.


















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 9




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank



Method Blank



Method Blank

Alkali Metals





LCS - % Recovery






ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 9



PassLimits

QualifyingCode











LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery



LCS - % Recovery

Alkali Metals






LimitsPass

LimitsQualifying

Code

Spike - % Recovery

Result 1



Spike - % Recovery









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 9



LimitsPass

LimitsQualifying

Code

Duplicate




Duplicate



Duplicate









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 9


Comments

Report amended to add in PFAS data










N11


Authorised By





Glenn Jackson








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 9






Abbotsford

VIC 3067


Report 560582-W





Sample Matrix Water
















13C4-PFBA (surr.) 1 % 75




13C8-PFOA (surr.) 1 % 87

13C5-PFNA (surr.) 1 % 73

13C6-PFDA (surr.) 1 % 52












13C8-FOSA (surr.) 1 % 20




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 11





Sample Matrix Water

















13C3-PFBS (surr.) 1 % 100


13C8-PFOS (surr.) 1 % 76






13C2-4:2 FTS (surr.) 1 % 114

13C2-6:2 FTS (surr.) 1 % 99

13C2-8:2 FTS (surr.) 1 % 58

PFASs Summations






Chloride 1 mg/L 12




Alkali Metals

Calcium 0.5 mg/L 74



Sodium 0.5 mg/L 2.3



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 11
























ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 11






Sample Detail

Chloride

Sulphate (as S

O4)

Total A

lkalinity (as CaC

O3)

Alkali M

etals

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_PB016_170811










ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 11



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 11




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank



Method Blank



Method Blank

Alkali Metals





LCS - % Recovery





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 11



PassLimits

QualifyingCode











LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery



LCS - % Recovery

Alkali Metals






LimitsPass

LimitsQualifying

Code

Spike - % Recovery












ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 11



LimitsPass

LimitsQualifying

Code




Spike - % Recovery









Spike - % Recovery








Spike - % Recovery






Spike - % Recovery

Result 1



Spike - % Recovery








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 11



LimitsPass

LimitsQualifying

Code

Duplicate













Duplicate









Duplicate








Duplicate








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 11


Duplicate




Duplicate



Duplicate








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 11


Comments









Code Description

N11


Authorised By





Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 11






Abbotsford

VIC 3067


Report 560584-W





Sample Matrix Water
















13C4-PFBA (surr.) 1 % 69




13C8-PFOA (surr.) 1 % 81

13C5-PFNA (surr.) 1 % 75

13C6-PFDA (surr.) 1 % 57












13C8-FOSA (surr.) 1 % 43




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 11





Sample Matrix Water

















13C3-PFBS (surr.) 1 % 96


13C8-PFOS (surr.) 1 % 83






13C2-4:2 FTS (surr.) 1 % 104

13C2-6:2 FTS (surr.) 1 % 90

13C2-8:2 FTS (surr.) 1 % 62

PFASs Summations






Chloride 1 mg/L 15




Alkali Metals

Calcium 0.5 mg/L 77



Sodium 0.5 mg/L 6.2



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 11
























ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 11






Sample Detail

Chloride

Sulphate (as S

O4)

Total A

lkalinity (as CaC

O3)

Alkali M

etals

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_PB017_170811










ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 11



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 11




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank



Method Blank



Method Blank

Alkali Metals





LCS - % Recovery





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 11



PassLimits

QualifyingCode











LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery



LCS - % Recovery

Alkali Metals






LimitsPass

LimitsQualifying

Code

Spike - % Recovery












ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 11



LimitsPass

LimitsQualifying

Code




Spike - % Recovery









Spike - % Recovery








Spike - % Recovery






Spike - % Recovery

Result 1



Spike - % Recovery








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 11



LimitsPass

LimitsQualifying

Code

Duplicate













Duplicate









Duplicate








Duplicate








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 11


Duplicate




Duplicate



Duplicate








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 11


Comments









Code Description

N11


Authorised By





Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 11






Abbotsford

VIC 3067


Report 560587-W





0990_PB018_170811-2

















13C4-PFBA (surr.) 1 % 80 72

13C5-PFPeA (surr.) 1 % 82 76

13C5-PFHxA (surr.) 1 % 91 85

13C4-PFHpA (surr.) 1 % 87 80

13C8-PFOA (surr.) 1 % 89 82

13C5-PFNA (surr.) 1 % 79 71

13C6-PFDA (surr.) 1 % 61 51

13C2-PFUnDA (surr.) 1 % 45 38

13C2-PFDoDA (surr.) 1 % 40 34

13C2-PFTeDA (surr.) 1 % 28 24









13C8-FOSA (surr.) 1 % 73 20

D3-N-MeFOSA (surr.) 1 % 24 INT



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 8





0990_PB018_170811-2






D5-N-EtFOSA (surr.) 1 % 12 INT

D7-N-MeFOSE (surr.) 1 % 31 INT

D9-N-EtFOSE (surr.) 1 % 26 INT


D3-N-MeFOSAA (surr.) 1 % INT 10








13C3-PFBS (surr.) 1 % 101 94

18O2-PFHxS (surr.) 1 % 95 88

13C8-PFOS (surr.) 1 % 83 73






13C2-4:2 FTS (surr.) 1 % 115 106

13C2-6:2 FTS (surr.) 1 % 100 91

13C2-8:2 FTS (surr.) 1 % 67 58

PFASs Summations





Sum of PFASs (n=28) 0.1 ug/L < 0.1 < 0.1

Chloride 1 mg/L 7.8 12



Total Alkalinity (as CaCO3) 20 mg/L 330 390

Alkali Metals

Calcium 0.5 mg/L 73 70

Magnesium 0.5 mg/L 29 28

Potassium 0.5 mg/L 1.1 1.1




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 8
























ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 8






Sample Detail

Chloride

Sulphate (as S

O4)

Total A

lkalinity (as CaC

O3)

Alkali M

etals

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_PB018_170811-1


2 0990_PB018_170811-2










ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 8



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 8




LimitsPass

LimitsQualifying

Code

Spike - % Recovery

Result 1

Sulphate (as SO4) M17-Au19878 CP % 105 70-130 Pass


LimitsPass

LimitsQualifying

Code

Duplicate













Duplicate









Duplicate










ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 8


Duplicate






Duplicate


Chloride M17-Au19877 CP mg/L 7.8 7.9 <1 30% Pass

Sulphate (as SO4) M17-Au19877 CP mg/L < 5 < 5 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 8


Comments









Code Description

N11


Authorised By





Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 8






Abbotsford

VIC 3067


Report 560588-W





Sample Matrix Water
















13C4-PFBA (surr.) 1 % 85




13C8-PFOA (surr.) 1 % 98

13C5-PFNA (surr.) 1 % 86

13C6-PFDA (surr.) 1 % 65












13C8-FOSA (surr.) 1 % 74




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 10





Sample Matrix Water

















13C3-PFBS (surr.) 1 % 102


13C8-PFOS (surr.) 1 % 86






13C2-4:2 FTS (surr.) 1 % 119

13C2-6:2 FTS (surr.) 1 % 105

13C2-8:2 FTS (surr.) 1 % 70

PFASs Summations






Chloride 1 mg/L 12




Alkali Metals

Calcium 0.5 mg/L 86



Sodium 0.5 mg/L 6.3



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 10
























ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 10



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 10




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank



Method Blank



Method Blank

Alkali Metals





LCS - % Recovery





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 10



PassLimits

QualifyingCode











LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery



LCS - % Recovery

Alkali Metals






LimitsPass

LimitsQualifying

Code

Spike - % Recovery












ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 10



LimitsPass

LimitsQualifying

Code




Spike - % Recovery









Spike - % Recovery








Spike - % Recovery






Spike - % Recovery

Result 1



Spike - % Recovery








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 10



LimitsPass

LimitsQualifying

Code

Duplicate













Duplicate









Duplicate








Duplicate








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 10


Duplicate




Duplicate



Duplicate








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 10


Comments









Code Description

N11


Authorised By





Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 10






Abbotsford

VIC 3067


Report 560609-W-V2





Sample Matrix Water
















13C4-PFBA (surr.) 1 % 97


13C5-PFHxA (surr.) 1 % 127

13C4-PFHpA (surr.) 1 % 140

13C8-PFOA (surr.) 1 % 154

13C5-PFNA (surr.) 1 % 105

13C6-PFDA (surr.) 1 % 79












13C8-FOSA (surr.) 1 % 73




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 11





Sample Matrix Water

















13C3-PFBS (surr.) 1 % 128

18O2-PFHxS (surr.) 1 % 135

13C8-PFOS (surr.) 1 % 85






13C2-4:2 FTS (surr.) 1 % 187

13C2-6:2 FTS (surr.) 1 % 148

13C2-8:2 FTS (surr.) 1 % 72

PFASs Summations






Chloride 1 mg/L 22




Alkali Metals

Calcium 0.5 mg/L 27



Sodium 0.5 mg/L 47



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 11
























ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 11






Sample Detail

Chloride

Sulphate (as S

O4)

Total A

lkalinity (as CaC

O3)

Alkali M

etals

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_QCMW197_170823

Aug 23, 2017 Water M17-Au33049 X

2 0990_PB30_170823


3 0990_PB31_170823


4 0990_QCMW198_170824

Aug 24, 2017 Water M17-Au33052 X









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 11



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 11




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank






Method Blank



Method Blank



Method Blank

Alkali Metals





LCS - % Recovery





ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 11



PassLimits

QualifyingCode











LCS - % Recovery









LCS - % Recovery








LCS - % Recovery






LCS - % Recovery



LCS - % Recovery



LCS - % Recovery

Alkali Metals






LimitsPass

LimitsQualifying

Code

Spike - % Recovery









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 11



LimitsPass

LimitsQualifying

Code







Spike - % Recovery









Spike - % Recovery








Spike - % Recovery






Spike - % Recovery

Result 1



Spike - % Recovery








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 11



LimitsPass

LimitsQualifying

Code

Duplicate













Duplicate









Duplicate








Duplicate








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 11


Duplicate




Duplicate


Total Alkalinity (as CaCO3) M17-Au32307 NCP mg/L 550 580 5.0 30% Pass

Duplicate


Calcium M17-Au32583 NCP mg/L 0.6 0.5 6.0 30% Pass






ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 11


Comments

V2 - Split report for PB030









Code Description

N11


Authorised By





Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 11






Abbotsford

VIC 3067


Report 560609-W-V3





Sample Matrix Water
















13C4-PFBA (surr.) 1 % 99


13C5-PFHxA (surr.) 1 % 131

13C4-PFHpA (surr.) 1 % 143

13C8-PFOA (surr.) 1 % 154

13C5-PFNA (surr.) 1 % 105

13C6-PFDA (surr.) 1 % 77












13C8-FOSA (surr.) 1 % 76




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 11





Sample Matrix Water

















13C3-PFBS (surr.) 1 % 130

18O2-PFHxS (surr.) 1 % 131

13C8-PFOS (surr.) 1 % 86






13C2-4:2 FTS (surr.) 1 % 197

13C2-6:2 FTS (surr.) 1 % 158

13C2-8:2 FTS (surr.) 1 % 78

PFASs Summations






Chloride 1 mg/L 26




Alkali Metals

Calcium 0.5 mg/L 43


Potassium 0.5 mg/L 13

Sodium 0.5 mg/L 40



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 11
