AP42 chapter 12 reference · 2015-09-10 · 4P42 Section: Reference: Title: 12.2 91 Rouge Steel...

4P42 Section:

Reference:

Title:

12.2

91

Rouge Steel Company, Coke Ovens Combustion Stack B Particulate and Opacity Survey, Ford Motor Company Stationary Source Environmental Control Office, Michigan,

November 29-December 2,1982.

EPA

Text Box

Note: This is a reference cited in AP 42, Compilation of Air Pollutant Emission Factors, Volume I Stationary Point and Area Sources. AP42 is located on the EPA web site at www.epa.gov/ttn/chief/ap42/ The file name refers to the reference number, the AP42 chapter and section. The file name "ref02_c01s02.pdf" would mean the reference is from AP42 chapter 1 section 2. The reference may be from a previous version of the section and no longer cited. The primary source should always be checked.

.

Figure 1

STEEL LIBRARY SYSTEM

a Report T i t l e : U Plan t and Locat ion: - 8oqe 5+e\ c o . /Dear&-

ay Whom: ficd Stack Test Review Attached: d d

Reviewed By:

Problems Seen by Reviewer:

I , ..

C o n f i d e n t i a l i t y Status: ~(,.,Mu/h I f s ta tus i s c o n f i d e n t i a l , l i s t c o n f i d e n t i a l pages o r sect ions:

Source o f Determinat ion o f t h e C o n f i d e n t i a l i t y Status:

Report Encoded By:

Date Encoded:

Form Numbers:

Commen t s :

, - I '

-30-

8 Rouge Steel Company Coke Ovens Combustion Stack B

, P a r t i c u l a t e and Opaci ty Survey

j November 29-December 2, 1982

c

/-

. - Stationary Source Environmental Control Office Environmental and Safety Engineering Staff

A P ~ Z Section lz.z_

Report Sect. 2%- Reference 3-

/ ’ - ....

Rouge Steel Company Coke Ovens Combustion Stack B

P a r t i c u l a t e and Opacity Survey

November 29-December 2, 1982

. Conducted By

Ford Motor Company Stationary Source Environmental Control Of f ice

Survey and Evaluation

Survey Conducted By: Report Prepared By:

CONCUR: n

Rouge Steel Company Coke Ovens Combustion Stack B

Par t iculate and Opacity Survey

Table o f Contents

Subject

I . Introduction . . . . . i . . . . . . . . . . . . ..: ... 11. Process Description. . . . . . . . . . . . . . . . . . . . 111. Sumnary. . . . . . . . . . . . . . . . . . . . . . . . IV. . Results. . . . . . . . . . . . . . . . . . . . . . . . .

2 1

6 8

14 . . . . . . . . . . . . . . . . . . . . . V. Discussion'.

L is t o f Appendices

A. B. c. D. E. F. G . H. I .

.

,

Location o f Sampling Ports and Points. 15 Sampling Procedures. . . : . . . . . . . . . . . . . . .

22 Analytical Procedures. . . . . . . . . . . . . . . . . 25 Field Data Sheets. . . . . . . . . . . . . . . . . . . 49 Opacity Data Sheet . . . . . . . . . . . . . . . . . . 65 Production Data. . . . . . . . . . . . . . . . . . . .

Labqratory 74

64

. . . . . . . .

. . . . . . . . . . . . . . . . . . . . . . Sample Calculations. . . . . . . . . . . . . . . . . . 77 E q u i w e n t Cali bration. . . . . . . . . . . . . . . . .

List o f Tables L

I . Process Operation Data . . . . . . . . . . . . . . . . 7 5 . . . . . . . . . . . . . . . . . . 11. Test Data Sumnary. 4 111. Stack Gas Velocity and Flow Results. . . . . . . . . . . *

IV. Par t iculate Sampling Results . . . . . . . . . . . . . 11

VI. Blast Furnace Gas 'Composition. . . . . . . . . . . . .

Schematic o f TypicalFKoppers Coking Oven . . . . . . . 2. Sampling Port Location . . . . . . . . . . . . . . . . 3 . Location o f Sampling Points. . . . . . . . . . . . . . .

Part iculate Sampling -Train . . :. .: . . . . . . . . :. . . . .

V . Opacity Six-Minute Averages. 13 . . . . . . . . . . . . . . . . . . . . .

.. i' Lis t o f Figures .-

13 17 18 21

1.

4.

. *&

I, 7 . . . ~. . . . . .

\,+ i i

.. I '<.

I . I n t r o d u c t i o n

On the week o f November 29, 1982 the Rouge Steel Company Coke

Oven Combustion Stack was t e s t e d i n order t o compare t o t a l f i l t e r a b l e

p a r t i c u l a t e emissions w i t h opaci ty .

was t o determine the r e l a t i o n s h i p between p a r t i c u l a t e dnissions and

opac i t y so t h a t t h e Rouge Steel Company cou ld apply t o the State

o f Michigan f o r a r e v i s i o n t o the Michigan S ta te Implementation

Plan f o r a s u b s t i t u t e o p a c i t y l i m i t as al lowed under the terms

o f Paragraph III.F.3. o f t h e Rouge Consent Decree, as amended.

The i n t e n t o f these t e s t s

A t o t a l o f s i x p a r t i c u l a t e t e s t s were performed on Combustion

Stack B. V i s i b l e emission readings were taken du r ing each o f t he

t e s t s by M r . T. Shurmur o r Mr . R. Rode o f t he Rouge Steel Company

Environmental S t a f f , both c e r t i f i e d opaci ty readers.

Operating, charging, and pushing data were taken dur ing each

An enriched b l a s t furnace gas sample was c o l l e c t e d d a i l y t e s t .

and analyzed by the .Rouge S tee l Company Coke Oven Laboratory.

Refer t o Appendix G f o r t h e ana lys i s .

11. Process Description

Coking i s a process by which coal i s destructively d i s t i l l e d

in a reducing atmosphere t o produce vola t i le gases and a residue

of re la t ively nonvolatile coke.

operation u t i l i ze s a Koppers combination gun-flue type byproduct

coke oven battery.

The Rouge Steel Company coking

On each s ide of a byproduct oven wall is a gas f lue . Fuel

gas is fired on one side of the wall a t a time.

used t o direct exhaust f l u e gas into a regenerator.

ac t s t o pre-heat both combustion a i r and fuel gas.

hour, the direction of fuel gas and combustion a i r flows reverse

over the en t i r e battery.

the b u r n i n g fuel gas.

The other side i s

The regenerator

Every. half

As a resu l t , the opposite f lue contains

Refer to Figure 1 for a schematic drawing

i l l u s t r a t i n g a typical Kopper's Coking Oven.

The vo la t i le byproduct from the coking chamber i s drawn t h r o u g h

an ascension pipe into a collecting main.

t o the byproduce plant fo r processing and dis t r ibut ion.

f lue gas from both the coke and pusher sides i s directed t h r o u g h

a 225 feet combustion stack.

I t is then transported

The waste

During the week of t h i s survey several ovens w i t h i n 6-battery

were being r ebu i l t on the day s h i f t .

and 65, were out of service d u r i n g Test 1 on November 29.

remainder o f the survey, ovens 1-4 were placed back in service

a f t e r the completion of wall repairs.

( o u t of a to ta l of 61) were out of service fo r the remainder o f

Eleven ovens, Nos. 1-9, 39

For the

A total of seven ovens

7. i

FIGURE 1

SCHEMATIC OF TYPICAL KOPPERS COKING OVEN BATTERY B

ROUGE STEEL COMPANY

r I L

Pinion W a l l This i s a typ ica l coke oven-flue diagram f o r Battery B showing three coking ovens, four regenerators. and two p in ion walls. regenerators on a #1-#4-#5. 82-83 sequence or reversal . t ranspor t o f waste f l u e gas through the dual-purpose valve box and i n t o the waste gas f lue and exhausted through the stack.

B las t furnace gas and a i r are fed i n t o t h e i r labeled The opposite f l u e i s used f o r

.1

4

‘7 \.-

11. Process Description ( C o n t . )

the survey.

schedule d u r i n g Tests 4-6.

Two ovens were charged b u t removed from the push

For safety reasons, no pushing operations are allowed while

wall repairs a re being performed. Because of t h i s , the oven

charge times and coking durations a re , by necessity, a l tered t o

conform w i t h allowable push times.

could only be performed dur ing daylight hours a f t e r 2 p.m. when

Consequently, stack t e s t s

construction was finished fo r the day.

were increased to 24 hours o r more on most ovens as opposed t o

the normal 18-hour coking times typically observed on t h i s

battery.

As a r e su l t , coking times

-Table I is a sumnary of operating data pertaining t o t h i s

survey. Additional operational information appears i n Appendix F .

5

... . i

Table I

Process Operation Sumnary

P a r t i c u l a t e Emission Test November 29-December 2 , 1982

Rouge Stee l Company--Coke Ovens--B Combustion Stack

Test Number Test Date

Enriched Blast Furnace Gas

1 2 3 4 5 6 Units 11-79-82 11-30-82 11-30-82 12-i-82 12-i-82 12-2-82

774 96.0 #fl/Ct In tegra tor Flow x 100 81 2 789 761 737 858

BTU Content ( Cal orimeter) 98.6 94.9 93.6 93.9 94.1 BTU Contenti Lab Analysis ) 108 114 114 118 118 ---- BTU/CF

Waste Heat Temperature

Pusher Side Coke Side

530 515 514 526 531 529 O F . ' 460 428 436 439 440 443 OF.

Number o f Coke Pushes 5 5 3 6 2 6 ,' Number o f Charges 5 4 3 7 3 6 L-

Average Weight o f Coal per Charge 33,300 33,100 30,100 33,400 33,000 33,600 Lb

. . . . _ . . . -

. . . .

6

-.., : I

111. Summary

The measured and calculated results of this survey are

sumnarized in Table 11.

.035 to .065 lb./1000 lbs.

with the average opacity ranging between 11 and 40%. All pertinent

data and calculations can be found in the appendices to this

report.

The particulate emissions range from

The opacity varied from tes t to t e s t

- . .. . -

7

Table I 1

S u m r y o f Results

i


1 2 3 4 5 6 11-79-82 11-%-82 1130-82 2-i-82 12-i-82 12-7-82

Emissions (Lb./1000 Lbs.) .046 .065 .049 .035 .043 .055 Average Test Opacity (%) 20 40 38 11 25 25 Maximum 6-Minute Opaci ty (%) 29 49 43. 32 50 51

Ovens Charged per Test 5 4 3 7 3 6

Six-Test Averages

Stack and Production Data

Exhaust Gas Flow 110,000 ACFM 63,900 SCFM

Exhaust Gas Temperature 424 OF. Moisture Weight o f Charge Fuel Usage Rate

7.6 % 32,800 Lb.

789,000 CFH

. . ... . . . .. . . . . -..

a

I V . Results

S i x p a r t i c u l a t e t e s t s were perfonned i n t h e four-day per iod.

The i n d i v i d u a l t e s t r e s u l t s along w i t h the s ix-minute v i s i b l e

emission readings a re presented i n the tab les t h a t f o l l o w .

taneous v i s i b l e emissions and opac i t y cha r t s a r e i nc luded i n

Appendix E.

Instan-

Supplemental i n f o r m a t i o n showing the sample p o r t and p o i n t

l oca t i ons , sampling and a n a l y t i c a l procedures, f i e l d and product ion

data sheets, sample c a l c u l a t i o n s , and equipment c a l i b r a t i o n a re

shown i n t h e remaining appendices t o t h i s r e p o r t .

. .. .- ~ .. . . .. . . . . . - .. -. -... . . . I

9

Table 1I;A

ROUGE STEEL CIMPWY -- COKE OVENS -- B COMBUSTION STACK STACI WS VELOCITY bND FLOY RESULTS

..-.

PHYSICAC DATA C

WTE OF TEST

TIRE Of TEST

MRlsEp OF RAVERSE POINTS

PITOT TlJE CMfFICIENT

KRSVPED DATA ~~

B(\RrnIC PRESSURE

STAU DIUlEfCll

STnCK STMIC PRES3LmE

STACK CAS EWERATWE

CIILCULArn #TA ___________ 5 T K K US PRESSURE

MOISTUllE

EXCESS A I R

DRY rnLuar,n EIGHT

YET MNEtIJLAR UEIGHT

*VERNE 59. ROOT OF VELOCITY PRESSURE

STACK CROSS SECTIONAL bREA

S T M CAS VaOCITY - S T M UJND.

STACK CAB VELOCITY - STD. am. STACK CAS FLW - STACK COND. STAU Sag FLW - DRY STD. COND.

s1m CAS FLOY - Yn STO. m.

UNITS

S T M T FINIS)(

INCHES Wt

I)(c)(ES

II(MS WO

DEG F

IWCHES Hc

MLURE x z

LBILB-MOLE

LBILB-MOLE

1M.WO.. .s SO. FT.

FTlilIN

FTIMIN

ACFM

DStFil

YSCFil

TEST WVnBEP 1 2 3 AVERAGC

lIIzpIR2 11/50182 11/30182

141s 1520

12

# . E l

29.0s

1 3 2 . 6

-6.74

421.

29.10

6.6

t ( 6 . 0

29 .00

28.27

8.260

95 . I 3

1126.

658,

116600.

57708.

b i a a o .

13SS IS07

12

0.80

29.32

1 3 2 . 0

4 , 7 4

419.

29.27

7.8

230.0

2 9 . 0 0

28.15

0.290

9S.03

1230.

722.

117eoe.

63300.

moo.

1640 1749

12

0 . 7 8

29.32

132.E

-8 .74

420,

29,27

7.7

220.0

2 9 . 0 0

28.16

1.2S6

m.03

1060 .

622.

l o l o e e ~

S4SOO.

59100.

421.

7.3

219.7

29. 60

a.1v

0.269

1140.

665.

toaoeo.

smoo . 63200.

.. * . . 10

PHYSICAL DATA ----- DATE OF TEST

T I M OF TEST

Table I I IB ROUGF STFEL COftPRNY -- COKE OVENS -- B COMBUSTION STACK

STACK CAS VELOCITY AND FLOY RESULTS

NUMBER O f TRAVERSE POINTS

PITOT TUBE COEFFICIENT

MAGUREB DATA ------- BAROMETRIC PRESSURE

STACK DIAMETER

STACK STATIC PRESSURE

STACK CAS TEMPERATURE

WITS

CALCULATED DATA --------I--- .. STACK C&S PRESSURE

W I S T U I I E

EXCESS A I R

DRY N O L E C U M YEICHT

MET noLEctnna YEICHT

AUERAGE SO. RDDT OF VELOCITY PRESSURE

STACK CROSS S E C T I O W L AREA

STACK CAS VQPCITY - STACK COND.

STAEK co18 VELOeITY - 610. WWD.

STKK CAS FLOY - STACK CUNO.

S T K K WLS FLW - DRY STO. CmCD.

STAn U S ROY - YET STD. CUND.

U + + U + U + + ~ + m ~ + * u ~ - * u + ~ + ~ +

+U+tUU+*UI+Ulrn+U++U~++++~+*u+~U STWDMD COWDITIONS~ ~1 DE^ F nm n.92 IN. ~6

S T M T F X N I W

TEST hlMEEII 4 5 6 AVERAGE

12/01/82 12/01/E2 12/02/E2

1358 1643 140b 1SlO 1751 1513

12 12 12

0.80 0 . 7 8 1.78

INCl iES HC 29.40 29.40 29.48

INCHES 132.0 132.0 132.1

INCHES H 2 0 -0.74 -0.74 -0.74

KG F 428. 426. 430. ' 4 a .

INCHES HG

WLum x 7.

LBILB-HOLE

LB/LB-WLE

IN. m.r. 5

w. n.

F T I U I N

F T l l l I N

Am

PScFn

ysm

29.35

7 . 9

~ 0 . 0

2 9 . 0 0

28.14

0,273

95.03

1160.

678.

110000.

59400.

64400.

29.35

7 . 9

230.0

29.00

28.14

0.m

95.03

1170.

683.

111000.

SPEOO.

b4900.

B . 4 3

7 . 9

lEO.0

29.00

28.14

0.281

95.83

1170.

bel *

lll8OO. '- 59600.

b4700.

7 . 9

210.0

2 9 . 0 0

28.14

0.279

1170.

681.

~111000 .

&boa.

M700.

. . . ,_. . . 2 - _ . . . . . . . . > . . . . . . .

. I

PHYSICAL MIA

11

Table I V A

ROUGE STEEL COWANT -- COKE OVENS -- B COMBUSTION STACK

PAl lTICULATE S A N P L I W RESULTS

TEST NUMBER LMITS 1 2 3 AVERAGE

DATE OF EST 11/29/82 11/30/67 11150182

TIME OF E S T

NOZZLE D I M T E R

IR4Su)ED WTA --____- KTERED W L E VOLUME

START 1415 1JJS 1640 FIWISI( 1520 1597 1749

INCWES 0.4990 0.4990 V.4990

CU. FT. 47.044 48.721 45.582

RTER CORRECTION FACTOR

AVER(Ic€ O R I F I C E PRESSURE DROP

VOLUME OF W21 CONOENWTE IR 61 . O 7S.O 68.0

I. YEICWT OF IW ADSORBED GRABS 10.6 12.4 12.7 .. . ...,

TOT& WLE TIME

PPOBE YAW E I G H T

YEIGHT, F I L T E R CATCH

H I W T E S 60.0 60.0 61.0

BAKS 8.0564 0.0304 0.0234

C R A W 0.0415 0,0847 0.0576

CALCULATED M T A I_______----

METERED W L E WLUM - STD. CUND. W . FT. 47.736 ' 49.100 45.900

TOTAL WLE CORR. WL. - 6TD. COWD. CU. FT. 51.116 S3.226 49.710

TOTAL P W T I C U L A T E YEIGHT GRAMS 0.0779 0.1151 1.0811

PARTICULATE CCUC. - S T W tom. GRIACF 0 .0137 8.0196 0.9148 9.0160

P w x c u L m YEIW conc. - RT STD. corn. WI~OMWT 0.0478 e.iaeb 1 . m 0 . 0 ~ ~

P Y T I C U L A T E YEICHT CONC. - YET STD. COND. 011000tYET 0.0458 0.0652 0.0491 0.0534

PAl lTICULATE FLOY RATE L B I H R 12.4 19.6 12.7 14.9

NOZZLE WE4

I S O K I E T I C RATIO

SO. Fl. 0.081358 8.9013S8 1.001358

x 96.5 P0.4 98.2 9 5 . 8

. . .. . . . , ; .,,

.. 0

12 Table I V B - -. . - -

ROUGE STECL C W A N I -- COKE O W N S -- E CO~BUSTIOW STACK

PHYSICAL DaTL I-___---

DATE OF TEST

T I E OF TEST

WZZLE D I M E T Q

PARTICULPTE SAMPLIHC RESULTS

TEST wnm UNITS 4 5 6 4VERff i .Z

12/01/82 12/01/82 12/02/82

START 1358 i643 1406 F I N I S H 151 0 17Sl 1513

INCHES a.mo 0.4991 4.4990

EASURED DATA ------ METERED S W L E VOLUIE

AMRACE KTER E M P E R A T W E

WETER C P R f C T I O W FAeToll

N E P ( u x M I F I C E P R E S N P E DROP

MLv)(E LW Ht4 CONDENSATE

YEICHT OF H2O ADSORBED

TOTAL SAMPLE T I N E

PROBE y(LsI( E I G H T

E I G H T , FILER CATCH

.

_I

i CALCULATED 0614 ____---_-I_

RUERED w P L E umw - STD. WD.

TOTAL MMPLE CORR. WJL. - STD. COND.

TOT&L P W T I W L A T E YEICWT

PARTICULATE COWC. - STACK COND.

P W T I C L R A T E YEIGHT C O K . - MY STD. MIND.

PARTICULATE YEICHT CONC. - Yn STD. C W D .

PWTIWLATE FLOY RATE

lRnZLE MEA

I~INETIC umxo

CU. FT.

DEC F

CU. FT.

CU. FT.

GRANS

GRIPCF

W10001DRY

*/lOOO*YET

LB/HII

59. FT.

I

49,156 50.560 50,396

66.3 63.4 67.6

0.9W1 ,0 .9971 0.9971

2.45 2.48 2.48

74.8 7 5 . 4 n.1

13.8 15 .9 15.1

6O.U 60.0 6 0 . 0

4.0280 0.0236 6.0385

0.0332 0.0534 0.0609

48.610 50.280 49.056

s2.754

0.0612

O.PI04

0.0369

0 . O m 9.86

O.OOl3S8

95.5

54.571

4.0771

0.6127

0.1448

0.0426

12.1

0.001358

98.1

54.119

0.1994

0.016f 1.8152

0.8SE4 0.8467

1.0554 0.0443

15.7 12.5

0 . oatae

97.5 97.1

I --.' ~ . . . . . ..

- :


Minutes I

0-6 6-12

18-24 24-30 30-36 36-42

48-54 54-60

12-18

42-48

Average

13

Table V

Opaci t y S i x-Mi nute Averages B Combustion Stack

November 29-December 2, 1982

1 2 3 4 5 6 11-79-82 11-70-82 11-30-82 12-i-82 12-i-82 12-7-82

17 49 24 46 18 48

17 31 29 37 23 35 14 49 14 34 25 30

21 38

20 40

* Observations not taken a f t e r dusk.

Opacity (%)

37 12 41 5 38 3 36 4 35 4 43 6 43 32 40 25 33 14

a

38 11

14 6 10 12 10 25 8 15

26 15 50 15 41 30 38 45 * 51

39

25 25

,.--. ! \c.

V . Oiscussion

The survey was conducted on four consecutive days beginning

November 29, 1982. All s ix tests were within the allowable l imit

o f .IO lb./1000 lbs . , varying from .035 lb./1000 lbs . t o .065 lb . /

1000 lbs.

from as low as 0-10% on test four, t o as h i s h as 30-50% on tests two and

three.

The opacity during the six tests covered a wide range

All o f the sample t r a in leak checks were w i t h i n the allowable

l imi t of .02 cfm. However, tests three and four were leak checked

a t the cyclone bypass since the sample t ra in f a i l ed the leak check

a t the nozzle.

fee t , and test times were s ixty minutes. Isokinetic ratios were

All sample volumes were in excess of t h i r t y cubic

a l l within the 90-110% l imi t .

As mentioned previously i n the process description, t h i s survey

These operations was performed in association w i t h oven wall repairs.

prevented the pushing o f any ovens on "B" Battery between the hours

of 7 a.m. and 2 p.m.

unti l a f t e r the f i r s t oven was charged in the afternoon.

readings corresponding w i t h tests three and f i v e are incomplete

as a r e su l t of the tests being concluded in darkness.

As a r e su l t , stack tes t ing did n o t begin

Opacity

- ~. . .______ . . . . .. - . . ._i.-_ ..~ .. .... I -

15

APPENDIX A

LOCATION OF SAMPLING PORTS AND POINTS

,,-\ ...

. -_ . . . .. . - ~. .

16

('

, APPENDIX A

LOCATION OF SAMPLING PORTS AND POINTS

The sampling s i te is greater than 9 duct diameters downstream from

the l a s t major flow disturbance.

Method 1 o f the "Standards of Performance for New Stationary

Sources." Federal Register, a total of twelve velocity and sampling

points were considered adequate.

For this reason and based on

Schematic drawings showing both the sampling port and sampling po in t

locations are presented i n Figure 2 and 3, respectively.

. .

--.

17

FIGURE 2

COKE OVEN COMBUSTION STACK B SAMPLING PORT LOCATION

225' r I 100' i

I.D.

Level -

18 FIGtiRE 3

COKE OVEN COMBUSTION STACK 8 LOCATION .OF SAMPLING POINTS

. _. . . ._ . - . . . . .

- - -

I I

SAMPLE POINT NO.

1 2 3

132" I .O.

DISTANCE FROF! STACK WALL

5-314'' 19-114'' 39-118''

.

,.-.. \

19

Appendix B

Sampling Procedures

Particulate Sampl i ng Train

The following parameters are measured during the par t iculate emission

survey:

o

o Moisture Content

o Particulate Emissions

Exhaust Gas Velocity, Temperature, and Flowrate

Velocity and flow measurements a re consistent with Methods 1 and 2 of

40 CFR, P a r t 60, Appendix A.

precalibrated S-type p i t o t tube a t the recomnended number of traverse

points.

S tack velocity i s measured w i t h a

Isokinetic sampling conforms t o Method 5 procedures. Exhaust gas

is extracted from the stack through a nozzle and heated glass-lined probe.

The sample then passes through a heated 115mn Gelman Type AE glass f ibe r

f i l t e r .

Figure 3 ) .

Four impingers of a modified design follow the f i l t e r (see

The moisture collecting impingers a re placed i n ser ies in an i c e

bath. The f i rs t two each contain 150 ml of d i s t i l l e d water. The th i rd

impinger is l e f t empty. About 200 grams of s i l i c a gel a re contained in

the fourth impinger.

The clean, dry exhaust gas passes f ina l ly to the metering portion o f

the sampling t ra in .

meter, and calibrated or i f ice .

by a SybronlTaylor Model OA570 oxygen meter.

T h i s consists of a leakless vacuum pump, d ry gas

A portion o f the gas i s analyzed immediately

PO

Appendix B (Cont.)

S i x thermocouples a re l o c a t e d throughout the sar!!pling t r a i n as

shown i n the drawing (F igu re 3 ) .

potent iometer w i t h d i g i t a l readout mounted on the face o f t he meter box.

A lso on t he box i s a twin- tube manometer which i s used t o mon i to r stack

gas v e l o c i t y pressures and o r i f i c e d i f f e r e n t i a l pressures.

They are connected t o a m u l t i p o i n t

A l l sampling t r a i n l e a k checks a re consis tent w i t h Method 5 procedures

and s p e c i f i c a t i o n s .

. . ._ . . . . . . . . .

. . . ~ ~ . . . . .

~ --... ._/__ _. . . __

22

APPENDIX C

ANALYTICAL PROCEDURES

- .. .. . . . . .- -..- - . . . . . . - . - . . ____ .. ._ ,.-___.

. . ~ . . . . -.

23

Appendix C

Analytical Procedures Part iculate Sampling Train

1 ,-,

I - -

Particulate Analysis

Analytical procedures are consistent with Method 5 of 40 CFR, Part 60,

Appendix A.

After the conclusion of each tes t , the sampling probe i s disconnected

from the cyclone, bypass assembly, and nozzle.

probe liner are washed thoroughly w i t h a known quantity of acetone.

r inse i s transferred t o a clean sample bot t le and labeled accordingly.

The cyclone, f i l t e r assembly, and flask are disassembled, capped, and

labeled for t ranspor t .

grease d u r i n g disassembly.

The nozzle and glass

T h i s

All glass j o i n t s are wiped clean of s i l icone

In the laboratory, the glass f ibe r f i l t e r i s removed from the f i l t e r

assembly and returned t o i t s original aluminum fo i l envelope.

being placed in a drying oven maintained a t 105 C. f o r two hours, the

f i l t e r is removed t o a desiccator and stored overnight prior t o we igh ing .

The f i l t e r is then weighed on a n analytical balance having a sens i t i v i ty of

0.1 milligram.

After 0

The corresponding f ront f i l t e r holder half and cyclone bypass are

washed w i t h a known quantity of acetone.

appropriate sample bot t les .

to dryness, below the boiling p o i n t , in tared porcelain crucibles. The

crucibles are then placed i n a desiccator overnight and weighed on an

analytical balance. A weight correction i s made for the blank.

These rinses are added t o the

The acetone samples and a b l ank a r e evaporated

24

Appendix C (Cont.)

Mois ture Analysis

A n a l y t i c a l procedures a re c o n s i s t e n t w i t h Methods 4 and 5 of

40 CFR, P a r t 60. Appendix A where appl icable.

The s i l i c a ge l i s re tu rned t o i t s o r i g i n a l conta iner and prepared

f o r t ranspor t .

f o r each t e s t by measuring the condensate volume increase i n the f i r s t

three impingers o f t he c o l l e c t i o n t r a i n and the weight g a i n o f t he s i l i c a

gel i n the f o u r t h impinger.

Mois ture percentage i n the exhaust gas i s determined

. Enriched Bast Furnace Gas Analysis

The ovens i n "8" B a t t e r y a r e heated by enriched b l a s t furnace gas.

-, 1. .,'

A sample o f t h i s gas i s obtained on a d a i l y basis by the Rouge Coke Oven

Laboratory.

C2H6 i n a d d i t i o n t o determining BTU content of the gas.

, . The l a b analyzes f o r H2, 02, N2, CO, CH4, C02, C2H4 and

. . ... .. . .~ . .---. - .

25

{- ../.I

APPENDIX D

F I E L D DATA SHEETS

... __ . . __ - ... . ..

\ f FORD MOT Z6 R COMPANY

STATIONARY SOURCE ENVIRONMENTAL CONTROL O F F I C E

NOTES -

/- \

(-. . .

ORIFICE COEFFICIENT 'CHECK

L e .

AH = 10.03175) (Ah) ('bar)

FORD MOTOR COMPANY

Fi 1 ter Type I @r//r&,& Sample Box No. / Nozzle Diameter , # 8 ~

Filter No. a Probe No. I Nozzle Material SS

Cyclone & Flask No. / - Probe Material f y k V Meter Box No. z

Sil ica Gel No. 2 Probe Lenqth 5-/ Meter Box AH /. 32

STATIONARY SOURCE EN\IIRO!iMENTAL CONTROL OFFICE

Plant: h ’ r n .Date: ;/- 2 5 - F7- Initials: DSCU -W Test No.: /

..

7 Samolina Train Information I

27

I....

Li L:

L

! -

...~ .. - ... .

,-..

29 FORD MOTOR COMPANY

STATIONARY SOURCE ENVIRONMENTAL CONTROL OFFICE

SOURCE d.ls. % c , c B PLANT / I C 0 DATE N-30 I N I T I A L S ~ s J - * b TEST NO. d

NOTES -

2 (Tm-avg + 460) 9 ("m) (Pbar + Ahfl3.6)

AH = l0.03175) (Ah) ('bar) (T,-,,t+ 460)

e r 2

-I

1

1 AH = 10.03175)

AH =

--__ ..

Filter Type I&/,,-d4s Sample Box No. 2 Nozzle Diameter .Ha& Filter No. 87 Probe No. 2 Nozzle Material 5 5

r . a. 2 Probe Material &k?z Meter Box No.

&Silica Gel No. 3 Probe Length 7 ' Meter Box A H / 82,



Source: &w&. S ~ C K B Plant: RCO Date: I / - 30 - B L Init ials: >sw -%MJ Test No.: a

,-..

W V

U U 0

-

>. CL U z e 4 e in

E:

31

\ U

In L

c

C

0 c

OIC O Z I-- uo

I- V U

ul

zn 2 . se

I

NhJ

h ' n r'

I-

$/$

-!-

-e

r- ..

~~ ~

. . . - .



SOURCE &t? SVKK 6 PLANT RC 0 DATE //- 33 - 8 2 I N I T I A L S 3 5 ~ ' - ZW TEST NO. 3

2 ( T m - a ~ g + 460) 8

"m) ('bar t 'hP3.6) AH = 10.03175) (Ah) ('bar)

(Tm-out+ 460) c r d 2 1

AH = 10.03175)

AH =


F i l t e r Type I &/E ,,rs;ns Sample Box No. 1 Nozzle Diameter .62L

F i l t e r No. pg Probe No. 3 I4ozzle Ma te r ia l SS

Cyclone & Flask No. 3 Probe M a t e r i a l prey Meter Box No. 2 - S i l i c a Gel No. f Probe Lenqth 7 ' Meter Box AH /.?a

~ ..


I-

L

P. .. Source: YLP .-%c.K 0"

Plan t : RC 0

Date: //- 3c -2a- I n i t i a l s : 2 1 s ~ - *J

Time Reading Date Prel im. ..---

t

Meter and o/ c O r i f i c e OK

Surge Tank 0 /c r

Pump and

Test No.: 3

r Leak Test D a t a 1

Meter Box, Cord, Sample Box, Probe

P i t o t Tube Tota l Pressure L i n e

P i t o t Tube I S t a t i c Pressure L ine

I n i t i a ; 1 Time I F ina l I Time , { Readin Readin

I Imoinaer Data 1

- .\

.+-.

..

\

35

I

1

- .

i.. L'

I

W V

LL LL 0

I

I-

Y) ? h

1 1 1 1 I I I I 1 . 1 I 1 1 1 I


STATIONARY SOURCE ENVIRONMENTAL CONTROL O F F I C E

AH = 10.03175) (Ah) ('bar) (Tm-out+ 460)

SOURCE &Y,+ ~ M C A B PLANT Beco DATE /a-/-ad INITIALS p ~ u - V%l T E S T NO. 4

2 (Tm-avg + 460) e ("m) ('bar + Ah/13.6)

i AH = 10.03175)

AH =

I - .

Impinger Number

Final Volume (rnl)

Volume to1 lected(m1)

Impinger Contents

I n i t i a l Volume (rnl)


STATIONARY SOURCE ENVIRONNENTAL CONTROL OFFICE

Source: 4n4.4 5,mcx R 7 Plant:

Date : - - I n i t i a l s : &w% Test No.: ’ ,y I

1 2 3 4

/ f z D nc? 0 / S i l i c a Gel ‘VS- xz- ci7 ,Z&-$6

-5 / z ?7 / 3 . 23 1- /J-t, - 240.2-

1 Irnpinger Data 1

1 Total I

39

I a I l l

0 In 0 0 N N

I I I I 1

5: 0 0 ul I

0 \ r

->

Y

U LL 0

2

=I- O Z I-- V O un Y I-

V Y vl

$-

41

FORD MOTOR COMPANY STATIONARY SOURCE ENVIRONMENTAL CONTROL OFFICE

PLANT r(L

TEST NO.

NOTES -

'._._

AH = 10.03175)

AH =

F i 1 t e r Type k/g {if 4 4 Sample Box No. / Nozzle Diameter +.$a& F i l t e r No. Probe No. / liozzle Mater ia l 55

Si l ica Gel No. L Probe Length Meter Box AH 6 PL ,Cyclone .5 Flask No. Probe Mater ia l jfW Meter Box No. i?

I

I Leak Test Data

P i t o t Tube Stat ic Pressure Line

'._.I

L

S I a

43 i t - + I

I 1 1 1 1 L

\ U

0 v) 0 l-l ru N

I I I I 1 1 1 1

0 L n

0 5: 1

In 0 c -

11111111 ,

J Z :a

I I

45

FORO MOTOR COMPANY STATIONARY SOURCE ENVIRONMENTAL CONTROL O F F I C E

SOURCE .<bwc /? PLANT R c o DATE /&-& - 82 INITIALS L J -* T E S T NO.-L

c

I 1

c

I' 1 '

AH = f0.03175) (Ah) ('bar) (Tm-,,t+ 460)

AH = 10.03175)

AH =

- ' f

Filter Type 1,9/gns dLLLff Sample Box No. Nozzle Diameter v r p ~

-Cyclone ti Flask No. 6 Probe Material &&f Meter Box No. z, Filter No. / u / Probe No. / Nozzle Material 53

7 Meter Box AH 4 q-



Filter Type 1,9/gns dLLLff Sample Box No. Nozzle Diameter v r p ~

-Cyclone ti Flask No. 6 Probe Material &&f Meter Box No. z, Filter No. / u / Probe No. / Nozzle Material 53

7 Meter Box AH 4 q- .Silica Gel No. Probe Length 7 / .Silica Gel No. Probe Length 7 /

Prelim. Reading

Meter and I Orifice <-

I '

_I

.-

I Leak Test Data I

& Meter Box, Cord, L - e O r

Pitot Tube d/Cd

Pump and Surge Tank

Sample Box, Probe

Total Pressure Line

Pi tot Tube Static Pressure Line

3- /rO

0 IC

I Total I I

..- .

47

\ I

I

L

i z r U Y

3 v1

L C c c

.C

a a c

v

-

I 3 C a . -

- n

49

APPENDIX E

OPACITY DATA SHEETS

. . ~ . . ~ . . . .... _ - ~

50 ,.-A

, I

-. _.

_. c

!:

.-

ROUGE S!EEL C m A N y ENVIRONMEIiTAL CWL;LANCE

VISIBLE ~ S S I O N RE~DINGS N O u . aq, I r a 1

S40KE AND/OR EQUIVlLerr OPACITY N O . \

Date ii 19-82 Teat number I Location c o c F a u € ~ I

Observer SCl,f7InYR Stack No. B Corn&. STX

Observer Certification Date 7 / 3 2

\ ,

Observation Poin

Obeervation Began

Process Exh. Volume Plume : Color -

: Distance Visible : Attached

Relative Humidit

' / .. t !

51 nsmu MISSION WINGS WOV 79 1-7.: SMOKE AND/OR EpUIVLLEKl OPACITY

T E S T , J C 1 Co*,T'Q-

Date I I J7! S L Teat number 1 Location Observer Stack No.

Observer Certification Date

Observation Point

Obaervation Began

Plume : Color : DiEtance Viaible : Attached ;Detached

_- ,

Relative Humidity

B6CKgtOund bescription

I _.'

Date 1 1 - 8 , . - Teat number 1 Location C O F F O a ~ r n L

Observer c -6 .a r n t Stack No. e ’ c o m o - : rc

Observer Certification Data ‘i’2

Observation Point

Observation Began

Plume : Color - : Distance Visible- : Attached ;Detached

\-,

Relative Humidit

_I

aacxpound kacription

Date II/L , - Teat number 1 Location Observer Stack No. Observer Certification Date

Observation Poin

ObeeITatiOB Began

Plume : Color : Diatance Viaible

‘.- : Attached ;Detached

Relative Hlrmidity

aac&ground Ueacription -

---

..

.-. , .

!

0 L'

' i ....

. . - ... . . ._ . __ . . . .

54 ROUGE S m L CQ4T'Lnly

EIWIRONbENTAL CCI,FLIANCE

VISIBLE WSSION READINGS

SMOKE AND/OR EQUIVALENT OPACITY

Observer Obeerver Certification Date

Obeervation Point Fd57 hF ( / 4 / . f 7 g / c TZaJd. - /J//- n/ -n, rr4- a. Ri.& ,

Shck Di.. I(!: Height b-r--

Observation Began & 4 S - Wed I

Distsace From Stack f I & I e '

Control 4 u i p .

Procees

Plum : Color Exh. Volume U F U ; ' F .

: Distance Visible : Attached ;Detached

sky Condition o L / E P YindSpeed 6-5( rn Vind Direction df 4

Temperature 5-5- OF.

Relative Humidity *'

CC ~7

Remarks:

baclrground hecr ipt ion

+ €.ai? 9 - 4

vxsmm MISSION FEADINCS

SMOKE AND/OR EQUIVYENT OPACITY

Date Teat number 2’ Location Observer Stack No. Observer Certification Date

Observation Point

Observation Began Ended Dirtonce From S b c k

Stack Dia. . Height Control Quip. Process &. Volume ami- OF.

Plume : Color .

: Distance Visible x Attached ;Detached

Sky Condition Vind Speed mi

Temperature OF.

Relative Humidity z

Vind Direction

Remarks:

bacrgrouad bescription

_ ' , 56 -

ROUGE STEEL C m m

nsmm ~ S S I O N R E U ) ~ G S

ENVIRONMENTAL COMPLIANCE

i? D E c I , 1982

TE.i7. NO, , '..

SMOKE AND/OR EQUIVILENT OPACITY - Date 11-1-32 Test mber 1 Location C o w E O V E N 5 - . E c o m a , S'.' Observer 5- <'R Stack No. .. Observer Certif

Observation Point

M. Volume Plume : Color : c : Distance Visible

: Attached

Relative H u m i d i t . . L f C I i i 51°F C 1 . L ;

:C) :,; ( 5,: T

fi 971 Pol: r

nacrground Description L

. - ... ._. .. . . __ -

Date 12-1-32 Test number 1 Location Observer Stack No. Observer Certification Date

Observation Point

30Vs 2 - Observation Began Ended 3 Distance h m Stack 4 - Stack Dia. Eeight 1. Control Equip. 6

C- Process kh. Volume A C C I H ; * F . 8 Plume : Color 9

: Distance Visible 10

: Attached ;Detached 11

Slqr Condition - 12

Vind Speed m >

Relative Humidity $ 3 2

.. L 1 5 1 i I,',. la

L - -

Vind Direction 14 Temperature *F. 15

m

19 * ' I '!,-I ;,'I,- Ramarks :

A

I -

128 b6c~gound hacr ipt ion

129

L

c

E

..

! \./'

. .

... .

v I s m m MISSION READINGS SMOKE AND/OR EQUIVaLENT OPACITY

Date / /Teat number Location _L, Observer Observer Certification Data

Observation Point

Obaervation Began 4 4 & Wed Diatance Fron Stack

Stack D i a . Height *

Control Equip. Process

Plume t Color EA. Volume sw- *P.

: Diatance Viaible : Attached ;Detached

Sky Condition Uind Speed WH

Temperature *P. Relative Humidity L

Uind Direction

Remarks:

bac~grDund kacription

Location Cs G F 2 T; < - - Uate 4 6 7 : Test number 1

Obsener 5 h v r? m ,,6 Stack No. 'R COPY ->ll.cA

Observer Certification Date

Observation Point

Observation Began

Plume : Color : Distance Visible

Vind Speed Vind Directio

Relative H u m i d i t

~ ~ ~ g o u n d Deecription

I. .. ,

60

VISIBLE MISSION READLliGS _ _ . - " 7 - -- - - - . _ S H O U AND/OR EpUIVUT OPACITY

Uate 1 2 J . Teet number Location Observer Stuck No. Observer Certification Date

Observation Point

Observation Began Ended Distance Pmm Stack Stack Dia. Xeight Control Equip. Process

*F. - M. Volume urn; Plume : Color

: Distance Visible : Attached ;Detached

Sky Condition Uind Speed m

Temperature *F.

Relative Humidity %

Uind Direction

Remarks:

aaclrground hncription

. ... ~. - . . .

i

:. . . . > : . - . , I .

-. .. , i : 8. -

I .

APPENDIX F

'-PRODUCTION-DATA

. .. . . . .. -

.-.. , .I

.

W W U Y

E V L L L c1 VI= VI VI*.'

m o

a w a

66 FORO MOTOR COMPANY

STATIONARY SOURCE ENVIRONMENTAL CONTROL OFFICE COKE OVEN COMBUSTION DATA

PAGE 2

S t P P l ,~G,owo-*

Plant : No. o f Ovens: lo! - I @ 8 c.7 43

Bat te ry : No. of Reversals: e .. Test No: I Name : 13K2 Date: lI/aq/gL

W a l U Y

T U L L L c1 V I S V I m e

m o

a w a

Y U 0 V ?

433 3'q p I- t=

n.iw % 9k.b 2.7 7 . 3

i

c.0 ,c\ 5icr,

W L v) u) W L P

C W a J V > .r o m a J W Y Y 0 0 u v

a

- -

1

hrs

!

i


STATIONARY SOURCE ENVIR0NME;lTAL CONTROL OFFICE COKE OVEN COMBUSTION DATA

PAGE 1

Plant: No. o f Pushes:

Bat te ry :

T e s t No: Date:

0) E I-

Y U 0

V

- 7

VI

8 E ala > L

VI a ! m

Y a l O L

o a

vn

14 0 I3 8 13 I, 13.8 dl I3 -8

t

No. o f Charges:

Name :

+



PAGE 2

Plant: R O U C P ?>l'ep I No. o f Ovens:

Battery: 8 No. o f Reversals:

Test No: 2 - 3 Name: D t 2 Date: I \ /30 /82 ..



PAGE 2

Plant: No. o f Ovens:

Battery : No. o f Reversals:

Test No: Name :

Date:

. . . 2

h - : ?

70

STATIONARY SOURCE ENVIRONMENTAL CONTROL OFFICE FORD MOTOR COMPANY

COKE OVEN COFlBUSTION DATA PAGE 2

J & d U , > ! , P l a n t : 6 tCP I No. of Ovens: ...

' 5 A i s l Battery: R - . No. o f Reversals: 15 ir Wu

Test No: 4-5 Name: JT~ 2 Date: I ~ / I / S A :

1 :

2.2.

,e 7 1 FORD MOTOR COMPANY


PAGE I

Plant : No. o f Pushes:

Ba t te ry : No. o f Charges:

Test No: Name : Date:

72 FORD MOTOR COMPAf!Y

-..


L - -

- I

i

PAGE 1 '*

P lant : RC u L Step-1 Bat te ry : R Test NO:

Date: 1 3 . / C l I L / J d .

'~ No. o f Pushes:

No. o f Charges:

Name :

.r ala a w W L I L L o a a

Y m c , m v w m m v l

m w mp&u, v v n m n

Nu+ ' 3 h Actual mnH 0 H 0

0F Gar - O Y w O L - L

-- -

j 14:3c.

34 7 I I 427 '

..

I I I I

1

L

!0.5 10.5 IO. 5 -


COKE OVEN COMBUSTION DATA STATIONARY SOURCE ENVIRONMENTAL CONTROL OFFICE

PAGE 1 ‘,

P l a n t :

Battery:

Test No: Date:

No. o f Pushes:

No. o f Charges:

Name :

a. a. 2 .a

I

flTllH70 CFH W

2.0 a . 2 2.1 22 2.1 22.2 2.1 2.2 & . I 2.5 2.1 2.2 2.0 2.2

2 . \ 2, L I I

74

. - . . . ..... . .

APPENDIX G

LABORATORY DATA ANALYSIS - .

63

I I I I - .. ....

.- -- . . -. . I_ - . . . .

-, . ..

11-29-82 10 a.m.

7.75 .76 50.75 21.34 1.42 17.97

76 Table V I

Enriched B las t Furnace Gas Composi t i o n

Coke Ovens Laboratory

11-30-82 8:35 a.m.

8.12 .73 49.67 22.33 1.62 17.55

12-1-82 8:40 a.m.

9.27 1.05 49.26 21.36 1.91 17.15

Average Average

8.38 0.85 49.89 21.68 1.65 17.56

8TU/CF 108 114 118 113

.

APPENDIX H

SAMPLE CALCULATIONS

7a

SAMPLE CALCULATIONS ................... GAS FLOW ANALYSIS

SOURCE - ROUGE STEEL COMPANY -- COKE OVENS -- B COMBUSTION STACK TEST - 1

MEASURED OATA ------------- STACK DIAMETER OS 132.0 IN.

STACK GAS TEMPERATURE TS 420. OEG F

STACK STATIC PRESSURE PSP -0.74 INCHES H20

BAROMETRIC PRESSURE PBAR 29.05 INCHES HG

PITOT TUBE COEFFICIENT CP 0.81

AVERAGE SO. ROOT OF VELOCITY PRESSURE DELPV 0.260 IN.H20.*.5

(..

.. . .. ...... .~ . . Y

79

r- . L I

. . . . .- . . . . .. - . - . . . - . . -

SAMPLE CALCULATIDNS ----------_-------- STACK GAS FLDU OS ........................................................................... OS - VS . A S

OS 0 1117. 95.09

OS = 106200. ACFM

STACK GAS FLOW AT YET STANDARD C 0 o I T I D N S OUSTD ........................................................................... WSTD = VSTD AS

WSTD - 650.1 - 05.03

OYSTD * 61780. YSCFU

STACK GAS FLDY AT DRV STANDARD tDNDITIDNS ODSTD ........................................................................... ODSTD - OUSTD . ( 1 . - ( Xu /1DD.))

ODSTD - 61780. * ( 1 . - ( 6.611 / l oo . ) )

ODSTD = 57600. DSCFM

. - . . . . -. -

.. . . __ . . . .

81

SAMPLE CALCULATIONS ................ 1.. PARTICULATE ANALYSIS

SOURCE - ROUGE STEEL COMPANY -- COKE OVENS -- B COMBUSTION STACK TEST - 1

MEASURED DATA __----_______ UETEREO SAMPLE VOLUME

UETER CORRECTION FACTOR

AVERAGE UETEP TEMPERATURE

AVERAGE ORIFICE PRESSURE DROP

VOLUME OF I420 CONDENSATE

WEIGHT OF W O WSORBEO

NOZZLE -DIAMETER

TOTAL SAUPLE TIME

WEItKT Of PROBE CATCU

WEIGHT OF FILTER CATCH

vy

O W C F

TM

OELU

VI

VSG

ON

TUETA

WPROBE

WF

47.044 W. FT.

O.BBT1

47. OEG F

2.16 INCUES W O

61.0 ML

10.6 GRAMS

0.4990 INCHES

60. MINUTES

0.0364 GRAMS

0.0415 6RAMS

. . . -_ . - . , ~ .. . .

a2

.. - . L.

~

. - ... . . - . __ . . . . . . -. . - ._ . . _ _

. a3

SAMPLE CALCULATIONS ------------------- ISDKINETIC RATIO I . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . I - 100. * VTSTD / ( THETA * AN VSTD )

I - 100. * 5 1 . 1 2 / ( 60.00 0 . 0 0 1 3 6 * 6 5 0 . 1 )

I - 9 6 . 5 0 X

TOTAL WEIGHT OF PARTICULATE MATTER COLLECTED WPT ........................................................................... WPT = WPRDBE + WF

WPT 0 .03640 + 0.04150

WPT = 0 . 0 7 7 9 0 GRAMS

PARTICULATE CONCENTRATION AT STACK CDNDITIDNS CSTK . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . CSTK - 1 5 . 4 3 * 17 .647 * PS * WPT / ( VTSTD a ( TS 460 . 1 )

CSTK - - 1 5 . 4 3 - 17.647 * 29.00 * 0 . 0 7 7 9 0 / ( 5 1 . 1 2 * ( 4 1 9 . 6 * 460. )

CSTK - 0,01368 GR/ACF

PARTICULATE WEIGH7 CONCENTRATION AT DRY STANDARD CONDITIONS WCD ________________________________________----------------------------------- WCD - 849 .0 - WPT / ( VMSTD * MWD 1

UCD - 8 4 9 . 0 * 0 , 0 7 7 9 0 / ( 4 7 . 7 4 . 2 9 . 0 0 )

WCD I 0 .04777 . X / 1 o o O l DRY

PARTICULATE WEIGHT CONCENTRATION A t WET STANDARD CONDITIONS WCW ........................................................................... WCW = 8 4 9 . 0 a WPT / ( VTSTD * MWW

WCW = 849.0 * 0 . 0 7 7 9 0 / ( 51.12 * 28.27 1

WCW * 0.04576 f f / l O W X WET

PARTICULATE FLOW RATE WR

WR - 0.132 - WPT - OWSTD / VTSTD

WR - 0 . 1 3 2 0.07790 - 61780 . / 51 .12

W R - 12.43 LB/HR

0

a4

.

... . . __

APPENDIX I -

EQUIPMENT LALIBRATION .

r;,

85

APPENDIX I

EQUIPMENT CALI BRATION

A. Dry Gas Meter

The d r y gas meters i n the sampling t r a i n s a re c a l i b r a t e d aga ins t a

standard meter which has been p r e v i o u s l y c a l i b r a t e d aga ins t a sp i rometer .

B; Probe Tenperature Thennocouples

The Dor i c pyrometers and probe thermocouples a re c a l i b r a t e d aga ins t ASTM

mercury-in-glass reference thermometers. A temperature range from 32OF.

t o 210°F. i s u t i l i z e d f o r c a l i b r a t i o n purposes.

C. P robe/P i to t Tubes

The S-type p i t o t tube mounted on t h e sampling probe i s c a l i b r a t e d i n the

same stack t h a t f lows a re t o be measured i f the v e l o c i t y p r o f i l e i s

co rs tan t .

c s l i b r a t e d ir, a constarlt f l o w s tack \ r i t h un i fo rm v e i o c i t y .

is performed against a standard p i t o t tube with a nozzle i n p lace or, t he

probe t o be ca l ib ra ted .

,- - I. In other instances t h e p r o b e / p i t o t tube asser;lbly i s p re*< ious ly

The c z l i b r a t i o n

D. G r i f i c e

The f l o w o r i f i c e i n the sampling t r a i n i s ca l ibra- ted i n con junc t ion w i t h the

a e t e r c a l i b r a t i o n . Resul ts a re inc luded w i t h the meter c a l i b r a t i o n data.

E. Nozzles

Probe nozzles are c a l i b r a t e d i n t h e f i e l d p r i o r t o t e s t i n g .

a re made on th ree d ianeters us ing a p r e c i s i o n v e r n i e r c a l i p e r .

Measuren;ents

. . . . . i? . . . . ,..

--.

=--r . ''~ i.

.' .

.

. .

. . .

a7 FORD MOTOR COMPANY


P ITOT TUBE CALIBRATION DATA * I 0.78 7' Pl2oLosEs, Y+xn. No== #t 0.80

SOURCE. %,by 5 STACK DIMENSIONS bo" 6 PLANT Sts+A*le NIPPLE LENGTH 3 'A.

I N I T I A L S j!:~';& ul II STATIC PRESSURE - -08 DATE

BAROMETRIC PRESSURE w. 0 1 TEST NO. Prrm T I M E 6400

- P i t o t &iz= - Tube No. 2 C P ' G I '~

.- Pi to t @zz= E

Tube No. 1 Cp= 6

. .. . . __. . __ .-

c. aa

Y '

FORD MOTOR COMPADY STATIONARY SOURCE ENVIRONMENTAL CONTROL OFFICE

PITOT TUBE CALIBRATION DATA 7' Rcbe w 0 . l

STACK DIMENSIONS NIPPLE LENGTH STATIC PRESSURE BAROMETRIC PRES- TTMC

7 '../

I I I I I

L I I I Total ll.04C 14.561. 2I.a Average ,773 - . m= 5

,#-- cP= @z% =.k& = 5-2 cp= Pitot

Tube No. 1 G Tube No. 2

~~ ~

__- ___. . -- (4;

h l f.,

a9 s .

FORD MOTOR COMPNY STATIONARY SOURCE ENVIRONMENTAL CONTROL OFFICE

P ITOT TUBE CALIBRATION DATA 7' ?robe No.2

SOURCE Boilu 5 STACK DIMENSIONS NIPPLE LENGTH STATIC PRESSURE

I N I T I BAROMETRIC PRESSURE TEST NO. T I M E

-. L.

1

I I I I . Tota l I I I 1 A v e r a g e

.

!pz= = P i t o t = .605 =

Tube No. 2 I ~

' .-/' P i t o t

Tube No. 1 s-1 cP=

, '1 - . . . .. . I ._. _. . -- .. . . -. .

' V

! J ' 3

3

I A

3

3

,

SSECO METER BOX NO. 2 C A L I B R A T I O N DaTn

DATE!ll-l7-82 S T D . nETER N O , : 9lb79? 1 N I T I A L S : T P I D BOX-MFTER N O . , 661006 E m . PRESS.: 29.59 N O . OF T U I 6 L S : 9

T R I A L TIME STANDARD WETFR DATA I C O P P . FACTOR 0.9862) T E N P DEL P STliPT F I N I S H N E T UOL.STP COPD.UOL

NO. n w . DC F IN.YZO CU.FT. CV.FT . CU.FT. SCF SCF ___-- ---- _____ __--__ _---__- ------- ----___ ------- -------- 1 19.077.0 -0.170138.VS3146.19Z 7.439 7.231 7.131

2 12.0 7 7 . 0 -0.195 146.392 152.216 5.824 5.660 5.S82

3 9.0 77.0 - 0 . 1 2 0 152.216 157,237 5 . 0 2 1 4.880 4.812

4 8 . 0 77.0 -0.250 lS7.237 162.17Z 4.V35 4.7V6 4.730

5 8.0 77.0 -0 .270 162.172 167.604 5.432 5.279 5.206

6 7.0 77.0 -0.300 167,604 17Zb95 5.091 4.947 4.879

7 7.0 77.0 -0.335 172.695 178.113 5.418 5 . 2 6 4 5.191

8 8.0 77.0 -0.360 178.113 18S.077 b.9h4 h.766 6.672

9 6 . 0 77.0 -0,420 185.077 190.787 5.710 5.547 5.470

T R I A L METER SOX DATA 1 - I N 1-OUT DEL P S T A R T F I N l S H STP VOL. DELTA C O R R .

N O , DC F DC F IN.HZO CU.FT . C U . F T . SCF H D E L . H _____ --___ __-__ _-__-- ------_ ------- -_----- ----- ----- 1 09.0 87.0 0 . 5 0 0 928.233 935.750 7.174 1.8R 1.87

2 97.5 94.0 0.750 935,750 9.1 ,691 5.5Cb 1.82 1.82

3 104.0 99.5 1 . 0 0 0 941.691 94b.845 4 . R 0 6 .84 1 ,84

4 109.0 104.5 1.250 946.845 951.V.1 4.714 .87 1.88

5 114,s 108.0 l.SO0 951.941 957.565 S.lb5 . 8 6 1.87

b 118.5 110.5 1.750 957.5h5 962.R.R 4:8?8 .89 1.91

7 121.5 113.0 2.000 962,848 968.500 5.144 1.90 1.91

8 124.0 116.0 2 . 5 0 0 968.500 975.754 6.781 1.88 1.91

9 125.S119.S 3.00097SR.7)54981.700 5.380 1.89 1.92

~~

&=RAGE llElEP CORRECTION FACTOR? 1.0060 W E R A C E CORRECTED C A L I B R A T I O N CONSTANT I D E L T n W ) : 1.89

C A L l 8 @ A T 1 O N CONSTANT I D E L T A U l - 0 . 0 3 1 7 S I . D E L T A P*PBARIlMETEP TEMP OUT14601* III~ETEP TEMP AVEI46OI.TI~E/lCU.FT..IPB~*DELT~ P/13.6111**2.0)

I I ' d

.~.FOOTNOTEI STANDAPD C O N D I T I O N S I S T P I ! 29.92 IN. W t . AND 528 D F C R E E S RANKINE.***

AP42 chapter 12 reference · 2015-09-10 · 4P42 Section: Reference: Title: 12.2 91 Rouge Steel...

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Transcript of AP42 chapter 12 reference · 2015-09-10 · 4P42 Section: Reference: Title: 12.2 91 Rouge Steel...