Annual Report 2003-work-6 · 5. semester (Bc) Analytical Chemistry II 2/2/0/0 Bustin, Čakrt...

FOREWORD

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FOREWORD

The Faculty of Chemical and Food Technology (FCHPT) is one of six faculties of the Slovak University of Technology. The history of the Faculty dates back to 1939, when Law No. 188 of 25 July 1939 allowed the establishment of a Chemical Engineering branch at the Slovak University of Technology. The specialisation profile of the Faculty has developed steadily in accordance with the needs of the community.

The Slovak higher education has its rich history. Our Faculty follows in the footsteps of its famous predecessor in the education of technical chemistry, i.e., the famous Mining Academy in Banská Štiavnica constituted by empress Maria Theresa in 1762. The establishment of the Dr. M. R. Štefánik College of Technology in 1937 and subsequently, that of the Slovak College of Technology in 1939 succeded in keeping the high standard of technical education in Slovakia.

Within the time of its existence, the Faculty has educated more than 16 700 graduates (more than 3 600 graduates in food engineering). The Faculty has trained nearly 1 300 graduates in postgraduate doctorate courses granting the title PhD in chemical and technical sciences. Thus, the Faculty has helped considerably to increase scientific knowledge in industry, education system, scientific and research institutes, and administrative services.

The Faculty occupies a very specific position within the Slovak Republic and relates to the whole spectrum of chemical, food, pharmaceutical and consumer industries, and ecology. At present, some 1600 students study at the Faculty and they are trained by qualified pedagogical and research staff.

The Faculty currently offers study in BSc courses, MSc courses, and PhD. The undergraduate form of study is organized at two levels: Bachelor-of-Science and Master-of-Science programmes. The first level BSc course for all students lasts three years, and is run in two branches: Chemical Technology and Food Technology. This first level of the study ends by a state examination and a project granting the student the title Bachelor of Science (BSc). The nominal span of the study in the BSc course is 3 years. The second level MSc course is run in 9 majors with several possible specializations over two years. The MSc course ends by a state examination and by defending a diploma thesis. The graduate obtains the title Master of Science (MSc). In addition to the natural-science basis, students of all branches study basic engineering subjects, e.g. Chemical Engineering, Processes Control, Basics of Chemical and Food Processing Technology, as well as subjects on Economy, Law and Ecology.

The highest form of university education is currently the doctorate study, which in the past was run as a form of preparation for scientific work. In 1997 the Ministry of Education of the Slovak Republic approved the right of the Faculty to train and to administer examinations in PhD Courses. The Faculty has conferred the title PhD in 16 branches of the doctoral study. (Chemical Physics, Inorganic Chemistry, Organic Chemistry, Analytical Chemistry, Physical Chemistry, Macromolecular Chemistry, Biochemistry, Microbiology, Inorganic Technology and Materials, Organic Technology and Technology of Fuels, Technology of Macromolecular Materials, Chemical Engineering and Control of Processes, Chemistry and Technology of Environment, Chemistry and Food Technology, Biotechnology, Applied Informatics).

The Faculty has a widely oriented programme, leading to the development of basic scientific fields in chemistry, chemical technology and food processing. This wide scientific orientation of Departments at the Faculty allows goal-oriented training of undergraduates and thereby their quicker transition to industry. There are several scientific schools at the Faculty which are successful at winning grants from domestic and international sources and at organising scientific meetings. The Faculty generally maintains an important international position. In addition to basic research, the Faculty participates in widely applied research for practice. The cooperation with many factories and companies allows for a swift application of research results in practice. At the same time the Faculty obtains considerable financial support.

The Faculty participates in issuing the specialized scientific journals: Chemical Papers, Fibres and Textile, Plastics and Rubber, Journal of Radioanalytical and Nuclear Chemistry, Biology, Folia Microbiologica, Vinič a Víno (Wineyard and Wine).

The scope and quality of the scientific activity keep the Faculty at a level, which is comparable with other top research and university centres in the world. This can be proved by the above mentioned number of grants, staff invitations to participate in conferences abroad, wide cooperation with foreign universities and institutions, and memberships in international organizations.

Any further details about the activities of the Faculty of Chemical Technology can be found in the Annual Report 2003. March 2004

Prof. Dušan Bakoš, PhD, DSc Dean

PRESIDIUM OF THE FACULTY

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PRESIDIUM OF THE FACULTY

Dean: Prof. Dušan Bakoš, PhD, DSc Vice-deans: Assoc. Prof. Ján Dvoran, PhD Assoc. Prof. Pavel Kovařík, PhD Prof. Ján Šajbidor, PhD, DSc Assoc. Prof. Zdenek Židek, PhD

SCIENTIFIC COUNCIL

Chairman: Prof. Dušan Bakoš, PhD, DSc Vice-chairman: Prof. Ján Šajbidor, PhD, DSc Members: Prof. Vladimír Báleš, PhD, DSc Prof. Fedor Malík, PhD, DSc Prof. Stanislav Biskupič, PhD, DSc Prof. Milan Melník, PhD, DSc Prof. Dušan Bustin, PhD, DSc Prof. Ján Mikleš, PhD, DSc Assoc. Prof. Gabriel Čík, PhD Assoc. Prof. Tomáš Bleha, PhD, DSc Prof. Pavel Fellner, PhD, DSc Assoc. Prof. Anton Gáplovský, PhD, DSc Prof. Ľubor Fišera, PhD, DSc Assoc. Prof. Milan Kováč, PhD Prof. Milan Hronec, PhD, DSc Ján Maťaš Assoc. Prof. Svetozár Katuščák, PhD Prof. Jan Roda, PhD Assoc. Prof. Pavel Kovařík, PhD Assoc. Prof. Jozef Seginko, PhD Prof. Vladimír Kvasnička, PhD, DSc Assoc. Prof. Jozef Šimúth, PhD, DSc Prof. Jozef Lehotay, PhD, DSc Honorary Members: Vratko Kaššovic, PhD Prof. Stanislav Miertuš, PhD, DSc Jozef Kollár Štefan Prekop Ján Líška Prof. Ludo Zanzotto, PhD

ACADEMIC SENATE

Chairman: Prof. Marian Koman, PhD, DSc – from june 2003 (Assoc. Prof. Ján Dvoran, PhD – until may 2003) Vice-chairmen: Assoc. Prof. Pavol Hudec, PhD Andrea Baránková, student Members: Assoc. Prof. Jozef Augustín, PhD Assoc. Prof. Viktor Milata, PhD

Assoc. Prof. Monika Bakošová, PhD – from june 2003

Jana Pappová

Prof. Eberhard Borsig, PhD, DSc Assoc. Prof. Jozef Augustín, PhD. Zuzana Cvengrošová, PhD Assoc. Prof. Ivan Hudec, PhD. Assoc. Prof. Milan Čertík, PhD. Assoc. Prof. Jana Gabčová, PhD. Miroslav Hutňan, PhD Assoc. Prof. Mária Takácsová, PhD. Assoc.Prof. Anton Gatial, PhD. Tibor Jakubík, PhD. Assoc. Prof. Štefan Šutý, PhD. Jurčo Juraj* Assoc. Prof. Jozef Markoš, PhD. Špaňová Miroslava* Vladimír Lukeš, PhD. Majerčáková Katarína* Assoc. Prof. Monika Bakošová, PhD. Pápyová Barbora* Vladimír Kovár, PhD. Šeligová Janka* Dušan Špirko, PhD. Kovalčík Boris* Assoc. Prof. Anna Kolesárová, PhD. Bc. Púčeková Zuzana* Prof. Ľubor Fišera, DrSc. Bc. Repický Andrej* Zuzana Cvengrošová, PhD. Ing. Michal Jaššo* Assoc. Prof. Gabriela Kyselá, PhD. Ing.Radovan Herchel* Viera Jančovičová, PhD. (* student) Viliam Lendel, PhD.

DEPARTMENT OF ANALYTICAL CHEMISTRY

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Head of Department: Telephone: ++421252926043 Prof. Jozef Lehotay, PhD, DSc Fax: ++421252926043

E-mail: [email protected]

I. STAFF Full Professors: Dušan Bustin, PhD, DSc; Ján Krupčík, PhD, DSc; Ján Labuda (since 14.6.2003), PhD, DSc; Jozef Lehotay, PhD, DSc; Eva Matisová, PhD, DSc; Ján Mocák, PhD, DSc; Associate Professors: Ernest Beinrohr, PhD; Eva Benická, PhD; Eva Brandšteterová (till 17.10.2003), PhD; Miroslav Čakrt, PhD; Drahomír Oktavec, PhD; Miroslav Rievaj, PhD; Viktor Vrábel, PhD;

Assistant Professors : Tatiana Buzinkaiová, PhD; Andrea Hercegová, PhD; Svetlana Hrouzková, PhD; Elena Korgová, PhD; Pavol Májek, PhD; Alena Manová, PhD; Pavol Tarapčík, PhD; Mária Vaníčková, PhD;

Research Fellows: Miriam Bučková (till 31.8.2003), PhD; Adriana Ferancová, PhD; Katarína Hroboňová, PhD; Jarmila Laštincová (till 30.9.2003), PhD; Tatiana Rojkovičová; Jana Sádecká, PhD; Ivan Skačáni, PhD; Ivan Špánik, PhD; Peter Tomčík, PhD; Magdaléna Valachovičová;

PhD Students: Branko Balla (till 15.11.2003); Eva Blahová; Milena Dömötörová; Jana Ďungelová (till 8.10.2003); Andrea Fedurcová (since 1.10.2003); Gabriela Karasová; Michal Kirchner (since 1.10.2003); Peter Korytár (till 31.3.2003); Petra Kotianová; Janka Mydlová (since 1.10.2003); Milan Střelec (since 1.10.2003);

Technical staff: Marta Benešová; Ľubica Zajacová; Jana Otrubová (till 28.2.2003); Juraj Žemlička

II. TEACHING AND RESEARCH LABORATORIES

A. Teaching laboratories: Laboratory of capillary gas chromatography Laboratory of high performance liquid chromatography Laboratory of capillary isotachophoresis Laboratory of electroanalytical methods Laboratory of molecular spectrometry Clean laboratory for trace analysis with atomic spectrometry (AAS, OES-ICP) Laboratory of electrochemical pre-concentration for atomic spectroscopy Laboratory of organic elemental analysis Laboratory of fluorescence analysis Laboratory of chemometry Laboratory of bioanalytical chemistry B. Research laboratories: Laboratory of organic synthesis Laboratory of capillary gas chromatography Laboratory of high performance liquid chromatography Laboratory of capillary isotachophoresis Laboratory of electroanalytical methods Laboratory of molecular spectrometry Laboratory for atomic spectroscopy Laboratory of organic elemental analysis Laboratory of fluorescence analysis Laboratory of chemometry Laboratory of bioanalytical chemistry


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III. TEACHING

A. Undergraduate Study: 4. semester (Bc) Analytical Chemistry I 2/2/0/0 Krupčík, Labuda Laboratory Practice AC I 0/0/0/4 Valachovičová, Hercegová 5. semester (Bc) Analytical Chemistry II 2/2/0/0 Bustin, Čakrt Laboratory Practice AC II 0/0/0/4 Korgová Testing and Quality Control 1/1/0/0 Čakrt 6. semester (Bc) Semester Project 0/0/0/4 Rojkovičová 1. semester (MSc) Analytical Chemistry of Complex

Inorganic Mixtures 2/0/0/0 Oktavec

Anal. Chemistry of Complex Organic and Biol. Mixtures

2/0/0/0 Sádecká

Analytical Spectrometry 2/0/0/0 Beinrohr Laboratory Practice I 0/0/0/10 Sádecká 1. semester (MSc) Computer Evaluation of Analytical

Measurement 2/0/0/0 Májek, Mocák

Biosensors 2/0/1/0 Labuda 2. semester (MSc) Techniques of Mixtures Separation 2/0/2/0 Matisová, Valigura Laboratory Practice II 0/0/0/6 Sádecká Electrochemistry and

Electroanalytical Chemistry 2/0/1/0 Bustin

Analytical Separation of Compounds 2/0/1/0 Krupčík 2. semester (MSc) Trace Analysis and Microanalysis

Methods 2/0/0/0 Beinrohr, Čakrt

3. semester (MSc) Bioanalytical Chemistry 2/0/1/0 Labuda, Mocák Identification of Chemical Substances 2/0/1/0 Lehotay, Liptaj Laboratory Practice of Spezialisation 0/0/0/10 Sádecká Automatisation of Analytical

Chemistry 2/0/0/0 Rievaj

3. semester (MSc) Analytical Chemistry of Environment 2/0/0/0 Benická 4. semester (MSc) Laboratory of Diploma Work 0/0/0/27 Rojkovičová

IV. CURRENT RESEARCH PROJECTS

A. VEGA Project No 1/9128/02 Development and Application of Direct Injection Assays for HPLC Analysis of Some Drugs and Toxic Compounds in Biological Samples (Eva Brandšteterová, Jozef Lehotay).

The aim of the project was the development and the application of new assays with the possibility of direct injection of biological samples into the HPLC system. SPE (Solid Phase Extraction) precolumn was integrated directly into the HPLC system what improves validation parameter values and minimizes the personal contact with biofluids. Automated HPLC procedures for the analysis of chosen drugs, natural and toxic compounds were compared with applied electromigration methods.

Project duration: from 01.01.2002 to 31.12.2004 B. VEGA Project No 1/9129/02 Elektroanalysis by means of in-elektrode coulometric titration and interdigitated array of microelectrodes. Optimization of stages of trace analysis (Dušan Bustin).

The project is oriented to the investigation of in-electrode coulometric titration in porous electrodes for calibrationless determination of trace concentrations of metels and some non-metals and to the application of elaborated procedures for automated process analysis. It also intends to contribute to employment of chronoamperometry with the segments of interdigitated microelectrode arrays for the calibrationless analysis of electroactive species. Chronoamperograms are to be obtained under redox-cycling or isolated segment conditions. The multivarite statistical data analysis are to be used for authentification and classification of food products, environmental samples as well as for the software aided clinical diagnosis.

Project duration: from 01.01.2002 to 31.12.2004 C. VEGA Project No 1/9127/02 Development of optimum methods for analyses of enantiomers of biologically active chiral substances by high performance liquid, supercritical fluid and gas chromatography (Ján Krupčík).

This project intends to contribute to development of methods for the direct analysis of enantiomers of selected biologically active chiral compounds by high performance liquid (HPLC), supercritical fluid (SFC) and gas (HRGC) chromatography. Following subparts shall be studied in this project: (i) Computer assisted optimum methods shall be developed for direct


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separations of enantiomers of selected biologically active chiral compunds by HPLC, SFC and GC methods using commercially available modified cyclodextrins (GC) and macrocyclic antibiotics (SFC and HPLC). (ii) Two columns in series and two dimensional HRGC and or HPLC shall be applied for the separation of enantiomers in complex mixtures. (iii) Computer assisted deconvolution of the peak clusters obtained separating the racemic mixtures shall be applied to determine the enantiomerization barrier of the thermally labile enantiomers by dynamic HPLC, SFC and GC. (iv) Principal component analysis and cluster analysis shall be used to classify the enantioselectivity of modified a-, b- and g-cyclodextrin used in HRGC.

Project duration: from 01.01.2002 to 31.12.2004 D. VEGA Project No 1/9126/02 Large Volume Injection in Conventional and Fast Capillary Gas Chromatography (Eva Matisová).

The aim of the project is the development of the large volume sample injection methods in combination with conventional, fast capillary gas chromatography and GC-MS for trace analysis of volatile and semi-volatile organic compounds in multicomponent model and real environmental samples. A part of the project is connected with the development of comprehensive gas chromatography (GCxGC) and its combination with the large volume sample injection for the analysis of multicomponent samples of trace analytes. A part of the project is devoted to the application of the gained knowledge to the trace and ultra-trace analysis of multicomponent mixtures of organic compounds in environmental matrices including the sample pre-treatment for the large volume sample injection.

Project duration: from 01.01.2002 to 31.12.2004 E. NATO Project No SFP 977983 Minimisation of Pesticide Residues in Processed Products and the Environment (Eva Matisová).

The project refers to pesticide science and more specifically to pesticide chemistry, and analytical methodology of residues. Pesticide residues undergo significant changes in chemical structure and concentration during food processing. The research work in the project is planned to contribute to better understanding of the effects of food processing on pesticide residues. Perfection of the analytical methodologies for detection and determination of pesticide residues at extremely low concentrations allowed in baby foods will be one of the scientific contributions of the project. Existing methods will be modified or new methods will be developed, distinguished by sufficient precision and reliability of determination of residues at or below the concentration level of 0.01 mg/kg, required by the EU directives on baby food. The identification and assessment of the critical points in the food technology processes will be a contribution to food technology.

Project duration: from 01.02.2003 to 31.01.2006 F. Aktion Oesterreich-Slowakei: “Chemometrical Classification of Food and Biologically Important Samples” (national coordinator: Ján Mocák).

Bilateral scientific project between (a) Technische Universitaet Graz, Austria, and (b) Slovak University of Technology, Bratislava, Slovakia.

Project duration: from 01.01.2003 to 30.11.2003 G. VEGA Project No 1/9253/02: Electrochemical DNA biosensors for the characterization of interactions of the bound DNA, the determination of traces of compounds binding to DNA as well as activators and inhibitors of damage to DNA (Ján Labuda)

New biosensors with a DNA layer of controlled properties attached to screen-printed carbon electrodes have been prepared. Host-guest interactions for dsDNA and small molecules of selected chiral drugs and risk chemicals have been characterized using several voltammetric techniques. DNA structural changes and deep degradation as a consequence of chemical reactions of reactive oxygen radical species as well as DNA protection by selected antioxidants such as flavonoids were investigated. New analytical procedures for the simple and fast determination of trace amounts of chiral drugs were developed. The DNA biosensors were tested as simple and single-use sensors for the determination of DNA damage as well as the evaluation of antioxidative capacity of plant extracts of food industry interest.

Project duration: from 01.01.2002 to 31.12.2004 H. Project 035/2001 (USA – SK) The HPLC Study of Enantioselective Separations Using Molecular Modelling and Artificial Neural Networks on Macrocyclic Antibiotic Chiral Selectors (Jozef Lehotay).

The objective of this research project is to create a comprehensive method capable of the prediction and optimization of enantioselective separations achieved by the vancomycin chiral selector,VM-CS, in HPLC, CEC and CE. This will be accomplished by:1) development of QSERRs to describe the retention and enantioselective separations achieved in each chromatographic mode; 2) training ANN to select optimum format and conditions, i.e. to minimize k1’ and k2’ while optimizing k2’/k1’, using the independent variables identified by the QSERR studies. A key element in the optimal use of CSs is an understanding of the chiral recognition mechanisms responsible for the observed enantioselective separations. Thus, a second objective is the use of the QSERRs and stopped-flow kinetic studies to construct descriptions of the chiral recognition mechanisms operating in each mode and to correlate these results with molecular modelling studies. The aim of these studies is a better understanding of the fundamental processes involved in chiral recognition.

Project duration: from 01.07.2002 to 01.07.2005


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V. CURRENT EDUCATION PROJECTS

A. CEEPUS PL-110 02/03: “Development and improvement of modern analytical methods for monitoring the environmental pollution and introduction of the quality systems and accreditation to routine analytical laboratories” (Ján Mocák).

Educational project enables exchange of students and teachers among the following partner universities:(a) The University of Mining and Metallurgy, Cracow, Poland, (b) Karl-Frenzens-University, Graz, Austria, (c) The University of Maribor, Maribor , Slovenia, (d) The University of Pardubice, Pardubice, Czech Republic, (e) Slovak University of Technology, Bratislava, Slovakia.

Project duration: from 01.09.2002 to 31.08.2003 B. CEEPUS PL-110 03/04: “Development and improvement of modern analytical methods for monitoring the environmental pollution and introduction of the quality systems and accreditation to routine analytical laboratories” (Ján Mocák).

Educational project enables exchange of students and teachers among the following partner universities:(a) The University of Mining and Metallurgy, Cracow, Poland, (b) Karl-Frenzens-University, Graz, Austria, (c) The University of Maribor, Maribor , Slovenia, (d) The University of Pardubice, Pardubice, Czech Republic, (e) Slovak University of Technology, Bratislava, Slovakia.

Project duration: from 01.09.2003 to 31.08.2004 C. CEEPUS PL-0130-03/05: Education in Separation Methods for Organic Environmental Analysis in XXI. Century (Ján Krupčík).

The main objective of this project is to improve the quality of MSc and PhD education in Analytical Chemistry at the cooperating universities, with the emphasis on modern analytical separation methods. This will be accomplished by exchange both of graduated and PhD students as well as teachers between the University of Technology Graz, University of Pardubice, Nicolaus Copernicus University in Toruń, University of Łódź, University of Veszprém, Medical Academy in Gdańsk and the Slovak University of Technology in Bratislava. Special attention will be paid on the application of hyphenated techniques and on the fitting of the educational process to the needs and settings of the European Community.


D. Bilateral project MŠ SR/DAAD No 5/2002, SRN: Investigation/detection of environmental risk species by DNA-based biosensors (Ján Labuda).

The topic of the project is an investigation of interactions of species of environmental interest with deoxyribonucleic acid (DNA). Toxic chemical species interact with living organism by various ways including association and follow-up structural and chemical changes of biological material. Toxic species can be accumulated by DNA and initiate subtle or deep damage to DNA. With respect to body aging and cancer processes, the changes of DNA due to its chemical interactions are of great interest. We aspect to investigate metalorganic and metalloid species as well as metal complexes with organic ligands which are able to intercalate into cavities between DNA bases pairs.


VI. COOPERATION

A. Cooperation in Slovakia

Institution Type of cooperation Responsible person

Duration

Faculty of Electrical Engineering and Information Technology (Microelect.)Bratislava

Interdigitated array of microelectrodes Řeháček V., research fellows, Ilkovičova 3, 841 04 Bratislava 01.01.1994-

Central Agricultural Inspection and Testing, Bratislava

Field experiments for determination of residues of pesticides in fresh and processed products for baby food

Raučinová Ľuba, RNDr., Hanulova 9, 844 40 Bratislava

01.03.2002-31.12.2003

Pharmaceutical Faculty, Comenius University, Bratislava

Chiral Separation of some anaestetics using HPLC method

Čižmárik Jozef, professor, Odbojárov 10, 832 32 Bratislava

01.01.1988-


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Technický a skúšobný ústav stavebný, n.o., Bratislava

Development of a new method for determination of amonia

Zajíček Milan, Ing. CSc., Studená 3, 826 34 Bratislava

19.11.2003-31.12.2003

Bell/Novamann International, Bratislava

Development of HPLC method for determination of Atorvastatin Ca - chiral separation

Veverka, Ing. CSc., Továrenská 14, 815 71 Bratislava

04.12.2003-31.12.2003

Elektrokarbon, Topolčany Chemical Analysis of Elements Si, B, Fe.

Štefke Ľubomír, Ing., research worker, Tovarnícka 412, 955 22 Topoľčany

20.02.2003-30.03.2003

Biomin, Cífer Chemical Analysis of Se and Sr in Eggs. Kvaka Valdemar, PharmDr. CSc., director of concern, Ľ. Pavetitša 1, 919 43 Cífer

20.02.2003-20.03.2003



26.03.2003-09.06.2003



27.03.2003-09.07.2003

Prvá správcovská spoločnosť, Bratislava

Chemical Analysis of S in Plaster. Baratka, Ing., director of concern, Mlynské Nivy 61, 824 98 Bratislava

09.04.2003-20.05.2003

Istran, Bratislava Preparation and Chemical Analysis of Solutions.

Beinrohrová Mária, Ing., director of concern, Vigľašská 12, 851 06 Bratislava

02.09.2003-22.12.2003

B. International Cooperation


Duration

UFZ Environmental Research Centre Leipzig, FRG

joint projekt

Wennrich Reiner, Dr., Head of the Section UFZ Leipzig-Halle, Permoserstr. 15, D-04318 Leipzig, Germany

01.01.2003-

Depart. Anal. Chemistry, Faculty of Natural Sciences, Charles University, Prague, Czech Republic

study stay of students

Barek Jiří, prof., Head of the Laboratory UNESCO Laboratory of Environmental Electrochemistry, Charles University, 128 43 Prague

01.01.2002-

Institute for Chemical Technologies and Analytics Vienna University of Technology, Austria

Analysis of volatile and semivolatile compounds in air

Puxbaum Hans, professor, Getreidemarkt 9/164/AC-Analytical Chemistry A-1060 Vienna, Austria

01.01.1997-31.12.2003

Department of Chemistry, Gilman Hall, Iowa State University, Ames, Iowa, USA

Chiral separation of optical active compounds by HPLC and HRGC

Armstrong Daniel Wain, professor, Iowa State University/Ames, National Laboratory, Gilman Hall, Ames, IA 50011 USA

01.01.1997-

Department of Organic Chemistry, University of Gent, Gent, Belgium

Chiral separations by HRGC

Sandra Pat, professor, Gent University, Department of Organic Chemistry 9000 Gent, Belgium

01.01.1996-

Nicholas Copernicus University, Toruň, Poland

Trace analysis in GC and HPLC development of new chemical bounded phases

Buszewski Boguslaw, professor, NCU, Faculty of Chemistry, Gagarin Street 7, 87-100 Toruň, Poland

01.01.1995-

School of Chemistry, Monash University, Melbourne, Australia

Electrochemistry. It started during the working stay in Melbourne in 1992-94.

Bond Alan, professor,head of Department,Clayton, Vic. 3800, Australia

01.02.1992 -

Department of Building Materials, University of Mining and Metallurgy, Cracow, Poland

Electroanalytical chemistry and chemometrics, common CEEPUS projects (exchange of students and teachers)

Bobrowski Andrzej, professor, Al. Miczkiewicza, PL-30-059 Cracow, Poland

01.09.2001 -


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Department of Analytical Chemistry and Radiochemistry, Technical University, Graz, Austria

Food analysis, bilat. scient. project Austria-Slovakia 37s15 „Chemometrical Classification of Food and Biologically Important Samples"

Lankmayr Ernst, professor, vice-head of Department,Techniker str. 4, A-8010 Graz, Austria

01.03.2002 -

Department of Chemistry, Loughboorough University, Loughborough, U.K.

Electrochemistry and sonoelectrochemistry of molecular and colloidal redox systems

Marken Frank, lecturer, Loughborough, Leicester-shire LE11 3TU, UK

01.07.2002-

Department of Analytical Chemistry, Masaryk University, Brno, Czech Republic

Chemometrics, food analysis, classification of food products

Havel Josef, head of Department, Kotlarska 2, 61137 Brno, Czech Republic

01.05.2002-

C. Membership in Domestic Organizations and Societies

Name Organisation or Society Position

Valid date

Bustin Dušan Chemical Papers Editorial Board member 01.01.1991- Bustin Dušan Scientific Council of FCHPT member 01.02.1990- Krupčík Ján Analytical Group of SCHS chairmann 01.01.1992- Labuda Ján Academy Senate of FCHPT member 01.03.2002-

Lehotay Jozef Union of Slovak Scientific Society, Analytical Chemistry Groupe chairmann 04.03.2001-

Lehotay Jozef The Ministry of Education SR, Scientific Agency (VEGA) member 30.04.2002-

Lehotay Jozef Commission for air/pollution (TNK 28) member 01.01.1999- Lehotay Jozef Commission for waste managment (TNK 31) member 01.01.1999- Lehotay Jozef Scientific Council of FCHPT member 01.02.2003-

Lehotay Jozef Agency for support of science and technique Ministry of education member of advisory board 10.09.2003-

Matisová Eva EU Centre of Excellence in Environmental Health Research Institute of Preventive and Clinical Medicine, Bratislava

member of advisory board 01.01.2003-

Mocák Ján Slovak Medical Society, Bratislava, Slovakia (honorary member) member 01.10.1998 -

Mocák Ján Scientific journal “Laboratorna diagnostika“ (Laboratory Diagnostics), Bratislava, Slovakia member of advisory board 01.09.1996-

D. Membership in International Organisations and Societies


Valid date

Beinrohr Ernest Gesselschaft Deutcher Chemiker, Frankfurt, Germany member 01.06.1990-

Bustin Dušan IUPAC Fellowship, Switzerland member 07.03.2002-

Krupčík Jozef European Commission Science, Research and Developments, expert for the evaluation of proposals, Brussel, Belgium

other 01.01.1999-31.12.2003

Labuda Ján Federation of European Chemical Societies and Professional Institutions, the Division of Analytical Chemistry (Delegate of SCHS)

other 06.09.1999-

Labuda Ján Sensors, Editorial Board of the journal, Basel, Schwitzerland member 01.01.2001-

Lehotay Jozef European Commission Science, Research and Developments, expert for the evaluation of proposals, Brussel, Belgium

other 23.02.1999-

Lehotay Jozef Chemical Analysis, Editorial Board of the journal, Warszawa, Poland member 07.11.2001-

Mocák Ján Versailles Project of Advanced Materials and Standards (VAMAS), Group of Statistics, BAM, Berlin, Germany member 01.02.1995-

E. Visitors from Abroad

Name Organisation or Institution State

Date / Duration

Bobrowski, A. University of Mining and Metallurgy, Cracow Poland March 2003 (10 days)


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Pecková, K. Faculty of Natural Science, Charles University, Prague Czech Republic

May-June 2003 (1 month)

Kalcher, K. University of Maribor, Maribor Slovenia April-May (11 days)

Ševčík, J. Charles University, Prague Czech Republic May 2003 (1 days)

Mattusch, J. University of Leipzig, Halle Germany July-August 2003 (10 days)

Kriváň, V. University Ulm, Ulm Germany October 2003 (2 days)

Langmayr, E. University of Graz, Graz Austria November 2003 (3 days)

Simoni, M. University of Maribor, Maribor Slovenia November 2003 (19 days)

Pecková, K. Faculty of Natural Science, Charles University, Prague Czech Republic

November 2003 (5 days)

F. Visits of Staff Members and Postgraduate Students in Foreign Institutions

Name Organisation / Institution / Conference State

Date / Duration

Balla, B. Masaryk University, Brno Czech Republic March 2003 (3 days)

Balla, B. University of Maribor, Maribor Slovenia September-Oktober 2003 (19 days)

Beinrohr, E. Swiss Federal Institute for Environmental Science and Technology, Zurich Switzerland February 2003

(3 days) Blahová, E., Rojkovičová, T.

5th Balaton Symposium on High-Performance Separation Methods, Siofok Hungary September 2003

(3days) Blahová, E., Karasová, G. International conference Vitamins 2003, Pardubice Czech

Republic September 2003

(3 days)

Bučková, M. University of Rostock, Rostock Germany January-August 2003 (8 months)

Dömötörová, M. 1st Int. conference Recent Advances in Food Analysis, Prague

Czech Republic


Ferancová, A. University of Rostock, Rostock Germany May-August 2003 (3 months)

Ferancová, A. International conference Vitamins 2003, Pardubice Czech Republic

September 2003 (3 days)

Hercegová, A. Umweltforschungszentrum Leipzig-Halle Germany September-Oktober 2003 (18 days)

Hercegová, A. 1st Int. conference Recent Advances in Food Analysis, Prague

Czech Republic


Hroboňová, K., Lehotay, J., Rojkovičová, T.

32nd Conference Synthesis and Analysis of Drugs, V. Karlovice

Czech Republic


Karasová, G. Nicolas Copernicus University, Faculty of Chemistry, Toruň Poland November-December

2003 (33 days)

Korytár, P. Netherlands Institute for Fisheries Research, IJmuiden Netherlands January-March 2003 (3 months)

Kotianová, P. Technical University, Wien Austria January-December 2003 (12 months)

Krupčík, J., Lehotay, J.

26th International Supposium on Capillary Chromatography&Electrophoresis, Las Vegas USA May 2003 (13 days)

Krupčík, J. International Symposium Elsevier, Amsterdam Netherlands June 2003 (4 days)

Krupčík, J. Maria Curie projects evaluation, Bruxelles Belgium September 2003 (6 days)

Krupčík, J. Johanes Keppler University, Department of Analytical Chemistry, Gent Belgium October 2003

(5 days)

Krupčík, J. Nicolas Copernicus University, Faculty of Chemistry, Toruň Poland October 2003

(5 days)

Labuda, J. Charles University, Prague Czech Republic

January 2003 (2 days)

Labuda, J. Charles University, Prague Czech Republic April 2003 (2 days)

Labuda, J. Environmental Research Centre, Leipzig Germany May 2003 (23 days) Labuda, J. International Symposium on Sensor Science, Paris France June 2003 (9 days)

Labuda, J. University of Florence, Florence Italy October 2003 (6 days)


10

Labuda, J. Charles University, Prague Czech Republic

Labuda, J. Academy of Sciences, Warszawa Poland November 2003 (6 days)

Lehotay, J. Farmaceutical Faculty, Brno Czech Republic April 2003 (1 days)

Lehotay, J. Congressus Pharmaceuticus Hungaricus XII, Budapest Hungary May 2003 (5 days)

Lehotay, J. Farmaceutical Faculty Charles University, H. Králové Czech Republic June 2003 (4 days)

Lehotay, J. 10th Beijing Conference and Exhibition on Instrumental Analysis, Peking China October 2003

(9 days)

Lehotay, J. Nicolas Copernicus University, Faculty of Chemistry, Toruň Poland October 2003

(4 days)

Lehotay, J. Johanes Keppler University, Department of Analytical Chemistry, Gent Belgium October 2003

(5 days)

Lehotay, J. Farmaceutical Faculty Charles University, H. Králové Czech Republic


Manová, A. Workshop Quality Assurance of Analytical Data, Komorní Lhútka

Czech Republic March 2003 (3 days)

Matisová, E. Charles University, Prague Czech Republic April 2003 (4 days)

Matisová, E. NATO meeting, Projekt No. SFP977983, Defense des Cultures crop protection Conference, Marseille France May 2003 (9 days)

Matisová, E. Netherlands Institute of Fisheries, International Symposium A Century of Chromatography 1903-2003, Amsterdam

Netherlands June 2003 (7 days)

Matisová, E. ICP, Department of Food Chemistry and Analysis, Prague

Czech Republic June 2003 (3 days)

Mocák, J. University of Pardubice, Pardubice Czech Republic

February 2003 (2 days)

Mocák, J. University of Pardubice, Pardubice Czech Republic April 2003 (2 days)

Mocák, J. Technische University of Graz, Graz, Conference YISAC 03, Benátky Austria, Italy June 2003 (16 days)

Mocák, J. University of Mining and Metallurgy, Krakow Poland June-July 2003 (10 days)

Mocák, J. University of Pardubice, Pardubice Czech Republic

August-September 2003 (12 days)

Mocák, J. Technische University of Graz, Graz Austria September 2003 (4 days)

Mocák, J. International Conference - Conferentia Chemometrica 2003, Budapest Hungary October 2003

(3 days)

Mocák, J. Austrian Eschange Office (OAD), Graz Austria November 2003 (3 days)

Mocák, J. Masaryk University, Brno Czech Republic


Mocák, J. Austrian Eschange Office (OAD), Graz Austria November 2003 (3 days)

Rojkovičová, T. ACHEMA, Frankfurt Germany May 2003 (5 days)

Špánik, I. Department of Chemistry, Texas A&M University, College Station USA January-July 2003

(6 months)

Tomčík, P. Physical and Theoretical Chemistry Laboratory, Oxford University England January-December

2003 (12 months)

VII. THESES AND DISSERTATIONS

A. Graduate Theses (Bc Degree) for state examinations after three years of study Name Title of Thesis Supervisor

Hlúbiková, S. On-line coupling of electrochemical and photometric methods and their use for determination of toxic species in waters. Beinrohr, E.

Kružlicová, D. Evaluation of food antioxidants using DNA biosensor. Labuda, J.

Kujovský, M. Determination of trace concentrations of toxic species in waters by flow-through coulometric and chronopotentiometry. Beinrohr, E.

Lachová, M. The sample preparation and the HPLC analysis of natural fenolic antioxidants in plant materials. Brandšteterová, E.

Nováková, K. DNA based biosensor. Vaníčková, M.


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Ondrušová, E. Application of micelles in separation methods. Sádecká, J.

Ruščáková, M. DNA structures as building parts of the biosensors for the determination of drugs and food antioxidants. Korgová, E.

Sloviaková, G. The analysis of "live" and "dead" watter. Buzinkaiová, T. Škvarková, L. New pesticides and their utilization in practise. Hercegová, A.

Vančová, M. The interaction study of chiral separation of some phenylcarbamic acid derivatives by HPLC method. Lehotay, J.

B. Graduate Theses (MS Degree) for state examinations after five years of study Name Title of Thesis Supervisor

Bachratá, S. Use of DNA biosensor at the determination of antioxidants. Labuda, J.

Fabuľová, A. The posibility of preparation of plant and food samples for HPLC analysis of antioxidants. Brandšteterová, E.

Fedurcová, A. Study of enthalpic and entropic contribution to chiral separation of some chiral derivatives of phenylcarbamic acid by HPLC method. Lehotay, J.

Fričová, J. Use of dual-column gas chromatography in analysis of selected constituents of food. Benická, E.

Kirchner, M. Analysis of pesticide residues with fast gas chromatography. Matisová, E. Mydlová, J. Direct separation of enantiomers by capillary gas chromatography. Krupčík, J.

Plevák, D. In-Electrode Coulometric Titrations: Determination of some toxic species in waters. Beinrohr, E.

Ponická, M. Interaction and determination of drugs using DNA biosensor. Vaníčková, M. Skubáková, rod. Macúšová, M.

Methods for determination of dissolution profiles in the evaluation of pharmaceutical formulations. Tarapčík, P.

Střelec, M. On-line connection electrochemical and photometric methods and its utilization for determination of harmful species in waters. Manová, A.

Szopková, M. Use of DTC chelates in extraction of metal ions. Oktavec, D. Tóthová, A. Isotachophoresis in micellar media. Sádecká, J.

Varga, M. New ways for the increasing of the electrochemical determination using DNA biosensor. Ferancová, A.

Veľasová, G. The comparison of the possibilities of various sample pretreatments for ITP analysis of drugs in body liquids. Buzinkaiová, T.

C. Dissertations (PhD) Name Title of Thesis Supervisor

Balla, B. Application of multidimensional data analysis to classification of biological materials, food products and natural substances. Mocák, J.

Ďungelová, J. Interaction study of enantiomeric separation of opticaly active compounds by HPLC. Lehotay, J.

F. Inauguration Theses Name Title of Thesis Head of board

Labuda, J. Chemically modified electrodes as modern chemical sensors and biosensors. Bustin, D.

VIII. PUBLICATIONS A. Journals [1] Breza, M., Biskupič, S., Manová, A.: On the structure of lead(II) complexes in aqueaous solutions. Part IV.

Binuclear clusters. Part IV. Binuclear clusters. Polyhedron 22, 2863-2867 (2003). [2] Čižmáriková, R., Račanská, E., Hroboňová, K., Lehotay, J., Ághová, Z., Halešová, D.: Synthesis, pharmacological

activity and chromatographic separation of some novel potential beta-blockers of the aryloxyaminopropanol type. Pharmazie 58, 237–241 (2003).

[3] Ďungelová, J., Lehotay, J., Čižmárik, J., Armstrong, D.W.: Study of mechanism of enantioseparation. IV. Enantioseparation of some derivatives of phenylcarbamic acid using pi-complex stationary phase in HPLC. J. Liq. Chromatogr. 26 (14), 2331–2350 (2003).

[4] Ďungelová, J., Lehotay, J., Rojkovičová, T.: HPLC Chiral Separations Using the Macrocyclic Antibiotics. Chem. Anal. (Warsaw) 48, 1–18 (2003).

[5] Hroboňová, K., Lehotay, J., Čižmárik, J.: Study of mechanism of enantioseparation. Part V. HPLC chiral analysis of alkoxysubstituted esters of phenylcarbamic acid on beta-cyclodextrin stationary phase. Chem. Anal. 48, 473-482 (2003).

[6] Korbut, O., Bučková, M., Labuda, J., Gründler, P.: Voltammetric detection of antioxidative properties of flavonoids using electrically heated DNA modified carbon paste electrode. Sensors 3, 1-10 (2003).

[7] Korenková, E., Matisová, E., Slobodník, J.: Study on the feasibility of coupling large-volume injection to fast gas chromatography with mass spectrometric detection for analysis of organochlorine pesticides. J. Sep. Science 26, 1193-1197 (2003).


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[8] Krolicka, A., Bobrowski, A., Kalcher, K., Mocák, J., Svancara, I., Vytras, K.: Study on Catalytic Adsorptive Stripping Voltammetry of Trace Cobalt at Bismuth Film Electrodes. Electroanal. 15, 1859-1863 (2003).

[9] Krupčík, J., Oswald, P., Benická, E., Mydlová, J.: Kalibrácia odozvy plameňovoionizačného detektora při analýze vyššie vriacich ropných destilačných frakcií klasickou a rýchlou kapilárnou plynovou chromatografiou. Chem. Listy 97, 41-44 (2003)

[10] Krupčík, J., Oswald, P., Májek, P., Sandra, P., Armstrong, D.W.: Determination of the interconversion energy barrier of enantiomers by separation methods J.Chromatogr. 1000, 779-800 (2003).

[11] Labuda, J., Bučková, M., Heilerová, Ľ., Šilhár, S., Štepánek, I.: Evaluation of the redox properties and anti/pro-oxidant effects of selected flavonoids by means of a DNA-based electrochemical biosensor. Anal. Bioanal. Chem. 376, 168-173 (2003).

[12] Matisová, E., Dömötörová, M.: Fast gas chromatography and its use in trace analysis. Fast gas chromatography and its use in trace analysis. J. Chromatogr. A 1000, 199-221 (2003).

[13] Murphy, M. A., Marken, F., Mocák, J.: Sonoelectrochemistry of molecular and colloidal redox systems at carbon nanofiber -ceramic composite electrodes. Electrochim. Acta 48, 3411-3417 (2003) .

[14] Rojkovičová, T., Hroboňová, K., Lehotay, J., Čižmárik, J.: Coupled column chromatography for separation and determination of enantiomers of phenylcarbamic acid derivatives in serum.Pharmazie 58 (2), 108–110 (2003).

[15] Rojkovičová, T., Lehotay, J., Čižmárik, J.: Kinetic Study of Derivates of Phenylcarbamic Acid Enantiomers in Rabbit Blood Serum Using an On-line Coupled Column Liquid Chromatographic System. Pharmazie 58 (7), 483–486 (2003).

[16] Sádecká, J., Karasová, G., Polonský, J.: Determination of pantothenic acid in food by capillary isotachophoresis. European Food Research and Technology 216 (5), 440–444 (2003).

[17] Sádecká, J., Polonský, J.: Determination of inorganic anions in saliva by capillary isotachophoresis. Talanta 59, 643-649 (2003).

[18] Sádecká, J., Polonský, J.: Determination of organic acids in tobacco by capillary isotachophoresis. J. Chromatogr. A 988, 161-165 (2003).

[19] Tomčík, P., Banks, C.E., Compton R.G.: Sonoelectrochemistry in Acoustically Emulsified Media: The Detection of Lead. Electroanalysis 15 (21), 1661-1666 (2003).

[20] Tomčík, P., Mrafková, L., Bustin, D.: Microanalytical Determination of Formaldehyde by Direct Titration with Hydroxylamine Using Interdigitated Microelectrode Array Biamperometric End-point Indicator. Microchim. Acta 141, 69-72 (2003).

[21] Vaníčková, M., Labuda, J., Lehotay, J., Čižmárik, J.:Interaction of some esters of 2-, 3-, 4-alkoxyphenylcarbamic acids with surface-bound DNA at a dsDNA modified electrode. Study of local anaesthetics: part 164. Pharmazie 58, 570-572 (2003).

[22] Vrábel, V., Kožíšek, J., Marchalín, Š.: Diethyl 2-methyl-6-(2-thiazolidinyl)-4-(2-thienyl)-1,4-dihydropyridine-3,5-dicarboxylate. Acta Cryst. E59, 376-377 (2003).

[23] Vrábel, V., Kožíšek, J., Marchalín, Š.: Diethyl(2’R,4R,4’R)-2-(4’-ethoxycarbonyl-2’-thiazolidinyl)-6-methyl-4-(2’’-thienyl)-1,4-dihydropyridine-3,5-dicarboxylate. Acta Cryst. E59, 1964-1966 (2003).

[24] Vrábel, V., Marchalin, Š., Kožíšek, J.: Isopropyl 2-methyl-4-(3-nitrophenyl)-5,7-dioxo-4,5,6,7-tetrahydro-1H-yrrolo[3,4-b]pyridine-3-carboxylate. Acta Cryst. E59, 1570-1571 (2003).

[25] Vrábel, V., Oktavec, D., Marchalín Š.: 2,3-Dimethyl 5-isopropyl 1-ethoxymethyl-6-methyl-4-(3-nitrophenyl)-1,4-dihydropyridine-2,3,5-tricarboxylate. Acta Cryst. E59, 306-307 (2003).

[26] Žiaková, A., Brandšteterová, E., Blahová, E.: Matrix solid-phase dispersion for the liquid chromatographic determination of phenolic acids in Melissa officinalis. Journal of Chromatography A 983, 271-275 (2003).

[27] Žiaková, A., Brandšteterová, E.: Validation of HPLC determination of phenolic acids present in some Lamiaceae family plants. Journal of Liquid Chromatography & Related Technologies 26 (3), 443-453 (2003).

[28] Ďungelová, J., Lehotay, J., Rojkovičová, T., Čižmárik, J.: Chirálne separácie niektorých liečiv na báze makrocyklických antibiotík v HPLC, SFC a CEC. Chiral Separation of Some Drugs Using Macrocyclic Antibiotics in HPLC, SFC and CEC. Čes. slov. Farm. 52 (3), 119-125 (2003).

[29] Rojkovičová, T., Lehotay, J., Čižmárik, J.: Vplyv sacharidových častí v teikoplanínovej stacionárnej fáze na separáciu niektorých enantiomérov fenylkarbámového typu metódou hplc. Influence of Saccharide Part of Teicoplanin Stationary Phase on Separation of Some Phenylcarbamic Derivates by HPLC Čes. slov. Farm. 52 (2), 97–101 (2003).

[30] Heilerová, Ľ., Bučková, M., Tarapčík, P., Šilhár, S., Labuda, J.: Comparison of antioxidative activity data for the aqueous extracts of lemon balm (Melissa officinalis L.), oregano (Origanum vulgare L.), thyme (Thymus vulgaris L.) and agrimony (Agrimonia eupatoria L.) obtained by conventional methods and the DNA-based biosensor. Czech. J. Food Sci. 21 (2), 78-84 (2003).

[31] Karasová, G., Brandšteterová, E., Lachová, M.: Matrix solid phase dispersion as an effective preparation method for food samples and plants before HPLC analysis. Czech J.Food Sci. 21 (6), (2003).

[32] Laštincová, J., Pospíšilová, L., Matúšková, L., Kaderová, E., Beinrohr, E.: Determination of total contents of Cd, Pb, Cr, Ni, As, Cu, Zn, Co, V, Mo in some Slovak soils. Chem. Pap. 57 (2), 131-135 (2003).

[33] Manová, A., Beinrohr, E., Jurica, Ľ.: Preconcentration of Hg(II) and total Hg in waters for flame AAS in a flow-through electrochemical cell. Chem. Pap. 57 (3), 197-200 (2003).

[34] Mocak, J., Balla, B., Bobrowski, A., Blažíček, P.: Proper Ways of Comparison of Two Laboratory Methods. Chem. Pap. 57 (3), 143-146 (2003) .

[35] Beinrohr, E., Manová, A.: Modern electroanalytical methods in the analysis of environmental samples. Slovak Geol. Mag. 9 (2-3), 119-122 (2003).

[36] Čižmárik, J., Ďungelová, J., Lehotay, J., Armstrong, D.W.: Thermodynamic Study of HPLC Separation of Some Enantiomers of Phenylcarbamic Acid Derivatives Acta Fac. Pharm. Univ. Com. 50, 30-37 (2003).

[37] Čižmárik, J., Ďungelová, J., Lehotay, J., Armstrong, D.W.: Thermodynamic Study of HPLC Separation of Some


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Enantiomers of Phenylcarbamic Acid Derivatives Acta Fac. Pharm. Univ. Com. 50, 30-37 (2003). [38] Čižmáriková, R., Račanská, E., Hroboňová, K., Lehotay, J., Mišíková, E.: Synthesis and Enantioseparation of

Some Aryloxyaminopropanol Derivatives and Their Effects on the Central Nervous System. Acta Fac. Pharm. Univ. Com. 50, 38-50 (2003).

[39] Čižmáriková, R., Račanská, E., Hroboňová, K., Lehotay, J., Mišíková, E.: Synthesis and Enantioseparation of Some Aryloxyaminopropanol Derivatives and Their Effects on the Central Nervous System. Acta Fac. Pharm. Univ. Com. 50, 38-50 (2003).

[40] Balla, B., Pivovarníkova, H., Balla, J., Varmusova, E., Mocák, J.: Objective Determination of the Cut-off Value for Diagnosis Verification Using Commercial Software. Lab. Diag. 8, 15 (2003).

[41] Buzinkaiová, T.: Praktické úlohy z Analytickej chémie, Chemická olympiáda - kategória A - šk. rok 2002/03. Republikové kolo. Practical excercise in analytical chemistry. Chemical competition of secondary schools - category A -school term 2002/03. Chemické rozhľady, č.1, 21-23 (2003), Vyd. IUVENTA Bratislava

[42] Buzinkaiová, T.: Riešenie úloh z chemickej praxe - analytická chémia. Chemická olympiáda - kategória A - 40. ročník - šk. rok 2003/04. Školské kolo - študijná časť. Chemické rozhľady, č.1, 207-208 (2003), Vyd. IUVENTA Bratislava

[43] Buzinkaiová, T.: Úlohy z chemickej praxe - analytická chémia, Chemická olympiáda - kategória A - 40. ročník - šk. rok 2003/04. Školské kolo - študijná časť. Excercise from chemical practice - Analytical chemistry, Category A Chemické rozhľady, č.3-4, 179-180 (2003), Vyd. IUVENTA Bratislava.

[44] Mocák, J., Balla, B., Varmusova, E., Pivovarnikova, H., Balla, J.: Laboratory Diagnosis Based on the Use of Statistical Methods. Lab. Diag. 8, 29-30 (2003).

B. Conferences [1] Karasová, G.*, Sádecká, J., Polonský, J.: Determination of inorganic anions in saliva by capillary isotachophoresis.

In: Proc. 23rd International symposium „Industrial toxicology `03”, Bratislava, SR, June 18-20, 2003, Slovenská spoločnosť priemyselnej chémie Bratislava, p.178-181 (2003), ISBN 80-968011-5-5. (Po)

[2] Kotianová, P.*, Dudešek, M.: Vehicles exhaust and other sources of atmospheric aerosols. In: Proc. 23rd International symposium „Industrial toxicology `03”, Bratislava, SR, June 18-20, 2003, Slovenská spoločnosť priemyselnej chémie Bratislava, s.253-256, ISBN 80-968011-5-5. (Po)

[3] Kotianová, P.*, Puxbaum, H.: Atmospheric organic aerosol (Markers and source/receptor model). In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 8, 1P-40, 609-610 (2003). ISSN 0009-2770. (Po)

[4] Manová, A., Beinrohr, E., Střelec, M.*: Off-line preconcentration nad GFAAS determination of As in waters. In: Proc. 23rd International Symposium Industrial Toxicology ´03, Bratislava, SR, June 18-20, 2003, Slovenská spoločnosť priemyselnej chémie Bratislava, p.282-284 (2003). ISBN 80-968011-5-5. (Po)

[5] Rievaj, M.*, Tomčík, P., Bustin D.: Possibilities of IDA Microelectrodes Application in Trace Analysis. In: Proc. 23rd International symposium „Industrial toxicology `03”, Bratislava, SR, June 18-20, 2003, Slovenská spoločnosť priemyselnej chémie Bratislava, p. 285-289 (2003). ISBN 80-968011-5-5. (Po)

[6] Mocák, J.*, Balla, B.: Multivariate data analysis based on the analyses of tumor and cardiovascular markers. In: Proc. Slovenian Chem. Days, Maribor, Slovenia, September 25-26, 2003, Sloven. Chem. Soc., CD-ROM, p. 62/1-62/7 (2003). ISBN 86-435-0565-X. (PPr)

[7] Kotianová, P.*, Puxbaum, H.: Utilization of liquid extraction for analysis of organic aerosols. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 8, 1L-05, 609-610 (2003). ISSN 0009-2770. (Pr)

[8] Labuda, J.*, Vaníčková, M., Bučková, M., Ferancová, A., Korgová, E. Štepánek, I.: Single-use DNA biosensors for the study and determination of antioxidants and species binding to DNA. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 840-841 (2003). (Pr)

[9] Balla, B.*, Mocák, J.: Efficiency, determination of the cut-off values, ROC curves and software used for the diagnosis prediction. In: Proc. Slovenian Chem. Days., Maribor, Slovenia, September 25-26, 2003, Sloven. Chem. Soc., CD-ROM, p. 23/1-23/5 (2003). ISBN 86-435-0565-X. (Pr)

[10] Vaníčková, M., Ponická, M., Labuda*, J., Lehotay, J., Čižmárik J.: DNA biosensors-application at the study and determination of local anaesthetics. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. listy 97, 861 (2003). (Po)

[11] Beinrohr, E.*, Dzurov, J.: Prietoková coulometria s využitím pórovitých elektród. Flow-through coulometry with porous electrodes. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 839-839 (2003). ISSN 0009-2770. (Pr)

[12] Lehotay, J.: Súčasné možnosti analytickej chémie v oblasti stopovej analýzy. Present Possibilities of Analytical Chemistry in Trace Analysis In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 607-608 (2003). (Pr)

[13] Manová, A.*, Střelec, M., Beinrohr, E.: Off-line spojenie elektrochemickej a fotometrickej metódy a využitie tejto techniky na stanovenie arzénu vo vodách. Off-line connection of electrochemical and photometric method and utilisation of the technique in As determination in waters. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 614-614 (2003). (Pr).

[14] Mocák, J., Balla, B.: Chemometricky podporovaná diagnostika civilizačných ochorení. Chemometrically aided diagnosis of civilization diseases. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 736-737 (2003). (Pr)

[15] Buzinkaiová, T.: Analýza vybraných antiarytmík metódou kapilárnej izotachoforézy. The analysis of selected antiarytmics by capilary isotachophoresis. In: Proc. 15th International Conference Chromatographic methods and human health. November 10-13, 2003, Piešťany, Slovakia, SCHS, 2003, s.89-90. ISSN 1335-5236. (Po)

[16] Májeková, M., Račková, L., Májek P.*: Antioxidačné vlastnosti a rozdeľovanie substituovaných pyridoindolov. In: Proc. 15th International Conference Chromatographic methods and human health. November 10-13, 2003, Piešťany, Slovakia, SCHS, 2003, s.55-56. ISSN 1335-5236. (Po)

[17] Mocák, J.*, Balla, B.: Počítačom podporovaná lekárska diagnóza s využitím multivariantnej analýzy dát. Computer-


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aided medical diagnosis using multivariate data analysis. In: Analýza dat a statistické metody pro praxi. Statistické metody v praxi, seminár Bohdaneč, 14-16.4.2003, (K. Kupka, ed.) vyd. Trilobyte, Pardubice, ČR, s. 47-54 (2003). ISBN 80-239-1379-4. (PPr)

[18] Zima*, J., Dvoraková, J., Barek, J., Labuda J.: Determination of 1-naphthylamine on carbon paste electrode modified by cyclodextrines. In: Sborník, Moderní elektrochemické metódy XXIII., Jetrichovice 20.-22. 5. 2003, Eds. J. Barek, T. Navrátil, L. Novotný, s. 106-110. ISBN 80-86238-29 6. (Pr)

[19] Lehotay, J.: Najnovšie trendy v stopovej a ultrastopovej analýze. Trends in Trace and Ultratrace Analysis In: LABOLARIM 2003, XIV. medzinárodná konferencia o analytických metódach v potravinárstve, 18.-19. február 2003, Banská Bystrica, Slovensko, Zborník príspevkov, STU Bratislava, s. 7–11 (2003), ISBN 80-227-1887-4. (Po)

[20] Mocák, J.*: Praktické určovanie neistôt – prípadová štúdia o stanovení čísla kyslosti. Determination of uncertainties in practice - case study concerning acid number calculation In: Zborník referátov: Neistoty merania. Bratislava, február 2003. Chemmea - Slovalco, Žiar n. Hr. 2003, p. 4-12. (PPr)

[21] Mocák, J.*: Praktický návod výpočtu kombinovanej neistoty. Practical guide to the combined uncertainty calculation. In: Zborník referátov: Neistoty merania. Bratislava, február 2003. Chemmea - Slovalco, Žiar n. Hr. 2003, p. 13-23. (PPr)

[22] Balinova, A., Lentza-Rizos, C., Hajšlová, J., Matisová, E.*, Sakaliene, O., Kaya, U.: Minimisation of Pesticide Residues in Procesed food – an Integrated study. In: 3rd Symposium, Mediterranean Group of Pesticide Research, Crop Protection, Aix en Provence, France, May 20-24, 2003. Book of abstracts, Poster 4 (2003). (Po)

[23] Blahová, E.*, Brandšteterová, E., Fabulová, A.: Application of polymer sorbents in sample-handling of complex matrices before HPLC analysis. In: 5th Balaton Symposium on High Performance Separation method, 3.–5. September 2003, Siófok, Hungary, Book of Abstracts, P-118. (Po)

[24] Blahová, E.*, Brandšteterová, E., Fabulová, A.: HPLC determination of phenolic antioxidants in fruit-green tea. In: Vitamíny 2003 – Přírodní antioxidanty a volné radikály, 15.–17. september 2003, Pardubice, Česká republika, Sborník konference, s. 232 (P-47). ISBN 80-7194-549-8. (Po)

[25] Dömötörová, M.*, Matisová, E., Hercegová, A., Kirchner, M., Otrekal, R.: Optimisation of Matrix Solid-Phase Dispersion Method for the Analysis of Pesticide Residues in Apples. In: 1st International Symposium on Recent Advances in Food Analysis, Prague, Czech Republic, November 5-7, 2003, Book of Abstracts, P-46, s.162 (2003). ISBN 80-7080-528-5. (Po)

[26] Ďungelová, J., Lehotay, J.*, Krupčík, J., Čižmárik, J., Armstrong, D.W.: Selectivity Tuning of Serially Coupled Columns in Chiral HPLC. In: 26th International Symposium on Capillary Chromatography and Electrophoresis, May 18–22, 2003, Las Vegas, Nevada, USA, Internet publication, P 133. (Po)

[27] Ďungelová, J., Lehotay, J., Krupčík, J., Čižmárik, J., Armstrong, D.W.: Series-coupled chiral columns for the separation of some enantiomers by HPLC. In: 32. konference Syntéza a analýza léčiv, 16.–19.9. 2003, Velké Karlovice, Sborník, str. 63–64 (2003), ISSN 80-900306-5-3.(Po)

[28] Ďungelová, J., Lehotay, J., Rojkovičová, T.*, Čižmárik, J., Armstrong, D.W.: Influence of Temperature on Chiral HPLC Separation of Some Local Anaesthetic Drugs on Pirkle Type Column. A Thermodynamic Study. In: 5th Balaton Symposium on High Performance Separation method, 3.–5. September 2003, Siófok, Hungary, Book of Abstracts, P-23. (Po)

[29] Ferancová*, A., Bučková, M., Korgová, E., Sádecká, J., Labuda J.: Biosensors based on DNA modified screen-printed electrodes. In: Vitamíny 2003 – Přírodní antioxidanty a volné radikály, 15.–17. september 2003, Pardubice, Česká republika, Sborník konference (Eds. J. Blattná, A. Horna), s. 29-30. ISBN 80-7194-549-8. (Po)

[30] Ferancová, A., Bučková, M., Korgová*, E., Labuda J.: Detection of species leading to DNA damage and DNA protection. In: Proceedings, 23th International Symposium „Industrial Toxicology 03“ , 18.-20. 6. 2003, Bratislava, Slovak Republic, Eds. V. Romančík, V. Koprda, p. 268. ISBN 80-968011-5-5, ISSN 1335-3160. (Po)

[31] Ferancová, A., Korgová*, E., Labuda, J.: Detection of polycyclic aromatic hydrocarbon derivatives at cyclodextrin modified carbon electrodes. In: Proceedings, 23th International Symposium „Industrial Toxicology 03“ , 18.-20. 6. 2003, Bratislava, Slovak Republic, Eds. V. Romančík, V. Koprda, p. 269 (2003). ISBN 80-968011-5-5, ISSN 1335-3160. (Po)

[32] Hercegová, A.*, Matisová, E., Dömötörová, M., Kirchner, M.: Modern Sample Pretreatment Techniques Combinated with Fast GC for Pesticide Residues Analysis. In: 1st International Symposium on Recent Advances in Food Analysis, Prague, Czech Republic, November 5-7, 2003, Book of Abstracts, P-78, s.176 (2003). ISBN 80-7080-528-5. (Po)

[33] Hroboňová, K.*, Lehotay, J., Čižmárik, J.: HPLC Determination of Glucose, Fructose and Saccharose in Honey. In: Proc. 15th International Conference Chromatographic methods and human health. November 10-13, 2003, Piešťany, Slovakia, SCHS, 2003, s.77-78. ISSN 1335-5236. (Po)

[34] Hroboňová, K.*, Lehotay, J., Čižmárik, J.: HPLC Separation of Some Anestetics of Phenylcarbamic Type. In: 32. konference Syntéza a analýza léčiv, 16.–19.9. 2003, Velké Karlovice, Sborník, str. 52– 53 (2003). ISBN 80-900306-5-3. (Po)

[35] Karasová, G.*, Brandšteterová, E., Lachová, M.: MSPD as Preparation Method before HPLC Analysis of Phenolics in Tea Samples. In: Vitamíny 2003 – Přírodní antioxidanty a volné radikály, 15.–17. september 2003, Pardubice, Česká republika, Sborník konference, s. 233 (P-48). ISBN 80-7194-549-8. (Po)

[36] Karasová, G.*, Sádecká, J., Polonský, J.: The Use of Capillary Isotachophoresis for the Determination of Pantothenic Acid in Foods. In: 5th Balaton Symposium on High Performance Separation method, 3.–5. September 2003, Siófok, Hungary, Book of Abstracts, P-50. (Po)

[37] Kirchner, M.*, Matisová, E., Dömötörová, M., Hercegová, A.: Utilisation of Fast GC with Splitless Injection for Pesticides analysis. In: 1st International Symposium on Recent Advances in Food Analysis, Prague, Czech Republic, November 5-7, 2003, Book of Abstracts, P-90, s.182 (2003). ISBN 80-7080-528-5.(Po)

[38] Krupčík, J., Májek, P., Sandra, P., Armstrong, D.W.: On the Challenges of Chemometrics in Analytical Separation Sciences. In: 26th International Symposium on Capillary Chromatography and Electrophoresis, May 18-22, 2003,


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Las Vegas, Nevada, USA, Internet publication. (Po) [39] Matisová, E.*, Dömötörová, M., Kirchner, M.: In: 3rd Symposium, Mediterranean Group of Pesticide Research,

Crop Protection, Aix en Provence, France, May 20-24, 2003, Book of abstracts, Poster 51 (2003). (Po) [40] Rojkovičová, T.*, Lehotay, J., Fedurcová, A., Čižmárik, J., Armstrong, D.W.: HPLC of Chiral Derivatives of

Alkoxyphenylcarbamic Acid Using a Teicoplanin Aglycone Chiral Statinary Phase. Effect of Temperature on Chiral Discrimination. In: 5th Balaton Symposium on High Performance Separation method, 3.–5. September 2003, Siófok, Hungary, Book of Abstracts, P-188. (Po)

[41] Sádecká J.: Capillary isotachophoresis of some water-soluble vitamins. In: Proc. 15th International Conference Chromatographic methods and human health. November 10-13, 2003, Piešťany, Slovakia, SCHS, 2003, s.91. ISSN 1335-5236. (Po)

[42] Serdt, K.*, Lankmayr, E., Mocák, J., Balla, B., Wenzl, T., Bandoniene, D.: UV-Vis, NIR, FTIR and chemometrical classification of pumpkin seed oils. In: 7th International Symposium Instrumental Analysis, September 21-24, Pecs, Hungary, 2003, Book of Abstracts, p. 101. (Po)

[43] Labuda, J.*, Vaníčková, M., Bučková, M., Ferancová, A., Korgová, E.: Analytical application of DNA modified screen-printed electrodes based on DNA association interactions and damage. In: Book of abstracts, Workshop on New trends in nucleic acid based biosensors, Florence, Italy, 25.-28.10. 2003, p. 11. (PPr)

[44] Labuda, J.*, Vaníčková, M., Bučková, M., Ferancová, A., Korgová, E.: DNA electrochemical biosensors for the detection of DNA interactions and damage. In: Book of Abstracts, International Symposium on Sensor Science I3S 2003, Paris, France, 16.-20. 6. 2003, p.2. (PPr)

[45] Labuda, J.*: DNA modified screen-printed carbon electrodes as chemical sensors. In: Book of Abstracts, Workshop on surface modification for chemical and biochemical sensing, Bialowieza, Poland, 13.-16. 11. 2003, Ed:Pielaszek research, Warsaw, Poland, p. 34 (2003). ISBN 83-89585-01-04. (PPr)

[46] Lehotay, J., Rojkovičová, T., Ďungelová, J., Čižmárik, J., Armstrong, D.W.: HPLC separation of some enantiomers on chiral stationary phase based on macrocyclic antibiotics. In: Proc. 10th Beijing Conference and Exibition on Instrumental Analysis, October 13-16, 2003, D 143–144. (PPr)

[47] Mocák, J.*, Balla, B.: New Ways of Computer Aided Clinical Diagnosis. In: Conferentia Chemometrica, ACE & CC 2003 . Budapest, Hungary, 2003, Abstract Book (K. Héberger, ed.) p. L16. ISBN 963-508-391-2. (PPr)

[48] Bobrowski, A.*, Mocák, J., Bas, B., Dominik, J., Pereira, H.: Chemometric characterisation and comparison of the analytical methods for the determination of chromium in water samples. In: Book of Abstracts, 13th International Symposium Spectroscopy in Theory and Practice. Nova Gorica, Slovenia, August 27-30, 2003, p. 26. ISBN 961-6311-16-6. (Pr)

[49] Serdt, K.*, Balla, B., Wenzl, T., Lankmayr, E., Mocák, J.: Chemometrical Classification of Pumpkin Seed Oil. In: Book of Abstracts, 10th YISAC´03, June 3-5, Venice, 2003, p. 41. (Pr)

[50] Ďungelová, J.*, Lehotay, J., Čižmárik, J.: Chromatografická separácia esterov kyseliny fenylkarbámovej na Pirklovej kolóne. Chromatographic Separation of Some Esters of Phenylcarbamic Acid using Pirkle Column. In: Študenská vedecká konferencia, PríF UK a SAV, Bratislava, SR, 9.–10. apríl 2003, Zborník abstraktov prác diplomantov a doktorandov, str. 198, 2003. (Po)

[51] Fedurcová, A.*, Lehotay, J., Rojkovičová, T., Čižmárik, J., Armstrong, D.W.: Termodynamická štúdia chromatografického systému pri chirálnych separáciách enantiomérnych derivátov fenylkarbámovej kyseliny metódou HPLC. Thermodynamic Study of Chiral Separations of Some Phenylcarbamic Enantiomers by HPLC. In: Proc. 15th International Conference Chromatographic methods and human health. November 10-13, 2003, Piešťany, Slovakia, SCHS, 2003, s.52-53. ISSN 1335-5236. (Po)

[52] Karasová, G.*, Brandšteterová, E.: MSPD extrakcia a HPLC stanovenie fenolických látok v čaji. MSPD extraction and HPLC determination of phenolic compounds in tea. In: Proc. 15th International Conference Chromatographic methods and human health. November 10-13, 2003, Piešťany, Slovakia, SCHS, 2003, P-20, s. 75. ISSN 1335-5236. (Po)

[53] Meričko, D.*, Rojkovičová, T., Lehotay, J., Čižmárik, J.: Využitie chirálnych stacionárnych fáz na báze makrocyklického antibiotika na separáciu niektorých derivátov kyseliny fenylkarbámovej metódou HPLC. Use of chiral stationary phases based on macrocyclic antibiotic in the HPLC separation of some derivatives of phenylcarbamic acid. In: Študenská vedecká konferencia, PríF UK a SAV, Bratislava, SR, 9.–10. apríl 2003, Zborník abstraktov prác diplomantov a doktorandov, s. 63 (Po)

[54] Mydlová, J.*, Špánik, I., Benická, E., Krupčík, J., Sandra, P.: Dekonvolúcia píkov v analyze pesticídov metódou GC-MS. Peak deconvolution in the gas chromatographic analysis of pesticides. In: Proc. 15th International Conference Chromatographic methods and human health. November 10-13, 2003, Piešťany, Slovakia, SCHS, 2003, P 33. ISSN 1335-5236. (Po)

[55] Rojkovičová, T.*, Lehotay, J., Fedurcová, A., Čižmárik, J., Armstrong, D.W.: Štúdium entalpického a entropického príspevku pri chirálnych separáciách niektorých derivátov fenylkarbámovej kyseliny metódou HPLC. Enthalpic and Enthropic Study of Chiral Separation of Some Phenylcarbamic Derivatives Using HPLC. In: 32. konference Syntéza a analýza léčiv, 16.–19.9. 2003, Velké Karlovice, Sborník, str. 81–82 (2003). ISBN 80-900306-5-3 (Po)

[56] Rojkovičová, T.*, Lehotay, J., Meričko, D., Čižmárik, J., Armstrong, D.W.: Vplyv metylových skupín v teikoplanínovej chirálnej stacionárnej fáze na separáciu enantiomérnych derivátov fenylkarbámovej kyseliny metódou HPLC. Influence of Methyl groups in Teicoplanin Stationary Phase on Separation of Phenylcarbamic Enantiomers by HPLC. In: Proc. 15th International Conference Chromatographic methods and human health. November 10-13, 2003, Piešťany, Slovakia, SCHS, 2003, s.54, ISSN 1335-5236. (Po)

[57] Mocák, J.*, Balla, B.: Použitie mnohorozmernej analýzy dát a umelých neurónových sietí na klasifikáciu objektov - aplikácia na analýzu bielych vín. Utilization of multidimensional data analysis and artificial neural networks for analysis of objects - application to white wine analysis. In: Konference Víno a zdraví, 7. 11. 2003, Brno, Česká republika, Abstrakty, p. 5. (PPr)

[58] Beinrohr, E.*: Stanovenie arzénu, antimónu, selénu, kadmia a ortuti metódami prietokovej coulometrie.


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Determination of arsenic, antimony, selenium, cedmium and mercury by flow-through coulometry. In: Zborník konferencie Chemické analýzy pri zabezpečení ochrany zdravia obyvateľstva, 2.-3.10.2003, Donovaly, SR, Ed: ŠŠZÚ Banská Bystrica, str. 9, ISBN 80-967858-6-9. (Pr)

[59] Benická, E.*, Fričová, J.: Súčasné možnosti plynovej chromatografie v analýze potravín. Current application of gas chromatography in food analysis. In: Proc. 15th International Conference Chromatographic methods and human health. November 10-13, 2003, Piešťany, Slovakia, SCHS, 2003, L-18, s.33-34. ISSN 1335-5236. (Pr)

[60] Blahová, E.*, Brandšteterová, E., Fabulová, A.: Použitie polymérnych sorbentov na úpravu komplexných vzoriek pred HPLC analýzou. The use of polymer sorbents in handling of complex samples before HPLC analysis. In: Proc. 15th International Conference Chromatographic methods and human health. November 10-13, 2003, Piešťany, Slovakia, SCHS, 2003, L-23, s. 43. ISSN 1335-5236. (Pr)

[61] Blahová, E.*, Žiaková, A., Brandšteterová, E.: Využitie polymérnych sorbentov pri úprave zložitých vzoriek pred HPLC analýzou. The utilization of polymer sorbents for pretreatment of complex samples before analysis by HPLC. In: Študenská vedecká konferencia, PríF UK a SAV, Bratislava, SR, 9.–10. apríl 2003, Zborník abstraktov prác diplomantov a doktorandov, s. 188 (Pr)

[62] Čižmáriková, R.*, Račanská, E., Hroboňová, K., Lehotay, J., Mišíková, E.: Syntéza, farmakologická aktivita a HPLC enantioseparácia potencionálnych b-adrenolytík. Synthesis, pharmacological activity and HPLC enantioseparation of some b-adrenolitics. In: 32. konference Syntéza a analýza léčiv, 16.–19.9. 2003, Velké Karlovice, Sborník, str. 27 (2003). ISBN 80-900306-5-3 (Pr)

[63] Fedurcová, A.*, Rojkovičová, T., Lehotay, J., Čižmárik, J.: Kinetická degradácia enantiomérnych derivátov kyseliny fenylkarbámovej v králičom sére použitím on-line zapojenia achirálnej a chirálnej kolóny. Kinetics of Degradation of Enantiomers of Phenylcarbamic Derivatives in Rabit Serum Using Achiral and Chiral columns in on line mode. In: Študenská vedecká konferencia, PríF UK a SAV, Bratislava, SR, 9.–10. apríl 2003, Zborník abstraktov prác diplomantov a doktorandov, str.200 (2003).

[64] Karasová, G.*, Sádecká, J., Polonský, J.: Stanovenie kyseliny pantoténovej v potravinách kapilárnou izotachoforézou. Determination of pantothenic acid in food using capillary isotachophoresis. In: Študenská vedecká konferencia, PríF UK a SAV, Bratislava, SR, 9.–10. apríl 2003, Zborník abstraktov prác diplomantov a doktorandov, s. 226 (Pr)

[65] Krupčík, J.*, Mydlová, J., Májek, P., Benická, E., Hrouzek, J.: Dekonvolúcia chromatograficky neseparovaných píkov. Matematical deconvolution of nonseparated chromatographic peaks. In: Proc. 15th International Conference Chromatographic methods and human health. November 10-13, 2003, Piešťany, Slovakia, SCHS, 2003, s.13-14. ISSN 1335-5236. (Pr)

[66] Lehotay, J.*, Čižmárik, J., Hroboňová, K., Rojkovičová, T.: Použitie HPLC metódy na štúdium kinetiky rozkladu enantiomérov derivátov kyseliny alkoxyfenylkarbámovej v biologickom materiáli. Kinetic Study of Enantiomer Decomposition of Alkoxyphenylcarbamic Derivatives Using HPLC. In: 32. konference Syntéza a analýza léčiv, 16.–19.9. 2003, Velké Karlovice, Sborník, str. 5 – 6 (2003). ISBN 80-900306-5-3. (Pr)

[67] Lehotay, J.*, Čižmárik, J., Hroboňová, K., Rojkovičová, T.: Separácia enantiomérov v HPLC. Štúdium interakčného mechanizmu. Separation of Enantiomers in HPLC. Study of interaction. In: Proc. 15th International Conference Chromatographic methods and human health. November 10-13, 2003, Piešťany, Slovakia, SCHS, 2003, L-4, s.11-12. ISSN 1335-5236. (Pr)

[68] Oktavec, D.*, Kaderová, E.,Lehotay, J.: Použitie klasických separačných metód pri analýzach anorganických systémov. Analysis of Inorganic Systems By Using Classical Separation Methods. In: Proc. 15th International Conference Chromatographic methods and human health. November 10-13, 2003, Piešťany, Slovakia, SCHS, 2003, s. 25-26, ISSN 1335-5236. (Pr)

[69] Otrekal, R.*, Kirchner, M., Matisová, E.: Analýza pesticídov kapilárnou plynovou chromatografiou a jej kombináciou s SBSE predkoncentračnou technikou. Analysis of Pesticides by Fast Capillary Gas Chromatography in Combination with SBSE Preconcentration Pechnique. In: Študenská vedecká konferencia, PríF UK a SAV, Bratislava, SR, 9.–10. apríl 2003, Zborník abstraktov prác diplomantov a doktorandov, s. 64 (2003). (Pr)

[70] Pivovarníková, H.*, Frajt, J., Kőhlerová, E., Gazdič, P., Vargová, M., Mocák, J., Balla, J., Balla, B.: C-reaktívny proteín - prínos pre posudzovanie kardiovaskulárneho rizika. C-reactive protein - a contribution to diagnosing cardiovascular risk. In: VIII. zjazd Slovenskej kardiologickej spoločnosti, 9-11. októbra 2003, Abstrakty in: Cardiology, č.12 (Suppl.1), 21S, (2003).

[71] Špánik, I.: Preparatívna elektroforéza. The preparative-scale electrophoresis. In: Proc. 15th International Conference Chromatographic methods and human health. November 10-13, 2003, Piešťany, Slovakia, SCHS, 2003, L-17, s.31-32. ISSN 1335-5236. (Pr)

[72] Vigh, Gy.*, Shave, E., Lim, P., Lalwani, S., Hwang, A., Špánik, I.: Recent Developments in Preparative-Scale Electrophoretic Separations. In: HPCE 2003, San Diego CA, January 17-22, 2003, Internet publication (Po).

[73] Fourest*, B., Perrone, J., Tarapčík, P., Giffaut, E.: The Hydrolysis of Protactinium(V) Studied by Capillary Diffusion. In.: Proc. Int. Conf. Migration 03, September 15.-20. 2003, Gyeongju, Korea, (Pr)

[74] Krupčík, J.: Current state and prospects of capillary chromatography. Seminarium at Nicolas Copernicus University, Toruň, Poland, pr

[75] Manová, A.*, Beinrohr, E.: Flow injection electrochemical hydride generation atomic absorption spectrometry for the speciation of inorganic selenium. Konferencia Analysis in Geology and Environment, 12.-14.11.2003, Spišská Nová Ves

[76] Buzinkaiová, T.: Kvalitatívna a kvantitatívna analýza v Chemickej olympiáde. Qualitative and quantitative analysis in chemical competition of secondary schools. "17.seminár pre stredoškolských učiteľov chémie ""Príprava študentov stredných škôl na vysokoškolské štúdium chémie"". 27.-28.8.2003, Bratislava /PPr/"

[76] Mocák, J.: Štatistické metódy v praxi. Statistical Methods in Practice. Analýza dat / Statistické metody v praxi. Celostátní seminář. 14.-16.4.2003, Bohdaneč, ČR. (PPr)

[77] Krupčík, J.: Súčasný stav a perspektívy kapilárnej plynovej chromatografie. Current state and prospects of capillary


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chromatography. IX. Letná škola o kapilárnej plynovej chromatografii, 2.-5.9.2003, FCHPT STU v Bratislave (Pr) [78] Krupčík, J.: Teoretické základy plynovej chromatografie. Theoretical base of gas chromatography. IX. Letná škola

kapilárnej plynovej chromatografie, 2.-5.9.2003, FCHPT STU v Bratislave (Pr) [79] Krupčík, J.: Základy kvalitatívnej a kvantitatívnej analýzy v plynovej chromatografii. Introduction to qualitative and

quantitative analysis by gas chromatography. IX. Letná škola kapilárnej plynovej chromatografie, 2.-5.9.2003, FCHPT STU v Bratislave (Pr)

[80] Labuda, J.: Funkčnosť a analytické využitie biosenzorov. Function and analytical utilisation of biosensors UK PřFa odborná skupina analytickej chémie pri Českej chemickej spoločnost, Praha, Česká republika (2003). (Pr)

[81] Májek, P.: Špeciálne metódy hodnotenia rozsiahlych súborov chromatografických meraní. IX. Letná škola kapilárnej plynovej chromatografie, 2.-5.9.2003, FCHPT STU v Bratislave. (Pr)

[82] Matisová, E.: Rýchla plynová chromatografia a jej využitie v stopovej analýze. Fast gas chromatography and its use in trace analysis.. UK PřFa odborná skupina analytickej chémie pri Českej chemickej spoločnost, Praha, Česká republika (2003). (Pr)

[83] Špánik, I.: Základy plynovej chromatografie. Introduction to gas chromatography. IX. Letná škola kapilárnej plynovej chromatografie, 2.-5.9.2003, FCHPT STU v Bratislave. (Pr)

DEPARTMENT OF BIOCHEMICAL TECHNOLOGY

18


Head of Department: Telephone:++421252967085 Prof. Fedor Malík, PhD, DSc Fax:++421252967085 E-mail: [email protected]

I. STAFF Full Professors: Ján Šajbidor, PhD, DSc Associate Professors: Michal Rosenberg, PhD; Daniela Šmogrovičová, PhD; Ernest Šturdík, PhD; Katarína Dercová, PhD; Mária Šturdíková, PhD; Milan Čertík, PhD;

Assistant Professors : Helena Hronská, PhD; Lucia Sláviková;

Research Fellows: Ľudmila Krištofíková; Dušan Slugeň, PhD;

PhD Students: Michal Brygin; Silvia Firáková; Katarína Furdíková; Katarína Kundríková; Martin Rebroš; Radoslav Selecký; Milan Valach; Igor Voštiar;

Technical staff: Vlasta Sládková; Jaroslava Telgárska;


A. Teaching laboratories: Laboratory of Bioanalytical Chemistry Laboratory of Biotechnology Laboratory of Fermentation Beverages Laboratory of Pharmaceutical Biotechnology Laboratory of Ecological Biotechnology B. Research laboratories: Laboratory for the design of bioactive compounds Laboratory for biotechnological production of organic acids and fine chemicals Laboratory for study, isolation and transformation of microbial lipids Laboratory of secondary metabolites Laboratory of wine microbiology and oenology Laboratory of bioengineering Laboratory for solid-state fermentations Laboratory for solid-state fermentations Laboratory for microbial degradation of xenobiotics Laboratory of brewing technology and ethanol production

III. TEACHING A. Undergraduate Study: 5. semester (Bc) Principles in Biotechnology 2/0/0 Šajbidor Xenobiochemistry 2/0/0 Dercová 6. semester (Bc) Terminal Work 0/0/4 Čertík, Dercová, Malík, Rosenberg,

Šmogrovičová, Šturdík, Šturdíková

1. semester (MSc) Enzymology and Enzyme Engineering

2/0/0 Augustín

Laboratory in Enzymology and Enzyme Engineering

0/2/0 Sláviková

Information Systems and Data Processing

1/1/0 Šmogrovičová, Dômény


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Food Biotechnology 2/0/1 Malík, Slugeň 1. semester (MSc) Bioanalytical Methods 2/0/0 Šajbidor Laboratory in Bioanalytical Methods 0/0/2 Brygin, Čertík, Rebroš, Sláviková Biosynthesis and Transformation of

Metabolites 2/0/0 Rosenberg

Laboratory in Biosynth. and Transformat. of Metabolites

0/0/1 Rosenberg

1. semester (MSc) Terminal Work 0/0/5 Čertík, Dercová, Krištofíková 2. semester (MSc) Bioanalytical Methods 2/0/0 Šajbidor Laboratory in Bioanalytical Methods 0/0/2 Brygin, Čertík, Rebroš, Sláviková Bioengineering 0/2/0 Slugeň Pharmaceutical Biotechnologies 2/0/0 Šturdíková 2. semester (MSc) Laboratory in Pharmaceutical

Biotechnologies 0/0/1 Šturdíková, Firáková

Molecular Biology and Genetics 2/0/0 Čertík Technical Microbiology 2/0/0 Šturdík Information Systems and Data

Processing 1/1/0 Šmogrovičová, Dômény

2. semester (MSc) Nutritional and Functional Properties of Food

2/0/0 Slugeň

Terminal Work 0/0/5 Čertík, Dercová, Rosenberg, Šajbidor, Šmogrovičová, Šturdíková

Special Praxis Ecochemical Biotechnologies 2/0/0 Dercová 3. semester (MSc) Laboratory in Ecochemical

Biotechnologies 0/0/2 Dercová

Malting and Brewing 2/0/0 Šmogrovičová Laboratory in Malting and Brewing 0/0/1 Šmogrovičová, Selecký Chemistry and Microbiology of Wine 2/0/0 Malík 3. semester (MSc) Laboratory in Chemistry and

Microbiology of Wine 0/0/1 Slugeň, Selecký

Microbial Biomass and Distillery 2/0/0 Šmogrovičová, Augustín Laboratory in Microbial Biomass and

Distillery 0/0/1 Šmogrovičová

Biochemical and Genetic Regulations 2/0/0 Šturdík, Valach 3. semester (MSc) Laboratory in Biochemical and

Genetic Regulations 0/0/1 Valach, Brygin

Genetic Manipulations 2/2/0 Čertík Special Laboratory Excersises 0/0/6 Čertík, Dercová, Krištofíková, Malík,

Rosenberg, Šmogrovičová, Šturdíková, Valach

4. semester (MSc) Diploma Work Augustín, Čertík, Dercová, Dômény, Krištofíková, Rosenberg, Šmogrovičová, Šturdík, Šturdíková


A. VEGA Project No 1/9131/02 Application of microorganisms in food industry and agriculture - biotechnological aspects (Ján Šajbidor)

Osmotolerant Saccharomyces cerevisiae important for the production of Tokay type wines were characterised. Their metabolic activity in ethanol presence and high temperature was studied. Selected strains were immobilised on a new type of hydrogele and it was successfully tested in large-scale pilot experiments. Alcaligenes xylosoxid and Pseudomonas stutzeri useful bacteria for bioremediation technologies were tested. Valuable results were presented in papers deals with relationship between structure of xenobiotics and their biodegradability. Experiments with Nocardia species, the strain applicable in food industry as tartaric acid producer continued. Activity of fumarase in our producer Dipodascus magnusii - enzyme for malic acid production by fermentation of sugar medium - have been approximately ten times higher in comparison with earlier published data. We suppose application of this solution in industrial production of malic acid like as former mentioned result. New types of biosensors based on electrochemistry or microcalorimetry principles for monitoring of ethanol production from sucrose, glucose, lactose or biotransformation of glycerol to dihydroxyacetone was published in scientific journals. Individual part of our research is overproduction of secondary metabolites for food industry and pharmacy. New trends in fortification of cereals with essential fatty acids via solid-state fermentations (for human nutrition or animal feed) were published. Very interesting result were obtained during the study of lipogenesis regulation in filamentous fungi.



20

B. VEGA Project No 1/0067/03 Immobilized technologies: Implementation of new immobilization techniques/technologies into plant fermentation and biotransformation and their industrial applications (Ernest Šturdík)

One of the main aims of the project has been to test the selected variety of hydrogels for cell immobilization by techniques of entrapment and encapsulation. These should be applied in fermentation technologies applicable in industrial praxis, mainly in production of ethanol from whey or starch hydrolysates or for production of low- or non-alcoholic beer. Yeast cells were used when immobilized in hydrogels (alginate, pectate, carrageenan) and tested in fermentation processes under batch, semi-continuous and continuous conditions regarding to study effect of immobilization on biological part as well as on transport and stability parameters. Electrochemical and microcalorimetric biosensors have been constructed and successfully applied to monitor the processes mainly of ethanol fermentation as well as on glycerol biotransformation. Project duration: from 01.01.2003 to 31.12.2005

C. VEGA Project No 1/9130/02 Biotechnological aspects of classical and alternative fermented beverages production (Daniela Šmogrovičová)

The aim of the project is an improvement of classical beverages fermentation productivity - beer (bottom fermented and special), production of different categories of wine (still, petillant, sparcling and wines "under veil") and production of fermented beverages with lowered content of alcohol but the traditional character and taste. An increase in gravity results in higher metabolic activity and increased ethanol production, but an effect of osmotic pressure and toxicity of produced ethanol affected yeast viability. Since immobilised cells show various modifications in physiology and metabolic activity, biochemical composition and morphology, as well, an application of immobilised yeast can improve their ability to ferment concentrated substrates in dependence on carrier and technique used for immobilisation and protect the yeast cells against osmotic and ethanolic stress. Immobilisation also influence yeast by metabolites co-production and consequently flavour and character of fermented beverage. Integration of up-to-date knowledge about yeast properties and metabolism should result into elucidation of ethanol tolerance mechanism, improvement of fermentation and production of alternative beverages.

Project duration: from 01.01.2002 to 31.12.2004 D. National project 2003 SP 27/028 0E 02/028 0E 02 Quality, safety and functionality of

primary food resources (Milan Čertík) The project is coordinated by Research Institute of Plant Production where some tasks of the project are carried out in our Faculty. Objectives of these tasks are focused on a) Enhancement of nutritional value of various types of cereals by polyunsaturated fatty acids, b) Evaluation and selection of primarily food resources and preparation of functional food with preventive-medical properties, c) Study of genotype dependence on lipid profile in oil seeds, d) Identification of essential fatty acids donors in cereals.

Project duration: from 22.10.2003 to 31.12.2005 E. National project 2003 SP 27/028 0E 01/028 0E 01 Quality, safety and functionality of

primary food resources (Michal Rosenberg, Milan Čertík) The project is coordinated by Research Institute of Food where one of the task is carried out in our Department. The task is aimed on preparation of conjugated linoleic acid (CLA) from microorganisms. The first step is focused on finding of an effective method for isolation and purification of CLA and on optimizing of suitable analytical method based on gas chromatography for determination CLA content in isolated lipids. Project duration: from 1.5.2003 to 31.12.2005


A. CEEPUS H-158 Green Network in Central Europe (Daniela Šmogrovičová). The network relays mainly on the institutional and personal contacts that were established in a previous CEEPUS network (H-0115). The main objective of this network was to emphasise and strengthen the ecological approach in university education in the fields of horticulture and food science. Continuing this activity in a considerably renewed and extended frame, the present collaboration program focuses on three connecting components of the quality of life: the safety, quality and health aspects of horticultural and food production, landscape ecology and meliorization as well as management of ecological conflicts with the tools of landscape architecture.



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VI. COOPERATION



Duration

Allcop, Bratislava Licence agreement Štubňa Slavomír, director, Kopčianská 61, 851 01 Bratislava

01.01.2003 - 31.12.2003

Water Research Institute, Bratislava Toxicity of chlorophenols

Tóthová Lívia, Nábr. arm. gen. L. Svobodu 5, 812 49 Bratislava

01.01.2000 - 31.12.2005

Soil Science and Conservation Research Institute

Sorption of pentachlorophenol on organomineral complex - zeolite and humic acids

Barančíková Gabriela, Rejmanova 1, 080 01 Prešov

01.01.2000 - 31.12.2005

Institute of Chemistry, Slovak Academy of Sciences, Bratislava

Development of biosensors

Gemeiner Peter, head of the research group, Dúbravská cesta 9, 842 38 Bratislava

01.01.2003


Study of adaptation properties of yeasts under stress conditions

Breierová Emília, head of the Culture Collection of Yeasts, Dúbravská cesta 9, 842 38 Bratislava

01.09.2000


Preparation and isolation of recombinant proteins

Šimuth Jozef, head of laboratory of gene engineering, Dúbravská cesta 9, 842 38 Bratislava

01.01.2003

Research Institute of Plant Production, Piešťany

Quality, safety and functionality of primary food resources

Miština Timotej, director, Bratislavská cesta 122, 921 68 Piešťany

22.10.2003 – 31.12.2005

Research Institute of Food, Bratislava

Quality, safety and functionality of primary food resources

Kováč Milan, director, Priemyselná 4, 824 75 Bratislava

01.05.2003 -



Duration

Department of Pharmaceutical Sciences, North Dakota State University, Fargo, North Dakota, USA

Prediction of the fate of xenobiotics in the environment

Baláž Štefan, professor, Sudro Hall 108, Fargo, North Dakota, USA

01.01.1996

School of Biological Sciences, University of Porthsmouth, UK

SPMD – monitoring of POPS

Vrana Branislav, asistant professor, King Henry I. Street PO12DY, Portsmouth, Hampshire, UK

01.09.2003 -01.09.2005

Institute of Soil, Water and Environmental Sciences, The Volcani Center A.R.O, Bet Dagan, Israel

Sequestration of persistent organic pollutants

Tandlich Roman, asistant professor, P.O.Box 6, Bet Dagan, 50250 Israel

01.10. 2002 - 30.09. 2003

Mega a.s., Stráž pod Rálskem, Czech Republic

Encapsulation of microorganisms to PVA Gel

Novák Luboš, director, Pod Vinicí 83 471 27 Sztráž pod Rálskem, Czech Republic

01.02.2003 - 19.12.2003

Office International de la Vigne et du Vin, Paris, France

Evaluation of wine

Dutruc-Rosset Georges, general director, 18, rue d´Aquesseau 75008 Paris, France

01.01.1983


22

Faculty of Chemistry, Technical University Brno, Czech Republic

Study of stress conditions on carotenogenic yeasts

Márová Ivana, vicedean, Purkyňova 118, 61200 Brno, Czech Republic

01.01.2003 -



Valid date

Šajbidor Ján Slovak Society for Agriculture, Forestry, Food and Veterinary Sciences member 01.01.1987 -

Slugeň Dušan Slovak Society for Agriculture, Forestry, Food and Veterinary Sciences member 01.01.1987 -

Čertík Milan Slovak Society for Agriculture, Forestry, Food and Veterinary Sciences member 01.01.2001 -

Malík Fedor Editorial boards of journal Vinič a víno. presidentmember 01.01.2001 -



Valid date

Šmogrovičová Daniela Editorial boards of the journal Kvasný prumysl member of advisory 01.01.1999 -

Malík Fedor Editorial boards of the journal Kvasný prumysl member of advisory 01.01.1985 - Šmogrovičová Daniela European Brewing Convention Brewing Science Group member 01.12.1998 -

Malík Fedor Editorial boards of journal Mitteilungen Klosterneuburg, Wien member 01.01.2003 -

Čertík Milan The American Oil Chemist´s Society member 01.01.1994

Čertík Milan National Geographic Society member 01.01.2002 -

Čertík Milan The European Federation of Biotechnology member 24. 09. 2003 -



Date / Duration

Čepička, J. University of Chemical Technology, Prague Czech Republic

October 2003 (2 days)



Date / Duration

Malík, F. International Wine Competition, Tsesolloniki Greece February 2003 (6 days)

Malík, F. Vinalies International, Paris France February 2003 (8 days)

Malík, F. Selection Mondial, Bruxelles Belgium April 2003 (4 days)

Malík, F. Prix Zarcillo, Valladolid Spain May 2003 (6 days)

Malík, F. Vino Ljubljana Slovenia June 2003 (5 days)

Malík, F. Mundus Vini, Neustadt/Weinstr. Germany August 2003 (4 days)

Malík, F. Internatiomal Wine Competition, Csopak Hungary September 2003 (2 days)

Malík, F. Embassy of Slovak Republic, Moscow Russia December 2003 (5 days)

Šmogrovičová, D. European Brewery Convention Brewing Science Group, Dresden Germany September 2003

(3 days)

Šmogrovičová, D. 20th Brewing and Malting Days, Frýdek-Místek Czech Republic



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Voštiar, I. Postdoc study stay. Linkoping Univeristy, Division of Biotechnology, Sweden 2002 - 2003

Valach, M. XII. Conference of young microbiologists, Brno Czech Republic

June 2003 (2 days)

Rebroš, M. XII. Conference of young microbiologists, Brno Czech Republic

June 2003 (2days)

Brygin, M. XII. Conference of young microbiologists, Brno Czech Republic

June 2003 (2 days)

Rebroš, M. Study state stay. Mega, a.s., Stráž pod Rálskem Czech Republic

June 2003 (6 days)

Šmogrovičová, D. CEEPUS H-158 Network coordination meeting, Budapest Hungary November 2003

(2 days)



Angelovičová, M. Regulation of microbial overproduction of biologically active polyunsaturated fatty acids in the regime of solid state fermentation. Čertík, M.

Bieliková, S. Fermentation systems for VHG beer production using immobilised yeast cells. Šmogrovičová, D.

Czabany, T. Gene characterization and expression of enzymes involved to biosynthesis of essential fatty acids. Čertík, M.

Daniš, M. Polyunsaturated fatty acids as endogenne bioregulators. Čertík, M. Diničová, Z. Biotechnological aspects of apple-milk fermentation. Malík, F. Garajová, S. Isolation of ethanoltolerant yeast from wine I. Malík, F. Gdovin, M. Production of lactic acid with immobilized cells Bacillus coagulans. Rosenberg, M. Gerová, M. Natural sweeteners produced with osmophilic yeasts. Krištofíková, Ľ. Graczová, M. Isolation, analysis and application of phytosterols. Čertík, M. Kmecová, K. Biotechnological production of carotenoids and their applications. Čertík, M. Maruna, M. Bioactive diterpenoids of actinomycetes. Šturdíková, M. Nádaský, P. The influence of aldehydes on sensoric stability of beer. Šmogrovičová, D. Németh, R. Quo vadis natural sweet wine? Malík, F.

Oláhová, M. Study of adaptation properties of microorganisms under stress conditions. Čertík, M.

Paluch, M. Production of ethanol with Zymomonas mobilis. Rosenberg, M. Santová, J. Chlorinated phenols as possible stress factors for microbila cell. Dercová, K. Skokanová, M. Biodegradation and toxicity of chlorophenols. Dercová, K. Strieženec, V. Isolation of ethanoltolerant yeast from wine II. Malík, F. Žuffa, J. Bioremediation of heavy metals contaminated soil and water. Dercová, K. B. Graduate Theses (MS Degree) for state examinations after five years of study

Name Title of Thesis Supervisor Balogh, P. Microbial production and transformation of flavonoids. Šturdíková,M. Finďová, M. Microbial degradation of polycyclic aromatic hydrocarbons. Dercová, K. Firáková, S. Relations structure-bioactivity of flavonoids. Šturdík, E.

Guzmický, J. The influence of non-alcoholic beer fermentation condition on its analytical parameters. Dômény, Z.

Guži, R. Preparation and biotechnological utilization of ethanol biosensor. Šturdík, E. Ivanová, M. The beer stability in dependence of storage conditions. Šmogrovičová, D.

Kačenová, D. Production of erythritol by the and immobilized cells of osmophilic yeasts. Krištofíková, Ľ.

Kundríková, K. Immoblization of organic acid producers into PVA gel. Rosenberg, M.

Matis, T. Development of biosensor for monitoring of glycerol as biotechnological substrate. Šturdík, E.

Nagyová, K. Application of immobilized cells in cintinuous ethanol fermentation. Šturdík, E

Račková, H. Regulation of biosynthesis of cytotoxic metabolite produced by actinomycete. Šturdíková, M.

Rusnáková, A. Preparation and characterisation of microbial enzyme inhibitor. Šturdíková, M.

Selecký, R. Optimisation of bioengineering fermentation parameters during production of non-alcoholic beer. Dômény, Z.

Stankovská, M. Bacterial biocoenosis of solid surfaces of water course. Augustín, J. Strhanová, K. Effect of heavy metals on yeast strains producing carotenoids pigments. Čertík, M.

Škrinárová, B. Physiological regulation of gama-linoleic acid production in the process of fungal solid state fermentations. Čertík, M.

Vadrnová, R. Production of ethanol by Zymomonas mobilis bacteria. Rosenberg, M.


24

Vidová, M. Continuous production of lactic acid. Rosenberg, M.

VIII. PUBLICATIONS A. Journals

[1] Cvengroschová M., Šepeľová G., Šmogrovičová, D. Effect of mashing-in temperature on free amino nitrogen concentration and foam stability of beer. Monatsschrift für Brauwissenschaft 56 (7/8), 128-131 (2003)

[2] Cvengroschová M., Šepeľová G., Šmogrovičová, D. Influence of pre-isomerised hop on taste and foam stability of beer. Monatsschrift für Brauwissenschaft 56 (11/12), 2003 (in press).

[2] Dercová, K., Kyseľová Z., Barančíková G., Sejáková Z., Maľová A.: Biodegradácia a bioremediácia pentachlórfenolu (PCP). Biodegradation and bioremediation of pentachlorophenol Chem. Listy 10: 991-1002 (2003)

[3] Dercová, K., Tandlich R., Brežná B.: Application of terpenes as possible inducers of biodegradation of PCBs Fresenius Environmental Bulletin 12(3): 286-290 (2003)

[4] Marták, J., Schlosser, Š., Sabolová, E., Krištofíková, Ľ., Rosenberg, M.: Fermentation of lactic acid with Rhizopus arrhizus in a stirred tank reactor with a periodical bleed and feed operation. Process Biochem. 38, 2003, s. 1573-1583.

[5] Šepeľová, G., Cvengroschová M., Šmogrovičová, D.: Reduction of vicinal diketones by yeast in dependence on carbon dioxide pressure. Monatsschrift für Brauwissenschaft 56, (3/4), 44-47 (2003)

[6] Tkáč ,J., Voštiar I., Gorton, L., Šturdík, E., Gemeiner, P.: Improved selectivity of microbial biosensor using membrane coating Biosensors and Bioelectronics

[7] Tkač, J., Voštiar I., Mandenius C.F.: Evaluation of disintegration methods for release of recombinant protein from Escherichia coli for analytical puposes. iotechnology and Applied biochemistry (in presss)

[6] Voštiar, I., Tkáč, J., Mandenius C.-F.: Monitoring of the heat-shock response in E.coli using optical biosensor Monitoring of the heat-shock response in E.coli using optical biosensor Analytical Biochemistry Vol. 322, 156-163, 2003

[7] Šmogrovičová, D., Dömény, Z.: Degradácia a-acetolaktátu imobilizovanou a-acetolaktátdekarboxylázou. Degradation of a-acetolactate by immobilized a-acetolactate decarboxylase. Kvasny Prum. 49 (7-8) 182-185 (2003)

[8] Čertík, M., Dercová, K., Finďová M., Jakubík M., Sejáková Z.: Effect of polyaromatic hydrocarnons (PAHs) on the membrane lipids of bacterial cell. Biológia 58(6): 1111-1117 (2003)

[9] Čertík, M., Shimizu, S.: Isolation and lipid analyses of subcellular fractions from the arachidonic acid producing fungus Mortierella alpina 1S-4. Biologia, 58(6), 2003, 1101-1110.

[10] Valach, M., Šturdík, E. Fermentačná produkcia etanolu. Fermentation production of ethanol Bulletin potravinárskeho výskumu, v tlači ale isto vide v roku 2003

[11] Dömény, Z., Kovács, A., Malík, F., Slugeň, D., Šmogrovičová, D.: Vplyv jablčno-mliečnej fermentácie na senzorický profil vína - imobilizované systémy. Influence of malic-lactic fermentation on sensoric wine profile - imobilized systems Vinič a víno 3 (4), 86-87, (2003).

[12] Dömény, Z., Kovács, A., Šmogrovičová, D., Slugeň, D.: Malovýroby medoviny. Príprava substrátu a hlavné kvasenie. Small-scale production of honey wine. Vinič a víno 3 (2), 40-41, (2003).

[13] Slugeň, D., Malík, F.: Moderné trendy nakvásania bielych rmutov. Modern trends in white mash fermentation. Vinič a víno 3 (5), príl. 2-4, (2003).

[14] Maliar, T., Jedinák, A., Šturdík, E. Inhibícia patofyziologických proteináz ako nástroj terapie závažných ochorení Inhibition of pathofyziologic proteinases as a instrument of momentous affections therapy Nova Biotechnol. 3, 152-165, 2003

[15] Malík, F.: Malokarpatské víno. Little Carpatian Wine. Beverage&Gastro 3 (9-10), 20-21 (2003) [16] Malík, F.: Slovenské vína dnes. Slovak wines today. Beverage&Gastro 3(7-8), 28-29 (2003) [17] Malík, F.: Slovenské vína v minulosti. Slovak wines in the past. Beverage&Gastro 3(5-6), 30-31 (2003) [18] Malík, F.: Stredoslovenské víno. Middle Slovakian wine. Beverage&Gastro 3 (11-12), 26-27 (2003) [19] Malík, F.: Touriga National a iné. Touriga National and other ones. Kvasný průmysl 49(2), 47 (2003) [20] Čertík, M. Vitamín F z mikroorganizmov - komerčná realita alebo akademická kuriozita? Vitamin F from

microorganisms - commercial reality or academic curiosity? Quark, 9(9), 2003, 21-22 [21] Malík, F., Šuranská, Z.: Úspešné slovenské vína. uccessfull slovak wines. Vinič a víno 3, 7-8 (2003) [22] Malík, F.: Ako kategorizovať vína. How to categorise wine. Vinič a víno 3, 62-63 (2003) [23] Malík, F.: Alsasko zem skvelých vín. Alsasce land of excelent wine. Vinič a víno 3, 38-39 (2003) [24] Malík, F.: Brusel - hlavné mesto vína. Brusel - capital of wine. Vinič a víno 3, 65-66 (2003) [25] Malík, F.: Dva dni v Csopaku. Two days in Csopak. Vinič a víno 3, 5 (2003) [26] Malík, F.: Falcké vína. Wins of Pfalz. Vinič a víno 3, 8-9 (2003) [27] Malík, F.: Krater plný dobrého vína. Crates full of good wine. inič a víno 3, 1 (2003) [28] Malík, F.: O konkurze trochu inak. Something else about competition. Vinič a víno 3, 113 (2003) [29] Malík, F.: O konkurze v Budapešti, o tokajskom.. About Budapest concurs, about tokay... Vinič a víno 3, 14 (2003) [30] Malík, F.: Úchytka z Penafiel. Catch of Penafield. Vinič a víno 3, 12-85 (2003) [31] Malík, F.: V kraji kde bociany neodlietajú. At the land of stork never flying away. Gastro 14(5-6), 34-35 (2003) [32] Malík, F.: Vína Saint-Emilionu. Saint Emilion´s wines. Vinič a víno 3, 4-5 (2003) [33] Malík, F.: Vína z Locorotonda. Locorotondo wines. Vinič a víno 3, 2-3 (2003) [34] Malík, F.: Vinalies Internationales v Paríži po deviaty raz. 9-th Vinalies Internationales in Partis. Vinič a víno 3, 45

(2003) [35] Malík, F.: Zlatá Ljubljana. Golden Ljubljana. Vinič a víno 3, 89 (2003) [36] Slugeň, D.: In honorem dei et in honorem vini. In honorem dei et in honorem vini. Vinič a víno 3 (4), 88, (2003). [37] Slugeň, D.: Víno EÚ nielen v číslach. Wine in the European Union not only in nubers. Vinič a víno 3 (4), 78-79,

(2003).


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[38] Vitálová Z., Slugeň, D.: Champagne zo Chantant. Champagne from Chantant. Vinič a víno 3 (5), 117, (2003). [39] Vitálová, Z., Slugeň, D.: Bonvináni - prípad Rossini. Bonvinanes - case Rossini. Vinič a víno 3 (1), 22-23, (2003). [40] Vitálová, Z., Slugeň, D.: Víno v trojštvrťovom takte. Wine in the threequarter tact. Vinič a víno 3 (3), 68-69,

(2003). [41] Vitálová, Z., Slugeň, D.: Víno v trojštvrťovom takte. Wine in the threequarter tact. Vinič a víno 3 (4), 92-93, (2003). [42] Slugeň, D.: Ze života vína. From the life of wine.Vinič a víno 3 (5), 110-111, (2003).

B. Conferences [1] Čertík, M., Sláviková, L. Masrnová, S., Škrinárová, B., Angelovičová, M.: Fungal solid state fermentations –

promising method for developing new bioproducts containing dietary polyunsaturated fatty acids. Proceedings of International Conference “Food Safety and Quality in Transition Countries”, Nitra, 2003, 22-25.

[2] Čertík, M., Sláviková, L., Lai, M.H.: Preparation of bioproducts enriched with polyunsaturated fatty acids based on solid state fermentations. Proceedings of 8th Asean Food Conference, Hanoi, Vietnam, 2003, 654-658.

[3] Čertík, M., Sláviková, L., Škrinárová, B., Angelovičová, M., Slugeň, D., Šajbidor, J., Lai, M.H.: Effect of plant extracts on polyunsaturated fatty acid production during solid state fermentation. Proceedings of 8th Asean Food Conference, Hanoi, Vietnam, 2003, 101-104

[5] Šturdíková, M., Koreňová, A., Végh, D., Boduszek, B., Kravcová, A., Uher, M.*:: Inaktivácia elastázy a katepsínu B tienyl a furyl derivátmi kyseliny aminometylfosfónovej. Inactivation of elastase and cathepsin B by furyl and thienyl derivatives of aminomethylphosphonic acid. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy, 755-778 (2003), 8P-22. ISSN 0009-2770.( Po)

[6] Voštiar, I., Tkáč, J., Mandenius C.-F.: Validation of an optical biosensor method for metabolic stress monitorinf in E.coli. Abstracts from 11th European Congress on Biotechnology, August 24-29, 2003, Basel, Switzerland, 190-191, 2003

[7] Čertík, M., Sláviková, L.: Characterization and application of bioproducts enrichred with polyunsaturated fatty acids based on fungal solid state fermentations. Proceedings of International Conference “Food Safety and Quality in Transition Countries”, Nitra, 2003, 18-21.

[8] Malík, F.*, Slugeň, D.: Slowak wines. History of past and today´s situation in Slovakia. New varieteies, modern technologies, perspective of white and red wines. I Balkan and II Macedonian Symposium for Vine Growing and Wine Production. 25.11 - 28. 11. Skopje, macedonia (2003).Pr

[9] Šmogrovičová, D.: Physiology of brewer’s yeast in stress conditions. Lectures of Joint Meeting of the Yeast Genetics & Physiology and Emerging Fermentation Systems. EBC Sub-Groups. Dresden – Germany, Sept. 17-19, CD (2003)

[10] Breierová, E., Omelková J., Čertík, M., Strhanová, K.: Ovplyvnenie toxického účinku ťažkých kovov aeráciou u karotogénnych kvasinkových druhov. Influence of aeration on toxic effect of heavy metals in carotogenic yeasts. In: Zborník zo XIV. medzinárodnej konferencie LABORALIM, Banská Bystrica, 2003, 119-121. (ISBN 80-227-1887-4)

[11] Brygin, M., Navrátil, M., Šturdík, E.: Monitoring laktózy počas etanolovej fermentácie na enzýmovom termistore Monitoring of lactose during ethanol fermentation using enzyme thermistor. "Zborník príspevkov ""Drobnicov memoriál"" 2. Ročník, Senec 2003, 108 - 109."

[12] Brygin, M., Navrátil, M., Šturdík, E.: Monitoring laktózy pomocou enzýmového termistora. Monitoring of lactose using ezyme thermistor. "Zborník prednášok z XIV. Medzinárodnej konferencie o analytických metódach v potravinárstve ""LABORALIM"", Banská Bystrica 2003, 122 - 125."

[13] Čertík, M.: Využitie kinetických parametrov na sledovanie biosyntézy lipidu a kyseliny arachidónovej tukotvornou hubou Mortierella alpina v submerzných kultiváciach. The use of kinetic parameters for monitoring lipid and arachidonic acid biosynthesis by oleaginous fungus Mortierella alpina during submerged cultivations. (ISBN 80-227-1887-4). Zborník zo XIV. medzinárodnej konferencie LABORALIM, Banská Bystrica, 2003, 46-50. (ISBN 80-227-1887-4).

[14] Čertík, M., Sláviková, L., Masrnová, S., Škrinárová, B., Angelovičová, M., Šajbidor, J.: Biokonverzia exogénnych olejov na kyselinu gama-linolénovú vláknitou hubou Thamnidium elegans v procese polosuchých kultivácii. Bioconversion of exogenous oils to gamma-linolenic acid by filamentous fungus Thamnidium elegans in the process of solid state fermentation. Zborník zo XIV. medzinárodnej konferencie LABORALIM, Banská Bystrica, 2003, 133-136. (ISBN 80-227-1887-4)

[15] Dömény, Z., Malík F., Šmogrovičová, D., Krištofíková Ľ.: Vplyv jablčno-mliečnej fermentácie na analytické parametre vína. The influence of malo-lactic fermentation on analytical parameters of wine. XIV. medzinárodná konferencia o analytických metódach v potravinárstve. Laboralim Banská Bystrica 17.-19. februára 2003, s. 152.

[17[ Dömény, z., Šmogrovičová, D., Brygin M.: Vplyv teploty fermentácie na anylytické a senzorické parametre medoviny. The influence of fermentation temperature on analytical and sensorical parameters of fermented honey XIV. medzinárodná konferencia o analytických metódach v potravinárstve. Laboralim Banská Bystrica 17.-19. februára 2003, s. 156.

[18] Firáková, S.*,Šturdík, E., Maliar, T.: Vzťahy medzi štruktúrou a biologickou aktivitou flavonoidov Structure biological activity relationship of flavonoids. "Zborník príspevkov ""Drobnicov Memoriál"", 2.ročník, 12. - 14.novenber 2003 Senec, s.38-39"

[19] Krištofíková, Ľ., Rosenberg, M., Rebroš, M.: Produkcia erytritolu imobilizovanými bunkami Moniliella tomentosa. Production of erythritol by immobilized cells of Moniliella tomentosa. "In: Zborník abstraktov z medzinárodnej konferencie “LABORALIM 2003 o analytických metódach v potravinárstve"" . Banská Bystrica, 18.-19.2. 2003, s.235-238, ISBN 80-227-1887-4"

[20] Magdolen, P., Rosenberg, M., Krištofíková, Ľ.: Komplexná frakcionácia repných rezkov. Complex fractionation of beet slice. "In: Zborník abstraktov z medzinárodnej konferencie “LABORALIM 2003 o analytických metódach v potravinárstve"" . Banská Bystrica, 18.-19.2. 2003, s.263-266, ISBN 80-227-1887-4"

[21] Magdolen, P., Rosenberg, M.: Zhodnotenie medov s vysokým obsahom oligosacharidov. Evaluation of honeys


26

with the high level of oligosaccharides. "In: Zborník abstraktov z medzinárodnej konferencie “LABORALIM 2003 o analytických metódach v potravinárstve"". Banská Bystrica, 18.-19.2. 2003, s.267-270, ISBN 80-227-1887-4"

[22] Rebroš, M., Rosenberg, M., Krištofíková, Ľ.: Biotechnologická produkcia etanolu – baktérie alebo kvasinky? Biotechnological production of ethanol - bacteria or yeasts? "In: Zborník abstraktov z medzinárodnej konferencie “LABORALIM 2003 o analytických metódach v potravinárstve"". Banská Bystrica, 18.-19.2. 2003, s.287-290, ISBN 80-227-1887-4"

[23] Rosenberg, M., Sláviková, L., Krištofíková, Ľ.: Vplyv intenzity aerácie na selektivitu tvorby kyseliny mliečnej. The influence of aeration intensity on the lactic acid formation selectivity. "In: Zborník abstraktov z medzinárodnej

konferencie “LABORALIM 2003 o analytických metódach v potravinárstve"". Banská Bystrica, 18.-19.2. 2003, s.291-294, ISBN 80-227-1887-4"

[24] Sláviková, L., Čertík, M., Masrnová, S., Navrátil, M., Šajbidor, J.: Stanovenie množstva biomasy vláknitých húb v submerzných a polosuchých kultiváciach bioluminiscenčnou metódou. Determination of biomass of filamentous fungi in submerged and solid state cultivations by bioluminiscence method. Zborník zo XIV. medzinárodnej konferencie LABORALIM, Banská Bystrica, 2003, 299-302. (ISBN 80-227-1887-4)

[25] Šmogrovičová, D., Dömény, Z., Selecký R., Valach M.: Mikrobiologická kontrola kontinuálnej fermentácie mladiny pomocou bioluminometra. Microbial monitoring of continual wort fermetations using bioluminometer. XIV. medzinárodná konferencia o analytických metódach v potravinárstve. Laboralim Banská Bystrica 17.-19. februára 2003

[26] Valach, M., Dömeny, Z., Tkáč, J., Šturdík, E.: Stanovenie etanolu v pive ampérometrickým biosenzorom. Estimation of ethanol in beer using amperometric biosensor. "Zborník prednášok z XIV. Medzinárodnej konferencie o analytických metódach v potravinárstve ""LABORALIM"", Banská Bystrica 2003, 348 -351."

[27] Čertík, M.*, Rapta, P., Breierová, E., Strhanová, K.: Využitie EPR spektroskopie pri sledovaní účinku karotenoidov ako zhášačov radikálov tvorených kvasinkami v stresových podmienkach. The use of EPR spectroscopy for determination of carotenoids effect as radical scavengers generating by yeasts grown under stress conditions. Zborník zo XIV. medzinárodnej konferencie LABORALIM, Banská Bystrica, 2003, 129-132. (ISBN 80-227-1887-4)

[28] Hronská, H., Rosenberg, M., Krištofíková, Ľ.: Mikrobiálna produkcia kyseliny vínnej pomocou baktérií Nocardia sp.. Microbial production of tartaric acid by bacterial cells of Nocardia sp. "In: Zborník príspevkov ""Drobnicov memoriál"", II ročník, Senec 12-14.11.2003. s.63-64"

[29] Malík, F.: Technologické trendy výroby vína vo svete. Technological trends in wine production in world. Vinobranie 2003. Veľký Krtíš. Zborník odborných prednášok, str.7-9, 2003.

[30] Rosenberg, M, Krištofíková, Ľ, Magdolen, P.: Produkcia nízkokalorických sladidiel. Production of low-calorie sweeteners. "In: Zborník abstraktov z medzinárodnej konferencie “LABORALIM 2003 o analytických metódach v potravinárstve"" . Banská Bystrica, 18.-19.2. 2003, s.51-55, ISBN 80-227-1887-4"

[31] Valach, M.: Vývoj ampérometrického biosenzora pre monitoring etanolu. Development of amperometric biosensor for monitoring of ethanol. "Zborník príspevkov ""Drobnicov memoriál"" 2. Ročník, Senec 2003, 67-68"

[32] Cvengroschová, M., Šepeľová, G., Šmogrovičová, D.: Mashing-in temperature influence on FAN content and foam stability. Abstracts of papers and posters on 20th Brewing and Malting Days. Kvasny Prum. 49, 256 (2003)

[33] Čertík, M.*, Breierová, E., Rapta, P., Žitňanová, I.: Scavenging and antioxidant properties of carotenoids generating by yeasts stressed by heavy metals. Proceedings of XXXI. International Conference of Yeasts, Smolenice, 2003, 42.

[34] Čertík, M., Breierová, E., Strhanová, K., Bronišová, Ž., Oláhová, M.: Alternations in lipid composition of carotenogenic yeasts grown under heavy metal presence. Proceedings of XXXI. International Conference of Yeasts, Smolenice, 2003, 41.

[35] Šmogrovičová, D., Dömény, Z., Navrátil M.: Non-alcoholic beer production. 31st Annual Conference of Yeasts, Smolenice 19. - 21. 5. 2003.

[36] Šmogrovičová, D., Selecký, R., Dömény, Z., Molek, J.: The fermentor influence on low-alcoholic beer parameters. Abstracts of papers and posters on 20th Brewing and Malting Days. Kvasny Prum. 49, 256 (2003)

[37] Wein, S., Simončíková, P., Gašperiková, D., Ukropec, J., Čertík, M., Klimeš, I., Šeboková, E.: Comparison of the effect of GLA and a-3 PUFA on a diet-induced insulin resistance. Comparison of the effect of GLA and a-3 PUFA on a diet-induced insulin resistance. Proceedings of 76th Physiological days, Plzeň, 2003, 55

[38] Čertík, M.*, E. Berierová, P. Rapta, J. Márová, J. Omelková, K. Strhanová: Environmental stress and carotenogenic yeasts: membrane lipids, carotenoids formation and scavenging radicals. Proceedings of XXXI. International Conference of Yeasts, Smolenice, 2003, 18.

[39] Horváthová, V., Šlajsová, K., Šturdík, E.: Hydrolysis of raw starches by glucoamylase from Saccharomycopsis fibuligera IFO 0111. "Book of abstracts. ""Structure and stability of biomacromolecules"" Košice 2003."

[40] Šmogrovičová, D.: Physiology of brewer’s yeast in stress conditions. Abstracts of Lectures. Joint Meeting of the Yeast Genetics & Physiology and Emerging Fermentation Systems. EBC Sub-Groups. Dresden – Germany, Sept. 17-19, 2003

[41] Šmogrovičová, D.: Stress of free and immobilised brewing yeast.. 31st Annual Conference of Yeasts, Smolenice 19. - 21. 5. 2003

[42] Brygin, M., Navrátil, M., Šturdík, E.: Monitoring of lactose during ethanol fermentation on enzyme thermistor In: Zborník abstraktov z Tomáškových dňov 2003, Brno 2004

[43] Cvengroschová, M., Šepeľová, G., Šmogrovičová, D.: Vplyv teploty vystierania na obsah FAN a stabilitu peny Mashing-in temperature influence on FAN content and foam stability. Souhrny přednášek a posterů. 20. Pivovařsko-sladařské dny

[44] Rebroš, M., Rosenberg, M., Krištofíková, Ľ.:Microbial production of bioetanol. "In: Zborník príspevkov ""Drobnicov memoriál"", II ročník, Senec 12-14.11.2003. s.114"

[45] Rebroš, M., Rosenberg, M., Krištofíková, Ľ.: Mikrobiálna produkcia etanolu.Microbial production of ethanol. "In: Zborník abstraktov ""Tomáškovy dny 2003"". XII. Konference mladých mikrobiológů. Brno, 4-6.6.2003, s.43"


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[46] Šepeľová, G., Cvengroschová, M., Šmogrovičová, D.: Vplyv teploty na rýchlosť kvasenia a organoleptické vlastnosti piva. Temperature influence on fermentation speed and organoleptic beer properties. Abstracts of papers and posters on 20th Brewing and Malting Days. Kvasny Prum. 49, 256 (2003)

[47] Šmogrovičová, D., Selecký, R., Dömény, Z., Molek, J.: Vplyv fermentora na parametre nízkoalkoholických pív. The fermentor influence on low-alcoholic beer parameters. Souhrny přednášek a posterů. 20. Pivovařsko-sladařské dny

[48] Brygin, M., Navrátil, M., Šturdík, E.: Vývoj biosensora pre laktózu na enzýmovom termistore. Development of biosensor for lactose on enzyme thermistor In: Zborník abstraktov z Tomáškových dňov 2003, Brno 2003

[49] Rebroš, M., Rosenberg, M., Krištofíková, Ľ., Vadrnová, R., Stloukal, R.: Imobilizované biosystémy vo fermentačných technológiách. Immobilized biosystems in fermentation technology. "In: Zborník abstraktov ""Tomáškovy dny 2003"". XII. Konference mladých mikrobiológů. Brno, 4-6.6.2003, s.16"

[50] Tkáč, J., Voštiar, I., Gemeiner, P., Šturdík, E.: Gluconobacter oxydans biosensors. IXth International Workshop on Bioencapsulation, May 25-27, 2003, Strasbourg, France

[51] Malík, F.: Apelačné systémy I. a II.. Appelation systems I. and II. Profesionálny kurz sommeliérov SR 2003, Modra, Október 22, 2003

[52] Malík, F.: Degustátorský a technologický seminář - bílá vína. Wine taster´s and technological seminary - white wines. Národní salon vín ČR, Valtice, November 7, 2003

[53] Malík, F.: Degustátorský a technologický seminář - červená vína. Wine taster´s and technological seminary - red wines. Národní salon vín ČR, Valtice, November 21, 2003

[54] Malík, F.: Nové aspekty při výrobě vína. New topics of wine production. Oborový den vinařů a vinohradníků. Zemědelská a.s. Čejkovice, Máj 24, 2003

[55] Malík, F.: Povídaní o světových vínech. Talk about wines of world. Hotel Atom Ostrava, Júl 10, 2003 [56] Malík, F.: Senzorické hodnotenie vína. Sensoric evaluation of wine. Profesionálny kurz sommeliérov SR 2003,

Modra, Október 22, 2003 [57] Malík, F.: Světové trendy výroby vín. World trends in wine production. Sdružení znojemských vinařů. Znojmo,

Marec 29, 2003 [58] Malík, F.: Technologické zvláštnosti při výrobě vína ve středoeuropském regionu. Technological specifics of wine

production in the middle european region. "Kurz ""Sommeliér"" 2003/2004. VAV Valtice, September, 25, 2003" [59] Malík, F.: Technologie výroby bíleho a červeného vína ve středoeuropském regionu. Technology of the white and

red wine production in the middle european region. "Kurz ""Sommeliér"" 2003/2004. VAV Valtice, Október, 16, 2003"

[60] Malík, F.: Vína nového sveta. New world wines. Profesionálny kurz sommeliérov SR 2003, Modra, Október 21, 2003

[61] Malík, F.: "Vinařské oblasti Slovenska; světová vína - základní charakteristika." Slovak wine appelations, woorld wines - basic characteristic. Akademie sommeliérů Makro/Metro I. základní část. Národní salon vín, Valtice, April 2, 2003

[62] Malík, F.: Víno a jeho poslanie v spoločnosti. Wine and its role in the society. Univerzita tretieho veku. STU Bratislava, Marec 21, 2003

[63] Malík, F.: Vinohradníctvo a vinarstvo súčasnosti. Present status of viticulture and oenology. Profesionálny kurz sommeliérov SR, Modra Október 19, 2003

[64] Malík, F.: Vinohradníctvo a vinárstvo Španielska, Portugalska a Nemecka. Viticulture and oenology of Spain, Portugal and Germany. Profesionálny kurz sommeliérov SR. Assoc. sommeliérov SR. Modra, Marec 21, 2003

[65] Šmogrovičová, D.: Quo vadis pivovarníctvo? Quo vadis brewing industry? Seminár pri príležitosti 45. výročia založenia chmeľníc „Vývoj kvality chmeľu pestovaného na Slovensku“. Bratislava 24. 4. 2003

[66] Vitálová, Z.*, Slugeň, D.: Kodályova koncepcia totálnej komunikácie. Kdaly´s method of total communication. Medzinárodná odborná konferencia Kodályova metóda vo výchove a vzdelávaní pedagógov v 21. Storočí, 13.12. Galanta (2003).Pr

C. Books and Textbooks [1] Malík, F.: Víno moja vášeň. Wine my passion. Albert Marenčin Vydavateľstvo PT Bratislava, s. 230 ISBN 80-

88912-46-6 [2] Malík, F.: Ze života vína. Form the life of wine. Filip Trend Publishing Pardubice, s. 221 ISBN 80-86282-27-9 [3] Vitálová, Z., Slugeň, D.: Hudba a víno. Music and wine. SSFS, Bratislava, 132 s., (2003), ISBN 80-967829-3-2.

E. Others [1] Malík, F.: Adventná prechádzka po chotári. Advent walk trough parish. Pravda 20. 12.. 2003 [2] Malík, F.: Antico Caffé Greco. Pravda 17. 5. 2003 [3] Malík, F.: Ausbruch z Csopaku. Ausbruch from Csopaku. Pravda 11. 10. 2003 [4] Malík, F.: Biele Verdejo, červené Tempranillo. White Verdejo, red Tempranillo. Pravda 24. 5. 2003 [5] Malík, F.: Celosvětově rozšířená odrůda Sauvignon. World widespread variety Sauvignon. MF Dnes, 19. 12. 2003 [6] Malík, F.: Čarovné bublinky. Glamorous bubles. Pravda 27. 12. 2003 [7] Malík, F.: Červená repa, červené víno. Red beet, red wine. Pravda 15. 11. 2003 [8] Malík, F.: Doctor Zarcillo. Pravda 31. 5. 2003 [9] Malík, F.: Dornfeldersauce. Pravda 13. 9. 2003 [10] Malík, F.: Huwelyk met wijn.Pravda 26. 4. 2003 [11] Malík, F.: Château Intanto. Pravda 19. 7. 2003 [12] Malík, F.: In honorem vini. Pravda 2. 8. 2003 [13] Malík, F.: In vino sanitas. Pravda 11.1.2003 [14] Malík, F.: Kaštieľ Belá. Belá castle.Pravda 8. 11. 2003 [15] Malík, F.: Keď víno smrdká. When wine is going smell. Pravda 12. 4. 2003 [16] Malík, F.: Kyslé čierne. Sour black. Pravda 8. 3. 2003


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[17] Malík, F.: Limbašský smútok. Limnach sorrow. Pravda 3. 5. 2003 [18] Malík, F.: "Mamutova ""lipka"". “"Mamuta´s ""lipka""". Pravda 16. 8. 2003 [19] Malík, F.: Matuzalem za milión. Mathozalem for million. Pravda 29. 3. 2003 [20] Malík, F.: Matyšákovo slamové. Matyšák´s straw wine. Pravda 1. 2. 2003 [21] Malík, F.: Modrý Portugal najspíš nepochází z Portugalska. Blue portuguese probably does not originate in

Portugal. MF dnes, E8, 2.4.2003 [22] Malík, F.: Moravský zubáč. Moravian zander. Pravda 31. 10. 2003 [23] Malík, F.: Naša (vínna) cesta. Our (wine) way. Pravda 22. 11. 2003 [24] Malík, F.: Nemecké gastrosobáše. German gastroweddinds.Pravda 27. 9. 2003 [25] Malík, F.: Obed v senáte. Dinner in senate. Pravda 5. 4. 2003 [26] Malík, F.: Opité pagáčiky. Drunken oil-cakes. Pravda 18.1.2003 [27] Malík, F.: Panenské z Katovky. Virgin wine form Katovka. Pravda 9. 8. 2003 [28] Malík, F.: Pedro Luxo. Pedro Luxo. Pravda 23. 8. 2003 [29] Malík, F.: Plemenito rdeče. Plemenito rdeče. Pravda 26. 7. 2003 [30] Malík, F.: Primitivo z Apúlie. Primitivo form Apulia. Pravda 10. 5. 2003 [33] Malík, F.: Primus pamonicus. Primus pamonicus. Pravda 13. 12. 2003 [34] Malík, F.: Prvý európsky dúšok. First european swallow. Pravda 12. 7. 2003 [35] Malík, F.: Ranč MM. Pravda 7. 6. 2003 [36] Malík, F.: Rizling vlašský nepochádza z Talianska. Welsch risling does not originate in Italy. Pravda 28. 6. 2003 [37] Malík, F.: Rudkovo malinové a muflonie klobásy. Ruddy´s raspberry and mouflon meat sausage. Pravda 22. 2.

2003 [38] Malík, F.: Rulandské modré přivezl do Čech Karel IV. Pinot noir was brought to Czechia by Charles IV. MFDnes, E

5-6, 24. 10. 2003 [39] Malík, F.: Rulandské pochádza z Burgundska. Rulander originated in Burgundy. Pravda 18. 10. 2003 [40] Malík, F.: Saint-Emillion, aleluja! Saint-Emillion, aleluja! Pravda 25. 10. 2003 [41] Malík, F.: Sladké ľadové s bábovkou. Swett ice wine with biscuit. Pravda 8. 2. 2003 [42] Malík, F.: Svätovavrinecké dozrieva na Vavrinca. Saint Laurents matureted at Laurent day. Pravda 6. 12. 2003 [43] Malík, F.: "Světová ""chardonnaymanie"" sa zrodila v Americe. ""World ""charonannaymania"" was born in

America." MF dnes, E 4-5, 11. 7. 2003 [44] Malík, F.: Sviečková pána dekana. Sirloin of mister dean. Pravda 25.1.2003 [45] Malík, F.: Tokajské menu. Tokay menu. Pravda 4.1.2003 [46] Malík, F.: Tramín z marcipánu. Traminer form marzipan. Pravda 20. 9. 2003 [47] Malík, F.: V kasíne pri víne. In casino with wine. Pravda 15. 3. 2003 [48] Malík, F.: Vajnorské milosci. """Milosci"" from Vajnory." Pravda 6. 9. 2003 [49] Malík, F.: Veltlínske zelené poznal už Matej Bel. Greener Weltliner was known by Matej Bell. Pravda 30. 8. 2003 [50] Malík, F.: Víno a bociany. Wine and storks. Pravda 12. 4. 2003 [51] Malík, F.: Víno a pirohy. Wine and pasty. Pravda 4. 10. 2003 [52] Malík, F.: Víno a strašidlá. Wine and ghosts. Pravda 13. 6. 2003 [53] Malík, F.: Víno svätého Juraja. St. Goeorge´s wine. Pravda 22. 3. 2003 [54] Malík, F.: Všetko o víne. All about the wine. Pravda 15. 2. 2003 [55] Malík, F.: Zlatá šťuka. Golden jakepike. Pravda 1. 3. 2003 [56] Šmogrovičová, D., Malík F.: Diplomové práce absolventov Katedry biochemickej technológie FCHPT STU v

Bratislave. Diploma works of graduate at Department of Biochemical technology FCHPT SUT in Bratislava. Kvasny Prum. 49 (7-8) 208-209 (2003)

[57] Šmogrovičová, D.: 31. Výročná konferencia o kvasinkách. 31st Annual conference of yeasts. Kvasny Prum. 49 (7-8) 209 (2003)

DEPARTMENT OF BIOCHEMISTRY AND MICROBIOLOGY

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Head of Department: Telephone: ++421259325514 Ass.Prof. Ľudovít Varečka, PhD Fax: ++421252493198


I. STAFF Full Professors: Katarína Horáková, PhD, DSc,Milan Miko, PhD, DSc; Associate Professors: Daniela Hudecová, PhD; Soňa Jantová, PhD; Mária Mikulášová, PhD. Assistant Professors : Barbora Dudová; Karin Kaiserová, PhD; Helena Paulíková, PhD; Martin Šimkovič, PhD; Andrea Šovčíková, PhD; Research Fellows: Boris Lakatoš, PhD PhD Students: Petra Ditteová; Roman Hudec, Martina Hunová, Michal Kaliňák; Silvia Letášiová Technical staff: Eva Drobná-Secretary; Dagmar Adamíková; Gabriela Chytilová; Margita Kosárová; Ján Škvara; Eva Sameková


A. Teaching laboratories: Laboratory of Animal Cell Cultures Laboratory of Biochemistry of Cancer Cells Laboratory of Fungal Biochemistry and Physiology Laboratory of Immunochemistry Laboratory of Microbiology

B. Research laboratories: Laboratory of Animal Cell Cultures Laboratory of Biochemistry of Cancer Cells Laboratory of Fungal Biochemistry and Physiology Laboratory of Immunochemistry Laboratory of Microbiology

III. TEACHING

A. Undergraduate Study: 1. semester (Bc) Biology 2/0/0 Jantová, Šovčíková Laboratory Practices in Biology 0/0/1 Olejníková, Kaliňáková, Šovčíková,

Letášiová 3. semester (Bc) Microbiology I 2/0/0 Hudecová Laboratory Practices in Microbiology I 0/0/2 Hudecová, Mikulášová, Olejníková,

Kaliňáková 4. semester (Bc) Biochemistry I 2/0/0 Varečka Laboratory Practices in Biochemistry

I 0/0/2 Paulíková, Lakatoš, Hunová, Hudec,

Kaliňák 5. semester (Bc) Principles of Human Nutrition 2/0/0 Miko 6. semester (Bc) Laboratory Project 0/0/4 Miko, Horáková, Varečka, Hudecová,

Jantová, Mikulášová, 1. semester (MSc) Biochemistry II 2/0/2 Varečka, Paulíková, Lakatoš, Hudec,

Hunová, Microbiology II 2/0/2 Hudecová, Mikulášová, Kaliňáková,

Olejníková Immunochemistry 2/1/2 Šovčíková, Hudec


30

Laboratory project I 0/0/5 Miko,Horáková, Varečka, Hudecová, Jantová, Mikulášová

2. semester (MSc) Molecular Biology and Genetics 2/1/0 Mikulášová, Paulíková, Čertík Applied Microbiology 2/0/0 Hudecová Bioenergetics 2/0/2 Miko Mechanisms of Action of Natural

Compounds 2/0/2 Varečka, Lakatoš, Kaliňáková

2. semester (MSc) Laboratory project II 0/0/5 Miko, Horáková, Varečka, Hudecová, Jantová, Mikulášová

3. semester (MSc) Genetic Manipulations 2/2/0 Čertík Clinical Biochemistry 2/0/0 Chandoga Clinical Biochemistry-Laboratory

Practices 0/0/2 Lakatoš, Šimkovič

Cell cultures 2/0/2 Jantová 3. semester (MSc) Laboratory project III 0/0/5 Miko, Horáková, Varečka, Hudecová,

Jantová, Mikulášová Lab. Practices of the branch

Biomedical Engineering,…

0/0/2 Miko, Horáková, Varečka, Hudecová, Jantová, Mikulášová

4. semester (MSc) Master`s Thesis 0/0/27 Miko, Horáková, Varečka, Hudecová, Jantová, Mikulášová


A. VTP Project No 2/9012/21 Preparates for biological protection of plants on Trichoderma fungus basis (Ľudovít Varečka)

The aim of the project is elaboration of effective technology/technologies for preparation of myceliar specimens of fungus Trichoderma suitable for biological protection of plants:

a) by submerged cultivation of fungus on defined cultivation media (for specimens containing conidia, mycelia and elicitating enzymes)

b) by surface cultivation on defined media respectively on waste substrates from food industry (conidia and mycelia).

c) Proposal of Trichoderma specimens adaptation into the forms convenient for different kinds of application (conidia suspensions, granules, mixtures)

Project duration: from 1.1.2001 to 31.12.2003 B. VEGA Project No 1/0109/03 Transport processes in filamentous fungi and their adaptative

mechanisms (Ľudovít Varečka) In the project devoted to study the transport processes in filamentous fungi several aspects of transport and physiology were studied.

In Trichoderma viride the process of chloride transport was studied by means of 36Cl radionuclide. It was found that chloride anions enter the vegetative mycelia in a saturatable, pH- and temperature-dependent manner with selectivity for chlorides and bromides. Further properties of transport suggest that chloride anions are transported by a specific and electrically silent transport protein. In Penicillium simplicissimum the process of citrate transport into the vegetative mycelia has been described and the conditions were found which led to the induction of novel citrate uptake system driven by protonmotive force. Its role in the citrate metabolism is being currently analysed.

Project duration: from 01.01.2003 to 31.12.2005 C. VEGA Project No 2/3188/23 Characterisation of basal transport of Ca2+ in non-excitable

cells (Ľudovít Varečka) The main goal of the project is to prove or disprove the existence of the carrier in mediating the inward basal passive Ca2+ transport and to find out whether this process proceeds using and electrogenic or electroneutral mechanism. Further goals of the project is to find out information about factors which determine the magnitude of the basal Ca2+ influx, particularly, to find out whether it responds to the immediate conditions, or it is predetermined by (genetic) mechanisms.

Project duration: from 01.01.2003 to 31.12.2005 D. Bilateral Cooperation Austria-Slovakia - Membrane transport of organic acids in

filamentous fungi (Ľudovít Varečka) This project is a continuation and expansion of our previous collaboration, where we investigated citrate uptake in P. simplicissimum. Additionally, this priject is carried out in colleboration with the Austrian Science Fund Project P 15491 ("Energetics of citrate transport through the plasma membrane of Penicillium simplicissimum. A study using plasma membrane vesicles").


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The aims of this proposal are:

1.) To study the induction of high affinity uptake systems for pyruvate, citrate, 2-oxoglutarate and succinate in Trichoderma viride, P. simplicissimum, Beauveria brongniartii and Aspergillus nidulans.

2.) To improve and validate the measurement of the plasma membrane potential using di-S-C3(3) or di-S-C3(5) in T. viride, P.simplicissimum, B. brongniartii and A. nidulans.

3.) To measure the PMF using method above and a method to determine the proton gradient.

4.) To fing out if the induction of these uptake systems is accompanied by a change in the proton motive force and by an increased expression on the plasma membrane H+-ATPase

Project duration: from 01.06.2003 to 31.5.2004 E. VEGA Project No 1/9247/02 New coordinating compounds of zinc, their preparation, study

of physico-chemical properties and their biological activity (Daniela Hudecová) The main goal of this project is the preparation of new coordinating compounds of zinc binding the molecules of ligands with predicted biological activity with emphasis on the study of their physico-chemical properties (spectroscopic and thermic properties, structure and stability in solutions) and their biological activity. In the frame of project is selected wide scale of complexes of zinc from the reason of their perspective using in the pharmacy, food and cosmetic industry.



VI. COOPERATION



Duration

Institute of Molecular Physiology and Genetics, SAS, Bratislava

Characterisation of basal Ca2+ transport in non-excitable cells ( Joint grant)

Dr. Jozef Orlický, Senior Research Scientist, Vlárska 5, 833 34 Bratislava

Cancer Research Institute, SAS, Bratislava

Cytotoxicity of Novel Xenobiotics and Their mode of Action

Dr. Darina Slameňová, Head of Group, Vlárska 7, 833 91 Bratislava

01.01.1991 -

Tissue Bank, Hospital Ružinov, Bratislava

Cultivation and growth of human and animal tissue cultures on new biomaterials

Dr. Jana Dragúňová, Ružinovská 6, 826 06 Bratislava

01.01.1998 -

Dept. of Chem. Theory of Drugs, Fac. of Pharmacy, Comenius University, Bratislava

Study of antimicrobial activity of newly synthesized copper complexes

Dr. Aladár Valent, Associate professor, Kalinčiakova 8, 832 32 Bratislava

01.01.1999 -

Institute of Chemistry, Faculty of Science, PJŠU, Košice

New coordinating compounds of zinc, their preparation, study of physico-chemical properties and their biological activity (Joint grant)

Prof. Katarína Gyoryová, Full Professor, Moyzesova 11, 040 01 Košice

01.10.2001 -

Institute of Chemistry, SAS, Bratislava

Preparates for biological protection of plants on Trichoderma fungus basis (Joint grant)

Dr. Vladimír Farkaš, Senior Research Scientist, Dúbravská cesta 9, 845 38 Bratislava

01.01.2001 -



Duration

Laboratoire du Biomembranes et Messagers Cellulaires, Orsay

Apoptosis in dexamethasone treated murine thymocytes

Dr. Francoise Giraud, Director of Research, BMC CNRS - UMR 8619, Bat.440 Universite Paris XI, Orsay 914 05, France

01.01.2000 -


32

Institute of cellular and molecular botany, Friedrich Wilhelms Universität, Bonn

Characterisation of microorganisms indigenous to low-rank coal, study of solubilisation of lignite by these microorganisms

Dr. Udo Hoelker, Head of group, Kirschallee 1, 53 115 Bonn, Germany

01.01.2001 -

Institut für Mikrobiologie, Universität zu Innsbruck

Membrane transport of organic acids in filamentous fungi (Joint grant)

Dr. Wolfgang Burgstaller, Head of Group, Technikerstrasse 25, 6020 Innsbruck, Austria

01.01 2002 -

Institute of Food Research, Norwich

Rapid, specific detection of Listeria monocytogenes by antibody-based techniques and on-line sensor technology

Dr. Gary Wyatt, Senior Research Scientist, Norwich Research Park, Colnay, NR47UA - Norwich, Great Britain

Institute of Chemical Technology, Prague

Rapid, specific detection of Listeria monocytogenes by antibody-based techniques and on-line sensor technology

prof. Pavel Rauch, Head of Department, Technická 5, 166 28 Prague, Czech Republic



Valid date

Miko Milan Slovak Society for Biochemistry and Molecular Biology, Bratislava member

Miko Milan Editorial board of journal Biológia member

Miko Milan Editorial board of journal Acta fytotechnica et zootechnica member

Miko Milan Commission for evaluation of DrSc (DSc) thesis in Biochemistry member

Hudecová Daniela Czecho-Slovak Society for Microbiology, Bratislava member 01.01.1984 -

Hudecová Daniela

Scientific grant agency (VEGA)– Commission for cell and molecular biology , Bratislava- member 30.04.2002 -

Hudecová Daniela

Commission for evaluation of PhD thesis in Microbiolgy secretary 20.10.1997 -

Jantová Soňa Slovak Medical Society, Bratislava member 01.01.1980 -

Jantová Soňa Slovak Society for Biochemistry and Molecular Biology, Bratislava member 01.01.2002 -

Jantová Soňa Scientific grant agency (VEGA)– Commission for cell and molecular biology member 30.04.2002 -

Mikulášová Mária Czecho-Slovak Society for Microbiology, Bratislava member 01.07.1992 -

Mikulášová Mária Czecho-Slovak Society for Biology, Brno member 01.01.1993 -

Varečka Ľudovít

Editorial Board of journal General Physiology and Biophysics (GPB) member 01.01.1993 -

Varečka Ľudovít

Slovak Society for Biochemistry and Molecular Biology, Bratislava member of advisory board 01.10.1996 -

Varečka Ľudovít

Scientific board of Institute of molecular physiology and genetics SAS, Bratislava member 01.01.2001 -

Lakatoš Boris Slovak Society for Biochemistry and Molecular Biology, Bratislava member 01.01.2002 -

Andrea Šovčíková

Slovak Society for Biochemistry and Molecular Biology, Bratislava member 01.01.2003 -

Martin Šimkovič

Slovak Society for Biochemistry and Molecular Biology, Bratislava member 01.01.2002 -



Date / Duration

Daussant, J. C.N.R.S., Meudon France November 2003 (5 days)



Date / Duration


- 33 -

Kaliňák, M. Universität Innsbruck, Innsbruck Austria December 2003 (20 days)

Lakatoš, B. Université Paris Sud XI, Orsay France May-July 2003 (60 days)



Bajdichová, M. Reactivity of isothiocyanates and induction of apoptosis Paulíková, H. Bartková, M. Current trends in genotoxicity testing of chemicals in in vitro conditions Slameňová, D. Ditte, P. Demonstration of ageing in filamentous fungi during vegetative growth Varečka, Ľ. Gbelcová, H. Selected industrial preparations influencing oxidative stress Ďuračková, Z. Malachovská, V. QSAR "Quantitative Structure-Activity Relationship" in practice Kaliňáková, B. Marejková, M. Importance of integrons in the diffusion of resistance Majtán, V. Melkusová, P. The role of vitamins with antioxidazing effect in cancer prevention Horákova, K. Paulínyová, B. Changing concepts of dietary pulp: implications for carcinogenesis Miko, M.

Poláková, V. Analysis of DNA damage in chemically influnced mammalian cells as a genotoxicity marker Slameňová, D.

Potanková, V. Cytochrome c oxidase (complex IV) and mitochondrial pathology Miko, M. Repický, A. Chinolones and their biological activity Jantová, S.

Samáková, I. Effect of selected biologically active compounds on causal organisms of some mycotic diseases Hudecová, D.

Suchánová, M. Effect of phenolic acids on induction of SOS response in Escherichia coli PQ-37 Mikulášová, M.

Počarovská, M. Comparative study of photoinduced conidiation in filamentous fungi Varečka, Ľ. B. Graduate Theses (MS Degree) for state examinations after five years of study

Name Title of Thesis Supervisor Bernovská, V. Biological activity of newly synthesized bioinorganic compounds with

atom of zinc in the molecule. Hudecová, D.

Čomajová, M. Biomarkers of immunomodulatory effect of mineral fibers in exposed workers Tulinská, J.

Gocník, M. Effect of antibodies to HA2 glycoprotein of influenza virus on its replication Varečková, E.

Jančová, M. Study of genotoxic effects of natural compounds on microbial models Mikulášová, M. Jarošová, M. Chemically induced cell differentiation and oxidizing stress Paulíková, H. Józsová, M. Alternative methods of evaluation of toxicity of cosmetic compounds Jantová, S.

Letášiová, S. Screening and mode of action of halogensalicylate copper (II) complexes with heterocycle N-donor ligands Miko, M.

Marčeková, Z. Study of causative factors of fusing and non-fusing behaviour of colonies of Trichoderma viride chlorpromazine-resistant mutants Varečka, Ľ.

Ondková, S. Induction of internaline B expression for specific detection of Listeria monocytogenes by ELISA method Horáková, K.

Pančuchárová, H. Biochemical and transport properties of the membrane prepared from human erythrocytes Hudec, R.

Scholzová, E. Indomethacine and his analogues in chemotherapy. Interactions with transport system of glutathione conjugates Paulíková, H.

Sládeček, J. Study of biochemical aspects of resistance of psychiatric patients on psychotherapeutics therapy Lakatoš, B.

Stojnev, T. Molecular and biological characterization of clinical isolates of Salmonella enterica serovar Enteritidis Majtán, V.

Strelková, S Kinetic properties of the renal Na,K-ATPase in experimentally induced diabetes Vrbjar, N.

Tillinger, A. Genetic aspects of growth of vegetative colonies of filamentous fungi and conidia formation Varečka, Ľ.

Valkovičová, E. The effect of mineral fibers and smoking on the immune system of the rats Tulinská, J.

Vlková, M. The effect of commercially manufactured disinfectant substances on Stenotrophomonas maltophilia Majtán, V.


Kaiserová, K. Influx of Ca 2+ and resting membrane potential of cells Varečka, Ľ.


34

D. Dissertations (DSc) Name Title of Thesis Head of board

Varečka, Ľ. Transport systems related with Ca2+ homeostasis in non-excitable cells Biely, P.


[1] Brezová, V., Valko, M., Breza, M., Morris, H., Tesler, J., Dvoranová, D., Kaiserová, K., Varečka, Ľ., Mazúr, M., Leibfritz, D.: Role of radicals and single oxygen in photoactivated DNA cleavage by the anticancer drug camptothecin: an paramagnetic resonance study. Role of radicals and single oxygen in photoactivated DNA cleavage by the anticancer drug camptothecin: an paramagnetic resonance study. J. Phys. Chem.B. 107, 2415-2425, (2003)

[2] Čipák, L., Berczeliová, E., Pauliková, H.: Effects of flavonoids on glutathione and glutathione-related enzymes in cisplatin-treated L1210 leukemia cells. Neoplasma.50(6), 444-7, (2003)

[3] Gyoryová, K., Szunyogová, E., Kovarová, J., Hudecová, D., Mudroňová, D.: Biological and Physicochemical Study of Zinc(II)propionate with N-Donor Heterocyclic Ligands. J.: Thermal Analysis and Calorimetry 72, 578-596 (2003)

[4] Mikulašová, M., Košiková, B.: Modulation of mutagenicity of various mutagens by lignin derivatives. Modulation of mutagenicity of various mutagens by lignin derivatives. Mutat Res. 535(2), 171-80, (2003)

[5] Wojtowicz, H., Chojnacka, M., Mlochowski, J., Palus, J., Syper, L., Hudecova, D., Uher, M., Piasecki, E., Rybka, M. : Functionalized alkyl and aryl diselenides as antimicrobial and antiviral agents: synthesis and properties. Farmaco 58(12), 1235-42, (2003)

[6] Hudec, R.: Bielkoviny s obsahom motívov EF-ruky a C2 domén viažuce vápnik. Proteins containing EF-hand motifs and C2 domains that bind calcium. Biologické Listy 68(4), 283-300, (2003)

B. Conferences [1] Hudecová*, D., Ditteová, P., Valigura, D., Augustín, J., Melník, M.: Some new salicylatocopper(II) complexes and

their biological properties. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 650, (2003).

[2] Palus, J., Chojnacka, M., Osajda, M., Piasecki, E., Rybka, K., Uher, M., Hudecová, D.: New N-substituted benzisoselenazolones and related diselenides as potential antimicrobial and antitumoral agents. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, s. 776-777, (2003)

[3] Gyoryová, K*., Zalewicz, M., Chomič, J., Hudecová, D., Zeleňák, V.: Biologically active Zinc(II) complexes. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, s. 648, (2003).

[4] Valigura, D.*, Hudecová, D., Melník, M., Cibičková, D., Martiška, L.: Halogenosalicylatocopper(II) complexes characterization and antimicrobial activity. In: Progress in coordination and bioanorganic chemistry, edds. Melník, Sirota, Slovak Technical University Press, Bratislava 2003, p. 425-430 (ISBN 80-227-1891-2)

[5] Dudová, B., Ditteová, P., Hudecová, D., Palicová, M., Segľa, P., Melník, M.: Effects of N-heterocyclic copper carboxylates on the growth and morphology of filamentous fungi. In: Colloquium Fungi as Model Organisms in Research and Biotechnology II. Olomouc 5. - 6. 9. 2002. Czech. Mycol. 55, 106, (2003)

[6] Hudecová, D., Cibičková, D., Dudová, B., Valigura, D., Martiška, L., Melník, M: Some biological properties of new copper (II) halogenosalicylates. In: Colloquium Fungi as Model Organisms in Research and Biotechnology II. Olomouc 5. - 6. 9. 2002. Czech. Mycol. 55, 109-110, (2003)

[7] Hudecová, D., Henselová, M.: Microbial seeds contamination, one of the causes of low determination rate in Karwinskia humboldtiana (Rhamnaceae). In: Colloquium Fungi as Model Organisms in Research and Biotechnology II. Olomouc 5. - 6. 9. 2002. Czech. Mycol. 55, 125, (2003)

[8] Hudecová, D., Uher, M., Melník, M., Brtko, J.: Metalokojáty a perspektíva ich využitia. Metalkojates and the perspective of their utilization. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, s. 765, (2003).

[9] Hunová, M., Pokorný, R., Varečka, Ľ.: Induction of proteolytic enzymes by several inducers in a submerged culture of Trichoderma viride. In: Colloquium Fungi as Model Organisms in Research and Biotechnology II. Olomouc 5. - 6. 9. 2002. Czech. Mycol. 55, 111-112, (2003)

[10] Kaliňák, M., Šimkovič, M., Burgstaller, W., Varečka, Ľ.: Study of inducibility of citrate uptake into fungus Penicillium simplicissimum. In: Colloquium Fungi as Model Organisms in Research and Biotechnology II. Olomouc 5. - 6. 9. 2002. Czech. Mycol. 55, 112, (2003)

[11] Valent, A.*, Kohútová, M., Melník, M., Hudecová, D., Dudová, D.: Antimikróbna aktivita meďnatých komplexov. Antimicrobial activity of copper(II) complexes. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, s. 651-652, (2003)

[12] Augustín, J.*, Patoprstá, I., Hudecová D.: Senzorické hodnotenie fermentovaných, polofermentovaných a opakovane fermentovaných listov čajovníkok (Camelia sinensis). Sensory evaluation of the fermentation, poly- and repeated fermentation of the tea leaves (Camellia sinensis). In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, s. 793, (2003)

[13] Augustín, J., Hudecová, D., Patoprstá, I.: Stanovenie obsahu kofeínu a ťažkých kovov v listoch čajovníka (Camelia sinensis). Determination of the content of caffeine and heavy metals in tea leaves (Camelia sinensis). In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 2003, 97 (8) 792.

[14] Augustín, J., Hudecová, D.: Fungálny beta-1,3-D-glukán ako potravinový doplnok, izolát z hlivy ustricovitej (Plerotus ostreatus). Chemická štruktúra, zdroje a niektoré farmakologické účinky. Fungal beta-1,3-D-glucane isolated from mushroom Plerotus ostreatus as a food supplement. Chemical structure, sources and some pharmacological effects. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, s. 781-782, (2003).


- 35 -

[15] Hudecová, D., Kamenistá, A., Marčeková, Z., Varečka, Ľ.: Characterization of chlorpromazine-rezistant Trichoderma viride mutants. In: Colloquium Fungi as Model Organisms in Research and Biotechnology II. Olomouc 5. - 6. 9. 2002. Czech. Mycol. 55, 110-111, (2003)

[16] Varečka, Ľ., Šimkovič, M., Kaliňák, M., Kryštofová, S.: In: Colloquium Fungi as Model Organisms in Research and Biotechnology II. Olomouc 5. - 6. 9. 2002. Czech. Mycol. 55, 124, (2003)

[17] Mikulášová, M.*, Košíková,B., Jančová,M.: Význam rastlinných polyfenolov z hľadiska genotoxicity. Role of plant polyphenols in viewpoint of genotoxicity. In: 26.pracovné dni Českej a Slovenskej spoločnosti pre mutagenézu vonkajším prostredím, NCO NZO Brno (ČR). 5.-7.máj 2003, str.23-24 (PPr) ISBN 80-7013-381-3

[18] Augustín, J.*, Suli, J., Hudecová, D.: Stanovenie obsahu ťažkých kovov v čajovníkovýcj listoch (Camelia sinensis). Determination of the content of heavy metals in the tea leaves (Camelia sinensis). In: Zborník prednášok a posterových zdelení z XIV. medzinárodnej konferencie o analytických metódach v potravinárstve LABORALIM 2003, Banská Bystrica (SR), 18.-19.2.2003, s.102-106(Pr), ISBN 80-227-1887-4

[19] Varečka, Ľ.*, Chovanec, P., Pokorný, R., Martišková, K., Strigáčová, J., Šimkovič, M., Hudecová, D.: Aging-Related Phenomenona in Filamentous Fungus Trichoderma viride. In: 2nd International Meeting on Yeast Apoptosis, Smolenice (SR), 17.-20.9. 2003, s.52 (Po)

[20] Čipák, Ľ., Berzeliová, E., Paulíková, H.*: Effects of flavonoids on glutathione and glutathione-related enzymes in cisplatin-treated L1210 leukemia cells. In: XXII Xenobiochemické Sympózium, 9-11.6. 2003 Smolenice (SR), s. 94 (Po)

[21] Čipák, Ľ., Jantová, S.*: Effects of berberine on cell cycle and the induction of apoptosis on L1210 cells. In: XVIIth Biological Days. Memory in living systems. Brno (ČR), 19th-20th November, 2003, p.49 (Po), ISBN 80-210-3264-2.

[22] Jantová, S., Slameňová, D., Miko, M.*: Induction of the ssDNA breaks by 9-bromo-5-morpholino-tetrazolo[1,5-c]quinazoline. In: XXII Xenobiochemické Sympózium, 9-11.6. 2003 Smolenice (SR), s. 138-139 (Po)

[23] Miko, M.*, Letášiová, S., Poturnajová, M.: Why are N,N-bis alkyldimethyl-3,8-diazo-4,7-dioxododekan-1,10 diammonium bromides (ADDDBr) cytotoxic? In: XXII Xenobiochemické Sympózium, 9-11.6. 2003 Smolenice (SR), s. 154 (Po)

[24] Šovčíková, A.*, Chalupa, I., Sedlák, J., Floch, Ľ., Horáková, K.: Effects of selected isothiocyanates on the proliferation of different types of cancer cell lines. In: Jesenné pracovné dni. Genetická toxikológia a prevencia rakoviny. ÚEO SAV, Bratislava (SR), 20.-22. október, 2003, s.35 (Po)

[25] Šovčíková, A.*, Sedlák, J., Chalupa, I., Floch, Ľ., Horáková, K.: Modulation of cell cycle and induction of apoptosis in different types of cancer cell lines. In: XVIIth Biological Days. Memory in living systems. Brno (ČR), 19th-20th November, 2003, p.71 (Po), ISBN 80-210-3264-2.

[26] Valent, A.*, Kohútová, M., Melník, M., Hudecová, D., Švajlenová, O.: Štúdium antimikrobiálnej aktivity N-salicylidén-D,L-alfa-alaninátomeďnatých komplexov. Study of the antimicrobial activity of copper(II)salicylidene-alaninate complexes. In: 32. konference Syntéza a analýza léčiv, Velké Karlovice (ČR), 16.-19.9.2003, s.105 (Po)

[27] Dudová, B.*, Šimkovič, M., Kaliňák, M., Varečka, Ľ.: The study of Saccharomyces cerevisiae and Trichoderma viride Ca2+ homeostasis. Differences in the inhibitor effects. In: XXII Xenobiochemické Sympózium, 9-11.6. 2003 Smolenice (SR), s. 74-75 (Pr)

[28] Hudec, R.*, Kaiserová, K., Orlický, J., Varečka, L.: Parameter of basal transport of calcium ions in resealed human red blood cells ghosts. In: XXII Xenobiochemické Sympózium, 9-11.6. 2003 Smolenice (SR), s. 38 (Pr)

[29] Hudec, R.*, Lakatoš, B., Orlický, J., Varečka, Ľ.: Comparison of parameters of basal calcium ions transport into resealed human red blood cells ghosts and intact cells. In: Drobnicov memoriál, II. ročník, Senec (SR), 12.-14.11.2003, s. 49-50 (Pr)

[30] Kaliňák, M.*, Chovanec, P., Liptaj, T., Pronayová, N., Jakubík, T., Varečka, Ľ.*: Primary nd secondary metabolism in growth and conidation of Trichoderma viride under oxygen accessibility restriction. In: XXII Xenobiochemické Sympózium, 9-11.6. 2003 Smolenice (SR), s. 72-73 (Pr)

[31] Miko, M.: Mitochondria, apoptosis and xenobiotics.In: XXII Xenobiochemické Sympózium, 9-11.6. 2003 Smolenice (SR), s. 32 (Pr)

[32] Mikulášová, M.*, Košíková,B., Birošová,L.: Mechanizmus antimutagénneho účinku polyfenolových látok Mechanism of antimutagenic effect of polyphenols In: Jesenné pracovné dni. Genetická toxikológia a prevencia rakoviny. ÚEO SAV, Bratislava (SR), 20.-22. október, 2003, s.12 (Pr)

[33] Pokorný, R.*, Hudecová, D., Burgstaller, W., Varečka, Ľ.: Changes in properties of glutamate transport in Trichoderma viride vegetative mycelia upon adaptation to glutamate as carbon source. In: Drobnicov memoriál, II. ročník, Senec (SR), 12.-14.11.2003, s. 51-52 (Pr)

[34] Pokorný, R.*, Smoleňová, E., Holienčin, R., Liptaj, T., Hudecová, D., Varečka, Ľ., Hoelker, U.: Isolation of indigenous filamentous fungi from low-rank coal excavated from coal-mine Záhorie (Southwestern Slovakia) and their use for the caol-solubilisation. In: XXII Xenobiochemické Sympózium, 9-11.6. 2003 Smolenice (SR), s. 76-77 (Pr)

[35] Varečka, Ľ.*, Marčeková, Z., Kamenistá, A., Urban, H., Strigáčová, J., Hudecová, D.: Chlorpromazine-resistant mutanst as a tools for the study of life cycle of filamentous fungi. In: XXII Xenobiochemické Sympózium, 9-11.6. 2003 Smolenice (SR), s. 70-71 (Pr)

[36] Hudecová, D.: Nové trendy v ochrane rastlín. New trends in plant protection. In: XVII. seminár pre stredoškolských učiteľov chémie, FCHPT STU Bratislava, 27.8. 2003, (Pr)

DEPARTMENT OF CERAMICS, GLASS AND CEMENT

36


Head of Department: Telephone: ++421252926048 Assoc. Prof. Miroslav Jamnický, PhD Fax:++421252493198


I. STAFF Associate Professors: Miroslav Jamnický, PhD; Ján Majling, PhD (till 31.10.2003); Martin T.Palou, PhD (since 1.12.2003); Assistant Professors : Jozef Kákoš, PhD; Vladimír Kovár, PhD; Martin T.Palou, PhD (till 30.11.2003); Eva Smrčková, PhD;

Research Fellows: Jana Kozánková; Ladislav Pach, PhD (till 31.8.2003); Štefan Svetík;

PhD Students: Katarína Bodišová (since 1.10.2002); Martin Dovaľ (since 1.10.2003), Marian Rebroš (till 30.9.2003); Radovan Tóth (since 1.10.2001)

Technical staff: Ľudmila Illášová; Helena Jablonková (till 28.2.2003), Pavol Krutý; Mária Pelíšková; Iveta Zezulová;


A. Teaching laboratories: Teaching laboratory I Teaching laboratory II B. Research laboratories: Laboratory of ceramics Laboratory of glass Laboratory of inorganic binders Laboratory of sol/gel Laboratory of inorganic powders synthesis Laboratory of thermal analysis Laboratory of calorimetry Scanning electron microscopy laboratory X-ray diffractometer laboratory

III. TEACHING

A. Undergraduate Study: 6. semester (Bc) Materials technology 2/0/0 Majling Bachelor’s thesis 0/0/4 Jamnický, Kovár, Kozánková,

Smrčková, Svetík 1. semester (MSc) Inorganic chemistry III 2/2/0 Jamnický Solid state physics 2/0/0 Lokaj, Smrčková Raw materials and technical

mineralogy 2/1/0 Svetík, Kozánková

Specialised laboratory practices I 0/0/10 Kákoš, Kovár, Kozánková, Palou, Smrčková, Svetík

2. semester (MSc) High temperature processes 2/1/0 Kovár Applied heat technique 2/1/0 Kákoš, Kovár Specialised laboratory practices II 0/0/8 Smrčková, Kovár, Palou, Jamnický,

Kákoš Factory praxis two weeks Jamnický, Smrčková 3. semester (MSc) Technology of spec. inorg. materials 2/0/0 Kákoš, Majling Inorganic binders technology 2/0/0 Palou Technology of ceramics 2/0/0 Smrčková Technology of glass 2/0/0 Jamnický, Pach


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3. semester (MSc) Specialised laboratory practices III 0/0/10 Jamnický, Palou, Smrčková, Kákoš, Pach

4. semester (MSc) Master’s thesis laboratory 0/0/27 Jamnický, Kákoš, Kovár, Majling, Pach, Palou, Smrčková


A. VEGA Project No 1/9141/02 Superionic conducting oxide glass and glass-crystal composite materials containig copper cations (Miroslav Jamnický)

Preparation of mixed-halide glasses in the systems CuI – CuBr –Cu2O – P2O5 and CuI – CuBr –Cu2O – (P2O5 + MoO3) with the same structure of the oxide network, the same content of dopping salts (CuI + CuBr) but with the variable content of cuprous halides (the study of “mixed anion effect”). Determination of the structure of main structural units in the systems under study and characterization of their thermal, electrical and acoustical properties. Determination of correlations among composition, structure of oxide glass network, acoustical and electrical properties of the glasses prepared under study.

Project duration: from 01.01.2002 to 31.12.2004 B. VEGA Project No 1/0245/03 Effect of seeding additives on the phase and microstructure

envolvement during hydration of sulfoaluminate cements (Ján Majling) The hydration in a model of sulfoaluminate belite cement consisting of C2S, C4A3S, CS, C minerals was deeply explored in the term of chemical reactions. A computational mean has been developed to define the trajectory exploration of the stable conode corresponding to ettringite and gehlenite hydrate. The result of computational method has showed that C2S-C4A3S- CS- C system can be divided into two fields C2AS- C2S- C4A3S- CS and C2S-C4A3S-CS-C separated by a singular point of C2S-C4A3S-CS. According to theoretical computation, hydration reactions in each field as well as in singular point have to lead to the formation of two stable crystallohydrates: gehlenite hydrate and ettringite.

Project duration: from 01.01.2003 to 31.12.2005 C. Institutional project of FCHFT SUT No 191/03 Preparation of Al2O3 ceramics from

nanosize articles (Vladimír Kovár) Stabilization of colloidal particles in suspension and thickness of solvatation layers are important parameters for preparation of ceramics by colloidal processes. Effect of various additives on alpha Al2O3 ceramics preparation was investigated. Suspension were concentrated by pressure filtration and by isostatic membrane pressing. Further these technique of ceramics preparation will be examined.



VI. COOPERATION



Duration

Slovak University of Technology, Faculty of Electrical Engineering and Informati, Bra

Effect of organic additives on crystallization of boehmite gels

Kadlečíková Magdaléna, researcher, Ilkovičova 3, 812 19 Bratislava

Slovak University of Technology, Faculty of Mechanical Engineering, Trnava

Isostatic pressing of ceramic powders Turňa Milan, professor, Paulínska 16, 917 24 Trnava

University of Žilina, Faculty of Mechanical Engineering, Department of Physics,Žilina

Study of mixed cation effect in ion conductivity glasses using electrical conductivity spectra, study of transport mechanisms in fast i

Bury Peter, professor, 010 26 Žilina


38

Slovak Academy of Sciences, Institute of Inorganic Chemistry, Bratislava

The structure and properties of cuprous ion conducting glasses

Šajgalík Pavol, director, Dúbravská cesta 9, 843 69 Bratislava

Slovak Academy of Sciences, institute of Construction and Architecture, Bratislava

The performances of blended cements based on sulfoaluminate belite and Portland cement

Janotka Ivan, researcher, Dúbravská cesta 9, 842 20 Bratislava

Slovak Academy of Sciences, Institute of Informatics, Bratislava

Synthetic opals made by the Langmuir-Blodgett method

Bárdošová Mária, researcher, Dúbravská cesta 9, 842 37 Bratislava

AVANT, a.s., Lučenec (Engineering, investment and design)

Utilization of local raw materials for construction materials production

Molnár Alexander, director, Vajanského 2, 984 01 Lučenec

Ipeľské tehelne, a.s., Lučenec (Brick plant)

Mineralogical and thermoanalytical investigation of local raw materials for brick production

Dováľ Martin, director, M. Rázusa 29, 984 01 Lučenec

Novoker, a.s., Lučenec (Wall Tiles Producer)

Causes of defect formation and their identification in wall tiles

Sarvaš Ladislav, 984 01 Lučenec-Vidiná

Johns Manville Skloplast, a.s., Trnava (Glass fibre producer)

Optimization of drainage ovens of glass melting agregate

Kalinay Andrej, Strojárenská 1, 917 99 Trnava

RONA, a.s., Lednické Rovne (Glass work)

Causes of defect formation and their identification in glassware

Šimurka Peter, vice-director, Schreiberova, 020 61 Lednické Rovne

Slovglass, a.s., Poltár (Crystal glass producer)

Review and process optimization in lead glass polishing and in neutralization station

Zán Ľubomír, director, 987 01 Poltár

Technické sklo, a.s., Bratislava (Technical Glass Work)

Preparation of glass-ceramic materials by controlled processes of nucleation and crystallization

Chocholoušek Jozef, head of testing laboratory, Agátová, 844 03 Bratislava

Východoslovenské stavebné hmoty, a.s., Turňa nad Bod(construction materials producer)

Milling ability of cement clinker and various additives

Jaklovský Štefan, director, 044 02 Turňa nad Bodvou

Holcim, a.s., Rohožník (Cement Producer)

Effect of various gypsums on setting and hardening of cement

Hanzo Peter, director, 906 38 Rohožník

Považská cementáreň, a.s., Ladce (Cement Producer)

Determination of P2O5 content in Portland clinker fired with addition of meat-bone flour, determination of water soluble chromium in ce

Martauz Pavol, director, ul. J. Kráľa, 018 63 Ladce

TAZUS, a.s., Bratislava Artificial dense stones, fly ashes Zajíček Milan, director, Studená

3, 826 34 Bratislava

DATASYSTEM Laboratory, Bratislava

Thermal analysis evaluating optical transmittance, prospects and limitations

Kremničan Vladimír, director, Budovateľská 13, 821 08 Bratislava



Duration

Mount Allison University, Department of Chemistry, Sackville, Canada

Growth, morphology and thermoanalytical properties of fluoroapatite bio-glass-ceramics in lithium disilicate glasses

Mojumdar Subhash C., Sackville, NB, E4L 1G8, Canada


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University of Technology, Department of Chemistry, Materials and Forensic Science, Sydney, Australia

Light transmittance thermal analysis of hydroxyapatite xerogels

Ray Abhi S., professor, City campus, PO Box 123, Broadway, Sydney, 2007 Australia

University of Boumerdes, Faculty of Engineer Science, Department of Engineering Materials, Boumerdes

Silica fume treatment for improving durability of alkali resistant glass fibres in cement matrixes

Ayadi. Azzedine, professor, 350000 Boumerdes, Algeria

University of Machester, Department of Chemistry, Manchester, UK

Synthetic opals made by the Langmuir-Blodgett method

Hodge Paul, Oxford road, Manchester, UK

Enven eko-engineering a.s., Prague, Czech Republic

Evaluation of solid pollute substances (powders) and their separation in electrostatic precipitators during standard work of furnace

Ivičič Jan, head researcher, Počernická 96, 108 03 Praha 10, Czech Republic



Valid date

Slovak Silicate Society, Bratislava member Jamnický Miroslav Slovak Glass Society, Lednické Rovne member of advisory board 01.01.1997 -

Union of Glass Industry, Bratislava member

Palou Martin Slovak institute for standardization (technical comission No 40 Inorganic binders) member 01.01.2000 -

Smrčková Eva Slovak institute for standardization (technical comission No 56 Construction materials and testing)

member 01.01.2000 -



Valid date

Pach Ladislav American Ceramic Society, USA member 01.01.1994 - E. Visitors from Abroad


Date / Duration

Ivičič, J. Enven eko-engineering a.s., Prague Czech Republic March 2003 (1 day)

Mendiburu, E., Mendex GmbH (International business organization), Berlin Germany April 2003 (1 day)

Falca, A. Rovitex S.a.r.l., Crans-pres-Celigny Switzerland April 2003 (1 day)

Ivičič, J. Enven eko-engineering a.s., Prague Czech Republic April 2003 (1 day)

Ivičič, J. Enven eko-engineering a.s., Prague Czech Republic May 2003 (1 day)

Huang, J.-L. Department of Materials Science and Engineering, National Cheung Kung University, Tainan

Taiwan Republic of China

September 2003 (1 day)

Thomas, P. University of Technology, Faculty of Science, Department of Chemistry, Materials and Forensic Science, Sydney

Australia October 2003 (1 day)

Havlica, J. Technical university, Brno Czech Republic November 2003 (1 day)


40



Date / Duration

Palou, M. 11th Int. congr. chemistry of cement (ICCC), Durban South Africa May 2003 (10 days)

Palou, M. meeting of European comission for standardization, Budapest Hungary October 2003 (2 days)

Palou, M., Smrčková, E.

Thermal analysis in theory and practice (workshop), Brno

Czech Republic


Tóth, R. UNIDO International Centre for Science and High Technology, Trieste Italy one year



Želinská, K. Thermal dissociation of limestonen and dolomite by DTA and TG analysis Svetík, Š.

Krajčová, L. Study of glassy microporous filters in the phase separated natriumborosilicate glass system with appropriate carriers Kozánková, J.

Pavúčková, M. Determination of P2O5 content in Portland clinker fired with addition of meat-bone flour Smrčková, E.

Zán, P. Causes of defect formation and their identification in glassware Jamnický, M. B. Graduate Theses (MS Degree) for state examinations after five years of study

Name Title of Thesis Supervisor Andráš, A. Review and process optimization in lead glass polishing and in

neutralization station Jamnický, M.

Dováľ, M. Study of phase equilibrium in four phase oxide system Na2O-ZrO2-P2O5-SiO2 Majling, J.

Čičmancová, L. Effect of ettringite formation kinetics on its morphology Palou, M.

Chnapková, J. Effect of granulometry of sample on accuracy of its chemical composition determined by RFA Kovár, V.

Kahalová, G. Optimization of drainage ovens of glass melting agregate Kovár, V. Kokavcová, K. Preparing and properties of mixed-halide Cu+ionicaly conducted glasses Jamnický, M.

Peško, M. Study of effect of zeolite - ferous sulphate mixture addition on contents of water soluble Cr(VI) in Portland cement Smrčková, E.

Szolárd, I. Effect of E-glass composition on its crystallization Kákoš, J. Šúlyová, M. Determination of real phase composition of clinkers / cements Smrčková, E. Záhorcová, R. Initial stage of boehmite gel sintering Pach, L. C. Dissertations (PhD)

Name Title of Thesis Supervisor Holková, Z. Preparation and properties of porous sol-gel materials on Al2O3 base Pach, L.

Chocholoušek, J. Preparation of glass-ceramic materials by controlled processes of nucleation and crystallization Majling, J.

E. Habilitation Theses Name Title of Thesis Head of board

Palou, M. Ettringite in sulphoaluminate belite cements, formation mechanisms and kinetics Fellner, P.

F. Inauguration Theses

VII. PUBLICATIONS A. Journals [1] Holková Z., Pach L., Kovár V., Svetík Š.: Kinetic study of Al2O3 sintering by dilatometry. Ceramics – Silikáty 47 (1)

13-19 (2003). [2] Jamnický, M., Sedláček J., Znášik P.: The structure and properties of cuprous ion conducting glasses. Solid State

Phenomena 90-91 () 221-226 (2003). [3] Ayadi, A., Palou, M., Iratni A.: Silica fume treatment for improving durability of alkali resistant glass fibres in cement

matrixes. Solid State Phenomena 90-91 () 209-214 (2003). [4] Holková Z., Pach L., Majling J., Kákoš J., Kadlečíková M.: Effect of organic additives on crystallization of boehmite gels. Ceramics – Silikáty 47 (4) 149-154 (2003). [5] Majling, J.: Present status of the optical transmittance thermal analysis, a microstructure related method. Solid State


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Phenomena 90-91 () 75-78 (2003). [6] Lužáková, V., Smrčková, E.: Kvalita vápna a účinnosť kaustifikácie. Lime quality and caustification efficiency (in

Slovak). Papír a celulóza 58 (7-8) 216-219 (2003). B. Conferences [1] Hockicko, P.*, Bury P., Jamnický, M., Jamnický I.: Contribution of acoustic spectroscopy to understanding of

transport mechanisms in fast ion conductive glasses. In: Proc. 7th Int. colloqium ACOUSTIC ´03, Zvolen – Šachtičky, Sept. 4 – 5, 2003, pp. 15-18. ISBN 80-228-1247-1

[2] Hockicko, P.*, Bury P., Jamnický, M., Jamnický I.: Study of mixed cation effect in ion conductivity glasses using electrical conductivity spectra. In: Proc. 9th Int. worshop on applied physics of condensed matter, Malá Lučivná, June 11-13, 2003, pp. 174-178. ISBN 80-8070-088-5

[3] Földesová, M.*, Dillinger P., Lukáč P., Svetík Š.: Vplyv kalcinácie a chemickej modifikácie na štruktúru prírodných zeolitov. Influence of calcination and chemical modification on structure of natural zeolites (in Slovak) In: Proc. XVI conf. on thermal analysis and calorimetry THERMANAL 2003, Stará Lesná, Oct. 8-10, 2003, Ed.: Fajnor V. Š., Smrčková, E., Šimon, P., STU Bratislava 2003, PO 6 (2 pages).

ISBN 80-227-1955-2 [4] Černáková, Ľ.*, Kováčik D., Zahoranová A., Kozánková J., Hudec I.: Modification of polypropylene Surface by

Grafting with Acrylic Acid. In: Proc. 18th Bratislava int. conf. on Modified Polymers, Stará Lesná, October 5-8, 2003, Ed.: Omastová M., STU Bratislava, 2003, p. 52. ISBN 80-968433-2-X

[5] Černáková, Ľ*., Kováčik, D., Černák, M., Hudec, I., Kozánková, J.: Surface grafting of acrylic acid onto polypropylene foil. In: Proc. Int. conf. Polymer materials, Bratislava, October 29-30, 2003, Ed.: Alexy P., STU Bratislava, 2003. p. 45. ISBN 80-227-1959-5

[6] Brusilová A.*, Pulc V., Kozánková J., Pach L.: Vplyv mikroštruktúry na oteruvzdornosť nitridu kremíka. Influence of microstructure on wear resistance of silicon nitride ceramics (in Slovak) In: Proc. 7th Int. sci. conf. Mechanical engineering 2003, Bratislava, Nov. 5-6, 2003, Ed.: STU Bratislava, 2003, S2_06 (7 pages). ISBN 80-227-1960-9

[7] Bodišová K.*, Pach L., Záhorcová R.: Spekanie monolitného Al2O3 gélu. Sintering of monolithic Al2O3 gel (in Slovak) In: V. seminár Príprava keramických materiálov, Herľany, June 17 – 19, 2003, Ed.: HF TU Košice, pp. 77-80 (2003). ISBN 80-7099-643-9

[8] Kolektív autorov (medzi nimi Kovár V., Laček J., Majling J., Znášik P.): Encyclopaedia Beliana, tretí zväzok Č – Eg. Encyklopedický ústav SAV, Bratislava, 2003. ISBN 80-224-0761-5 [9] Janotka I.*, Drábik M., Palou, M. T.: Performance of mortars made from binary sulphoaluminate – belite (85 wt %)

Portland cement (15 wt %) blend. In: Proc. 15. Int. conf. IBAUSIL, Weimar (Germany), Sept. 24-27, 2003, Ed. Bauhaus-Universität Weimar, band 1, pp. 0635-0644 (2003). ISBN 3-00-010932-3

[10] Kozánková, J., Chocholoušek J., Mojumdar, S. C., Majling J.*: Growth, morphology and thermoanalytical properties of fluoroapatite. In: Proc. XVI conf. on thermal analysis and calorimetry THERMANAL 2003, Stará Lesná, Oct. 8-10, 2003, Ed.: Fajnor V. Š., Smrčková, E., Šimon, P., STU Bratislava 2003, PO 14 (2 pages). ISBN 80-227-1955-2

[11] Majling, J.*, Kremničan V., Kovár V., Pach L.: Thermal analysis evaluating optical transmittance, prospects and limitations. In: Proc. XVI conf. on thermal analysis and calorimetry THERMANAL 2003, Stará Lesná, Oct. 8-10, 2003, Ed.: Fajnor V. Š., Smrčková, E., Šimon, P., STU Bratislava 2003, PL 3 (6 pages). ISBN 80-227-1955-2

[12] Lukáč, P.*, Földesová M., Dillinger P., Svetík Š.: Zmeny sorpčných vlastností prírodných a chemicky modifikovaných zeolitov spôsobené teplotou a vysokoenergetickým žiarením. Changes of sorption properties of natural and chemically modified zeolites caused by temperature and high energy radiation (in Slovak). In: Proc. XVI conf. on thermal analysis and calorimetry THERMANAL 2003, Stará Lesná, Oct. 8-10, 2003, Ed.: Fajnor V. Š., Smrčková, E., Šimon, P., STU Bratislava 2003, PO 11 (2 pages). ISBN 80-227-1955-2

[13] Mojumdar, S. C.*, Kozánková J., Chocholouček J., Majling J., Fábryová D.: Fluoroapatite-material for medicine: Growth, morphology and thermoanalytical properties. In: Book of abstracts 49th Int. conf. on Analytical sciences and spectroscopy, Ottawa (Canada), June 1-4, 2003, Ed.: Carleton University, 2003, p. 98-99.

[14] Mojumdar, S. C.*, Kozánková J., Chocholouček J., Majling J., Fábryová D.: The growth of fluoroapatite bio-glass-ceramics, precipitated in lithium disilicate glass: thermoanalytical and morphological study. In: Abstract booklet 31st North American thermal analysis society conf., Albuquerque (USA), Sept. 22-24, 2003, Ed.: Perkin Elmer, 2003, p. 63.

[15] Mojumdar, S. C.*, Kozánková J., Chocholouček J., Majling J., Fábryová D.: The growth of fluoroapatite bio-glass-ceramics, precipitated in lithium disilicate glasses: thermoanalytical and morphological study. In: Proc. 31st North American thermal analysis society conf. (NATAS), Albuquerque (USA), Sept. 22-24, 2003. Ed.: Rich M. J., Michigan State University, pp. 621-630 (2003).

[16] Mojumdar, S. C.*, J. Kozánková J., Chocholuček J., Majling J., Nemecek V.: The microstructure and optical transmittance thermal analysis of sodium borosilicate bio-glasses. In: Abstract booklet 31st North American thermal analysis society conf., Albuquerque (USA), Sept. 22-24, 2003, Ed.: Perkin Elmer, 2003, p. 70.

[17] Mojumdar, S. C.*, Kozánková J., Chocholuček J., Majling J., Nemecek V.: Sodium borosilicate bio-glasses: microstructure and optical transmittance thermal analysis. In: Book of abstracts 49th Int. conf. on Analytical sciences and spectroscopy, Ottawa (Canada), June 1-4, 2003, Ed.: Carleton University, 2003, p. 102.

[18] Bodišová K.*, Pach L., Kozánková J.: Vplyv rýchlosti ohrevu na spekanie Al2O3 gélov. Influence of heating rate on sintering of Al2O3 gel (in Slovak). In: Proc. XVI conf. on thermal analysis and calorimetry THERMANAL 2003, Stará Lesná, Oct. 8-10, 2003, Ed.: Fajnor V. Š., Smrčková, E., Šimon, P., STU Bratislava 2003, SL 6 (4 pages). ISBN 80-227-1955-2

C. Books and Textbooks [1] Bardosova, M., Hodge P., Pach L., Pemble M. E., Smatko V., Tredgold R. H., Whitehead D.: Synthetic opals made

by the Langmuir-Blodgett method. Synthetic opals made by the Langmuir-Blodgett method.Thin Solid Films 437 ()


42

276-279 (2003). [2] Marcinčin A., Hudec I., Majling J.: Technológia materiálov. Technology of materials. Vysokoškolské skriptum, STU

Bratislava, 2002, 183 str n. ISBN 80-227-1798-3

DEPARTMENT OF CHEMICAL AND BIOCHEMICAL ENGINEERING

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Head of Department: Telephone: ++421-2-52496920 Assoc. Prof. Ing. Ľudovít Jelemenský, Phd Fax: ++421-2-52496743


I. STAFF Full Professors: Vladimír Báleš, PhD, DSc Associate Professors: Daniel Bobok, PhD; Ján Dojčanský, PhD; Graczová Elena, PhD; Jelemenský Ľudovít, PhD; Markoš Jozef, PhD; Mierka Otto, PhD; Polakovič Milan, PhD; Stopka Ján, PhD; Štefuca Vladimír, PhD Assistant Professors : Ačai Pavel, PhD; Bafrnec Milan, PhD; Bafrncová Soňa, PhD; Havalda Ivan; Molnár Attila, PhD; Šefčík Jaroslav; Šefčíková Milica, PhD, Timár Pavel, PhD; Vajda Milan, PhD Research Fellows: Antošová Monika, Besedová Eva, PhD; Grznárová Gabriela; Hroncová Viera; Illeová Viera; Juma Mohammad, PhD; Marták Ján; Schlosser Štefan, PhD; Steltenpohl Pavol, PhD; PhD Students: Benčo Róbert; Blažej Michal; Holíková Kristína; Juraščík Martin; Kertesz Rudolf; Kiša Michal; Krajčiová Michaela; Malík Fedor; Mierka Oto; Platková Zdenka; Vandáková Marcela; Znad T. Hussein; Technical staff: Dobrovodská Mária; Herzán Ľubomír; Hinca Miloš; Luknár Karol; Ördögová Marta; Rizman Viliam;


A. Teaching laboratories: Laboratory of Chemical Engineering Laboratory of Unit Operations Laboratory of Reaction Engineering Laboratory of Membrane Processes Laboratory of Chemical Engineering Thermodynamics Membrane Processes and Membrane Reactors Laboratory of Adsorption B. Research laboratories: Laboratory of Chemical Reaction Kinetics and Reaction Engineering Laboratory of Chemical Reaction Kinetics and Reaction Engineering Laboratory of Membrane Processes and Membrane Reactors Laboratory of Adsorption and of Bioprocess Engineering Laboratory of Bioprocess Engineering

III. TEACHING

A. Undergraduate Study: 1. semester (Bc) Material balances of technological

processes 0/2/0 Šefčíková, Ačai, S.Bafrncová, Illeová, Polakovič,

Štefuca, Timár, Vajda, 5. semester (Bc) Chemical Engineering I

Lectures,Exercises, Laboratory

2/3/1 Báleš, Jelemenský, Stopka Šefčík, Ačai, Antošová,

Bafrncová, Besedová, Havalda Mierka, Šefčíková,

Šefčík, Timár. Antošová, Bafrnec 6. semester (Bc) Chemical Engineering II

Lectures, Exercises, Laboratory 2/3/3 Grazcová, Polakovič, Štefuca

Stopka, Ačai, Bafrncová, Besedová, Havalda, Mierka,

Šefčík, Vajda, Antošová, Bafrnec, Grznárová Juma


44

6. semester (Bc) Engineering Thermodynamics, Lectures, Exercises

2/2/0 Mierka, Šefčíková, Timár

Technological Projects 0/0/4 Timár, Markoš, Mierka, Besedová, Polakovič

1. semester (MSc) Chemical Engineering Thermodynamics, Lectures, Exercises

2/2/0 Graczová, Steltenpohl

Diffusional Separation Processes, Lectures, Exercises

2/2/0 Polakovič, Juma

Hydrodyn. and Heat Transfer, Lectures, Exercises, Lab.

2/2/2 Stopka, Havalda

Mass Transfer Theory 2/1/0 Bobok 1. semester (MSc) Mathematical Methods in Chemical

Engineering 0/0/3 Havalda

Computer Chemical Engineering Calculations

0/0/3 Bafrncová, Molnár, Steltenpohl

Fire Engineering 2/2/0 Jelemenský 2. semester (MSc) Chemical Reaction Engineering I

Lectures, Exercises, Laboratory 2/2/2 Markoš, Vajda

Safety Engineering I 2/1/0 Jelemenský, Molnár Bioprocess Engineering I 2/0/1 Báleš, Polakovič Project of Equipment of Chemical and

Food Technology ( 0/0/3 Ačai, Bafrnec, Graczová, Markoš,

Mierka, Molnár,

2. semester (MSc) Advanced Laboratory of Chemical Engineering I

0/0/3 Graczová,Bobok,Juma,Stopka, Schlosser, Stefuca,Šefčík

Selected Unit Operations 2/0/0 Bobok, Schlosser

Explosion Prevention Lectures, Laboratory

2/0/2 Jelemenský, Molnár

Process Systems Engineering 2/0/2 Markoš, Juma Biochemical Engineering

Lectures 2/0/1 Polakovič

Basic Safety Engineering 2/1/0 Jelemenský 3. semester (Bc) Chemical Reaction Engineering II

Lectures, Laboratory 2/0/1 Markoš

Process Systems Engineering Lectures, Laboratory

1/0/2 Markoš, Juma

Advanced Laboratory of Chemical Engineering II

0/0/6 ˇBafrnec, Graczová, Markoš, Mierka, Polakovič,

Cost Engineering of Industrials 0/2/0 Bafrnec 3. semester (MSc) Solid Particles in Technology and

Environment 2/0/0 Timár

Design Projects 0/0/2 Mierka Membrane Processes 1/0/1 Schlosser Safety Engineering ll 2/1/0 Jelemenský 3. semester (MSc) Laboratory of Process Plant Safety 0/0/3 Jelemenský,Holíková Laboratory of Safety Engineering 0/0/4 Graczová, Jelemenský, Mierka,

Stopka, Štefuca, Timár Reaction Engineering II 2/0/0 Markoš Electrical Safety for Chemical Process

Plants, Lecture, .Exercises 2/1/0 Perniš

Safety Engineering 2/0/0 Jelemenský 4. semester( MSc) Diploma Work 0/0/27 Bafrnec, Bobok, Graczová, Jelemenský,

Markoš, Mierka, Polakovič, Schlosser, Stopka, Timár, Vajda


A. Institutional project 215/03 Modeling of nonstationary industrial production processes (Milan Bafrnec)

The aim of the project is the development of physical and mathematical models of industrial production processes, in which forming of materials, heat transfer and chemical reaction in solid phase occur. These processes are nonstationary and mainly proceed in equipment of rubber and plastic industries. For the achievement of the above mentioned goal,


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methods and computer programs for the solution of the models derived must be elaborated and further methods and apparatuses should be developed for the determination of quantities describing termodynamic and heat-transfer properties of plastic materials, elastomers, and composite materials produced from them. Project duration: from 1.1.2003 to 31.12.2005

B. VEGA Project No 1/0063/03, Pollutants separation from fluid mixtures (Daniel Bobok) Measurement of adsorption equilibrium data of pollutants on carbon adsorbents. Investigation of the resistance against mass transfer in solid phase pores. Modeling of adsorption separation in a fixed bed of adsorbent. Experimental estimation of extraction properties of pure solvents, prediction and verification of properties of mixed solvents, particularly aimed at extraction of BTX aromatics. Modeling and calculation of emissions of volatile organic compounds released from waste-water treatment plants. Project duration: from 01.01.2003 to 31.12.2005

C. VEGA Project No 1/0064/03, Mechanism of coal particle combustion in low oxygen concentration atmosphere (Jozef Markoš)

The project is devoted to the investigation of combustion of a single coal particle (representing the smallest unit of an industrial combustor) under conditions of low oxygen concentration and high concentration of carbon dioxide. The microstructure properties of the combusted particle will be investigated and the influence of its change during combustion on the mechanism and kinetics of the process will be studied. A mathematical model of the combusted particle, involving all partial processes inside the particle will be developed and compared with experimental data. Model parameters will be determined and optimal performance conditions will be proposed with the aim to minimize the emission of carbon monoxide. Project duration: from 2003 to 2005

D. VEGA Project No 1/0066/03 Designing and optimalisation of bubble column reactors (Vladimír Báleš)

The aim of the project is to study the use of mixed bubble column reactors (bubble columns, airlift reactors) for progressive food technologies. By monitoring fermentation process and transformation of glucose to gluconic acid at growth and non-growth conditions, the influence of biomass concentration on the hydrodynamic regime of the reactor and oxygen transfer through interfacial area will be studied. By developing a mathematical model for the non- steady state conditions involving reaction kinetics, gas hold up dynamics and oxygen transfer, the progress of bubble column reactors scale-up will be proposed. Project duration: from 2003 to 2005

E. FP 5: PRISM: Grant G1RT – CT –2001 – 05029, Process industries safety management – thematic network on human factors (Ľudovít Jelemenský)

www.prism-network.org

Project duration: from 2002 to 2004 F. VEGA Project No 1/8112/01 Integrated system for the safety analysis of chemical process

and loss prevention ((Ľudovít Jelemenský) The aim of the project is a further development of an integreated simulation program for safety analysis, which was developed by our research group within the framework of the foregoing project. An extension of the integrated program is suggested. This will be based on a detailed model of the process, which takes into account nonlinear dynamics and uncertainity. For the prediction of feasible disasters and problems occuring in a plant the attention should be focused on the assessment of causes and consequences of danger due to the existence of multiple steady states and unsteady failures following from nonlinear dynamics. Project duration: from 2001 to 2003

G. Project APVT-99-005002, Complex treatment of Alfalfa as a sustainable energy source by combination of conventional and biotechnological approaches (Vladimír Štefuca)

Technology proposal for isolation and purification of substances obtained by lucerne biomass fractionation - Isolation methods for products of lucerne juice fermentation - Production of biofuels, lactic acid and biogas -Alternative lucerne exploitation. Project duration: from 01.09.2002 to 31.08.2005

H. Research contract of the Department of Agriculture, Food and Safety, subtopic 14b, Isolation and research of properties of bioactive compounds from Amaranthus and their using in human nutrition (Vladimír Štefuca)

The project aim is the developing of procedures of isolation of proteins and lipid compounds from green parts and the corn of Amaranthus. The final objective is to design technological solution for the production of compounds from Amaranthus that can be used in human nutrition as alternative sources of more conventional compounds.


46

Project duration: from 01.09. 2003 to 31.08.2006

I. VEGA Peoject No 1/0065/2003, Kinetic and transport phenomena in enzyme technology (Milan Polakovič)

The project is aimed at the optimization of selected processes of enzyme technology when the investigation of these processes relies on the analysis of kinetic and transport phenomena, especially those of heat and mass transfer. There are three key thematic areas in this project: optimization of production of fructooligosaccharides, applications of flow calorimetry in the study of immobilized systems and the investigation of kinetics of enzyme reactions with macromolecular substrates. Project duration: from 01.2003 to 12.2005

J. Eureka project E, 2497, Environ Biomac, Bioreactor for innovative mass bacteria culture (Milan Polakovič)

The objective of this project is to develop a new cultivation technique where the growth kinetics and metabolic behaviour of bacterial communities are under control. The microorganisms will be produced in order to produce a cost-effective aerobic biodegradation of target xenobiotics and organic pollutants. Project duration: from 01. 2001 to 11. 2003

K. VEGA project No. 1/9136/02 Integrated reaction-separation systems with membranes, mechanism and modeling of mass transport and interactions in them (Štefan Schlosser)

Study of phenomena related to the formation and modeling of integrated systems with liquid, polymeric and ceramic membranes for biochemical or chemical reactions simultaneously carried out with separations. Development and testing of a new generation of solvents and liquid membranes on the basis of ionic liquids. Classical formulation of liquid membranes for the transport of organic acids and metals. Utilization of these solvents in pertraction and membrane based extraction. Study of microfiltration through polymeric hollow fiber membranes in submerged modules and ceramic membranes.

Project duration: from 01.01.2002 to 31. 12 2004


A. Leonardo da Vinci Pilot Project RO/00/B/F/PP141028 Eurocompetencies transfer in vocational guidance for young specialists in bioscience field (Vladimír Báleš)

Project duration: from 2001 to 2003

B. Slovak-Norwegian project : Norwegian Competences Transfer Into New Curricula of Environmental Engineering Education at the Slovak University of Technology in Bratislava ((Vladimír Báleš)


VI. COOPERATION



Duration

Rubber Research Institute Matador a.s. Púchov

Vulcanization conditions influencing the quality and economy of tire production

Klabník Miroslav, director,Terézie Vansovej 1054/45, 02032 Púchov

01.01.2003-10.12.2003

TOPVAR, a. s. Topoľčany

Decreasing of natural gas consumption for the multing process

REISEL Ján, Technical director, Krušovská 2092, 955 14 Topoľčany

01.02.2003 - 30.03.2003

BIOTIKA, a. s. Slovenská Ľupča

Solution for better cooling of fermentation broth

Krištofčák Jozef, director, 976 13 Slovenská Ľupča 566

01.02.2003 - 30.05.2003

ISTROCHEM, a. s. Bratislava

Optimization of energy consumption for sulfenax production

Jurkovič Karol, director, Nobelova 34, 836 05 Bratislava

01.06.2003 - 15.08.2003

Slovnaft, Vlčie hrdlo, Bratislava, Slovakia International project Varga, P., Slovnaf, Vlčie hrdlo,

Bratislava, Slovakia since 2001


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Slovnaft VURUP, a.s., Vlčie hrdlo, Bratislava, Slovakia

International project Mičíková, A., Slovnaft VURUP, a.s. , Vlčie hrdlo, Bratislava, Slovakia

since 2001

NCHZ, a.s. International project, engineering contract ZoD Goga, V., NCHZ, a.s., Nováky since 2001

Duslo, a.s. International project Orihel, J., Duslo, a.s., Saľa since 2001 Kappa, a.s. International project Vačok, Kappa, a.s., Stúrovo since 2001

Matador Púchov, a.s. International project Kvasnica, J., Matador Púchov, a.s., Púchov since 2001

SCP, a.s. International project Říha, SCP, a.s., Ružomberok since 2001

MŽP SR www.prism-network.org

Kobzova, D., MŽP SR, Bratislava

NCHZ, a.s. Engineering project, ZoD Čamaj, V., NCHZ, a.s., Nováky continually

Liko Bratislava a.s. Alfalfa phytomass exploitation Minárik, M., director, Wolkrova 4, Bratislava Since 01.09.2002

Liko Bratislava a.s. Amaranthus exploitation in human food Minárik, M., director, Wolkrova 4, Bratislava Since 01.06.2003

Institute of Chemistry Glycerol biosensor development

Gemeiner, P., Institute of chemistry, Dúbravská cesta 9, Bratislava

Since 1.2.2003

NCHZ, a.s. Study on the application of biocatalysis in chemical industry

M. Polakovič, FChP, Radlinského 9, 812 37 Bratislava

11.2002-06.2003

Slovnaft VURUP, a.s., Vlčie hrdlo, Bratislava, Slovakia

Engineering Contract, ZoD 114/2003 Review of the Newest Scientific Information about the Aromatics Extraction

Mikulec Jozef, director, Slovnaft VURUP, a.s., Vlčie hrdlo, Bratislava, Slovakia

01.07.2003-31.10.2003

Technical University in Košice, Faculty BERG

research cooperation, PhD student Š. Schlosser, SUT, 812 37 Bratislava, Radlinského 9 M. Búgel , TU Košice

2002-2004



Duration

ETH Zurich, CH Morbidelli, Massimo, professor, ETH Zurich, CH

ICPF AV ČR Drahoš, Jiri, professor, ICPF AV ČR

VŠCHT Praha, CR Hanika, Jirí, professor, VŠCHT Praha, CR

TU VŠB, Praha, CR Wichterle, Kamil, professor, TU VŠB, Praha, CR

EPSC, UK International project Turney, Rob, dr., EPSC, UK

UCL London, UK Bogle, David, professor, UCL London, UK

University of Gent, B Marin, Gui, University of Gent, B

Polimi, Milano, I Colombo, Simone, professor, Polimi, Milano, I

CIBA, CH Engineering contract, ZoD 40/2003 Krajnik, Paul, dr., CIBA, CH Federal Agricultural Research Center FP5 project Štefuca, V., SUT, 812 37

Bratislava, Radlinského 9 3 years

Institute National Polytechnique de Lorraine

cooperation in the study of adsorption for the removal of organic pollutants

Polakovič, M. SUT, 812 37 Bratislava, Radlinského 9 Since 1999

Technical University of Wroclaw

cooperation in the kinetics of starch enzyme action

Polakovic, M. SUT, 812 37 Bratislava, Radlinského 9 Since 1998

Ecole Polytechnique Fédérale de Lausanne

Eureka project Polakovič, M. SUT, 812 37 Bratislava, Radlinského 9 2001-2003

ETH Zurich scientific collaboration in the aggregation kinetics of milk proteins

Šefčíková, M., SUT, 812 37 Bratislava, Radlinského 9 Since 2000

Belair Bureau d'Etudes de l'Air, Lausanne

Eureka project Polakovič, M., SUT, 812 37 Bratislava, Radlinského 9 2001-2003


48

Faculty of Sciences and Technology, Basque Country University, Bilbao, Spain

Research Project: Advanced Characterisation of Polyfunctional Catalysts

González Velasco J. R., professor, Basque Country University, Bilbao, Spain

01.07.2002-30.06.2003

CIBA Spezialitätenchemie Grenzach GmbH, Koechlinstrasse 1, D-79639 Grenzach - Vyhlen

Engineering Contract, ZoD 114/2003 Measurement of the Phase Diagram of a Binary System

Krajnik P., Global Head of Engineering, CIBA Spezialitätenchemie Grenzach GmbH

01.06.2003-15.07.2003

CIBA Spezialitätenchemie Grenzach GmbH, Koechlinstrasse 1, D-79639 Grenzach - Vyhlen

Engineering Contract, ZoD 47/2003 Estimation of Vapor-Liquid Equilibrium Data for Binary Systems

Krajnik P., Global Head of Engineering, CIBA Spezialitätenchemie Grenzach GmbH

15.10.2002-28.02.2003

VUT Brno, EVECO Brno, W. L. Gore

Workshop: New Modern Technology for Reliable Lowering of Dioxine and Furan Emissions from Refuse Incinerating Plants

Stehlík P., professor, VUT Brno, Czech Republic 10.12.2003

Technical University of Trondheim,Norway

Bilateral project Báleš V., SUT, 812 37 Bratislava, Radlinského 9 Since 2003



Valid date

Bafrnec Milan Scientific Board of RRI member 01.01.1997 Bobok Daniel Slovak Society of Chemical Engineering member 03.05.1995 Graczová Elena Slovak Society of Chemical Engineering member 03.05.1995

Bafrncová Soňa Slovak Society of Chemical Engineering member 03.05.1995

Besedová Eva Slovak Society of Chemical Engineering member 03.05.1995 Steltenpohl Pavol Slovak Society of Chemical Engineering member 03.05.1995

Ordogová Marta Slovak Society of Chemical Engineering member 03.05.1995

Herzán Ľubomír Slovak Society of Chemical Engineering member 03.05.1995

Bobok Daniel Certificate Commmision of STU Bratislava member 15.03.2003 Timár Pavel Slovak Society of Chemical Engineering secretary 01.02.1995

Markoš Jozef Slovak Society of Chemical Engineering (advisory board) other Since 2000

Jelemenský Ľudovít

Slovak Society of Chemical Engineering (advisory board) other Since 2000

Štefuca Vladimír Slovak Society of Chemical Engineering member Since 2002

Vladimír Báleš Slovak Society of Chemical Engineering chairman Since 2002

Milan Polakovič

Slovak Society of Chemical Engineering Executive Board other Since 2002

Milan Polakovič Chemical Papers - editorial board other Since 1998

Báleš Vladimír Vlákna a textil - editorial board other Since 2003

Steltenpohl Pavol

Programme Committee of the 30th International Conference of the Slovak Society of Chemical Engineering (May 2003, Tatranské Matliare)

member 26.-30.05.2003

Steltenpohl Pavol Chemical Papers journal, Vol. 57(1) and 57(6) other 26.-30.05.2003

Schlosser Stefan Slovak Society of Chemical Engineering (council) other 2001-2004


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Valid date

Markoš Jozef Working party "Chemical Reaction Engineering" of EFCE member Since 2002 Stopka Ján Working party "Education" of EFCE member Since 2002 Milan Polakovič

Section on Applied Biocatalysis of European Federation of Biotechnology (scientific committee) other Since 2002

Vladimír Báleš European Federation of Chemical Engineering (executive committee) other Since 2002

Steltenpohl Pavol

Committee for Dissertation of the European Theses at the Basque Country University, Bilbao, Spain member 15.07.2003

Vladimír Báleš WP Bioreactor Performance EFB member Since 1988 Štefan Schlosser European Membrane Society member continually

Štefan Schlosser Working party Membranes of EFCE (delegate) other

Štefan Schlosser Congress CHISA, Praha (scientific committee) other continually

Štefan Schlosser PERMEA 2003 chairman 2003

Štefan Schlosser Euromembrane 2004, Hamburg (scientific committee) other 2004

Štefan Schlosser

Water Environment-Membrane Technology, Seoul (scientific committee) other 2004

Štefan Schlosser Ars Separatoria Acta (editorial board of journal) other continually



Date / Duration

Turney R. EPSC UK October, 3 days Krajnik, P. CIBA CH October, 3 days Embrey, D. Human Reliabity, Ltd. UK October, 3 days Coterlin, R. DNV UK October, 3 days Web, P. Basel Polyolefins, Ltd. UK October, 3 days Labude, H., J. Dupont G October, 3 days Teixeira, J., A. University of Minho P May, 2 days Hanika, J. VŠCHT, Praha CR December, 2 days

Bryjak, J. Technical University of Wroclaw, Institute of Chemical Engineering Pl July , 6 days

Howell, J. University of Bath UK September, 3 days

Nystrom, M. Lappeenranta University of Technology F September, 2 days

Ben Aim, R. NSA F September, 2 days Twardowski, Z. Chemetics Canada September, 2 days Bryjak, M. Wroclaw University of Technology PL August, 2 days



Date / Duration

Markoš, J. VŠCHT Praha, CR May, 2 days

Markoš, J. 4th European Congress of Chemical Engineering, Granada E September, 5 days

Jelemenský, Ľ.

4th European Congress of Chemical Engineering, Granada E September, 5 days

Molnár, A. 4th European Congress of Chemical Engineering, Granada E September, 5 days

Blažej, M. 4th European Congress of Chemical Engineering, Granada E September, 5 days

Markoš, J. 50th conference CHISA, Srní, Šumava CR October 4 days Jelemenský, Ľ: 50th conference CHISA, Srní, Šumava CR October, 5 days Molnár, A. 50th conference CHISA, Srní, Šumava CR October, 5 days Mierka, O., Jr. 50th conference CHISA, Srní, Šumava CR October, 5 days Krajčiová, M. 50th conference CHISA, Srní, Šumava CR October, 5 days


50

Holíková, K. 50th conference CHISA, Srní, Šumava CR October, 5 days

Blažej, M. 50th conference CHISA, Srní, Šumava CR October, 5 days Kiša, M. 50th conference CHISA, Srní, Šumava CR October, 5 days Blažej, M. VII Polish Conference on Multiphase Flow, Gdańsk PL October, 5 days Molnár, A. University of Gent, Gent B August, 3 days Jelemenský, Ľ. PRISM Seminar, Atheny GR September, 3 days Jelemenský, Ľ. PRISM Seminar, Amsterdam NL June, 2 days Jelemenský, Ľ. PRISM Seminar, Manchester UK February, 3days Štefuca Vladimír Federal Agricultural Research Center G March, 2 days Štefuca Vladimír Stuttgart, project meeting G September, 5 days Polakovič Milan Frankfurt, project meeting G May, 3 days Polakovič Milan EFB Section on Applied Biocatalysis meeting CH August, 2 days

Polakovič Milan 2nd Asian-European Symposium on Biorecognition in Downstream Processing A October, 1 day

Báleš Vladimír Bioprocess Engineering, doctoral/postdoctoral level course Kroatia September, 1 week

Vandáková Marcela

Bioprocess Engineering, doctoral/postdoctoral level course Kroatia September, 1 week

Illeová Viera ETH Zuerich CH December, 1 week Sefčík Jaroslav ETH Zuerich CH October, 1 week Ačai Pavol EPFL Lausanne CH November/1 week

Antošová Monika 2nd Asian-European Symposium on Biorecognition in Downstream Processing A October, 1 day

Šefčíková Milica ETH Zuerich CH September, 2 weeks Malík Fedor Biotrans 2003 CR June-July, 6 days Malík Fedor Bioprocess Engineering course D May-June, 7 days Malík Fedor Institute of Chemical Technology Prague CR November,3 days Vandáková Marcela Institute of Chemical Technology Prague CR November,3 days

Platková Zdenka Institute of Chemical Engineering Prague CR November,3 days

Steltenpohl Pavol Department of Chemical Engineering, Faculty of Sciences and Technology, Basque Country University, Bilbao

E 01.07.2002-30.06.2003

Steltenpohl Pavol Faculty of Sciences and Technology, Basque Country University, Bilbao E July, 7 days

Steltenpohl Pavol Faculty of Sciences and Technology, Basque Country University, Bilbao E September 8 days

Bobok Daniel 50th Conference CHISA 2003, Srní CR October, 4 days Bafrncová Soňa International Workshop Termodynamika 2003, Brejlov CR September, 2 days

Besedová Eva International Workshop Termodynamika 2003, Brejlov CR September, 2 days

Graczová Elena International Workshop Termodynamika 2003, Brejlov CR September, 2 days



Koreňová, Z. Calculation of adsorption heat for the system acetone – activated carbon Besedová, E.

Kotora, M. Modeling of a rectification column with chemical reaction Markoš, J. Lazor, M. Optimization of a chemical reactor for parallel reactions Markoš, J. Martauz, R Dynamic simulation of a pipe reactor for complex reactions Markoš, J. Sikula, I.: Hydraulic calculation of a sand filter Timár , P. Tvrdík, P. Analysis of the function of a triple-effect evaporator Timár, P. Tatárová, I. The influence of random errors in equilibrium data on the design of

adsorbers Polakovič, M.


Alexovič, M. Mathematical modeling of release of dangerous substances into the atmosphere Jelemenský, Ľ.

Both, L. Chemical-engineering calculations of reaction and absorption parts of ClO2 production Timár, P.


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Bunganič, R. Intensification of heat transfer in vulcanization presses Bafrnec, M. Dudeková, M Mathematical model of a reactor for nitric oxides production Stopka, J. Fáber, V. Hydraulic calculations of complex pipeline systems Stopka, J. Calík, K. Modeling of dense gas dispersion in the atmosphere Stopka, J.

Juraščík, M. Application of high-cell density airlift bioreactor to a continuous fermentation of cheese whey Klein, J.

Korbel, M. Kinetic properties of immobilized esterases Štefuca, V. Krajčiová, M. Modeling of self-ignition of coal Jelemenský, Ľ.

Kubaščíková, B. Properties of extraction systems containing components of the mixed solvent DMF and EG Graczová, E.

Máček, R. Membrane extraction and reextraction of Zn from aqueous solutions in hollow fiber contactors Vajda, M.

Malicher, M. Energy audit of the enterprise Ryba, s.r.o., Radoma Holding Mierka, O. Platková, Z. Production of fructosyltransferase in a laboratory batch reactor Polakovič, M.

Sebeš, K. Rate of adsorption of ethanol vapors from air on activated carbon particles

Bobok, D., Besedová, E.

Sűttő, T. Energy audit of the enterprise I.D.C. Holding a.s., Pečivárne Sereď Mierka, O. Šimo, M. Membrane based pertraction and extraction of organic acids Schlosser, Š. Vrzalová, E. Design of a safety control system for chemical industry Jelemenský, Ľ. C. Dissertations (PhD)

Name Title of Thesis Supervisor Molnár, A. Program tool for safety analyis of a chemical reactor Markoš, J.

VIII. PUBLICATIONS A. Journals [1] Čík, G., Hubinová, M., Šeršeň, F., Krištín, J., Antošová, M.: Photocatalytic degradation of 4-chlorophenol by .OH

radicals generated by thiophene oligomers incorporated in ZSM-5 zeolite channels Collect. Czech. Chem. Commun., 68, 2219-2230 (2003)

[2] Illeová, V., Polakovič, M., Štefuca, V., Ačai, P., Juma, M.: Experimental modelling of thermal inactivation of urease. J. Biotechnol., 105(3), 235-243 (2003) .

[3] Marták, J., Š. Schlosser, E. Sabolová, Ľ. Krištofíková and M. Rosenberg: Fermentation of Lactic Acid with Rhizopus arrhizus in the Stired Tank Reactor Using Periodical Bleed and Feed Operation. Process Biochem., 38 (2003) 1573-1583

[4] Molnár, A., Markoš, J., Jelemenský, Ľ.: Safety analysis of CSTR towards changes in operating conditions. Journal of Loss Prevention in Process Industries, 16, (2003), 373 – 380

[5] Šoóš, M., Graczová, E., Markoš, J., Molnár, A., Steltenpohl, P.: Design and simulation of a distillation column for separation of dichloropropane from a multicomponent mixture Chemical Engineering and Processing, 42, (2003) 273 – 284

[6] Blažej, M., Annus, J., Markoš, J.: The use of the dynamic pressure-step method for kLa measurement in the airlift reactor in coalescent and non-coalescent media. Inzynieria i Aparatura Chemiczna, 42, (2003), 5s, p. 24 – 26

[7] Besedová, E., Bobok, D.: Adsorption of Ethanol on Activated Carbon. Chem. Pap. 57(1) 27-34 (2003) [8] Blažej, M., Annus, J., Markoš, J.: Using of the dynamic pressure-step method for mass transfer coefficient

measurement in the internal loop airlift reactor. Chemical Papers, 57, (2003), 445 – 450 [9] Bobok, D.*, Besedová, E.: Diffusion of Ethanol Vapours in Activated Carbon Particles. Chem. Pap. 57(1) 39-44

(2003) [10] Cartland Glover, G., M., Blažej, M., Generalis, S., C., Markoš, J.: Three – dimensional gas – liquid simulation of an

airlift bubble column reactor Three – dimensional gas – liquid simulation of an airlift bubble column reactor Chemical Papers, 57, (2003), 387 – 392

[11] Molnár, A., Mierka, O., Jr., Markoš, J., Jelemenský, Ľ.: Chemical Papers, 57, (2003), 438 – 444 [12] Vajda, M ., Sabolová E., Schlosser Š. and Mikulová E.: Membrane-Based Extraction Joined with Membrane-Based

Stripping in a Circulating Arrangement II. Extraction of organic Acids. Chem. Papers, 57 (2003) 3 – 10 [13] Bobok, D., Besedová, E.: Effective Diffusivities of Water Vapours and Heptane Vapours in Particles of Molecular

Sieves 4A and 5A. Petroleum and Coal, 45(1-2), p.19-24, 2003 [14] Mierka, O., Stopka J., Mierka, O., Jr.: Zlepšené podmienky kogenerácie oproti minulosti. Improved conditions of

cogenration in comparison with the past. Ropa, uhlie, plyn a petrochémia, 45, (2003), 24 – 31 B. Conferences [1] Timár, P.*, Mierka, O.: Cooling of indistrial equipments. In: Proc. of 30-th international conference of Slovak society

of chemical engineering, May 26.-30. 2003, Tatranské Matliare ISBN 80-227-1889-0 (Pr) [2] Timár, P.*: Analysis of paper drying process based on industrial operation data. "In: Proc. of the International

conference ""Chemical technology of wood, pulp and paper"", Sept. 17.-19. 2003, Bratislava, pp. 155-160. ISBN 80-227-1942-0 (Pr)"

[3] Antošová, M.*, Polakovič, M., Vandáková, M., Báleš, V.: Separation of fructosyltransferase by liquid chromatography Separation of fructosyltransferase by liquid chromatography. In: Proc. 30th Int. Conf. Slovak Soc. Chem. Eng., Tatranské Matliare (Slovakia), May 26-30, 2003, Ed. Markoš, J., Štefuca, V., Slovak Society of Chemical Engineering, SEP7(CD ROM), P241, ISBN 80-227-1889-0. (Po)


52

[4] Bafrncová, S., Havalda I., Graczová E.: Calculation of VOC Emission from Industrial Wastewater Treatment. In: 30th International Conference of Slovak Society of Chemical Engineering, Tatranské Matliare , SR 2003. Zb. , cd verzia. ISBN 80-227-1889-0

[5] Blažej, M.*, Annus, J., Markoš, J.: Application of the dynamic pressure –step method for mass transfer coefficient measurement in airlift reactor with internal loop. In: Proceedings of the 4th European Congress of Chemical Engineering, ISBN 84-88233-35-3, 24 – 25 September, 2003, Granada, Spain, poster

[6] Cartland Glover, G. M., Blažej, M. (*), Generalis, S., C., Markoš, J.: Three dimensional gas – liquid simulation of an airlift bubble column reactor In: Proceedings of the 30th Conference of SSCHE, (CD ROM), May 2003, Tatranské Matliare, SK, ISBN 80-227-1889-0, poster

[7] Holíková, K. (*), Markoš, J., Jelemenský, Ľ.: Reaction-diffusion mathematical model for the combustion of single coal char particle. In: Proceedings of the 30th Conference of SSCHE, (CD ROM), May 2003, Tatranské Matliare, SK, ISBN 80-227-1889-0, poster

[8] Illeová, V.*, Polakovič, M., Štefuca, V.: Thermal inactivation of highly pure urease. In: Proc. 30th Int. Conf. Slovak Soc. Chem. Eng., Tatranské Matliare (Slovakia), May 26-30, 2003, Ed. Markoš, J., Štefuca, V., Slovak Society of Chemical Engineering, pp. 156. ISBN 80-227-1889-0. (Po)

[9] Malík, F.*, Štefuca, V., Báleš, V.: Immobilization, mass transfer, and kinetics of carboxylesterase in a flow calorimeter. In: Proc. 30th Int. Conf. Slovak Soc. Chem. Eng., Tatranské Matliare (Slovakia), May 26-30, 2003, Ed. Markoš, J., Štefuca, V., Slovak Society of Chemical Engineering, SEP7(CD ROM), 143 p. ISBN 80-227-1889-0. (Pr)

[10] Markoš, J. (*), Žajdlík, R., Jelemenský, Ľ., Holíková, K.: Study of the single char coal particle combustion. In: Proceedings of the 4th European Congress of Chemical Engineering, ISBN 84-88233-35-3, 24 – 25 September, 2003, Granada, Spain, poster

[11] Molnár, A. (*), Markoš, J., Jelemenský, Ľ.: Mathematical models for safety analysis of chemical reactors. The role of the model accuracy. Proceedings of the 4th European Congress of Chemical Engineering, ISBN 84-88233-35-3, 24 – 25 September, 2003, Granada, Spain, poster

[12] Molnár, A. (*), Markoš, J., Jelemenský, Ľ.: Possibilities of using HYSYS Simulation program for safety analysis of continuous stirred tank reactors. Proceedings of the 4th European Congress of Chemical Engineering, ISBN 84-88233-35-3, 24 – 25 September, 2003, Granada, Spain, poster

[13] Molnár, A. (*), Markoš, J., Jelemenský, Ľ.: Some considerations for safety analysis of chemical reactors. In: Proceedings of the 30th Conference of SSCHE, (CD ROM), May 2003, Tatranské Matliare, SK, ISBN 80-227-1889-0, poster

[14] Serrano Sánchez, A.M.*, Blas Suárez, F., Steltenpohl, P., González Marcos, J.A., González Velasco, J.R.: Mild MCP hydrogenolysis by Pt on Ru/ZrO2 catalysts. In: Proc. 4th European Congress in Chemical Engineering (September 2003, Granada, Spain) ISBN 84-88233-23-X, poster

[15] Vandáková, M.*, Polakovič, M., Platková, Z., Antošová, M., Báleš, V.: Optimization of fructosyltransferase production in shaken flasks using experimental design. In: Proc. 30th Int. Conf. Slovak Soc. Chem. Eng., Tatranské Matliare (Slovakia), May 26-30, 2003, Ed. Markoš, J., Štefuca, V., Slovak Society of Chemical Engineering, SEP7(CD ROM), 142 p. ISBN 80-227-1889-0. (Po)

[16] Znad, H., Dolgoš, O., Báleš, V. (*), Markoš, J.: A kinetic model for gluconic acid production by Aspergillus niger Proceedings of the 4th European Congress of Chemical Engineering, ISBN 84-88233-35-3, 24 – 25 September, 2003, Granada, Spain, poster

[17] Bafrncová, S., Havalda I., Graczová E., Besedová, E. : Emisie a emisné faktory VOC pri čistení odpadových vôd. Emission and emission factors of VOC at Industrial Wastewater Treatment. In: Termodynamika 2003, Brejlov, CZ-2001. cd verzia. ISBN 80-86238-37-7

[18] Bafrnec, M., Juma M.: Riadenie vulkanizácie založené na fyzikálne-matematickom modeli výrobného procesu Proceedings of Slovak Rubber conference 2003 Púchov SR, 21.-22.may 2003

[19] Bafrnec, M., Juma M., Toman J., Michálek J.: Stanovenie fyzikálnych vlastností gumárenských zmesí pre matematické modelovanie vulkanizácie. Determination of Physical Properties of Rubber Compounds Proceedings of Slovak Rubber conference 2003 Púchov SR, 21.-22.may 2003

[20] Bakalár, T., Š. Schlosser and M. Búgel: Adsorption isotherms and kinetics of sorption of copper from aqueous solutions on microparticles of polymeric ion-exchangers. In: Proc. 30th Conference of SSCHI, CD ROM with full papers, Tatranské Matliare (SK), 26-30 May 2003, 9 p.

[21] Bakalár, T., Š. Schlosser and M. Búgel Hybrid process for removal of copper from aqueous solutions by adsorption on microparticles combined with microfiltration. Hybrid process for removal of copper from aqueous solutions by adsorption on microparticles combined with microfiltration Proc. PERMEA 2003, full text of lecture on CD ROM, Tatranské Matliare (SK), Sept. 7-11 2003, 15 p.

[22] Besedová, E., Bobok, D.: Investigation of the adsorption of organic solvents vapours on activated carbon In: Proc. 30-th Int. Conf. SSChE, Tatranské Matliare, Slovakia, May 26th-30th. 2003, CD-ROM, ISBN 80-227-1889-0

[23] Besedová, E., Bobok, D.,Bafrncová, S.: Výpočet adsorpčného tepla z rovnovážnych údajov adsorpcie pár organických látok na aktívnom uhlí. Calculation of adsorption heat from equilibrium data of adsorption of organic vapours on activated carbon. In: Sborník příspěvku Termodynamika 2003, Brejlov,12.-13.9.2003, CD-ROM ISBN 80-86238-37-7

[24] Blažej, M. (*), Juraščík, M., Annus, J., Markoš, J.: Using of dynamic pressure-step method for mass transfer coefficient measurement in airlift reactor. In: Proceedings of the 30th Conference of SSCHE, (CD ROM), May 2003, Tatranské Matliare, SK, ISBN 80-227-1889-0,lecture

[25] Bobok, D., Besedová, E.: Diffusional Mass Transfer of Ethanol Vapours in Particles of Activated Carbons Proc.7th Int.Sci.Conf.Mech.Eng.2003, Bratislava, 5-6 November, 2003, SR, ISBN 80-227-1960-9

[26] Bobok, D., Besedová, E.: Effective Diffusion coefficients of Ethanol Vapours in Particles of activated carbons In: Proc. 30-th Int. Conf. SSChE, Tatranské Matliare, Slovakia, May 26th-30th. 2003, CD-ROM, ISBN 80-227-1889-0


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[27] Bobok, D., Besedová, E.: Ethanol Vapours diffusion in Particles of activated carbons Jubilejní 50. konf. chem. a proces. inženýrství CHISA 2003, 20.-23.10.2003. Srní, Šumava, CD-ROM

[28[ Bunganič R., Bafrnec, M.: Chemical-engineering study of curing process. Proceedings of Slovak Rubber conference 2003Púchov SR, 21.-22.may 2003

[29] Graczová, E., Bafrncová, S.: Application of ternary contribution for liquid-liquid equilibria prediction of multicomponent systems In: 30th International Conference of Slovak Society of Chemical Engineering, Tatranské Matliare , SR 2003. Zb. , cd verzia. ISBN 80-227-1889-0

[30] Graczová, E., Bafrncová, S. Prediction of LLE of multicomponent systems. In: Termodynamika 2003, Brejlov, CZ-2001. cd verzia. ISBN 80-86238-37-7

[31] Grznárová, G.*, Polakovič, M.: The dispersion of a solute applied to the chromatography tubing. In: Proc. 30th Int. Conf. Slovak Soc. Chem. Eng., Tatranské Matliare (Slovakia), May 26-30, 2003, Ed. Markoš, J., Štefuca, V., Slovak Society of Chemical Engineering, SEP7(CD ROM), 16 p. ISBN 80-227-1889-0. (Pr)

[32] Gutiérrez-Ortiz, M. A., González-Velasco, J. R., and Steltenpohl, P. : Preparation and characterisation of catalysts for polymer electrolyte fuel cell. In: 30th International Conference of Slovak Society of Chemical Engineering, Tatranské Matliare , SR 2003. Zb. , cd verzia. ISBN 80-227-1889-0

[33] Jelemenský, Ľ. (*), Harišová, J., Molnár, A., and Markoš, J.: Reliable risk estimation in the risk analysis of a chemical industry. Case study: Ammonia storage pressurized sphere tank. Reliable safety analysis of a chemical reacvtor with nonlinear behaviour. In: Proceedings of the 30th Conference of SSCHE, (CD ROM), May 2003, Tatranské Matliare, SK, ISBN 80-227-1889-0,lecture

[34] Juma, M., Bafrnec, M.,: Experimental determination of curing reaction heat using transient heat conduction equation Proceedings of Slovak Rubber conference 2003Púchov SR, 21.-22.may 2003

[35] Kertész, R., and Š. Schlosser: Design and simulation of two phase hollow fiber contactors for simultaneous membrane based solvent extraction and stripping of organic acids and bases. Proc. PERMEA 2003, full text of lecture on CD ROM, Tatranské Matliare (SK), Sept. 7-11 2003, 28 p.

[36] Kertész, R., Š. Schlosser and M. Šimo: Mass-transfer characteristics of a spiral channel SLM module in pertraction of phenylalanine. Proc. PERMEA 2003, full text of lecture on CD ROM, Tatranské Matliare (SK), Sept. 7-11 2003, 20 p.

[37] Kubišová, Ľ., E. Sabolová, Š. Schlosser, J. Marták and R. Kertész: Mass-transfer in membrane based solvent extraction and stripping of 5-methyl-2-pyrazinecarboxylic acid and co-transport of mineral acid in HF contactors. Proc. PERMEA 2003, full text of lecture on CD ROM, Tatranské Matliare (SK), Sept. 7-11 2003, 14 p.

[38] Mierka, O. (*), Timár, P., Stopka, J., Jelemenský, Ľ., Mošať, A., Mierka, O., Jr.: Transformation of a cogeneration unit into a trigeneration unit. In: Proceedings of the 30th Conference of SSCHE, (CD ROM), May 2003, Tatranské Matliare, SK, ISBN 80-227-1889-0,lecture

[39] Molnár, A. (*), Markoš, J., Jelemenský, Ľ.: Reliable safety analysis of a chemical reacvtor with nonlinear behaviour. In: Proceedings of the 30th Conference of SSCHE, (CD ROM), May 2003, Tatranské Matliare, SK, ISBN 80-227-1889-0,lecture

[40] Serrano Sánchez, A.M.*, Steltenpohl, P., González Marcos, M.P., González Marcos, J.A. González Velasco, J.R.: Propylene-SCR in lean-NO conditions over Ru and Ru-Pt/ZrO2. In: Proc. 4th International Symposium on Environment, Catalysis and Processes Engineering (April 2003, Fez, Morocco), oral presentation

[41] Serrano-Sánchez, A. M., Steltenpohl, P., González-Marcos, M. P., González-Marcos, J. A., and González-Velasco, J. R.: Evaluation of oxidising potential of Ru and Ru-Pt/ZrO2 catalyst for no with C3H6 and O2. In: 30th International Conference of Slovak Society of Chemical Engineering, Tatranské Matliare , SR 2003. Zb. , cd verzia. ISBN 80-227-1889-0

[42] Schlosser, Š.,R. Kertész, J. Marták and Ľ. Kubišová. Separation of organic acids by membrane based solvent extraction – recovery of MPCA. Proc. Int. conf. PERMEA 2003, full text of lecture on CD ROM, Tatranské Matliare (SK), Sept. 7-11 2003, 16 p.

[43] Vajda, M., Košúthová A. and Schlosser Š.: Membrane-Based Extraction Joined with Membrane-Based Stripping in a Circulating Arrangement III. Extraction of Zinc. In: Proc. 30 th conf. SSCHI, CD ROM with full texts, Tatranske Matliare (SK), May 26-30 2003, 13 p.

[44] Znad, H.*,Blažej, M., Baleš, V., Markoš, J.: A kinetics model for gluconic acid production by Aspergillus niger. In: Proc. 30th Int. Conf. Slovak Soc. Chem. Eng., Tatranské Matliare (Slovakia), May 26-30, 2003, Ed. Markoš, J., Štefuca, V., Slovak Society of Chemical Engineering, SEP7(CD ROM), 16 p. ISBN 80-227-1889-0. (Pr)

[45] Besedová, E., Bobok, D.: Meranie rovnovážnych charakteristík zeolitických adsorbentov. Measurement of equilibrium characteristics of zeolite adsobents. Odborný seminár Prírodné a syntetické zeolity – Súčasný stav poznatkov z výskumu a aplikácií na Slovensku, Odb. skupina pre zeolity, SSPCH FCHPT STU, Bratislava, 13.2.2003

[46] Blažej, M.*, Juračšík, M., Annus, J., Markoš, J.: Klasická sulfitová, dynamická a dynamická tlaková metóda a ich použitie na meranie kℓa v airlift reaktore s vnútornou cirkuláciou. Classic sulphite, dynamic and dynamic pressure methods for the calculation of kℓa in an airlift reactor with internal circulation. Zborník 50. konferencie CHISA, ISBN 80-86059-36-7, 20 – 23 október, 2003, Srní, Česká republika, prednáška

[47] Bobok, D., Besedová, E.: Efektívne difúzne koeficienty vody a heptánu v časticiach molekulového sita 4A a 5A Effective diffusion coefficients of water and n-heptane in particles of 4A and 5A molecular sieves Odborný seminár Prírodné a syntetické zeolity – Súčasný stav poznatkov z výskumu a aplikácií na Slovensku, Odb. skupina pre zeolity, SSPCH FCHPT STU, Bratislava, 13.2.2003

[48] Holíková, K. (*), Markoš, J., Jelemenský, Ľ.: Matematický model horenia častice uhlia pri nízkych teplotách A mathematical model of single coal particle combustion under low temperatures. Zborník 50. konferencie CHISA, ISBN 80-86059-36-7, 20 – 23 október, 2003, Srní, Česká republika, prednáška

[49] Jelemenský, Ľ., Krajčiová, M. (*), Kiša, M., Markoš, J.: Modelovanie prevencie samovznietenie uhlia Modelling of the self-combustion of coal Zborník 50. konferencie CHISA, ISBN 80-86059-36-7, 20 – 23 október, 2003, Srní,


54

Česká republika, prednáška [50] Kiša, M. (*), Mierka, O.,Jr., Jelemenský, Ľ., Stopka, J.: Počítačový model pre simuláciu havarijných únikov

nebezpečných látok. A computer model for simulation of relase of dangerous substances duting accidents Zborník 50. konferencie CHISA, ISBN 80-86059-36-7, 20 – 23 október, 2003, Srní, Česká republika, prednáška

[51] Mierka, O. (*), Timár, P., Stopka, J., Jelemenský, Ľ., Mošať, A., Mierka, O., Jr.: Rozšírenie kogeneračnej jednotky na trigeneračnú výrobu energetických médií. Transformation of a cogeneration unit into a trigeneration unit in the production of energy media. Zborník 50. konferencie CHISA, ISBN 80-86059-36-7, 20 – 23 október, 2003, Srní, Česká republika, prednáška

[52] Mierka, O., Jr. (*), Stopka, J.: Využitie metódy konečných prvkov pri vulkanizácii. Application of the finite element method for vulcanization. Zborník 50. konferencie CHISA, ISBN 80-86059-36-7, 20 – 23 október, 2003, Srní, Česká republika, prednáška

[53] Molnár, A. (*), Markoš, J., Jelemenský, Ľ.: Využitie simulačných programov na bezpečnostnú analýzu reaktorov. Application of simulation programs for the safety analysis of reactors. Zborník 50. konferencie CHISA, ISBN 80-86059-36-7, 20 – 23 október, 2003, Srní, Česká republika, prednáška

[54] Ačai, P.*, Štefuca, V., Illeová, V.: Experimental and mathematical modeling of FIA in enzyme flow calorimeter. In: Proc. 30th Int. Conf. Slovak Soc. Chem. Eng., Tatranské Matliare (Slovakia), May 26-30, 2003, Ed. Markoš, J., Štefuca, V., Slovak Society of Chemical Engineering, pp. 156. ISBN 80-227-1889-0. (Po)

[55] Malík, F.*, Štefuca, V., Báleš, V.: Investigation of kinetics of immobilized liver esterase by flow calorimetry. In: Proc. 6th Int. Symp. on Biocatalysis and Biotransformations , Olomouc (Czech Republic), June 28 - July 3, 2003, Ed. Barek, J., Bělohlav, Z., et al., Czech Chemical Society, P226,Chem. Listy, 97, 363-520 (2003), (Po)

[56] Marták, J., Š. Schlosser: New formulations of liquid membranes and solvents based on ionic liquids. Proc. PERMEA 2003, abstract of poster, Tatranské Matliare (SK), Sept. 7-11 2003, 118

[57] Mierka, O. (*), Jr., Stopka, J., Molnár, A.: Calculation of the temperature for exothermic reactions in case of a breakdown cooling. In: Proceedings of the 30th Conference of SSCHE, (Book of Abstracts), May 2003, Tatranské Matliare, SK, ISBN 80-227-1889-0, poster

[58] Polakovič, M.*, Bryjak, J., Mucha, T.: Kinetics of thermal and pH inactivation of alpha-amylase. In: Proc. 30th Int. Conf. Slovak Soc. Chem. Eng., Tatranské Matliare (Slovakia), May 26-30, 2003, Ed. Markoš, J., Štefuca, V., Slovak Society of Chemical Engineering, pp. 148. ISBN 80-227-1889-0. (Po)

[59] Polakovič, M.*, Gorner, T., Villiéras, F., Bersillon, J. L., de Donato, F.: Equilibrium and kinetics of salicylic acid adsorption on activated carbon using frontal analysis measurements in an HPLC micro-column. In: Proc. 30th Int. Conf. Slovak Soc. Chem. Eng., Tatranské Matliare (Slovakia), May 26-30, 2003, Ed. Markoš, J., Štefuca, V., Slovak Society of Chemical Engineering, pp. 102. ISBN 80-227-1889-0. (Po)

[60] Stopka, J., Š. Schlosser: Fouling phenomena in microfiltration of beer, solutions of model foulants and beer yeast suspensions Proc. PERMEA 2003, abstract of poster, Tatranské Matliare (SK), Sept. 7-11 2003, 183

[61] Šefčíková, M., Šefčík J., Šefčík J.: Character of spatial enzyme hydrolytic activity at treating od casein micelles. In: Proc. 30th Int. Conf. Slovak Soc. Chem. Eng., Tatranské Matliare (Slovakia), May 26-30, 2003, Ed. Markoš, J., Štefuca, V., Slovak Society of Chemical Engineering, pp. 102. ISBN 80-227-1889-0. (Po)

[62] Vajda, M., I. Havalda, R. Máček : Membrane Based Solvent Extraction and Stripping of Zinc in a HF Contactor Operating in a Circulating Mode. Proc. PERMEA 2003, abstract of poster, Tatranské Matliare (SK), Sept. 7-11 2003, 115

[63] Znad, H., Dolgoš, O., Blažej, M., Báleš, V.*, Markoš, J: A kinetics model for gluconic acid production by Aspergillus niger. In: Proc. 4th European Congress of Chem. Eng., Granada (Spain), September 21-25, 2003, P-11.1-023.

[64] Kiša, M.(*), Mierka, O., Jr., Jelemenský, Ľ., Stopka, J.: Simple mathematical model for hazardous substances release into air. In: Proceedings of the 30th Conference of SSCHE, (Book of Abstracts), May 2003, Tatranské Matliare, SK, ISBN 80-227-1889-0, lecture

[65] Fabíny, R., Markoš, J.(*), Blažej, M.: Modelovanie airlift bioreaktora – produkcia kyseliny glukónovej v nerastových podmienkach. Modelling of an airlift reactor - production of gluconic acid undre non-growing conditions. Zborník abstraktov z 50. konferencie CHISA 2003, ISBN 80-86059-36-7, 20 – 23 október, 2003, Srní, Česká republika, poster

[66] Blažej, M.*, Annus, J., Markoš, J.: The use of the dynamic pressure-step method for kLa measurement in the airlift reactor in coalescent and non-coalescent media. VII Polish Conference on Multiphase Flow, October 7 – 9, 2003, Gdansk, Poland, lecture

C. Books and Textbooks [1] Báleš, V., Mészáros, A., Muntean, O., Polakovič, M., Štefuca, V.: Biochemické technológie. Biochemical

Technologies. AB-ART, Bratislava. 128 s. (2003) ISBN: 80-89006-75-2. [2] Báleš, V.: Biotechnológia immobilizovaných buniek Biotechnology of immobilised cells In: BIOPRECESS

ENGINEERING:doctoral/post-doctoral level course, Supetar, Island of Brač (Croatia), September 7-13, 2003, ed. Berovič, M., Kieran, P.,Ljubljana, Faculta of Chemistry and Chemical Technology, p.185-201, ISBN 961-6286-54-4

[3] Schlosser, Š. (red.) Membrane Science and Technology in Visegrad and Other Countries Membrane Science and Technology in Visegrad and Other Countries SSCHI, 120 p.

[4] Schlosser, Š., R. Kertész (red.) PERMEA 2003 SSCHI, 200 p. + CD ROM, 2003 E. Others: [1] Kiša, M. Matematické modelovanie následkov havarijných únikov nebezpečných látok Mathematical modelling of

the consequences of release of dangerous substances during accidents Projekt dizertačnej práce, KCHBI FCHPT STU, Bratislava, 2003

[2] Molnár, A.: Program tool for safety analysis of a chemical reactor, PhD Thesis KCHBI FCHPT STU, Bratislava, 2003

[3] Molnár, A.: Safety analysis of a chemical reactor. DSM, Geleen, Limburg, Holandsko, september 2003, invited


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lecture [4] Molnár, A.: Safety analysis of a chemical reactor. University Gent, Faculteit Toegepaste Wetenschappen,

Chemische Proceskunde en Technische Chemie, Laboratorium voor Petrochemische Techniek, Belgicko, august 2003, invited lecture

DEPARTMENT OF CHEMICAL PHYSICS

56


Head of Department: Telephone: ++421252963420 Assoc. Prof. Viliam Laurinc, PhD Fax: ++421252493198


I. STAFF Full Professors: Fedor Valach, PhD, DSc Associate Professors: Pavol Fedorko, PhD; Oľga Holá, PhD; Viliam Laurinc, PhD; Peter Lukáč, PhD; Teodor Obert, PhD (part-time) Assistant Professors : Július Annus; Ladislav Bušovský; Eva Griačová (part-time); Vladimír Lukeš, PhD; Tibor Pálszegi, PhD; Ľubomír Tancer; Miroslav Tokarčík, PhD; Daniela Žilinská Research Fellows: PhD Students: Technical staff: Anton Adamko; Marián Babnič; Zdenka Halaburková


A. Teaching laboratories: Laboratory of Physics I. Laboratory of Physics II.

B. Research laboratories: Laboratory of X-ray Diffraction Laboratory of Electrical Properties of Conducting Polymers Laboratory of Gamma Radiation Source

III. TEACHING

A. Undergraduate Study: 1. semester (Bc) Seminar in Basic Physics 0/2/0 Bušovský, Fedorko, Holá, Lukáč,

Tancer, Žilinská 2. semester (Bc) Physics I 2/2/0 Bušovský, Holá, Laurinc, Lukáč,

Lukeš, Tokarčík, Valach Physics Laboratory I. 0/0/2 Annus, Bušovský, Pálszegi, Tancer,

Žilinská 3. semester (Bc) Physics II. 2/2/0 Fedorko, Laurinc, Lukáč, Lukeš,

Tokarčík, Valach Physics Laboratory II. 0/0/2 Annus, Bušovský, Pálszegi, Tancer,

Žilinská Physics I. 2/2/0 Holá, Bušovský 1. semester (MSc) Semestral project 0/0/4 Lukeš Modelling of the Molecular Properties 2/2/0 Laurinc, Lukeš 2. semester (MSc) Statistical Thermodynamics 2/1/0 Laurinc, Lukeš


A. VEGA Project No 1/0056/03 Interaction geometry of transition element atom with ligands in coordination compounds and metalloproteins (Fedor Valach)

A new bond valence sum model of interactions between the metal atom of dn and fn electron configurations and ligands in the crystal structures of coordination compounds and metalloproteins. Development of structural theory which enables the prediction of transition metal surrounding geometry within the range of metal oxidation states. Deriving the rules for the occupation of the crystal sites by the transition element atoms in the certain oxidation states of metalloproteins.


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Development of new refinement and validation procedure for the crystal structures of metalloproteins. Crystal structure refinement of Urtica dioica aglutinin isolectin I with Zn+2 ions. Prediction of murine monoclonal antibody 1696 complexation with transition metals.

Project duration: from 01.01.2003 to 31.12.2005 B. VEGA Project No 1/0055/03 Theoretical and experimental study of the electrical and

optical properties of new pi-conjugated aromatic and heteroaromatic compounds as precursors for the preparation of oligomers and nanostructures (Viliam Laurinc)

Quantum-chemical study of the electronic structure and properties of benzenoid and heterocyclic compounds of furan, thiophene, pyrrole, imidazole and pyrazine derivatives with potential electro- and photoactive properties. Theoretical investigation of the basic relations between structure (conformations, effective conjugation length, effect of substitutents) and microscopic quantities (dipole moments, polarizabilities, hyperpolarizibilies, HOMO-LUMO separation), and absorption and luminescence spectral characteristics. Measurements of the electrical conductivity of the prepared polymerised pi-conjugated structures. Study of the stability of the prepared compounds under gamma-irradiation (source 60Co)



A. KEGA Project No 3/108003 Interactive Multimedial Project for Teaching of Physics at Technical Universities in Slovak Republic (Viliam Laurinc, Oľga Holá)

Development of teaching methods on physics lectures at technical university, particularly at the Faculty of Chemical and Food Technology of SUT.


B. Institutional Project No. 302/03 The creation of new didactic methods in teaching of physics with applications in e-learning and distance learning (Oľga Holá)

The cooperation at the creation of the multimedia textbook of physics.


VI. COOPERATION



Duration

Faculty of Electrical Engineering and Information Technology, SUT Bratislava

e-learning Assoc.prof. P.Ballo, PhD 2000-

Faculty of Mathematics and Physics, Commenius University, Bratislava

Monitoring of Rn in atmosphere, water and soil Assoc.prof. K. Holý, PhD 1990-

Faculty of Civil Engineering, SUT Bratislava

Didactic methods Assoc.prof. J.Lukovičová, PhD 2000-

Institute of Polymers, Slovak Academy of Sciences, Bratislava

Optical measurements of polymers Prof. P.Hrdlovič, DSc 2000-

Faculty of Natural Science, Commenius University, Bratislava

Simulations of linear and nonlinear optical signals Dr. V.Szöcs, PhD 2000-

Faculty of Mathematics and Physics, Commenius University, Bratislava

e-learning Mgr. K.Holá 2003-



Duration


58

Institut für Organische Chemie, J.W.Goethe Universität, Frankfurt/M., Germany

X-ray crystallographic research Prof. E.Egert 1988-

Institute of Molecular Genetics, Academy of Sciences, Prague, Czech Republic

Protein synthesis Ing. J.Sedláček 2003-

Institut für Physikalische Chemie, Universität Wien, Vienna, Austria

Electronic excitation transport in polymers Prof. H.F.Kauffmann 1997-

Institute of Chemistry, University of Wroclaw, Wroclaw, Poland

X-ray crystallographic research Dr. R.Grobelny 1989-

Laboratorie de Cristallographie, Université de Genéve, Switzerland

X-ray crystallographic research Prof. A.F.Williams 2001-

Chemical Crystallography Laboratory, Oxford University, Oxford, UK

X-ray crystallographic research at low temperatures, crystallographic statistics Prof. C.K.Prout 1999-

Commissariat a l'Energie Atomique, Grenoble, France

Conducting polymers Dr. J.P.Travers 1999-

Institute of Macromolecular Chemistry, Academy of Sciences, Prague, Czech Republic

Conducting polymers Dr. J.Stejskal 2003-

Max-Planck Institut für Festkörperphysik, Stuttgart, Germany

Carbon nanotubes Dr. S.Roth 2000-



Valid date

Holá Oľga Union of Slovak Mathematicians and Physicists, Bratislava member 1970

Laurinc Viliam Union of Slovak Mathematicians and Physicists, Bratislava member 1975

Bušovský Ladislav

Union of Slovak Mathematicians and Physicists, Bratislava member 1975

Fedorko Pavol Union of Slovak Mathematicians and Physicists, Bratislava member 1977

Holá Oľga Slovak Physical Society, Bratislava member 1993 Laurinc Viliam Slovak Physical Society, Bratislava member 1993 Valach Fedor Slovak Physical Society, Bratislava member 1993 Bušovský Ladislav Slovak Physical Society, Bratislava member 1993

Fedorko Pavol Slovak Physical Society, Bratislava member 1993 Lukáč Peter Slovak Physical Society, Bratislava member 1993 Valach Fedor Slovak Chemical Society, Bratislava member 1970



Valid date

Valach Fedor International Society for Theoretical Chemical Physics, Erlangen, Germany member 1990


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Laurinc Viliam International Society for Theoretical Chemical Physics, Erlangen, Germany member 1990

Fedorko Pavol European Physical Society member 1994 Valach Fedor European Physical Society member 1994 Holá Oľga European Physical Society member 1994



Date / Duration

Grobelny, R. Institut of Chemistry, University of Wroclaw Poland August 2003 (5 days) F. Visits of Staff Members and Postgraduate Students in Foreign Institutions


Date / Duration

Fedorko, P. Departement de Recherche Fondamentale sur la Matiere Condensee, Commissariat a l'Energie Atomique, Grenoble

France Febr-May 2003 (90 days)



Lukeš, V. The application of diagramatic many body theories for the study of weak intermolecular interactions Kvasnička, V.

F. Inauguration Theses


[1] Fedorko P., Djurado D., Trznadel M., Dufour B., Rannou P., Travers J. P.: Insulator-metal transition in polyaniline induced by plasticizers. Synt. Metals 135-136, 327-328, (2003).

[2] Lukeš, V., Bittererová M., Biskupič S., Laurinc V.: Nature of interaction energy anisotropy in Li-HF van der Waals complex. The theoretical study. Theor. Chem. Acc. 109, 316-325 (2003).

[3] Lukeš, V., Breza, M., Végh, D., Hrdlovič P., Laurinc V.: Optical properties of furanic and thiophenic ethane-1,2-diones. A combined experimental and theoretical study. Synt. Met. 138, 399-408 (2003).

[4] Lukeš, V., Ilčin M., Laurinc V., Biskupič S.: On the structure and physical origin of weak interaction between H and CO2. Chem. Phys. 290, 93-100 (2003).

[5] Lukeš, V., Laurinc V., Ilčin M., Biskupič S.: Ab initio study of the Li-CO van der Waals complex. Czech. Coll. Chem. Commun. 68, 35-46 (2003).

[6] Pépin-Donat, B., Viallat A., Blachot J. F., Fedorko P., Lombard C.: Swelling, elasticity and transport properties of conjugated covalent electronic conducting gels: role of network structure. Synt. Metals 137, 897-898, (2003).

[7] Valach, F., Saunders A., Cowley A., Watkin, D. J.: Crystal structure of bis(2-chloro-6-fluorobenzoato)bis(pyridine)copper(II), Cu(C7H3ClFO2)2(C5NH5)2. Z. Kristallogr. NCS 218, 31-32 (2003).

[8] Williams, C. J., Morris H., Svorec J., Valková M., Valko M., Moncol J., Mazur M., Valach F., Melník M.: A study of copper(II) carboxylato complexes with the biological ligands nicotinamide and papaverine. J. Molecular Struct. 659, 53-60 (2003).

[9] Blažej, M., Annus, J., Markoš, J.: The use of the dynamic pressure-step method for kLa measurement in the airlift reactor in coalescent and non-coalescent media. Inzynieria i Aparatura Chemiczna 42, 24-26, (2003).

[10] Blažej, M.*, Annus, J., Markoš, J.: Using of the dynamic pressure-step method for mass transfer coefficient measurement in the internal loop airlift reactor. Chemical Papers 57, 445-450, (2003).

[11] Lukáč, P., Foldesová M.: Imobilizácia niektorých rádionuklidov zeolitmi a ich solidifikácia špeciálnou cementovou zmesou. Immobilisation of some radionuclides by zeolite and their solidification with special cement sluriess. Ropa, uhlie, plyn a petrochémia.45(1-2), 64-67 (2003).

[12] Lukeš, V., Cibulková Z., Vlčková S.: On the structural effects of the Head-to-Tail Coupled oligo (3-alkyloligothiophenes) on their optical properties. Petroleum and Coal 1-2, 45-48 (2003).

[13] Lukeš, V., Ilčin M., Laurinc V.: On the structure and physical origin of interaction between lithium and CO2. Petroleum and Coal 44, 153-159 (2003).

[14] Rapta, P, Lukeš, V., Matuszná K., Végh, D.: Experimental and theoretical study of optical and electrochemical properties of novel alkyl substituted 2,3-diaza-1,3-butadiene bithienyls. Petroleum and Coal 1-2, 63-68 (2003).

B. Conferences [1] Svetíková, M., Annus J., Čirka Ľ., Fikar M.: Real time control of a laboratory fan heater using dspace tools. In: 14th

Int. Conference Process Control 2003. Štrbské Pleso, (Slovakia), June 8-11, 2003. Ed.: pp. 211-1 - 211-4,


60

[2] Valach, F.*: New developments in bond-valence sum model of solids. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 863 (2003). (PPr).

[3] Holý, K.*, Bosá, I., Polášková, A., Böhm, R., Holá, O., Ondo-Eštok, D.: Ten years of continual mmonitoring of 222Rn concentration in Bratislava atmosphere. In: Proceedings of IRPA Regional Congress on Radiation Protection in Central Europe. The IRPA Regional Congress on Radiation Protection in Neighbouring Countries of Central Europe 2003. Bratislava (Slovakia), Sept. 22-26, 2003. V._3, 7 pages (2003). CD medium. ISBN 80-88806-43-7.

[4] Ondo-Eštok, D., Holý K., Stanys T., Polášková A., Holá O.: Behaviour of 222Rn and its daughter products in open atmosphere. In: Proceedings of IRPA Regional Congress on Radiation Protection in Central Europe. The IRPA Regional Congress on Radiation Protection in Neighbouring Countries of Central Europe 2003. Bratislava (Slovakia), Sept. 22-26, 2003. V._P6, 5 pages (2003), CD medium. ISBN 80-88806-43-7.

[5] Valach, F.*, Hoang N. N., Maris T., Saunders A., Cowley A., Watkin D.J., Prout C.K.: New trends in bond-valence sum model of coordination compounds. In: Progress in Coordination and Bioinorganic Chemistry, Monograph Series of the Int. Conf. on Coordination Chemistry held periodically at Smolenice in Slovakia, Ed.: M. Melník, A. Sirota, Slovak Technical University Press - Bratislava, Smolenice, pp. 45-50 (2003). ISBN 80-227-1891-2. (Pr)

[6] Blažej, M.*, Annus, J., Markoš, J.: Application of the dynamic pressure -step method for mass transfer coefficient measurement in airlift reactor with internal loop. In: Proceedings of the 4th European Congress of Chemical Engineering, Granada (Spain), Sept. 24-25, 2003. ISBN 84-88233-35-3. (Po).

[7] Čerňanský, A., Halama L., Holická Z., Žatkulák M., Annus J.: Microfiltration of Radioactive Sludge in a Long-Term Storage Pool. In: Proceedings 7th Int. Scientific Conf.: Mechanical Engineering 2003. Bratislava, (Slovak Republic), Nov. 5-6, 2003, Ed.: Publishing House of STU Bratislava, p.16 (2003), CD medium. ISBN 80-227-1960-9.

[8] Čerňanský, A., Taraba J., Holická Z., Žatkulák M., Annus J., Brokeš P.: Filtration Characteristics of Low Radioactivity Sludge. In: Proceedings 30th Int. Conf. of Slovak Society of Chemical Engineering. Tatranské Matliare (Slovakia), May 26-30, 2003. Ed.: J. Markoš and V. Štefuca. Slovak University of Technology, Bratislava. p.65 (2003), CD medium. ISBN 80-227-1889-0.

[9] Lukeš, V., Laurinc V.*, Pálszegi T.: Štúdium elektro-optických vlastností derivátov tiofénu. The study of the electro-optical properties of tiophene based derivatives. In: Zborník príspevkov 13. konferencie slovenských fyzikov, Smolenice (Slovakia), 25.-28. august 2003, Ed.: Edičné stredisko Vojenskej leteckej akadémie Košice, pp.141-142 (2003). ISBN 80-969071-8-2. (Po)

[10] Fedorko* P., Trznadel M., Pron A., Djurado D., Travers J. P.: Vodivé polyméry: prechod izolant-kov v polyanilíne. Conducting polymers: insulator-metal transition in polyaniline. In: Zborník príspevkov 13. konferencie slovenských fyzikov, 25.-28. August. 2003, Smolenice, Ed.: M. Reiffers, Edičné stredisko Vojenskej leteckej akadémie Košice, pp. 95-96, (2003). ISBN 80-969071-8-2. (Pr).

[11] Holá O.*, Holá K.: Nové didaktické postupy a prostriedky pri výučbe fyziky na vysokej škole. New didactic methods and tools in physics teaching at technical university. In: Zborník z medzinárodnej vedeckej konferencie Výskum a vyučovanie na katedrách fyziky v kontexte univerzitného vzdelávania, Nitra, jún 2003.Ed.:SPU Nitra, p.59-62 (2003). ISBN 80-8069-201-7.

[12] Laurinc V.*, Holá O.: Fyzika v novej štruktúre štúdia na FCHPT STU. Physics in the new structure of study at FCHPT STU. In: Zborník. z medzinárodnej vedeckej konferencie Výskum a vyučovanie na katedrách fyziky v kontexte univerzitného vzdelávania. Nitra (Slovakia), Jún 2003. Ed.: SPU Nitra, p.163-167 (2003), ISBN 80-8069-201-7. (Pr)

[13] Lukeš, V., Laurinc V.*, Ilčin M.: Medzimolekulové interakcie v systéme Li-C2H2. Intermolecular interactions in systems Li-C2H2. In: Zborník príspevkov 13. konferencie slovenských fyzikov, Smolenice (Slovakia), 25.-28. august 2003. Ed.: Edičné stredisko Vojenskej leteckej akadémie Košice, pp. 97-98 (2003). ISBN 80-969071-8-2. (Pr)

[14] Foldesová, M.*, Dillinger P., Lukáč, P., Svetík, Š.: Vplyv kalcinácie a chemickej modifikácie na štruktúru prírodných zeolitov. The influence of calcination and chemical modification on the structure of natural zeolites. In: Proc. 16. Int. Conf. Termanal 2003, Stará Lesná (Slovakia), Oct. 8-10, 2003. PO-06 (2003). ISBN 80-227-1955-2. (Po).

[15] Lukáč, P., Foldesová M., Dillinger P., Svetík Š.: Zmeny sorpčných vlastností prírodných a chemicky modifikovaných zeolitov spôsobené teplotou a vysokoenergetickým žiarením. Changes of sorption properties of natural and chemical treated zeolites due to temperature and gamma radiation. In: Proc. 16.Int. Conf. Termanal 2003, Stará Lesná (Slovakia), Oct. 8-10, 2003. PO-11 (2003). ISBN 80-227-1955-2. (Po).

[16] Blažej, M.*, Juračšík, M., Annus, J., Markoš, J.: Klasická sulfitová, dynamická a dynamická tlaková metóda a ich použitie na meranie kLa v airlift reaktore s vnútornou cirkuláciou. The sulphite, dynamic and dynamic pressure-step method and their use in kLa measurement in airlift reactor with internal loop. In: Zborník 50. konferencie CHISA, Srní, (Czech republic), 20.-23. október 2003, ISBN 80-86059-36-7. (Pr).

[17] Fedorko P., Djurado D., Payerne R., Dufour B., Pron A., Rannou P., Trznadel M., Travers J. P.: Transition isolant-métal dans la polyaniline induite par des plastifiants. Insulator-metal transition in polyaniline induced by plasticizers. In: 10èmes Journées Polymères Conducteurs - JPC 03, Dourdan (France), Sept. 15-19, 2003, Ed. A. J. Attias et al., pp. A4-A24, (2003). (Po).

[18] Végh, D., Lukeš, V., Végh Z., Pálszegi T.: Organic conductors based on 2,5-diamino-3,4-dicyanothiophene and diaminomaleonitrile. In: 10th Blue Danube Symposium on Heterocyclic Chemistry, Sept.3-6, 2003, Vienna (Austria), Ed.: STU Press, Bratislava. PO-197, (2003), ISBN 80-227-1938-2. (Po).

[19] Foldesová, M.*, Dillinger, P., Lukáč, P.: Štúdium sorpčných vlastností prírodných ionexov rádioindikátorovou metódou. The study of sorption properties of natural zeolites by radioindicatore method. In: Zborník odborného seminára Prírodné a syntetické zeolity - súčasný stav poznatkov z výskumu a aplikácií na Slovensku. CD medium. FChPT STU Bratislava, 13.febr.2003. (Po).

[20] Laurinc V., Lukeš, V., Ilčin M., Biskupič S.: The weak interaction in vdw complex H2...Cl(-).Central Europe Symposium of Theretical Chemistry, Nové Hrady (Czech Republic), 25-28 Sept. 2003. (Po).


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[21] Blažej, M.*, Annus, J., Markoš, J.: The use of the dynamic pressure-step method for kLa measurement in the airlift reactor in coalescent and non-coalescent media. VII. Polish Conference on Multiphase Flow, Gdansk (Poland), .Oct. 7-9, 2003. (Pr).

[22] Lukeš, V.*, Laurinc V., Ilčin M., Biskupič S.: The weak interaction in vdw complex Li...C2H2. Central Europe Symposium of Theretical Chemistry, Nové Hrady (Czech Republic), 25-28 Sept. 2003. (Pr).

C. Books and Textbooks [1] Ožvoldová M., Kvetan K., Štubňa I., Krajčovič J., Dillinger J., Halusková S., Laurinc V., Holá O., Fedorko P., Ballo

P., Červeň I: Fyzika online 2. Recenzovaná internetová učebnica pre dištančné vzdelávanie z fyziky v rámci STU. 2002-2003. Physics online 2. In: www.kf.sjf.stuba.sk, http://kf-lin.elf.stuba.sk/~ballo/fyzika_online. +CD medium.

E. Others [1] Holý K., Chudý M., Šivo A., Sýkora I., Ondo-Eštok D., Holá O., Polášková A., Richtáriková M., Merešová J., Šulc

M., Haško J.: Stanovenie predprevádzkových objemových aktivít rádionuklidov v prízemnej vrstve atmosféry a vo vodách v lokalite výstavby Cyklotrónového centra Slovenskej republiky (2.časť). The determination of preservice volume activities of radionuclides in the surface layer of the atmosphere and in waters in the locality of the Cyclotron Centre of Slovak Republik. (Part II). Oponovaná výskumná správa. KJF FMFI UK – 137/03 Bratislava, (35 str.+16 str.príloh), Január 2003, GU SAV Bratislava.

DEPARTMENT OF CHEMICAL TECHNOLOGY OF WOOD, PULP AND PAPER

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Head of Department: Telephone: ++421 2 52496359 Assoc. Prof. Svetozár Katuščák, PhD Fax: ++421 2 52493198


I. STAFF Associate Professors: Svetozár Katuščák, PhD; Pavol Krkoška, PhD Assistant Professors : Vlasta Lužáková, PhD; Pavel Mišovec, PhD; Štefan Šutý, PhD; Katarína Vizárová, PhD Research Fellows: Igor Šurina, PhD; Radovan Tiňo; Milan Vrška, PhD PhD Students: Michal Jablonský; Gabriela Szeiffová, Martina Cedzová Technical staff: Valeria Töröková, Pavol Vančo


A. Teaching laboratories: Laboratory of Chemical Treatment of Wood Laboratory of Pulping Technology Laboratory of Structure and Properties of Paper Laboratory of Wood Chemistry

B. Research laboratories: Laboratory of Natural Polymers Laboratory of Papermaking Fibres and Additives Laboratory of Structure and Analysis of Wood GC-MS Laboratory

III. TEACHING

A. Undergraduate Study: 6. semester (Bc) Semestral Project 0/4 members of department Paper and Printing 2/2 Krkoška, Panák 1. semester (MSc) Physics of Polymers and Paper 2/2 Krištofič, Šutý, Cifra Natural Polymers 2/1 Lužáková Chemistry and Analysis of Wood 2 Katuščák, Vizárová Pulping Technology 3/1 Vrška, Šutý 1. semester (MSc) Laboratory I. 8 Vizárová Environmental Management in Pulp

and Paper Industry 2 Vizárová, Katuščák

2. semester (MSc) Paper Machines 2/2 Čerňanský Engineering of Pulp Production 1/1 Vrška Paper Technology I. 3/0 Krkoška, Gigac, Šutý Chemical Treatment of Wood I. 3/0 Šurina 2. semester (MSc) Laboratory II. 8 Mišovec, Šurina, Vrška Practical Training Course 3 weeks 3. semester (MSc) Chemical Treatment of Wood

II. 2/0 Katuščák

Paper Technology II. 3/0 Krkoška, Gigac, Šutý Packaging Materials 2/0 Mišovec Papermaking aids 2/0 Lužáková, Vizárová 3. semester (MSc) Laboratory III. 9 Vrška, Šurina, Mišovec, Šutý Thesis 30 members of department


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A. VEGA Poject No 1/0061/03 Study of the oxidation in chemical processing of wood through new methods of separation and analysis (Svetozár Katuščák).

The elimination of chlorine in bleaching processes and its substitution by hydrogen peroxide, various peroxidic compounds in combination with oxygen, ozone and alkali extraction were studied. The most perspective oxidation agents studied in this project next to oxygen, ozone and hydrogen peroxide are peroxomonosulfuric acid and peracetic acid. Very good results for delignification efficiency, brightness and strength properties of pulp were obtained with combination two stage oxygen delignification and next ozone stage.The reaction products were identified by electroforetic analysis, HPLC and FTIR methods.

Project duration: from 01. 01. 2003 to 31. 12. 2005

B. VEGA Project No 1/8100/01 Interactions of nonprocess components under pulping conditions (Vlasta Lužáková).

An analytical procedure convenient for the isolation, fractionation and identification of wood extractive lipophilics as a significant pitch formation precursor in pulping and papermaking has been developed. The solvent extractions, SPE as well as GC-MS have been employed for this purpose. The procedure enables to follow interactions of the lipophilics and pitch control agents in pulp fibre suspensions. An original set of the three pitch formation precursors originated from wood has been formulated. The twelve dominant domestic woods pulped in Slovakia have been analysed from this aspect. The knowledge obtained enables the technological pitch problem decreasing by exclusion of problematic woods from industrial treatment or by convenient mixture of treated woods.


C. VEGA Project No 2/3161/23 Methodology of preparation of new cyclodextrin derivatives with ion-exchanging groups (Igor Šurina).

New derivatives of b-cyclodextrin are prepared by selective introduction of ion-exchanging groups. The point of the project was the preparation of mono-derivatives through tosylation, subsequently modified with quaternary ammonium group. From the epoxy-compound amino-derivative are prepared and quaternized. The prepared mono-derivatives with specifically bonded quaternary ammonium groups are modified with carboxymethyl groups. The derivatives are tested as stationary phases for gas chromatography.


D. APVT Project No 99-007302 Coated ink jet papers (Štefan Šutý). The project is realized in cooperation with Pulp and Paper Research Institute in Bratislava. Project research is focused on coated ink jet papers, which as a new generation of paper industry specialties with excellent properties are characterised by high added value. The impact of the physicochemical and structural properties on the interaction between ink and coating are studied. Laboratory research of surface finish and coating of base paper will be done by means of laboratory size press, coater and supercalender. The methods on the coating base paper properties evaluation, coating composition and its components as well as ink jet paper quality will be worked out.


E. Project No 2003 SP 260280C03 Production of new pulp and paper products from wood of lower quality - Effect of fibrous web structure and fibre properties on transfer and qualitative parameters of paper (Štefan Šutý).

The project is realized in cooperation with Pulp and Paper Research Institute in Bratislava. The research in this project is focused on the description of transfer and quality parameters of the paper and board using the physical and mechanical characterization of fibres and structural elements of fibre web. The transfer parameters are initial strength and dewatering of wet paper web. The structure of fibre web will be described by anisotrophy of paper, orientation of the fibres,internal strength of the paper, its porosity, distribution of the pores and formations of the paper. The covalence and bending stiffness together with structural components will be used for the prediction of tensile parameters of the materials for corrugated boards.It is being assumed using of research results in development of graphic papers with high ratio of hardwood pulp, magazine papers e.t.c.


F. Project No 2003 č. 661/2003 Preservation, Stabilization and Conservation of Traditional Information Supports in the Slovak Republic (Svetozár Katuščák)

This project covers program of saving, stabilization and conservation of traditional holders of information (books, archival documents etc.). Big portion of cultural heritage stored in historical books and archival documents is endangered with


64

destructive impacts of abiotic and biotic factors. This can cause irretrievable loss of cultural heritage of Slovak Republic. Solving of this problem is divided into two time steps. First includes years 2003 - 2005 and its subject covers basic research. Except of this, second step will also include applied research and development.

Project duration: from 01.10. 2003 to 31.10. 2005


VI. COOPERATION



Duration

Neusiedler SCP a.s. Ružomberok

Lipophilic wood extractives, anionic trash and pitch particles and their interaction with controll additives.

Ján Tomčík, head of CELPAP Division, Neusiedler SCP a.s. Bystrická cesta 13, 03417 Ružomberok

01. 06. 1998 -

Faculty of Natural Science, Comenius University, Bratislava

Determination of by-products of oxidation processes

Kaniansky Dušan, Prof., Mlynská dolina, 842 15 Bratislava

01.01.2003 -


Specialized education "Basic course From Wood to Paper"

Jakubík Peter, manager, Bystrická cesta 13, 034 17 Ružomberok

01. 03. - 30. 06. 2003


Specialized education "Basic course From Wood to Paper"

Jakubík Peter, manager, Bystrická cesta 13, 034 17 Ružomberok

01. 12. 2003 - 30. 06. 2004

Institute of Chemistry of Slovak Academy of Sciences, Bratislava

GC - MS analysis of derivatives of cyclodextrin

Šimkovic Ivan, project manager, Dúbravská cesta 9, 845 38 Bratislava

01. 01. 2003 -

Slovak National Library, Martin

Preservation of archived books and documents

Bukovský Vladimír, manager, SNK Martin

5.5.2002-

Pulp and Paper Research Institute, Bratislava

Coated ink-jet papers Boháček Štefan, president of board, VÚPC Bratislava, Lamačská 3

1.7.2002-

Slovak National Archives, Bratislava

Preservation of archived books and documents, education.

Hanus Jozef, manager, SNA Bratislava permanently

Pulp and Paper Research Institute, Bratislava

Surface modification of LC materials and evaluation of VOC emissions

Boháček Štefan, president of board, VÚPC Bratislava, Lamačská 3

01.01.2003-31.12.2003

Technical University, Zvolen Education Sedliačik Ján, TU Zvolen permanently



Duration

Dept. of Chem. Technology of Wood, Pulp and Paper, Technical University, Pardubice, Czech Republic

Education Milichovský Miloslav, Prof. TU Pardubice

French Institute of Papermaking and Graphics Industry, Grenoble, France

Education and Research

Roux, J. C., professor, Ecole Française de Papeterie et des Industries Graphiques, Grenoble, France

1989 -


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Valid date

Vrška Milan Slovak Chemical Society member 01.01.1980 -

Vrška Milan SNAS -acreditation group - for laboratory of PPRI Bratislava member 23.09.2002 -

Vrška Milan SUTN -Technical normalization commitee - TC 19 - pulp, paper, board member 26.05.2003 -

Katuščák Svetozár

SUTN -Technical normalization commitee - TC 72 - environmental management member

Krkoška Pavel Slovak Chemical Society member 1979 Katuščák Svetozár Wood Research , editorial board member



Valid date

Šutý Štefan Association of the pulp and paper industry, Czech republic (member of EUCEPA) member 01. 01. 2000 -

Šurina Igor Association of the pulp and paper industry, Czech republic (member of EUCEPA) member 01. 01. 1998 -



Date / Duration

Baudin, G. Ecole Française de Papeterie et des Industries Graphiques, Grenoble France September 2003

(3 days)

Roux, J. C. Ecole Française de Papeterie et des Industries Graphiques, Grenoble France September 2003

(3 days)

Chaussy, D. Ecole Française de Papeterie et des Industries Graphiques, Grenoble France September 2003

(3 days)

Alince, B. McGill University, Montréal, Québec Canada September 2003 (3 days)

Pikulik, I. PAPRICAN Canada September 2003 (3 days)

Milichovský, M. University Pardubice Czech Republic


Milichovský, M. University Pardubice Czech Republic May 2003 (1 day)

Paris, J. École Polytechnique Montréal, Quebec Canada September 2003 (3 days)

Bednar, F. École Polytechnique Montréal, Quebec Canada September 2003 (3 days)

Konvička, S. Biocel, Paskov Czech Republic April 2003 (1 day)

Cinciala, J. Biocel, Paskov Čzech Republic April 2003 (1 day)

Koťátko, Z. Biocel, Paskov Czech Republic April 2003 (1 day)



Date / Duration

Tiňo, R. Safe consortium, Brusel Belgia November 2003 (3 days)

Tiňo, R. Conference: Papír – tisk - obaly, Čejkovice Czech Republic


Krkoška, P. Conference: Papír – tisk - obaly, Čejkovice Czech Republic


Šutý, Š. Conference: Papír – tisk - obaly, Čejkovice Czech Republic


Šutý, Š. Meeting APPI, Prague Czech Republic



66

Krkoška, P. Conference of Restorers and Historians, Prag Czech Republic


Vizárová, K. Conference of Restorers and Historians, Prag Čzech Republic


Tiňo, R. Conference: Metso Paper Visegrad, Visegrad Hungary April 2003 (2 days)

Katuščák, S. Meeting BIOMAT, Espoo Finnland January 2003 (2 days)

Vrška, M. Exposition EMBAX PRINT, Brno Czech Republic May 2003 (1 day)

Jablonský, M. Exposition EMBAX PRINT, Brno Czech Republic May 2003 (1 day)

Szeiffová, G. Exposition EMBAX PRINT, Brno Czech Republic May 2003 (1 day)

Tiňo, R. Exposition EMBAX PRINT, Brno Czech Republic May 2003 (1 day)

Barteková, A. Exposition EMBAX PRINT, Brno Czech Republic May 2003 (1 day)

Šutý, Š. Exposition EMBAX PRINT, Brno Czech Republic May 2003 (1 day)

Szeiffová, G. Presentation of faculty on International Students Seminary, Lille France April 2003 (5 days)



ČULÁKOVÁ, Ľ. Determination of fibers age composition in recycled pulp suspension. Krkoška, P. KIRSCHNEROVÁ, S. Paper recycling. Vizárová, K.

VALACHOVÁ, V. Additives for oxygen delignification. Study of possible increase of oxygen delignification. Vrška, M.

PAUČINOVÁ, A. Impact of non-process compounds on the oxygen delignification. Vrška, M.

CÍBIKOVÁ, H. Document and image quality optical properties evaluation of lignocellulosic materials. Katuščák, S.

REPOVÁ, M. Image analysis utilization in lignocellulosic materials evaluation. Tiňo, R.

BREJČÁKOVÁ, E. Fire control and novel methods of fire control evaluation for wood materials. Katuščák, S.


Bohúňová, Z. Effect of polymers addition on paper properties. Mišovec, P. Boldišová, A. Effect of recycling on mechanical and optical paper properties. Mišovec, P.

Cedzová, M. Influence of light prehistory on paper properties during accelerated ageing. Vizárová, K.

Csáky, T. Environmental aspects of pulp bleaching. Vrška, M. Kalmárová, G. Extractives of willow (Salix viminalis). Šurina, I. Marková, D. Reduction of VOC emissions from cellulose composites. Katuščák, S. Pekarovič, P. Environmental friendly bleaching of hardwood kraft pulp. Vrška, M. Pleteníková, M. Archives documents preservation by application of laminating foil. Vizárová, K. Strežo, P. Ink-jet papers printing quality and coating properties. Šutý, Š. Viľčuková, Z. Paper acidity determination. Krkoška, P.


Barteková, A. Katuščák, S. Jablonský, M. Katuščák, S. Szeifová, G. Katuščák, S. Gigac, J.

VII. PUBLICATIONS A. Journals

[1] Alince, B., Tino R.: "Latex deposition on glass-monolayer, multilayer and the effect of ‘free charge’". Colloids and surfaces A: Physicochem. Enf. Aspects 218 (2003) 1-9


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[2] Šimkovic, I., Šurina, I., Vričan, M.: Primary reactions of sucrose thermal degradation. J. ANAL. APPL. PYROL. 70 (2): 493-504 DEC 2003

[3] Lužáková, V., Smrčková, E.: Kvalita vápna a účinnosť kaustifikácie. Lime Quality and Caustification Efficiency. Papír a celulóza 58, (7-8) 216-219 (2003).

[4] Mišovec P., Boldišová A.: Vplyv recyklácie na vlastnosti buničinových vlákien a papiera-akceptované. Influence of recycling on properties of pulp fibers and paper. Papír a celulóza

[5] Šutý, Š.,Tiňo R. Konferencia WPP 2003, aká bola? The conference Wood, Pulp and Paper 2003, what was it like? Papír a celulóza 58, (12) 366-367 (2003).

[6] Vizárová K.,Cedzová M.,Reháková M, Šutý Š. Vplyv svetelnej expozície na zmeny vlastností súčasných papierov v priebehu urýchleného starnutia. The influence light exposition on changes of contemporary papers properties in accelerated ageing. Papír a celulóza 58, (9) 264-266 (2003).

[7] Pikulik, I., Katuščák, S., Baudin G.: Od trvalo obnoviteľných surovinových zdrojov po tlačené dokumenty. From sustainable raw materials to printed documents. Papier a polygrafia, (3) 16-18(2003)

B. Conferences [1] Vizárová, K.*, Reháková, M., Hrehorová, E., Jančovičová, V., Jakubíková, Z.: Preparing and properties of polymer

protective films on the paper substrate. In: Proc. Int. Conference on Chemical Technology of Wood, Pulp and Paper, WPP2003. Bratislava (Slovak Republic), Sept. 17-19, 2003. Ed. by Baudin G., Fellegi J., Gellerstedt G., Katuscak S., Pikulik J., Paris J., pp. 412–416 (2003). ISBN 80-227-1942-0. (Po)

[2] Krkoška, P.: Describing of papermaking properties of pulp fibres via mathematical pathway. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97 (8) 670 (2003).

[3] Lužáková, V.*, Némethová K., Sidorová I.: Interakcie lipofilných extraktívnych látok dreva s protiživičnými prostriedkami. Chemické Listy 97, 8, 670 (2003). Interactions of lipophilic wood extractives with pitch control additives. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 8, 670 (2003).

[4] Vrška, M, Jablonský M., Hladová M.: Oxidačné postupy bielenia buničín. Oxidation processing in bleachimg of pulp. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97 (8) 671 – 672 (2003).

[5] Jakubíková, Z., Mikula, M., Šutý, Š., Trnovec, B.: Uhlová závislosť lesku vo vzťahu k hladkosti papiera. Angular dependence of gloss related to the paper smoothness. In: Zborník Polygrafického seminare, 23. – 24. 10. 2003, Pardubice, pp. 9-14, ISBN 80-7194-561-7

[6] Fišerová M.,Gigac J.,Majtnerová A.,Szeiffová G.: POSSIBLE UTILIZATION OF ANNUAL PLANTS IN PULP AND PAPER INDUSTRY. "In: PeerReviewed Proceedings of the International Conference "" Chemical Technology of Wood, Pulp and Paper"", September 17. - 19., (2003), Bratislava, Slovak Republic, ISBN 80-227-1942-0"

[7] Katuščák, S.: CHEMICAL TECHNOLOGY OF WOOD, PULP AND PAPER IN CULTURE, EDUCATION AND INDUSTRY. "PeerReviewed Proceedings of the International Conference ‘Chemical Technology of Wood, Pulp and Paper’", September 17. - 19., (2003), Bratislava, Slovak Republic, ISBN 80-227-1942-0"

[8] Krkoška, P.: DESCRIBING OF PAPERMAKING PROPERTIES OF PULP FIBRES USING MATHEMATICAL PATHWAY AND REGIONAL FIBRE SOURCES ‘PeerReviewed Proceedings of the International Conference ‘Chemical Technology of Wood, Pulp and Paper’", September 17. - 19., (2003), Bratislava, Slovak Republic, ISBN 80-227-1942-0"

[9] Reháková, M., Vizárová K.,Hrehorová E.,Račková K..: THE INFLUENCE OF INTERNAL AND EXTERNAL FACTORS ON THE INK-JET PRINT QUALITY IN THE AGEING PROCESS. "PeerReviewed Proceedings of the International Conference ‘Chemical Technology of Wood, Pulp and Paper’", September 17. - 19., (2003), Bratislava, Slovak Republic, ISBN 80-227-1942-0"

[10] Szeiffová, G.,Alince B.: WET WEB STRENGTH DEVELOPMENT "PeerReviewed Proceedings of the International Conference ‘Chemical Technology of Wood, Pulp and Paper’", September 17. - 19., (2003), Bratislava, Slovak Republic, ISBN 80-227-1942-0"

[11] Šutý, Š., Galbavá M.,Tiňo R,Vizárová K.,Szeiffová G.,Jablonský M.: POLYVINYLACETHATE AT THE PAPER PRODUCTION – ELECTROKINETIC PROPERTIES AN INTERACTIONS WITH PULP FIBRES "PeerReviewed Proceedings of the International Conference "" Chemical Technology of Wood, Pulp and Paper"", September 17. - 19., (2003), Bratislava, Slovak Republic, ISBN 80-227-1942-0"

[12] Tiňo, R.,Šutý Š,Vizárová K.,Jablonský M.: DEPOSITION OF LATEX PARTICLES ONTO PULP FIBERS – NEW ACTING OF POLYMERS IN PAPERMAKING "PeerReviewed Proceedings of the International Conference "" Chemical Technology of Wood, Pulp and Paper"", September 17. - 19., (2003), Bratislava, Slovak Republic, ISBN 80-227-1942-0"

[13] Hrehorová, E., Tiňo R., Šutý Š.: Paper properties of paperboards made from pulp fibres and synthetic latexes. Effect of particles size of latex. poster EMBAX Print, Brno 2003

[14] Tiňo, R., Šutý Š., Vizárová K.: Deposition of latex particles onto pulp fibres - new acting of polymers in papermaking. In. Seminar on Food safety in relation to novel packaging technologies - poster, Brussels, Belgium, November 2003

[15] Šutý, Š., Tiňo R., Krkoška P., Mišovec P., Panák J.: Metódy zušľachťovania papierenských obalových materiálov - sucasny stav a trendy. Methods of refinement of paper packing materials – present state and trends. Odborný seminár Papír, tisk a obaly, Čejkovice, ČR, november 2003

[16] Vizárová K.*, Cedzová M.,Reháková M, Šutý Š.: Vplyv svetelnej predhistórie na stálosť a trvanlivosť novodobých papierov The influence light prehistory on stability and durability modern papers XII. Seminář restaurátorů a historiků, Praha- Chodovec, 7.-10.10. 2003, 7a, Pr

DEPARTMENT OF ENVIRONMENTAL ENGINNERING

68


Head of Department: Telephone: ++421252495243 Doc. Ing. Gabriel Čík, PhD Fax: ++421252495243


I. STAFF Full Professors: Vasil Koprda, PhD, DSc; Milan Piatrik, PhD Associate Professors: Marta Čerňáková, PhD; Gabriel Čík, PhD; Ján Derco, PhD; Pavel Dillinger, PhD (till Sept. 2003); Miloslav Drtil, PhD; Margita Harangozó, PhD; Josef Prousek, PhD Research Fellows: Igor Bodík, PhD; Mária Főldesová; Miroslav Hutňan, PhD PhD Students: Eva Gašpariková; Marek Horňák; Lucia Mitaľová (since 01.10.2002); Andrea Bujnová; Katarína Svetková; Soňa Priesolová; Milada Hubinová (till 01.10.2003); Peter Chnapko; Angelika Kassai; Ladislav Maro; Marek Rybár; Katarína Srdošová; Jana Vanečková-Plchová; Monika Karacsoniová; Rastislav Kuffa (till 4.10. 2003), Jana Marová (since 1.10. 1998), Ľubomír Gajdoš (since 1.10. 2002), Angelika Kassai (since 01.10.2003), Juraj Farkas (since 1.10. 2003) Technical staff: Eleonóra Hornáčková; Marta Onderová;


A. Teaching laboratories: Laboratory of Water Chemistry Laboratory of Nuclear Analytical Chemistry Laboratory of Water Technology

B. Research laboratories: Laboratory of Air Protection Technology Laboratory of Microbiology and Ecotoxicology Laboratory of Organic Chemistry Laboratory of Radioecology Laboratory of Water and Wastewater Engineering Laboratory of Computer Modelling

III. TEACHING

A. Undergraduate Study: 5. semester (Bc) Nuclear Chemistry and Technology 1/1/0 Koprda 6. semester (Bc) Environmental Technology 2/0/0 Piatrik, Čík, Koprda 1. semester (MSc) Biology of Water, Air and Soil 2/0/0 Čerňáková Atmospheric and Water Chemistry 2/2/0 Prousek, Bodík Hydrology, Meteorology and

Pedology 2/0/0 Čerňáková

Nuclear Chemistry and Technology 2/0/0 Koprda 1. semester (MSc) Laboratory Practice I. 0/0/8 Harangozó, Bodík, Foldesová 2. semester (MSc) Air Protection Technology 2/0/0 Čík, Prousek Radioecology 2/0/0 Harangozó, Dillinger Wastewater Engineering 2/2/0 Derco, Drtil Laboratory Practice II. 0/0/8 Derco, Dillinger, Čík 3. semester (MSc) Risk Properties of Substances 2/0/0 Prousek, Čerňáková Elimination and Utilization of Wastes 2/0/0 Piatrik, Koprda Environmental Technological Project 2/1/0 Drtil, Derco Environmental Impact Assessment 2/0/0 Piatrik, Koprda 3. semester (MSc) Laboratory Practice III. 0/0/10 Drtil, Harangozó, Čík Control of Environmental Pollution 2/0/0 Harangozó Special Ecology and Ecotoxicology 2/0/0 Prousek


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Processes and Technology of Water Treatment

2/1/0 Hutňan, Bodík

3. semester (MSc) Air Protection Technology and Air Treatment

2/1/0 Čík, Prousek

4. semester (MSc) Diploma Work 0/0/30 all members of the staff


A. VEGA Project No. 2/2049/22 Penetration of Xenobiotics across Skin (Katarína Bauerová, ÚEF SAV ratislava); Department part: Penetration of Xenobiotics across Skin (Vasil Koprda)

Evaluation of kinetics of transdermal permeation of ionic species and effects of physico-chemical factors on this process were studied. Using some radionuclides of corrosion and fission products, namely 137Cs, and 60Co ions , the effect of valency and the concentration of ions on permeation velocity across the intact, and splitted skin of biologic animal models were studied. Using radioactively labeled substances the effects of solvent type (Transcutol) and structural type of chemical penetration enhancers (Azone), on barrier function of skin was investigated. The permeation across the skin of new drugs (onchomycotics Terbinafine and some oxygen scavengers were studied. The new biological models of 5 and/or 9 days rat skin were studied and snake shed skin was used for standardisation of transdermal permeation membrane. Effect of Cs+ and Co2+ concentration on their permeation rate through different skin models was evaluated. A row of experiments were aimed to reveal the transmembrane behaviour of radionuclide 137Cs+ and 60Co2+ across the different artificial skin substitutes constructed in the FCHFT.

Project duration: from 1.1.2002 to 31.12.2004 B. Part of the VEGA project No. 1/8909/01Syntheses directed towards novel structural well

defined pi-conjugated heterocyclic compounds and their oligomers (Gabriel Čík) Poly(3-dodecylthiophene), with different amounts of head-to-head configuration defects, was characterized by UV-VIS, H-NMR, photoluminescence, and Raman spectra. The heat-induced conformational sample changes were studied by EPR. For the study of these changes, a spin-probe technique was used. From the EPR spin-probe spectra rotational correlation times and order parameters were calculated.

Degradation of 4-chlorophenol by reactive oxygen species was studied, the latter being generated by photo-assisted reactions of thiophene oligomers, synthesized in channels of the Na-ZSM-5 zeolite. The photoreaction was carried out in an aqueous suspension of photocatalyst, irradiated with visible light. The spin-trapping method was used to detect the generated OH radicals. The main products of the photodecompsition of 4-chlorophenol were found to be phenol, hydroquinone and maleic acid.

Project duration: from 01.01.2001 to 31.01.2003 C. Project in cooperation with the Ministry of Environment of the Slovak Republic, No.

527/2003/II. emediation technologies of PCB. (Gabriel Čík) Remediation technologies of PCB

Project duration: from 01.12.2003 to 15.06.2004 D. Institutional Project No. 155/03 The Study of Sorption and Immobilisation of Radionuclides

from Nuclear Power Plant Cycle by Natural Adsorbers (Pavel Dillinger) The determination of sorption capacity of natural and chemically modified natural zeolites towards some cations was studied by static radioexchange method, AAS method, liquid scintillation counting method (LSC) and gamma spectroscopy . It was studied the sorption of Sr(II), Pm(III) and Cs and Co from mixture of radionuclides. Radionuclides Sr-90, Pm-147, Cs-137 and Co-60 were used as radiotracers. The structure, sorption and desorption properties of natural and chemically modified zeolites and the new types of natural and chemically modified sorbents - alginite, diatomite, precinal HMS were studied. The inluence of individual cations and their chemical forms, pH, temperature and competitive cations (K, Ca, Fe) on the sorption and desorption was studied as well. The sorption and desorption characteristics of these materials were compared with syntetic zeolite -Zeolon. We demonstrated that the sorption capacity of natural and chemically modified sorbents depends not only on these materials but also on the chemical properties of studied solutions (chemical spetation), higher temperature and pH above 7. The time dependence of permeation of 147-Pm(III) from aqueous solution was estabilished by the animal skin model and the age dependence of Pm permeation through the skin was examined. The skin from 5-day-old rats was found to represent the optimum animal model to study trasepidermal permeation of ions. The skin from 9-day-old rats was selected to study transfollicular permeation of ions. Radon and its short-lived decay products have been simultaneously monitored at the height 1,5m above the ground during various periods of a year. It was analysed an influence of meteorogical conditions on activity concentrations of Rn-222. The use of wet oxydation catalysis in industry was studied. The derivates of difenylamine in waste waters were degradated by wet catalytic oxidation.

Project duration: from 01.01.2001 to 31.12.2003 E. Institutional FCHFT STU Project No: 139/03: Advanced methods for water, wastewater,

sludge and organic wastes treatment (Ján Derco) The aim of the project is the research and evaluation of progressive methods of water treatment, wastewater treatment,


70

sludge treatment and disposal, organic wastes treatment and water quality controll. Research has been foccused on selected physical-chemical and biological processes.



A. Project No 2032040 Norwergian Competencies Transfer into New Curricula of Environmental Engineering Education at the Slovak University of Technology in Bratislava, Slovak-Norwergian bilateral cooperation. (Gabriel Čík)

The main objective of the project is to take advantage of Norwergian long time experience in the field of Environmental Engineering curricula. Effort will be focused on utilization of this through partnership assistance in the process of introduction of the above subject into curricula of the 3-degree university education (bachelor, engineer and PhD) at the Faculty of Chemical and Food Technology of the Slovak University of Technology in Bratislava.


B. OSF Project G/236/02/61300 Water Technology and Water Resources Protection (Ján Derco)

The aim of the project is to prepare Internet Distance Education Program on Water Technology and Water Resources Protection. An online version of this course is being prepared as a part of continuing education for professionals in the field.


VI. COOPERATION



Duration

Slovak Office of Standards, Metrol. and Test., Cyclotron Center of the SR, Bratislava

Applied radiation chemistry, production of positron radiopharmaceuticals

Ružička J., vicedirector; Kassai Z. , Dept.of positron emitters, Štefanovičova 3, 810 05 Bratislava

01.02.2000 -

Slovak Academy of Science, Bratislava Possibility of zeollite use in wastewater Sládek,P., director, Dúbravská

cesta 9, Bratislava 01.11.2003 - 31.12.2003

IPRES Engineering, s.r.o. Possibility of zeollite use in wastewater Šurka,F., president, Dúbravská

cesta 9, Bratislava 01.05.2003 - 31.12.2003

ASIO-SK s.r.o. Anaerobic-aerobic wastewater treatment Kratochvil,K., director, Malobytčianska ul., Bytča 01.01.1997 -

FELLEGI Int. Anaerobic treatment processes Fellegi,J., director, Na Hrebienku 38, Bratislava 01.03.2003 -

Stredoslovenská vodárenská spoločnosť a.s., Banská Bystrica

ISPA Tender evaluation - technical assistance, Reconstruction of wastewater treatment plant Zvolen

Hluchý Marián, director, Partizánska 5, 974 00 Banská Bystrica

05.11.2003 - 21.11.2003

Stredoslovenská vodárenská spoločnosť a.s., OZ Lučenec

Evaluation of wastewater treatment plant Poltár and proposal of reconstruction

Hoffmann Jozef, director, Komenského 4, 984 53 Lučenec

08.10.2003 - 31.12.2003

Sebex, spol. s r.o., Košice

Anaerobic Stabilization Of Sludge From Municipal Wastewater Treatment By Electrocoagulation. Conctract No 122/2003

Ing. Peter Smolnický, director, Letná 14, 040 01 Košice

21.07.2003 -30.10.2003

Dep. of Nuclear Physics, Faculty of Mathematic and Physics, Com. Univ., Bratislava

Determination of Rn-222 and its decay products in the atmosphere

Holý Karol, head of depart., Mlynská dolina, 824 15 Bratislava

01.011995 -

Dep. of Nuclear Chemistry, Faculty of Natural Sci., Com. Univ., Bratislava

Dep. of Nuclear Chemistry, Faculty of Natural Sci., Com. Univ., Bratislava

Mátel Ľubomír, head of depart., Mlynská dolina, 824 15 Bratislava

01.01.1992 -


- 71 -

Dep. of Chemistry, Matej Bel Univ., Banská Bystrica

Education studies in Environmental chemistry

Tomeček Otto, research worker,974 01 Banská Bystrica 01.01.2001 -

Water Research Institute,Bratislava LSC measurements of radionuclides

Vršková Marta, head of dep., Nabr. L. Svobodu 5, 812 49 Bratislava

01.01.1996 -

OSF Foundation IDEP Program - Grant G/236/02/61300

Katarína Pišútová-Gerber, Nadácia otvorenej spoločnosti - OSF, Baštová 5, 811 03 Bratislava

02.07.2002 - 30.06.2004

Chemical Institute of Faculty of Natural Sciences of Comenius University, Bratislava

Analysis of dust particles Krištín J., head of Dept. of Physical Methods, Mlynská dolina , 842 15 Bratislava

01.05.2002 -

Comenius University,Faculty of Pharmacy, Dpt. of Galenic Pharmacy, Bratislava

Penetration of Terbinafine across the skin

Duckova K., vicedean, ul.Odbojárov 10, 832 32 Bratislava

01.04.2002 -

Matej Bell University,Faculty of Natural Sciences, Dpt. of Environmental Chemistry

Cold electron radiation sterilisation Tolgyessy J., Prof.emeritus, Tajovského 40, 97401 Banská Bystrica

01.06.2001 -

Institute of Experimental Pharmacology of Slovak Academy of Sciences, Bratislava

Transdermal penetration, animal skin models

Bauerová K., department. head, Dúbravská cesta 9, 842 16 Bratislava

01.02.1998 -31.12.2004

Research Institute of Nuclear Power Stations, Trnava, Ltd., Dept. of RWPT

Nuclear wastes likvidation Chnapko P., doctoral study, Okružná 5, 918 64 Trnava 01.08.2002 -

Nuclear Regulatory Authority of the Slovak Republic

Nuclear and radiation safety - Advisory Committee of the director

Žiakova M., director, Bajkalská 27, 820 07 Bratislava 01.05.1999 -

Pharmacobiochemical Lab., School of Medicine, Comenius Univ., Bratislava

Transdermal transportation of coenzyme Q10

Gvozdjakova M., department head, Kucharska J., Hlboká 2, 811 04 Bratislava

01.05.2003 -



Duration

ASIO, s.r.o., Brno, Czech Republic

Anaerobic and aerobic wastewater treatment, domestic wastewater

Plotěný,K., director, ASIO s.r.o, Tuřanka, Brno, Czech Republic 01.01.1997 -

Institute of Chemical Technology, Prague, Czech Republic

Water and wastewater trechnology, sludge treatment,

Jeníček,P., department head, VŠCHT, Technická 6, Prague, Czech Republic

01.01.1993 -

ISMAC-CNR Milano FP6-2002-NMP-1, Proposal: No STPR 001495 OSSO

Alberto Bolognesi, ISMAC-CNR Milano, Italy 01.06.2003 -

Faculty of Chemistry, Brno, Czech Republic

Lectures on Wastewater Engineering

Prof. Ing. Jaroslav Fiala, CSc., Faculty of Chemistry TU Brno, Purkyňova 118, 612 Brno, Czech Republic

15. 02.2003-30.09.2003

CSIR Bio/CHEMTEK Johannesburg, South Africa

Workshop for the Sixth Framework Programme

Dr. Jozef Dudáš, CSIR Bio/CHEMTEK, Modderfontain 1645, Johannesburg, South Africa

15.01.2003 - 30.01.2003

Medway Sciences Univ. of Greenwich

Transdermal penetration of pharmacologically active substances

Hadgraft J.-head of Skin research, Central Ave., Chatham Maritime, Kent ME4 4TB, UK

01.02.1995 -


72



Valid date

Bodík Igor Association of Wastewater Treatment Experts of the Slovak Republic member of advisory board 13.05.1999 -

Čík Gabriel Slovak ChemicalSociety member 01.01.1991

Drtil Miloslav Association of Wastewater Treatment Experts of the Slovak Republic president 13.05.1999 -

Hutňan Miroslav

Association of Wastewater Treatment Experts of the Slovak Republic member 13.05.1999 -

Derco Ján Association of Wastewater Treatment Experts of the Slovak Republic member of advisory board 13.05.1999 -

Gašpariková Eva

Association of Wastewater Treatment Experts of the Slovak Republic member 13.05.1999 -

Horňák Marek Association of Wastewater Treatment Experts of the Slovak Republic member 13.05.1999 -

Hutňan Miroslav Slovak Society of Chemical Engineering member 30.04.1995 -

Koprda Vasil Slovak Nuclear Society (SNUS Acad. Board) president 01.01.2000 - Koprda Vasil Slovak Chemical Society, Bratislava member 01.01.1965 - Koprda Vasil Slovak Medical Society, Pharm.Soc member 01.01.1977 - Derco Ján Slovak Society of Chemical Engineering member 29.09.1995 - Prousek Josef Slovak Chemical Society member 01.01.1979 - Derco Ján Slovak Chemical Society member 01.05.1997 -

Derco Ján Common Field Committee -28-95-9 Chemistry and Technology of Environment member 18.12.1997 -

Derco Ján Common Field Committee - 36-05-9 Sanitary-technical buildings member 02.12.2003 -



Valid date

Bodík Igor International Water Association member 01.01.1990 - Derco Ján International Water Association member 01.01.1994 - Čík Gabriel European Photochemical Association, Mulheim, Germany member 01.01.1992

Drtil Miloslav Association of Wastewater Treatment Experts of the Czech republic member of advisory 01.01.1994 -

Derco Ján Association of Wastewater Treatment Experts in Czech Republic member 01.05.1997 -

Derco Ján Journal of Polish Environmental Study other 01.04.1995 - Derco Ján Council of European Water Association member 15.07.2002 -

Derco Ján Commom Field Committee - Chemistry and Technology of Environment Protection - Faculty of Chemistry TU, Brno member 01.02.2003 -

Prousek Josef Czech Chemical Society member 01.05.1979 - Prousek Josef European Photochemical Association member 01.01.1986 -

Koprda Vasil FECS Division for Chemistry and Environment -delegate for Slovakia member of advisory 01.04.2002 -



Date / Duration

Wanner,J. Institute of Chemical Technology, Prague Czech Republic

November 2003 (1 day)

Dohányos,M. Institute of Chemical Technology, Prague Czech Republic June 2003 (1 day)

Matoušek,J. Masaryk Unversity, Brno Czech Republic May 2003 (1 day)

Mašek,I. Faculty of Chemistry, TU Brno Czech Republic June 2003 (1 day)

Žáček,L. Faculty of Chemistry, TU Brno Czech Republic June 2003 (1 day)


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Date / Duration

Bodík,I. 5th International Conference Wastewater 2003, Olomouc, Association of wastewater treatment experts of the Czech Republic

Czech Republic May 2003 (3 days)

Gašpariková,E. 5th International Conference Wastewater 2003, Olomouc, Association of wastewater treatment experts of the Czech Republic


Derco,J. 5th International Conference Wastewater 2003, Olomouc, Association of wastewater treatment experts of the Czech Republic


Horňák,M. 5th International Conference Wastewater 2003, Olomouc, Association of wastewater treatment experts of the Czech Republic


Mitaľová,L. 5th International Conference Wastewater 2003, Olomouc, Association of wastewater treatment experts of the Czech Republic


Čík,G. NTNU - Norwergian University of Science and Technology, Trondheim Norway October 2003

(4 days)

Drtil,M. 5th International Conference Wastewater 2003, Olomouc, Association of wastewater treatment experts of the Czech Republic


Hutňan,M. Institute of Chemical Technology, Prague Czech Republic June 2003 (2 days)

Hutňan,M. Biogas Station, Mettmach Austria March 2003 (1 day)

Hutňan,M. K&H Kinetic, a.s., Klatovy Czech Republic April 2003 (2 days)

Derco,J. Municipality of Maribor, Environmental protection agency Slovenia October 2003

(2 days)

Derco,J. CSIR Bio/CHEMTEK, Modderfontain 1645, Johannesburg South Africa January 2003

(15 days)

Koprda,V. Workshop Persistent Toxic Substances Contamination in European Region, Brno

Czech Republic




Jakubčová,Z. Snake shed - an appropriate modell of Stratum Corneum for study of permeation of substances across the skin Koprda,V.

Kovarovičová,L. Apoptosis of the bacterial cells Čerňáková,M. Michalíková,M. Persistent organic pollutants in environment Čík,G. Cehulová,Z. Permeation of radio toxicological substances across the skin Koprda,V. Petheővá,T. Zero-valent iron utilisation for the colour wastewater treatment Prousek,J. Lukáčová,L. Ozonation of hexametylentetramine Derco,J. Kapusta,Š. Anaerobic degradation of domestic wastewater Bodík,I. Mišeková,E. Environmental impact assesments of technological processes Piatrik,M. Sebestyénová,M. Analyse of the rests from solid wastes combustion Harangozó,M. Gergelyová,P. Chemically modified zeolites - material of future? Főldesová,M.


Hudáková,M. Measuremt of radionuclide activities in human body using whole-body counter Koprda,V., Fulop,M.

Kapráľová,J. Study of physico-chemical properties of pentasile-type zeolite doped with Fe(III) Čík,G.

Cicmanová,K. Anaerobic Treatment of Corn and Corn Silage Hutňan,M.

Sojčáková,I. Influence of Organic Pollution on Dissolved Oxygen Concentration in Carrousel Activations Hutňan,M.

Píšová,P. Study of the assurance method for drinking water quality in its treatment and distribution Piatrik,M.

Tvrdoňová, M. The conditions of Pm sorption with natural sorbents Főldesová, M. Paholek,E. The influence of pH and competitive elements on Pm sorption Dillinger,P.


74

Kvapilová,L. The anaerobic-aerobic treatment method combination for domestic wastewater treatment Bodík,I.

Tresová,Z. Domestic wastewater treatment plants Bodík,I. Bettembuková,A. Ecotoxicological Influence of heavy metal chloride onSinapis Alba Fargašová,A. Dovičovičová,Ľ. Toxicological influences of K2Cr2O7 on Sinapis Alba and Daphnia Fargašová,A. Bubniaková,V. The estimation of nature radioactivity in natural waters Harangozó,M. Czafiková,R. The selection of suitable method for uraniun estimation in waters Harangozó,M. Mikolášková,D. Impact assessment of matters on bacterial growth in water Piatrik,M. Gavaľová,S. Utilisation of ozone for transformation of biologically resistant organics Derco,J.

Brindzová,Z. Utilization of zero-valent iron for the degradation of selected water pollutants by Photo-Fenton reaction Prousek,J.

Marková,L. Utilization of zero-valent iron for the degradation of selected water pollutants by the Fenton reaction Prousek,J.


Želinská,J. Contribution to study of anthropogene impacts on polychrome layers of artifacts Harangozó,M.

Halász,L. Katalytic wet oxidation Piatrik,M., Bodík,I. Kuffa,R. Heavy metals in biological treatment of wastewaters and sludges Derco,J. Popovičová,A. Adsorption of benzene and trichloroethylene on chosen carbon sorbent Čík,G.

D. Dissertations (DSc) Name Title of Thesis Head of board

Vaňura,P. The Separation Methods for Isolation and Speciation of Radionuclides Koprda,V. E. Habilitation Theses

Name Title of Thesis Head of board Hutňan,M. Utilization of Anaerobic Processes in Technology of Wastewater and

Waste Treatment Koprda,V.

Bodík,I. The Selected Aspects of Processes of Biologic Removal of Nitrogen from Waste Waters Koprda,V.


[1] Bodík, I., Kratochvil K., Gašpariková E., Hutňan M.: Nitrogen removal in an anaerobic baffled filter reactor with aerobic post-treatment. Bioresource Technology, 86 (1), 79-84 (2003)

[2] Čík, G., Hubinová, M., Šeršeň, F., Krištín, J., Antošová, M.: Photocatalytic degradation of 4-chlorophenol by .OH radicals generated by thiophene oligomers incorporated in ZSM-5 zeolite channels. Collect. Czech. Chem. Commun. 68, 2219-2030 (2003)

[3] Čík, G., Zálupský, P., Cirák, J., Tomčík, P., Végh, D. : Dipole moment of Langmuir monomolecular layer of mono n-octyl-ester of 3(3-thienyl)glutaric acid trimer at the air-water interface. Synth. Met. 139, 355-360 (2003)

[4] Hutňan, M., Horňák, M., Bodík, I., Hlavačka, V.: Anaerobic Treatment of Wheat Stillage. Chem. Biochem. Eng. Q. 17 (3), 233-241 (2003).

[5] Kassai, Z., Koprda, V., Bauerová, K., Harangozó, M., Bendová, P., Bujnová , A.,Kassai, A.: Penetration of radionuclides across the skin: Rat age dependent promethium permeation through skin in vitro. J. Radioanal. Nucl. Chem. 258(3) 669-672 (2003).

[6] Šeršeň, F., Čík, G., Veis, P.: Study of conformational changes in poly(3-dodecylthiophene) dependent on backbone stereoregularity using spin-probe technique. Appl. Polym. Sci. 88, 2215-2223 (2003)

[7] Šeršeň, F., Čík, G., Havránek, E.: Preparation and properties of zeolite fertilizer able to slowly release copper, Chim. Inz. Ekol. 12, (2003)

[8] Lukáč, P., Foldesová , M.: Imobilizácia niektorých rádionuklidov zeolitmi a ich solidifikácia špeciálnou cementovou zmesou Immobilisation of some radionuclides by zeolite and their solidification with special cement slurries. Ropa, uhlie, plyn a petrochémia.45(1-2), 64-67 (2003).

[9] Derco, J.: 25 rokov Katedry environmentálneho inžinierstva. 25 years of Department of Environmental Engineering Vodohospodársky spravodajca 12, 2003, str. 7-9.

[10] Derco, J.: Činnosť AČE jako člena EWA.. Activity of AWWTE as a member of EWA Vodohospodársky spravodajca 12, 21 (2003).

[11] Gašpariková E., Bodík, I.: Vplyv teploty na anaeróbny rozklad kalu a produkty jeho rozkladu. The temperature effect on anaerobic decay of the sludge and on the pruducts of the decay. Vodohospodársky spravodajca 46(10), 18-19 (2003)

[12] Tolgyessy, J., Harangozó, M., Dillinger, P., Tomeček, O., Foldesová, M.: Vývoj, stav a perspektívy nukleárnej analytickej chémie a rádioekológie v Slovenskej republike. Development, state and prospects of nuclear analytical chemistry and radioecology in Slovak republic. Acta Univ. Matthiae Belii 1, 109-119 (2003).

[13] Tolgyessy, J., Koprda, V., Harangozó, M., Tomeček O.: Priemyslové aplikácie elektronových urýchľovačov, Industrial applications of electron accelerators. Acta Univerfsitatis Matthiae Bellii, Ser. Chem. No.6 (2003).

[14] Bodík, I., Námer J., Thalmeinerová D.: Poslanie GWP a jeho začlenenie do života a aktivít slovenskej


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vodohospodárskej verejnosti. Mission of the GWP and its integration into slovak water management public life Vodohospodársky spravodajca 46(1), 6-7 (2003)

[15] Bodík, I., Námer J., Thalmeinerová D.: Publikácie Global Water Partnership – 1. časť. Vodohospodársky spravodajca 46(2), 14-15 (2003)

[16] Bodík, I., Námer J., Thalmeinerová D.: Publikácie Global Water Partnership – 2. časť. Vodohospodársky spravodajca 46(3), 6-7 (2003)

[17] Tölgyessy, J., Harangozó M., Ružička J., Baráni V.: Nebojme sa ožiarením sterilizovaných potravín. (Radiačne ošetrovanie potravín a obava ľudí). Radiation sterilization of foods. Enviromagazin 8 (5) 28 (2003).

[18] Tölgyessy, J., Harangozó M.: Environmentalistika pre šikovné ruky, Odpady l. Environmentalistics for clever man. Wastes I. Enviromagazin 8 (l) 27 (2003).

[19] Tölgyessy, J., Harangozó M.: Environmentalistika pre šikovné ruky, Odpady lI. Environmentalistics for clever man. Wastes II. Enviromagazin 8 (2) 23 (2003).

[20] Tölgyessy, J., Harangozó M.: Environmentalistika pre šikovné ruky, Odpady lII. Environmentalistics for clever man. Wastes III. Enviromagazin 8 (3) 15 (2003).

B. Conferences [1] Hubinová, M., Čík, G.*, Šeršeň, F. : Photocatalytic decomposition of 4-chlorophenol with OH radicals generated by

thiophene oligomers incorporated in ZSM-5 zeolite cannels. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97(8) 595-918 (2003), str. 816, (Po).

[2] Koprda, V.*, Krištín, J.: Dust particles in the urban atmosphere of the largest cities of Slovak Republic"In: Proc. Workshop ""Persistent toxic substances contamination in the European region, Brno, Nov. 11-13, 2003, Book of abstracts, pp. 195-198 (2003). (Po)"

[3] Čík, G.*, Hubinová, M., Šeršeň, F. : Properties of ZSM-5 zeolite doped with Fe(III) ions. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97(8) 595-918 (2003), str. 871-872, (Pr)

[4] Koprda, V.*: Energy sources for 21st century. "In: Proc. conf.23rd Intern. Symp. ""Industrial Toxikology ´03"" Bratislava, June 18-20, 2003, Procc. Ind. Toxicol ´03, pp. 128-136 (2003). ISSN 1335-3160, ISBN 80-968011-5-5 (Pr) "

[5] Koprda, V.*: Nuclear energy and environment in close future. In: Proc. IRPA regional congress on radiation protection in Central Europe, Bratislava, Sept. 22-26, 2003, Book of Abstr. Add. (2003). ISBN 80-88806-42-9 CD ROM (Pr)

[6] Derco, J. Mitaľová L., Gajdoš Ľ.: Ozonizácia odpadových vôd s obsahom rezistentných látok. Ozonation of wastewater containing refractory polutants. In: Zb. 5. Medzinárodná bienálna konferencia ´ODPADNÍ VODY – WASTEWATER 2003´. May 13 - 15, Olomouc, Česká republika, p. 317- 320 (2003). ISBN 80-239-0573-2 (Po)

[7] Derco, J*. Využitie dynamických simulačných programov pri navrhovaní biologických procesov odstraňovania dusíka. Use of dynamic simulation programs in biological processes of Nitrogen remowal design. In: Zb. 5. Medzinárodná bienálna konferencia ´ODPADNÍ VODY – WASTEWATER 2003´. May 13 - 15, Olomouc, Česká republika, p. 267- 274 (2003). ISBN 80-239-0573-2. (Pr)

[8] Derco, J*., Drtil M., Bodík, I., Hutňan M.: Internet Distance Education Program – Water Technology and Water Resources Protection. ICETA 2003. In: Proc. 2nd International Conference on Emerging Telecommunications Technologies and Applications and the 4th Conference on Virtual University. 11 – 13 September 2003, Košice, Slovakia, pp. 403-404 (2003) ISBN 80-89066-67-4. (Pr)

[9] Derco, J*., Mitaľová L., Gajdoš Ľ.: Ozonation of wastewater containing refractory polutants. In: Proc. 30th International Conference of Slovak Society of Chemical Engineering, May 26 - 30, Tatranské Matliare 2003, Slovakia, p. 12 (2003). ISBN 80-227-1889-0. (Pr)

[10] Derco, J*., Mitaľová L., Gajdoš Ľ.: Ozonation of wastewater containing refractory polutants. In: Proceedings of the 30th International Conference of Slovak Society of Chemical Engineering, May 26 - 30, Tatranské Matliare 2003, Slovakia, CDROM (2003) ISBN 80-227-1889-0. (Pr)

[11] Felegi J., Bodík, I., Hutta M., Gora R., Halmová T.: Proc. of the International Conference “WPP – Chemical Technology of Wood, Pulp and Paper”, September 17-19, 2003, Bratislava, Slovak Republic, pp.232-236, ISBN. The COD of lignin in non-wood delignification black liquors. The COD of lignin in non-wood delignification black liquors. In:Proc. of the International Conference “WPP – Chemical Technology of Wood, Pulp and Paper”, September 17-19, 2003, Bratislava, Slovak Republic, pp.232-236, ISBN 80-227-1942-0

[12] Hutňan, M.*, Horňák, M., Hlavačka, V.: Anaerobic treatment of wheat distillery slops. Anaerobic treatment of wheat distillery slops. In: Proc. 30. Int. Conf. SSChE on CD-ROM, May 26-30, 2003, Tatranské Matliare, Slovakia

[13] Hutňan, M.*, Horňák, M., Hlavačka, V.: Anaerobic treatment of wheat distillery slops. Anaerobic treatment of wheat distillery slops. In: Proc. 30. Int. Conf. SSChE, May 26-30, 2003, Tatranské Matliare, Slovakia p. 53. ISBN 80-227-1889-0. (Pr)

[14] Koprda, V.*: Jadrové technológie a životné prostredie. Nuclear technology and environment. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem.Listy 97(8) 799-800 (2003).

[15] Gašpariková E*., Bodík, I. Testy anaeróbnej rozložiteľnosti modelového substrátu. The tests of the model substrat anaerobic degradation. In: 4.Zborník prednášok 5. medzinárodná konferencia Odpadní vody 2003, Olomouc, 13,-15.5.2003, pp.329-332, ISBN 80-239-0573-2. (Po).

[16] Halász, L.*, Buday M., Piatrik M., Bodík, I.: Katalytická mokrá oxidácia odpadových vôd obsahujúcich deriváty difenylamínu. Katalytic wet oxydation of the wastewater containing difenylamine In: Zborník prednášok 5. medzinárodná konferencia Odpadní vody 2003, Olomouc, 13,-15.5.2003, pp.333-336, ISBN 80-239-0573-2. (Po).

[17] Foldesová, M.*, Dillinger P., Lukáč, P., Svetík, Š.: Vplyv kalcinácie a chemickej modifikácie na štruktúru prírodných zeolitov. The influence of calcination and chemical modification on the structure of natural zeolites. In: Proc. 16.Int. Conf. Termanal 2003, Stará Lesná , 8.-10.october (SR), PO-06 (2003). ISBN 80-227-1955-2. (Po).

[18] Lukáč, P.*, Foldesová , M., Dillinger, P., Svetík, Š.: Zmeny sorpčných vlastností prírodných a chemicky modifikovaných zeolitov spôsobené teplotou a vysokoenergetickým žiarením. Changes of sorption properties of


76

natural and chemical treated zeolites due to temperature and gamma radiation. In: Proc. 16.Int. Conf. Termanal 2003, Stará Lesná , 8.-10.october (SR), PO-11 (2003). ISBN 80-227-1955-2. (Po).

[19] Bodík, I.*, Drtil M., Hutňan M., Gašpariková E.: Rekonštrukcie komunálnych ČOV na odstraňovanie dusíka a fosforu. The reconstruction of municipal WWTP to nutrient removal. In: 3. konferencia s medzinárodnou účasťou “Rekonštrukcie stokových sietí a čistiarní odpadových vôd”. Liptovský Ján, 27.-29.10. 2003, p-218-227, ISBN 80-89062-24-5

[20] Bodík, I.*, Rajczyková E.: Súčasný stav a perspektívy malých ČOV na Slovensku. The present status and perspectives of the small WWTPs in the Slovak Republic In: Zb. 2. konferencia s medzinárodnou účasťou „Malé vodné diela a alternatívne zdroje energie“. Košice 11.-12.2.2003, p.27-32

[21] Bokroš, M.*, Tôlgyessy, J. , Piatrik, M.: Environmentálne výhody recyklácie starých automobilov a faktory ovplyvňujúce zavádzanie recyklácie. Environmental advancements of the wrecks recycling and influence factors of the recycling introduction. In: Zb. Medzinár. konf. TOP 2003 Technika ochrany prostredia.Častá – Papiernička, 24. - 25. 6. 2003 s.165-172 (2003). (Pr).

[22] Derco, J*., Dián M., Rajczyková E.: Overenie návrhu intenzifikácie ČOV Nové Zámky pomocou dynamických simulácii. Verifying of Nove Zamky WWTP design by dynamic ssimulation. In: Zb. 3. konferencia s medzinárodnou účasťou ´Rekonštrukcie sokových sietí a čistiarní odpadových vôd´. Liptovský Ján, 27. – 29. októbra 2003. str. 191-198 (2003). ISBN 80-89062-24-5.

[23] Derco, J*.: Matematické simulovanie procesov odstraňovania dusíka na ČOV. Mathematical simulation of nitrogen removal processes on WWTP. In: Seminár 'Výskum vplyvu antropogénnych faktorov na vodné systémy´. RVT 27-34. VÚVH 23. – 24. April 2003 (2003). CD ROM.

[24] Derco, J*.: Voda - surovina 21. storočia. Water - raw material of 21st century. In: Seminár pri príležitosti 25. výročia založenia Katedry environmentálneho inžinierstva. Bratislava 13. 6. 2003. str. 13-14.

[25] Kratochvíl, K.*, Bodík, I.: Porovnanie energetických nákladov komunálnych ČOV s anaeróbnym predčistením a bez anaeróbneho predčistenia. The comparison of the energetic costs in the municipal WWTP with and without anaerobic pre-treatment. In: Zb. 2. konferencia s medzinárodnou účasťou „Malé vodné diela a alternatívne zdroje energie“. Košice 11.-12.2.2003, p.37-43

[26] Piatrik, M.*, Plchová, J.: Systémy podpory proaktívneho správania podnikov k ochrane životného prostredia. Support systems of proactive behavior of enterprices to the protection an environment In: Zb. medzinár. ved. konf. Humanizácia a životné prostredie, Stavebná fakulta STU v Bratislave, Katedra humanitných vied, Bratislava 11. – 12. 9. 2003. s. 199-203, (2003). ISBN 80-227-1920-X. (Pr)

[27] Plchová, J.*, Piatrik, M.: Starostlivosť o životné prostredie v kontexte manažmentu kvality. Carefulness of environment in the context with quality management. In: Zb. medzin. konf.: Nové trendy rozvoje prumyslu. VUT Brno Fakulta podnikatelská, Brno 26.-27.11. 2003, zborník na CD bez číslovania strán. (2003). ISBN 80-214-2518-0. (Pr).

[28] Foldesová, M.*, Dillinger, P., Lukáč, P.: Štúdium sorpčných vlastností prírodných ionexov rádioindikátorovou metódou. The study of sorption properties of natural zeolites by radioindicatore method "In: Zb. na CD, Odb. sem. ""Prírodné a syntetické zeolity-súčasný stav poznatkov z výskumu a aplikácií na Slovensku, FChPT STU Bratislava, 13.2.2003. (2003). (Po)."

[29] Bugár, I., Kováč, J.*, Matuszna, K., Lukeš, V., Čík, G.: Polymer structure characterization of polythiophenes by fluarescence spectroscopy in solution. 12th International LASER PHYSICS Workshop (LPHYS´03), Hamburg, August 25-29, 2003, (Pr)

[30] Koprda, V.*, Kassai, Z., Bujnová, A., Bauerová, K.: Reduction of transdermal penetration of radioactive contaminants In: Proc. conf. 31st Technological Days, Piešťany, Oct.15-17, 2003, Abstr. (2003). (Pr)

[31] Čík, G., Hubinová, M.: Charakterizácia zeolitu ZSM-5 dopovaného s Fe3+ iónmi pomocou EPR spektroskopie Characterization of ZSM-5 zeolite doped with Fe(III) ions by EPR spectroscopy Odborný seminár: Prírodné a syntetické zeolity – Súčasný stav poznatkov z výskumu a plikácií na Slovensku, CD-ROM, FCHPT Bratislava, 13.2.2003, (Pr)

[32] Námer, J.*, Drtil, M.: Praktické skúsenosti s termofilnou aeróbnou stabilizáciou. Practical experience with autothermophylic aerobic sludge digestion. Odb. seminár AČE SR, KEI FCHPT STU a GWP, Zákon č.188/2003 o aplikácii kalu a dnových sedimentov. Bratislava, Dec.4, 2003.

DEPARTMENT OF FIBRES AND TEXTILE CHEMISTRY

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Head of Department: Telephone:++421 2 529685598 Prof. Ing. Anton Marcinčin, PhD Fax: ++421 2 524931198


I. STAFF Full Professors: Eberhard Borsig, DrSc, Anton Marcinčin, PhD Associate Professors: Michal Krištofič, PhD, Anna Murárová, PhD Assistant Professors : Jaroslav Legéň, PhD, Anna Ujhelyiová, PhD Research Fellows: Eva Bolhová, Ľubica Fleischmannová, Marcela Hricová, PhD Students: Martina Jurenková, Natália Karabcová, Eva Kormendyová, Zita Mlynarčíková, Andrej Rusnák Technical staff: Agnesa Chlebáková, Jarmila Nemčeková, Albína Pokorná, Edita Štábelová


A. Teaching laboratories: Laboratory of Macromolecular Chemistry Laboratory of Polymer Fibre and Fibrous Material Structure (DSC, TMA, Surface Properties Laboratory of Fibre Technology Laboratory of Textile Chemistry, Bleaching, Dyeing and Finishing (Ahiba, Pretema) Laboratory of Fibre and Textile Testing Laboratory for Fibre Spinning, Drawing and Texturing, extruders 16 and 30 mm

B. Research laboratories: Laboratory for Thermal and Electrical Properties of Fibres and Textiles (DTA, DSC 7, TGA 7 - Perkin Elmer, Derivatograph Q 1500 D, integral electromer Poly - stat PS-1, Alambeta) Laboratory for Thermomechanical Properties (TMA-50 M and TA) Laboratory for Mechanical Properties (Instron, model 1112) Laboratory of Rheolo- gical Properties (Dynamic viscoelastomer model Rheo.200, capillary rheometer, extrusiomer GOTTFERT 20 mm Laboratory for Structural Properties (Microscope Olympus model BHT, SALS) Laboratory for Exhaust Dyeing Process and its Evaluation (Ahiba, Pretema) Laboratory for Spinning of Fibres (extruders 16 and 30 mm resp.)

III. TEACHING A. Undergraduate Study:

5. semester (Bc) Macromolecular Chemistry (2-0 h) Borsig 6. semester (Bc) Technology of Materials (2-0 h) Marcinčin Bachelor Project (0-0-4 h) 1. semester (MSc) Macromolecular Chemistry II (2-1 h) Borsig Physics of Polymers and Paper (2-2 h) Krištofič Fibre Science and Technology (2-2 h) Marcinčin, Legéň Laboratory of Fibre Science and

Technology (0-0-8) Krištofič, Karabcová

1. semester (MSc) Structure of Fibrous Materials (1-1 h) Krištofič, Ujhelyiová Special and Modified Fibres (0-2 h) Marcinčin, Krištofič, Murárová,

Ujhelyiová 2. semester (MSc) Colorants and Textile Auxiliares (2-0 h) Murárová, Ujhelyiová


78

Technical Textiles (2-0 h) Krištofič, Borsig Principles of Textile Engineering (2-0 h) Ujhelyiová, Murárová Laboratory of Textile Engineering (0-0-8 h) Legéň, Mlynarčíková 2. semester (MSc) Physiology and Comfort of Textiles (0-2 h) Murárová, Hricová 3. semester (MSc) Textile Chemistry and Technology (2-2 h) Ujhelyiová, Bolhová Technology of Polymeric Films (2-0 h) Marcinčin, Krištofič Laboratory of Textile Chemistry and

Technology (0-0-10 h) Ujhelyiová, Bolhová

Fibre and Textile Testing (2-0 h) Legéň, Murárová 4. semester (MSc) Diploma Thesis (0-0-27 h)


A. VEGA Project No 1/8106/01. Dispersion of organic pigments in synthetic polymers with particle size close to nano-scale (Anton Marcinčin)

Project duration: from 2001 to 2003 B. Project APVT 20-010102 Nanocomposite fibres based on synthetic polymers (Anton

Marcinčin) Project duration: from 01.09.2002 to 31.08.2005

C. VEGA Project No 1/9147/02 Polymer composite fibres (Eberhard Borsig) Project duration: from 2002 to 2004

VI. COOPERATION



Duration

Fibrochem, a.s., Svit common papers A. Marcincin 2003

VUCHV, a.s., Svit contract 150/2003 contract 161/2003 scientific project 30300/K1/03

A. Marcincin 2003

VUTCH-Chemitex, spol. s r.o. Zilina preparation of CEC conference A. Marcincin 2003

Matador, a.s., division M-VTR- VUG, Puchov

contract 2/2003 A. Marcincin 2003

SH a.s., Senica preparation of int. project Biocelsol A. Marcincin 2003 TnUAD FPT Puchov common papers A. Murarova 2003 Quiltex a.s., Liptovsky Mikulas contract 76/2003 A. Murarova 2003

Polymer Institut of SAV common papers E.Borsig 2003



Duration

Institut of Chem. Fibres, Lodz, PL preparation of CEC conference A. Marcincin 2003

AUTEX, Gent, Belgium preparation of AUTEX conference A. Marcincin 2003

University of Zagreb preparation of ITC&DC conference A. Marcincin 2003

University of Maribor preparation and realisation of 3. CEC conference, Sept. 10. -12. Slovenia A. Marcincin 2003

TU Liberec preparation of TEXSCI conference 16. -18. June and ITSAPT project A. Marcincin 2003

Institut fur Makromolekulare Chemie, A. Ludwigs Univ. Freiburg, BRD

common papers E. Borsig 2003


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Valid date

A. Marcincin Council of Ministery of Education, SR, program: member

Development of young employees and PhD. student personalities member

VUTCH-Chemitex, spol. s r.o., Zilina, Managing Council of Certification member

VEGA Committee member Editor-in-Chief of journal Vlakna a textil member

Slovak Society of Industrial Chemistry, section Chemical Fibres member

E. Borsig Common branch council for awarding of DSc in 14-05-9 Macromolecular Chemistry chairmann

Common branch council for awarding of PhD in 14-05-9 Macromolecular Chemistry chairmann

Slovak Chemical Society, section Polymers member Advisory Board SAV for Chemical Sciences member A. Murarova Slovak Society of Industrial Chemistry Board member of advisory board and its Executive Committee member and its section Chemical Fibres chairmann Slovak Chemical Society, section Polymers member Co-editor of journal Vlakna a textil member Editorial Board of journal Vlakna a textil member A. Ujhelyiova Slovak Chemical Society, section Polymers member Slovak Society of Industrial Chemistry member M. Kristofic Executive Editor of journal Vlakna a textil member Slovak Society of Industrial Chemistry member Slovak Chemical Society, section Polymers member Editorial Board of journal Vlakna a textil member J. Legen Slovak Society of Industrial Chemistry member Slovak Chemical Society, section Polymers member M. Hricova Slovak Society of Industrial Chemistry member



Valid date

A. Marcincin Association of Universities for Textiles, Gent, Belgium member AUTEX Research Journal, Gent, Lodz, B, PL member of advisory Central European Conferences Committee member Scientific Council, TU Liberec, Faculty of Textiles member

member

member

E. Borsig General Assembly of National Representatives of European Polymer Federation, Eidhoven, Netherlands member

Editorial Board of Journal of Macromolecular Chemistry Pure and Applied Chemistry, USA member

Editorial Board of Chemické listy, Prague, Czech Rep. member

Committee for Awarding of DSc for scientific branches 14-05-9 Macromolecular Chemistry, Prague, CZ member

Committee for Awarding of DSc for scientific branches 28-03-9 Technology of Macromolecular Compounds, Prague, CZ

member



Date / Duration

J. Militky TU Liberec Czech Rep. 13.11.2003 (1 day)

Fridrichova TU Liberec Czech Rep. 01.09-05.09.2003 (5 days)

Dvorakova TU Liberec Czech Rep. 01.09-05.09.2003 (5 days)

J. Wiener TU Liberec Czech Rep. 26.5.-30.5.2003 (5days)


80

M. Prasil TU Liberec Czech Rep. 26.5.- 0.5.2003 (5days)



Date / Duration

E. Borsig Institut fur Makromol. Chemie, A.-Ludwigs Univ., Freiburg BRD 26.-29.02 (1 month)

A. Marcincin TU LIberec CZ 21.-22.01./2days M. Kristofic IWCH Lodz PL. 16.-18.03./3 days A. Marcincin Inst. fur Makromol. Chemie, A.-Ludwigs Univ. BRD 29.03.-06.04./9 days A. Marcincin Techtextil Frankfurt am Main BRD 07.-10.04./4 days A. Ujhelyiova Techtextil Frankfurt am Main BRD 07.-10.04./4 days A. Murarova Techtextil Frankfurt am Main BRD 07.-10.04./4 days J. Legen Techtextil Frankfurt am Main BRD 07.-10.04./4 days M. Kristofic Techtextil Frankfurt am Main BRD 07.-10.04./4 days A. Marcincin TU LIberec CZ 22.-24.04/3 days E.Bolhova INOTEX, Dvur Kralove CZ 13.-15.05./3 days M. Jurenkova INOTEX, Dvur Kralove CZ 13.-15.05./3 days Fleischmannova TU Liberec CZ 09.-18.06./10 days A. Ujhelyiova TU Liberec CZ 16.-18.06./3days J. Legen TU Liberec CZ 16.-18.06./3days N. Karabcova TU Liberec CZ 16.-18.06./3days M. Jurenkova TU Liberec CZ 09.-18.06./10 days E. Bolhova TU Liberec CZ 15.06-04.07./20 days E. Kormendyova TU Liberec CZ 15.06.-22.06./8 days E. Borsig European Polymer Federation, Stockholm S 21.-27.06./7 days A. Ujhelyiova TU Lodz PL 23.-28.06./6 days M. Kristofic TU Lodz PL 23.-28.06./6 days E.Borsig Polytech. Wroclawska, PL, Univ. Dresden, BRD PL, BRD 23.09.-03.10/9 days A. Marcincin TU Liberec CZ 29.-31.10/3 days A. Marcincin Univ. of Maribor, (Portorose) Slovenia 09.-12.09./4 days A. Murarova Univ. of Maribor, (Portorose) Slovenia 09.-12.09./4 days M. Kristofic Univ. of Maribor, (Portorose) Slovenia 09.-12.09./4 days



A. Andrejkova Dyeing of Wool by New Processes A. Ujhelyiova A. Augustinova New Trends in Research and Development of Polyamide Fibres E. Borsig Z. Strecka Polypropylene Fibres Dyed from Bath E. Bolhova I. Vassova Structure and Properties of Synthetic Fibres Modified by Nanoparticles A. Ujhelyiova


M. Girmanova Influence of Macromorphological Structure of Textiles on their Biophysical Properties A. Murarova

J. Kukulova Kinetics of Dyeing of the Modified Polypropylene Fibres A. Ujhelyiova Z. Martiskova Concentrated Dispersions for Pigmentation of Polyester Fibres A. Marcincin

A. Rusnak Polymer Blends on the Base of Polyesters as Additives for Modification of Fibres A. Marcincin

R. Radovcic Chemical and Physical Modification of PA 6 Fibres with Better End-use Properties M. Kristofic

J. Carna Influence of Compatibilizer on Properties of Nanocomposite Fibres E. Borsig

VIII. PUBLICATIONS A. Journals [1] Danko, M., Hrdlovič, P., Borsig, E.: Aké informácie o štruktúre polymérov môže poskytnúť fluorescenčná

spektroskopia? Chem. Listy 97, 1052-1060 (2003). [2] Danko, M., Hrdlovič, P., Borsig, E.: Characterization of interpenetrating polymer-like network based on


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polyethylene/poly/styrene-co-butylmethacrylate/PE/P/S-co-BMA// by non-radiative energy transfer. Journal of Photochemistry and Photobiology:Chemistry 154, 279-288 (2003).

[3] Danko, M., Hrdlovič, P., Borsig, E.: Monitoring of swelling of interpenetrating polymer network of polyethylene/poly(styrene-co-butylmethacrylate) (PE/P(S -co-BMA)) in toluene and cyclohexane using fluorescence spectroscopy. Polymer 44, 389-396 (2003).

[4] Pavlíková, S., Thomann, R., Reichert, P., Mulhaupt, R., Marcinčin, A., Borsig, E.: Fiber Spinning from Poly/propylene/-Organoclay Nanocomposite. Journal of Appl. Polymer Sci. 89, 604-611(2003).

[5] Kormendyiová, E., Marcinčin, A.: Mikroreológia a morfológia vláknotvorných zmesí polymérov. Vlákna a textil (Fibres and Textiles) 10, 28-33 (2003).

[6] Marcinčin, A., Borsig, E.: Nanocomposite Fibres for Technical Textiles. Vlákna a textil (Fibres and Textiles) 10, 104-108 (2003).

[7] Marcinčin, A., Brejka, O., Ujhelyiová, A., Kormendyiová, E., Staruch, R.: Morphology and Properties of Polypropylene/Polyester Blend Fibres. Morphology and Properties of Polypropylene/Polyester Blend Fibres. Vlákna a textil (Fibres and Textiles) 10, 3-8 (2003).

[8] Marcinčin, A., Ujhelyiová, A., Brejka, O.: Processing of polyester concentrates for masspigmenting of PET fibres. Processing of polyester concentrates for masspigmenting of PET fibres. Vlákna a textil (Fibres and Textiles) 10, 109-113 (2003).

[9] Mlynarčíková, Z., Borsig, E.: Polypropylénové kompozity, Časť 1. Vlákna a textil (Fibres and Textiles) 10, 130-137 (2003).

[10] Murárová, A., Hodul, P.: Influence of PET fibre macromorphology on dyeing. Influence of PET fibre macromorphology on dyeing. Vlákna a textil (Fibres and Textiles) 10, 9-16 (2003).

[11] Ujhelyiová, A., Bolhová, E. : Morfologická štruktúra a mechanickofyzikálne vlastnosti nanokompozitných materiálov. Vlákna a textil (Fibres and Textiles) 10, 138-143 (2003).

B. Conferences [1] Murárová, A., Jambrich, M.*, Balogová, J.: The influence of textiles material composition on itsphysiological

properties. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 712-713 (2003). [2] Bolhová, E.*, Ujhelyiová, A., Marcinčin, A.: Exhaust dyeing of modified polypropylene fibres. In: Proc. 5th Int. Conf.

Texsci 03. Liberec (ČR), June 16-18, 2003. Ed. TU Liberec, CD room pp. 1-6, Book of Abstract p. 46 (2003). ISBN 80-7083-711-X. (Po).

[3] Bolhová, E.*, Ujhelyiová, A., Marcinčin, A.: Farbenie modifikovaného polypropylénu vyťahovacím postupom. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 731-732 (2003).

[4] Fleischmannová, Ľ., Borsig, E., Mulhaupt, R.: Polypropylénové vlákna plnené anorganickým plnivom. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 731 (2003).

[5] Fleischmanová, Ľ.*, Borsig, E.: Polypropylen nanocomposite fibres filled by inorganic particles. Polypropylen nanocomposite fibres filled by inorganic particles. In: Proc. 5th Int. Conf. Texsci 03. Liberec (ČR), June 16-18, 2003. Ed. TU Liberec, CD room pp. 1-6, Book of Abstract p. 140 (2003). ISBN 80-7083-711-X. (Po).

[6] Hricová, M., Marcinčin, A.*, Karabcová, N., Mlynarčíková, Z.: Unvenness of spun dyed PP fibres related to rheological properties of pigment concentrates. In: Proc. 3rd CEC Conference 2003. Fibre -grade polymers, chemical fibres and special textiles. Portorose-SLOVENIA, Sep. 10-12. 2003. Ed. University of Maribor, CD-room pp.1- 4, Book of Abstract p. 45 (2003). ISBN 86-435-0564-1. (Po).

[7] Jurenková, M., Zemanová, E., Marcinčin, A.*: Thermomechanical analysis of the polypropylene/polyester blend fibres. In: Proc. 3rd CEC Conference 2003. Fibre -grade polymers, chemical fibres and special textiles. Portorose-SLOVENIA, Sep. 10-12. 2003. Ed. University of Maribor, CD-room pp. 1-4, Book of Abstract p. 51 (2003). ISBN 86-435-0564-1. (Po).

[8] Karabcová, N.*, Legéň, J.: Properties of blend PP/PET fibres modified cros-section. Properties of blend PP/PET fibres modified cros-section. In: Proc. 5th Int. Conf. Texsci 03. Liberec (ČR), June 16-18, 2003. Ed. TU Liberec, CD room pp. 1-6, Book of Abstract p. 47 (2003). ISBN 80-7083-711-X. (Po).

[9] Kormendyiová, E.*, Marcinčin, A.: Morphology and Properties of Polypropylene/Polyester Blend Fibres. In: Proc. 5th Int. Conf. Texsci 03. Liberec (ČR), June 16-18, 2003. Ed. TU Liberec, CD room pp. 1-6, Book of Abstract p. 48 (2003). ISBN 80-7083-711-X. (Po).

[10] Legéň, J.*, Murárová, A., Krištofič, M., Lustoň, J.: Compatibilisator influence on properties of Polypropylene/Polyethylene-terephthalate blend fibres. In: Proc. 5th Int. Conf. Texsci 03. Liberec (ČR), June 16-18, 2003. Ed. TU Liberec, CD room pp. 1-6, Book of Abstract (2003). ISBN 80-7083-711-X. (Po).

[11] Legéň, J., Krištofič, M., Murárová, A.*: Blend fibres polypropylene/polyethyleneterephthalate with different cross section. In: Proc. 3rd CEC Conference 2003. Fibre -grade polymers, chemical fibres and special textiles. Portorose-SLOVENIA, Sep. 10-12. 2003. Ed. University of Maribor, CD-room pp. 1-4, Book of Abstract p. 57 (2003). ISBN 86-435-0564-1. (Po).

[12] Mlynarčíková, Z., Kämpfer, D., Thomann, R., Mulhaupt, R., Borsig, E., Marcinčin, A.*: Syndiotactic polypropylene/organoclay nanocomposite fibres. Fibre -grade polymers, chemical fibres and special textiles. Portorose-SLOVENIA, Sep. 10-12. 2003. Ed. University of Maribor, CD-room pp. 1-4, Book of Abstract p. 60 (2003). ISBN 86-435-0564-1. (Po).

[13] Mlynarčíková, Z., Kämpfer, D., Thomann, R., Mulhaupt, R., Borsig, E., Marcinčin, A.:Príprava a vlastnosti nanokompozitných vlákien s matricou zo syndiotaktického polypropylénu. In: 55. zjazd chemických spoločností,

Košice, 8.9.-12.9.2003, Chem. Listy 97, 731 (2003). [14] Murárová, A.*: The influence of textiles material composition on their physiological properties. In: Proc. 3rd CEC

Conference 2003. Fibre -grade polymers, chemical fibres and special textiles. Portorose-SLOVENIA, Sep. 10-12. 2003. Ed. University of Maribor, CD-room pp. 1-4, Book of Abstract p. 61 (2003). ISBN 86-435-0564-1. (Po).

[15] Borsig, E.*, Fiedlerová, A., Lazár, M.: New knowledge of crosslinking mechnism polyethylene and polypropylene. In: Proc. XVI Konferencja naukova. Modifikacja polimerov. Wroclaw(Polsko), May 23-26, 2003. Ed. Politechnika


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Wroclaw, No 52, Seria 25, pp. 76-80 (2003). ISSN 0137-1398 (Pr). [16] Geraldes, M. J.*, Araujo, M., Marcinčin, A.: Engineering design of the thermal and physiological functional

performances in knits and woven structures. In: Proc. 3rd CEC Conference 2003. Fibre -grade polymers, chemical fibres and special textiles. Portorose-SLOVENIA, Sep. 10-12. 2003. Ed. University of Maribor, CD-room pp. 1-4, Book of Abstract p. 22 (2003). ISBN 86-435-0564-1. (Pr).

[17] Krištofič, M.*, Karabcová, N.: Copolyamides as additives for modification of polypropylene and polyamide fibres. In: Proc. 3rd CEC Conference 2003. Fibre -grade polymers, chemical fibres and special textiles. Portorose-SLOVENIA, Sep. 10-12. 2003. Ed. University of Maribor, CD-room pp. 1-4, Book of Abstract p. 13 (2003). ISBN 86-435-0564-1. (Pr).

[18] Marcinčin, A.*, Hricová, M., Lučivjanský, J.: Processing of polypropylene and polyaster pigment concentrates for spun dyed fibres. In: Proc. 3rd CEC Conference 2003. Fibre -grade polymers, chemical fibres and special textiles. Portorose-SLOVENIA, Sep. 10-12. 2003. Ed. University of Maribor, CD-room pp. 1-4, Book of Abstract p. 19 (2003). ISBN 86-435-0564-1. (Pr).

[19] Marcinčin, A.*: Nové vlákna pre inteligentné textílile. In: Proc. Int. Conf. Textil-Zdravie-Ekológia. Žilina (SR), Maj 14-15, 2003. Ed. DT Žilina, pp.1-5 (2003). (Pr).

[20] Marcinčin, A., Ujhelyiová, A., Kormendyiová.: Morphology and properties of polypropylene/polyester blend fibres. In: Proc. 3rd AUTEX Conf. Civiltex 2003. Gdaňsk-Polsko, June 25-27, 2003. Ed.Technical University of Lodž, Gdaňsk, pp. 122-127 (2003). ISBN 83-89003-32-5.

[21] Murárová, A.*, Legéň, J.: Physiological properties of textiles. In: Proc. 3rd CEC Conference 2003. Fibre -grade polymers, chemical fibres and special textiles. Portorose-SLOVENIA, Sep. 10-12. 2003. Ed. University of Maribor, CD-room pp. 1-4, Book of Abstract p. 24 (2003). ISBN 86-435-0564-1. (Pr).

[22] Ujhelyiová, A.*, Marcinčin, A., Bolhová, E.: Thermal and colouristic properties of blend PP/PES fibres. Thermal and colouristic properties of blend PP/PES fibres. In: Proc. 5th Int. Conf. Texsci 03. Liberec (ČR), June 16-18, 2003. Ed. TU Liberec, CD room pp. 1-8, Book of Abstract p. 18 (2003). ISBN 80-7083-711-X. (Pr).

[23] Borsig, E.*, Pavlíková, S., Thomann, R., Reichert, R., Mulhaupt, R., Fiedlerová, A., Marcinčin, A., Ujhelyiová, A.: Influence of the fibre spinning process on structure and morphology of polypropylene/organoclay nanocomposite. In: 18th Proc. Int. Conf. ModPol 2003 SAV. Stará Lesná (SR), Oct. 5-8, 2003. Ed. SAV Bratislava, CDroom p. 79, ISBN 80-968433-2-X. (Po).

[24] Danko, M.*, Hrdlovič, P., Borsig, E.: Quenching of pyrene fluorescence as technique for charactersation of swelling interpenetrating polymer network. In: Proc.18th Int. Conf. ModPol 2003 SAV. Stará Lesná (SR), Oct. 5-8, 2003. Ed. SAV Bratislava, CDroom p. 107, ISBN 80-968433-2-X. (Po).

[25] Fiedlerová, A.*, Chmela, Š., Janigová, I., Kleinová, A., Borsig, E.: Polypropylene grafting in water dispersion. In: Proc. 18th Int. Conf. ModPol 2003 SAV. Stará Lesná (SR), Oct. 5-8, 2003. Ed. SAV Bratislava, CDroom p.115 29, ISBN 80-968433-2-X. (Po).

[26] Hrčková, Ľ.*, Lazár, M., Borsig, E., Ratzsch, M..: Effect of peroxide on degradation and build -up reactions in polypropylene. In: Proc. 18th Int. Conf. ModPol 2003 SAV. Stará Lesná (SR), Oct. 5-8, 2003. Ed. SAV Bratislava, Cdroom p. 109, ISBN 80-968433-2-X. (Po).

[27] Borsig, E.*, Lazár, M., Kleinová, A., Fiedlerová, A.: Is Polyethylene Free-Radical Crosslinking Based on a Simple Recombination Reaction? In: Book of Abstract. 2nd Int. Symposium. Reactive polymers in inhomogeneous systems, in melts and at interfaces. Dresden (Germany), Sep.{Oct. 28/1 (2003). Ed.TU Dresden, L 21 (2003). (Pr).

[28] Borsig, E.*, Pavlíková, S., Thomann, R., Reichert, R., Mulhaupt, R., Fiedlerová, A.: Fiber spinning from Poly/Propylene/Organoclay Nanocomposite. In: Book of Abstract. Europolymer Congres 2003, Stockholm (Swedwen), June 23-27, 2003. Ed. Royal Institute of Technology Stockholm, pp. 39-40 (2003). (Pr).

[29] Murárová, A., Jambrich,M.*: The influence of textile material composition on its physiological properties. In: 42nd International Man-Made Fibres Congress, Dornbir (Austria), Sept. 17-19.2003. (Pr).

C. Books and Textbooks [1] Marcinčin, A., Hudec, I., Majling, J.: Technológia materiálov. Technology of materials Vysokoškolské skriptum, STU

Bratislava, 2002, 183 strán. ISBN 80-227-1798-3 E. Others [1] Murárová, A.: Fyzikálna modifikácia vlákien. Habilitačná práca, STU-FCHPT. 233 s., Bratislava (2002).

DEPARTMENT OF FOOD SCIENCE AND TECHNOLOGY

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Head of Department: Telephone: ++421252926055 Assoc. Prof. Štefan Schmidt, PhD Fax: ++421252493198


I.STAFF

Full Professors: Alexander Dandár, PhD, DSc Associate Professors: Jozef Augustín, PhD; Ladislav Dodok, PhD; Jarmila Hojerová, PhD; Jolana Karovičová PhD; Štefan Schmidt, PhD Assistant Professors : Gabriel Greif; Mária Greifová, PhD; Zlatica Kohajdová, PhD; Marta Kostičová; Vladimír Mastihuba, PhD; Stanislav Sekretár, PhD; Ladislav Staruch, PhD Research Fellows: Zuzana Smelíková, PhD PhD Students: Dagmar Bilaničová; Lucia Güllová; Helena Kanďárová; Kristína Kukurová; Denisa Lauková; Drahomíra Lukáčová; Ivana Niklová; Marek Vajdák Technical staff: Katarína Halásová; Jarmila Mikletičová; Helena Morávková; Margita Piatriková; Gabriela Sisáková;


A. Teaching laboratories: Laboratory of Sugar Technology Laboratory of Starch Chemistry and Technology Laboratory of Cereal Technology Laboratory of Canned Products Laboratory of Meat and Meat Products Laboratory of Food Preservation Laboratory of Milk Chemistry and Technology Laboratory of Cosmetology

B. Research laboratories: Laboratory of Sugar Technology Laboratory of Starch Chemistry and Technology Laboratory of Cereal Technology Laboratory of Canned Products Laboratory of Meat and Meat Products Laboratory of Milk Chemistry and Technology Laboratory of Cosmetology Laboratory of Food Preservation


5. semester (Bc) Fundamentals of Food Technology 2/0/0 Karovičová Fundamentals of Hygiene and

Sanitation 1/1/0 Hojerová

6. semester (Bc) Fats and Oleo Chemistry 1/1/0 Schmidt, Sekretár Packaging and Packaging Materials 1/1/0 Sekretár Cosmetic and Household Chemistry 1/1/0 Hojerová Semester Project 0/0/4 all members of the staff 1. semester (MSc) Food Engineering 2/0/1 Schmidt Chemistry and Technology of

Saccharides 2/0/2 Dodok, Kostičová

Theory of Food Preservation 3/0/1 Greif Dairy Technology I. 2/0/0 Greifová, Mastihuba


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1. semester (MSc) Laboratory Practice of Dairy Technology I.

0/0/2 Greifová, Mastihuba

Semester Project 0/0/5 all members of the staff 2. semester (MSc) Cereal Chemistry and Technology 4/0/1 Dodok Sugar Technology 4/0/0 Dandár Laboratory of the Specialization I. 0/0/4 all members of the staff Preserved and Frozen Food

Technology 2/0/1 Karovičová, Greif

2. semester (MSc) Meat and Poultry Technology I. 2/0/1 Staruch Raw Materials for Canning Industry 2/0/0 Karovičová, Staruch Laboratory of the Specialization I. 0/0/5 Staruch, Greif, Kohajdová Karovičová Fats, Detergents and Oleochemicals 4/0/0 Schmidt, Sekretár 2. semester (MSc) Laboratory Practice of Fats,

Detergents and Oleochemist 0/0/3 Sekretár, Hojerová

Dairy Technology II. 2/0/0 Mastihuba, Greifová Laboratory Practice of Dairy

Technology II. 0/0/3 Mastihuba, Greifová

Microbiology of Milk, Fats and Cosmetics

1/0/0 Greifová

2. semester (MSc) Semester Project 0/0/5 all members of the staff Manufacturing Practice 3. semester (MSc) Chemical Engineering Processes in

Saccharide Technology 2/0/0 Dandár

Technology Optimising in Canning Industry

1/0/1 Greif

Laboratory of the Specialization II. 0/0/4 Staruch, Kohajdová, Karovičová, Greif Semester Project III. 0/0/5 all members of the staff 3. semester (MSc) Chemistry and Technology of

Cosmetics 2/0/2 Hojerová

Laboratory Practice of Microbiology of Milk, Fats and C

0/0/2 Greifová

Laboratory of the Specialization II. 0/0/4 Meat and Poultry Technology II. 2/0/0 Staruch 3. semester (MSc) Laboratory of Meat and Poultry

Technology II. 0/0/2 Staruch

By-products inFood Industry 2/0/0 Augustín PC Application in Food Industry 2/0/0 Sekretár Laboratory of PC Application in Food

Industry 0/0/2 Sekretár

IV. URRENT RESEARCH PROJECTS

A. VEGA Project No 1/9133/02 Development, optimising and control of new food products with the aim to increase the food quality using biological active substances and modern technologies (Alexander Dandár)

Contamination level in extractor during saccharose extraction from sweet cossets was analysed. The content of substances in thick juice caused the incrustation in evaporator was modified by SUCAZUR biocide. The progress was made in analysis of cabbage juice during spontaneous and artificial managed fermentation. The content of lysine in rolls was increased about 1/3 by using of suitable additives. Significant results were obtained in the study of natural colorants with antioxidative properties on the quality of selected raw materials of plant origin. Original results were gained in utilization of natural antioxidants in their application in selected foods of plant and animal origin. Microbial quality of spices used without heat treatment was verified. An effect of lactic acid addition applied on the surface of butcher’s meat with the aim to extend its shelf life was evaluated. Effect of chickpea and amaranth fractions on rheological properties of the dough was studied. Optimal addition of these fractions with the aim to improve the quality of bred was analysed. Project duration: from 2002 to 2004

B. VEGA Project No 1/9132/02 Processes and factors having the influence on durability and safety of foods and on household chemistry (Š.Schmidt)

Principles of predictive microbiology in the evaluation of hygienic safety of food were used. Mathematical modelling of growth of hygienically relevant microorganisms in model systems, in food and in emulsion systems was worked out. Influence of biogenic elements, heavy metals and other biologically active substances on food quality with regard to properties of relevant raw materials, intermediates and final products were studied. Modification of food properties in fresh and preserved state was analysed.


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Correlation of microbial and physical - chemical parameters of quality of bovine and caprine milks was worked out. Influence of external and internal environmental determinants on micro flora and sensory properties during storage of durable cereal products was studied. Isolation, modification, characterisation of plant antioxidants and their use for stabilisation of selected types of fats and oils were realized. Antibacterial, antifungal and antiviral activities of isolates from frequent seasoning as well as employment of plant extractive substances in dairy products to stabilize their quality and durability were tested. Fast and selective methods for determination of indicators of over processing and for evaluation of food quality factors and the verification of methods for evaluation of effectiveness and safety of stabilizers and other permitted substances for cosmetic products according to legislation of Slovak Republic and European Community were developed. Project duration: from 2002 to 2004

C. VEGA Project No 1/0102/03 Probiotic bacteria and non-traditional raw materials in production of functional foods with aim to increase their nutritive parameters (J.Karovičová)

Project is concerned to the study of application of Lactobacillus bacteria as well as Saccharomyces cerevisiae yeasts in production of functional foods on the base of different type of lactic fermented vegetable juices. In production there were studied the following substances: organic acids, especially lactic, acetic and citric acids, as well as biogenic amine presence, (histamine, tyramine, kadaverine and putrescine ). Samples were analysed by capillary isotachophoresis with following validation of the method. Project duration: from 2003 to 2005

VI. COOPERATION A. Cooperation in Slovakia


Duration

Ministry of Agriculture of Slovak Republic, Bratislava

Consultations, grant No. 524 and 526 (13a and 13b)

Staruch,L Karovičová,J Schmidt,Š

from 2003

Food Research Institute, Bratislava

Member of editorial board of Bull. of Food Fesearch Dandár,A continue

Slovak Academy of Sciences, Bratislava

Modification of sachcarides development of biosensors Mastihuba,V from 2000

Research Institute of Plant Production, Piešťany

Food Quality and Safety Mastihuba,V 2003

TAURIS, Rimavská Sobota

Development and inovation of new meat products Staruch,L continue

Rajo, Co, Bratislava Development of improved the quality and safety control of dairy products (Z. o D. 56/2003 + 128/2003)

Hojerová,J continue

Palma – Henkel, Co, N.Mesto nad Váhom Educational process Schmidt,Š

Sekretár, S continue

Palma – Tumys, Bratislava

Educational process Schmidt,Š Sekretár,S continue

Institute of Dairy Research, Žilina

Consultation, development of improvement control of food safety for industry

Greifová,M Mastihuba,V Greif,G

continue

Slovak Society of Cosmetology, Bratislava

Co-operation at the Scientific Conferences Hojerová,J continue

ADIPO Ltd, Nitra Consultation Dodok,L continue Central Laboratory Milex – Progres, Co, Bratislava

Consultation Greifová,M Mastihuba,V continue

Dairy Plant, Levice Consultation Greif,G Mastihuba,V continue

De Miclén, Co, Levice Consultation of cosmetics safety Hojerová,J continue

Q-CHEM, Modra Modification of saccharides Bilaničová,D Mastihuba,V 2002-2003


86



Duration

NCAUR (National Centre for Agricultural Utilization Research), ARS, USDA, Peoria, IL, USA

Enzymatic modification of saccharides, publications Mastihuba,V 1998-2003

BBSRC Institute of Food Research, Norwich, UK

Development of improved control of food safety for industry

Mastihuba,V Greifová,M continue

Department of Saccharides Technology, Prague, Czech Republic

Publications Dandár,A continue

Dublin City University, Biomedical and Environmental Sensor Technology Centre, Dublin, Ireland


Mastihuba,V Greifová,M continue

Institute of Chemical Technology, Dep. of Dairy and Fat Technology, Prague, Czech Republic

Natural antioxidants

Schmidt,Š Mastihuba,V Greifová,M Sekretár,S

continue

Zentralstelle zur Erfassung und Bewertung von Ersatz- und Ergänzungsmethoden zum Tierversuch (ZEBET)

Development of the safety of cosmetics methods Kanďárová,H 2003

Milcom-Dairy Research Institute, Prague, Czech Republic


Greifová,M Mastihuba,V continue

Institute of Food Research, Manchester, UK

Research of Antioxidants Schmidt,Š Sekretár,S continue

Akademia Rolnicza, Krakow, Poland Cooperation Dandár,A continue

Zuckerforschungsinstitut Tulln, Austria Cooperation Dandár,A continue

Technical University, Lodž, Poland Cooperation Dandár,A continue

Research Institute of Sugar Technology, Prague, Czech Republic

Member of editorial Board of Sugar Papers Dandár,A continue



Valid date

Dodok,L Slovak Academy of Agricultural Sciences, Bratislava member from 1995

Dodok,L Slovak Institute of Technical Normalisation, Bratislava member 2003

Dodok,L Slovak Agricultural Academy, Nitra member continue Schmidt,Š Slovak CHemical Society member continue Schmidt,Š Editorial board of Bull. of Food Research member continue Schmidt,Š Committee of the Slovak Chemical Society member continue

Schmidt,Š Grant Agency of MŠ SR and SAV, editorial board VEGA No. 10 member continue


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Staruch,L Slovak Society of Agricultural, Forestry, Food and Veterinary Sciences, Bratislava member continue

Staruch,L Foundation SLOVAK GOLD, Bratislava member continue Staruch,L The Union of Slovak Butchers member continue

Staruch,L Slovak Institute of Technical Normalisation, Bratislava member 2003

Staruch,L Judge expert for Food Sciences for specialisation Food processing, development and food products member from 1999

Staruch,L. Committee DANUBIUS GASTRO member 2003

Augustín, J Slovak Society of Agricultural, Forestry, Food and Veterinary Sciences, Bratislava member continue

Hojerová,J Foundation SLOVAK GOLD, Bratislava member continue

Hojerová,J Incheba, Joint Stock Company-Technical Committee for Cosmetics member continue

Hojerová,J Slovak Society of Cosmetology president 1.1.2000-current

Hojerová,J Commission for Technical Standards No 79 (Cosmetics) of Slovak Institute for Technical Standards

member continue

Hojerová,J Editorial board of DERMA (The Scientific Journal for Dermatologists) member continue

Hojerova,J Editorial board of DERMA Revue (Journal for Cosmeticians and Cosmetic producers) member continue

Kanďárová,H Slovak Society of Cosmetology member 1.6.2002- current Greifová,M Slovak Chemical Society member from 1999 Greifová,M Scientific board of VÚM, Žilina member from 1.6. 2003 Mastihuba,V Slovak Chemical Society member continue

Dandár,A Slovak Society of Agricultural, Forestry, Food and Veterinary Sciences, Bratislava president continue

Dandár,A Slovak Academy of Agricultural Sciences, Bratislava member continue

Dandár,A Slovak Academy of Technical Sciences, Bratislava member continue

Dandár,A Slovak National Committee of International Commission for uniform methods of sugar analysis - ICUMSA

member continue

Dandár,A Slovak Agricultural Academy Nitra member continue Dandár,A SAPV, specialization of Food vice-president continue Dandár,A Editorial board of Bull Food Research member continue



Valid date

Dodok,L International Assotiation for Cereal science and Technology member from 1996

Schmidt,Š. Federation of European Chemical Societes, division of Food Chemistry member continue

Schmidt,Š Editorial board of European Journal of Lipid Science and Technology member continue

Staruch,L Editorial board for journal MASO member 2003 Staruch,L WEPSA - world poutry scientific association, Israel member continue Augustín,J Czechoslovak Microbiology Society member continue

Hojerová,J The International Federation of Societes of Cosmetic Chemists, USA member continue

Greifová,M Czechsloval Microbiology Society member continue Dandár,A American Chemical Society member continue

Dandár,A International Commission for Uniform Methods of Sugar Analysis - ICUMSA, Italy member continue

Dandár,A Commission International Technique de Sucrerie - CITS, Brussels, Belgium member continue

Dandár,A Verein der Zuckerfabriken Ostereichs, Vienna, Austria member continue Dandár,A Stowarzysesnie Technikov Cukrownikow, Wroclaw,Poland member continue Dandár,A Cooperation with industry, VR FCHPT VŠCHT Praha member continue

Mastihuba,V The Federal agricultural Centre, FAL, Braunschweig, Germany member continue


88



Date / Duration

Assoc. Prof. V. Filip, PhD. VŠCHT, Praha CZ June 2003/1 week

Assoc. Prof. M. Plecká, PhD. VŠCHT, Praha CZ June 2003/1 week

Assoc. Prof. P. Štern, PhD.

Institute of Hydrodynamics, Academy of Science of Czech Republic, Praha CZ 2.-3..9.2003/2days

MSc., Tramutola Barbara University of Partenza IT october-november

2003/10 days Dr. G. L.Coté ARS USDA, NCAUR, Peoria IL, USA 19.9.2003/1 day



Date / Duration

Kanďárová,H Zebet, Germany, Berlin, --scientific stadge Germany 1.5.2003-current Mastihuba,V Schmidt,Š Kostičová,M Dandár,A Gullová,L

Agrana Hohenau Austria 2003/1 day

Hojerová,J The Council Meeting of Committies of the Czech Society of Cosmetology, International Federation of Cosmetology, České Budejovice

CZ 3.-5.11.2003/3 days

Dandár,A Commission International Technique de Sucrerie - CITS, Brussels Belgium february, december

2003/5 days

Dandár,A 22. International Congres Commission International Technique de Sucrerie - CITS, Azucarera Ebro, Gualdalfeo SL, Madrid

Spain 18.5-2.6.2003/ 12 days

VII. THESES AND DISSERTATIONS A. Graduate Theses (Bc Degree) for state examinations after three years of study

Name Title of Thesis Supervisor Adamová, A. Spices and mixtures of spices Karovičová,J.

Bajúsová, B. Hygienical level of cosmetic products in Slovakia according to analyses of ŠZÚ Hojerová,J.

Čimbora, J. Characterisation and using of new species of fruits Karovičová,J. Debnárová, K. Sulphate raw materials for silicaty industry Svetík,Š. Jancurová, M. All about the sugar Dandár,A.

Kantorová, M. Antropozoonoses-BSE, occurrence, characteristic and case for meat consumation Staruch,L.

Kočišová, E. Taste and odour compounds of selected species of preserving raw materials Kohajdová,Z.

Koštálová, Z. Importance of pseudocereals in food manufacture and nutrition Dodok, L. Krajčová, E. Emulgated fats in food manufacture Schmidt,Š. Molnárová, E. Importance and function of flavonoides in nutrition Schmidt,Š.

Lešková, L. Antropozoonoses-ANTRAX-diseases pestilentially from animals to humans Staruch,L.

Ondrušek, P. Hygienic levelof cosmetical products on the Slovak market Hojerová,J. Peterková, Z. By-products formed in complex of agricultural and food processing Augustín,J. Plencnerová, S. Enzymatic change of lactose to compounds with surface activity Mastihuba,V. Poláková, L. Using of lactose Mastihuba,V. Rolínová, J. Microbiological acceptance of cosmetics products-actually questions Hojerová,J. Šimonová, I. Adulteration of food products Kukurová,K. Stojnev, S. Manufacture of functional foods Lukáčová,D.

Sulová, Z. Methods of safety evaluation of cosmetical compounds-synthetic dermal models Kanďárová,H.

Tkáč, R. Fishes and their technological processing Karovičová,J. Turčániová, I. Phototoxicity of cosmeticcompounds and Kanďárová,H.


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Achejev, V. Analysis of amino acids and polyphosphates content in selected poultry products. Staruch,L.

Bršelová, I. Utilization of capillary isotachophoresis for autentification of fruit juices. Karovičová,J. Čierniková, A. Protection of fats with packaging. Sekretár,S. Darnetová, L. Peroxidase as a base substance of oxidase biosensors. Mastihuba,V. Fábiánová, B. The stability of photoprotective substances. Hojerová,J.

Güllová, L. Efficiency verification of disinfecting and antiincrusting agents (SUCAZUR type) in sugar factory. Dandár,A.

Hubináková, K. Comparison of a classic method for living cells determination with the fast microsheet one in the process of growth monitoring of Listeria spp. Greifová,M.

Janočková, O. Time-intensity study of selected flavours. Karovičová,J. Jašeková, M. Lipid stabilization in microwave heating. Sekretár,S. Kalafusová, G. Study of microbiologic profile in selected poultry products. Staruch,L. Kaufmanová, J. The enzyme preparations for biosurfactans production from saccharides. Mastihuba,V.

Lešková, E. The growth and production of biogenic amines by Enterococcus faecium. Greifová,M.

Ližičárová, I. Antioxidative effect of plant origin lycopene. Schmidt,Š. Magdošková, Z. Galactose preparation from lactose. Mastihuba,V.

Mazáň, M. Effect of additives on the properties of final product made from frozen dough. Dodok,L.

Najšlová, M. The effect of NaCl and pH on the growth and production of amines by Enterobacter aerogenes. Greif,G.

Plevková, I. Organic acids determination in lactic acid fermented vegetable juices. Kohajdová,Z. Pokrievka, M. Microbiological outcome of lactic fermentation. Lauková,D. Priehodová, S. Analysis of hemicelluloses effect on starch properties. Dodok,L.

Rácová, J. Validation of the control methods of conservation substances used in cosmetic preparations within government health control. Hojerová,J.

Slezáková, P. Assessment of the wheat meal quality. Dodok,L. Süli, J. Analytical and sensory evaluation of tealeaves. Audustín,J.

Šamajová, Ľ. Thyramine production by Enterococcus faecium 106 in dependence on the medium. Greif,G.

Vajdák, M. Isolation and characterisation of lycopene from tomato paste. Schmidt,Š. Vreštiaková, J. Decreasing of foaming quality of egg white by enzyme hydrolysis. Hrčková,M. Zlacká, S. Study of microbiological contamination in extractor. Kostičová,M.


Kohajdová,Z. Analysis of selected metabolites of microorganisms in the lactic acid fermented vegetable juices by capillary isotachophoresis Karovičová,J.


[1] Filip, V., Plocková, M., Šmidrkal, J., Špičková, Z., Melzoch, K., Schmidt, Š.: Resveratrol and its antioxidant and antimicrobial efectiveness. Resveratrol and its antioxidant and antimicrobial efectiveness. Food Chemistry 83 (2003) 585–593.

[2] Horáková, K., Greifová, M., Seemannová, Z., Gondová, B., Wyatt, G. M.: A comparison of the traditional mathod of counting viable cells and a quick microplate method for monitoring the growth characteristics of Listeria monocytogenes. Letters in Applied Microbiology (2003)

[3] Hozová, B., Kukurová, K., Dodok, L.: Application of transglutaminase and fermizyme for sensory quality improvement of pastry. Nahrung/Food 47(3), 171-175 (2003).

[4] Karovičová, J., Kohajdová, Z., Šimko, P., Lukáčová, D.: Using of capillary isotachophoresis for determination of biogenic amines and D-isocitric acid in food products. Nahrung/Food 47 (3), 188-190 (2003)

[5] Schmidt, Š., Niklová, I., Pokorný, J., Farkaš, P., Sekretár, S.: Antioxidant activity of evening primrose phenolics in sunflower and rapeseed oils. Eur. J. Lipid Sci. Technol. 105, 2003, s. 427-435.

[6] Lauková, D., Valík Ľ., Görner, F.: Effect of lactic acid on the growth dynamics of Candida maltosa YP1. Effect of lactic acid on the growth dynamics of Candida maltosa YP1.Czech J. Food Sci., 21, 2003: 43-49.

[7] Karovičová, J., Kohajdová, Z.: Lactic acid fermented vegetable juices. Hort. Sci. 30 (4), 158-164, (2003). [8] Karovičová, J., Kohajdová, Z., Greifová, M., Lukáčová, D., Greif, G.:Porovnanie fermentácií zeleninových štiav. Bull

PV 41 (3), 197-213, (2003). [9] Karovičová, J., Kohajdová, Z., Lukáčová, D.: Využitie kapilárnej izotachoforézy na stanovenie biogénnych amínov

vo vybraných potravinárskych výrobkoch. Bull PV 41 (3), 187-195, (2003). [10] Lauková, D., Valík. Ľ.: Kvantitatívna analýza vplyvu substrátu a teploty na rast kvasinky Candida maltosa YP1

Quantitative analysis of growth Candida maltosa YP1 in dependance on substratum and temperature Bulletin potravinárskeho výskumu, 42, 2003, č. 4, s. xxx.


90

[11] Lauková, D., Valík Ľ., Görner, F.: Heat Resistance of vegetative cells of Candida maltosa YP1. Agriculture Agriculture (Poľnohospodárstvo), 49 (7), 2003: 375-380.

[12] Schmidt, Š., Šardzíková, I., Sekretár, S.: Výskyt, štruktúra a účinok prírodných antioxidantov. Influence, structure and activity of natural antioxidants. Bull. Potrav. Výsk. (Bull. Food Res.), 41, 2002, č. 4, s. 221-239.

[13] Šardzíková, I., Schmidt, Š., Farkaš, P., Sekretár, S., Kováč, M.: Isolation and antioxidant activity of phenolic compounds of evening primrose (Oenothera biennis L.). Bull. Potrav. Výsk. (Bull. Food Res.), 41, 2002, č. 4, s. 241-253.

[14] Greifová, M., Greif, G., Lešková, E., Mériová, K.: Enterokoky-ich hodnotenie v mliekarenskej technológii. Enterococci- their evaluation in milk technology. Mliekarstvo, 34 (2),42-45, (2003).

[15] Greifová, M., Greif, G., Novoroľníková, B., Kubová, A.: Biogénne amíny v mliečnych výrobkoch a ich tvorba enterokokami. Biogenic amines in milk products and their production by enterococci. Mliekarstvo, 34 (4),31-33, (2003).

[17] Hojerová, J., Traubnerová, K., Novotná, E.: Globálna harmonizácia legislatívy v oblasti kozmetiky a označovanie zložiek. Global harmonisation of cosmetic regulation and INCI labelling of ingredients. DERMA - interdisciplinárny časopis pre dermatovenerológiu a príbuzné odbory, III, 2, 2003 24-29

[18] Greifová, M., Mastihuba V.: Svetový deň mlieka na FCHPT STU v Bratislave. World Dairy Day at the Faculty of Chemical and Food Technology of Slovak University of Technology in Bratislava. Mliekarstvo 34(2), 7 - 8 (2003)

[19] Hojerová, J.: Účinné látky kozieho mlieka v kozmetike. Biological active ingredients of goat´s milk in cosmetics. Mliekarstvo 34 (4), 46-48, (2003)

[20] Schmidt, Š.: Vedecke a pedagogicke aktivity FCHPT v oblasti mliekarenstva. Mliekarstvo 34 (3), 19-22 (2003). [21] Dodok, L.: Z činnosti katedry potravinárskej technológie FCHPT STU Pekárstvo, Cukrárstvo 4(2), s.12 (2003). [22] Hojerová, J., Kanďárová, H.: Vyznáte sa v sortimente kozmetických prostriedkov ? 1.časť. Do you be familiar with

the cosmetic products ? Derma Revue,1,(1), 11-12, (2003) [23] Hojerová, J., Traubnerová, K., Novotná, E.: Ingredienty pre výrobu kozmetických prostriedkov Ingredients for

cosmetic products production. Derma Revue,1,(1), 24-25, (2003) [24] Hojerová, J.: Dekoratívna kozmetika. The decorative cosmetics. Slovenský Výber 7, (1), 13, (2003) [25] Hojerová, J.: Olej z hroznových semienok v kozmetike. Grape Seed oil in cosmetics Vinohrad 41 (6), 6-7, (2003) [26] Hojerová, J.: Solárna kozmetika - fotoprotektívne látky. The sunburn cosmetics- photoprotective ingredients.

Slovenský Výber 7, (7), 12-13,(2003) [27[ Hojerová, J.: Špecifiká pánskej kozmetiky. Specifies of cosmetics for men. Slovenský Výber 7, (9), 12-13,(2003) [28] Hojerová, J.: Vonná kozmetika - súčasť imidžu. The fragrance cosmetics - the part of the image. Slovenský Výber

7, (12), 20-21,(2003) [29] Hojerová, J.: Vyznáte sa v sortimente dekoratívnej kozmetiky ? Do you be familiar with the decorative cosmetics ?

Derma Revue,1,(4), 24-25, (2003) [30] Hojerová, J.: Vyznáte sa v sortimente vonnej kozmetiky ? Do you be familiar with the fragrant cosmetics ? Derma

Revue,1,(3), 18-21, (2003) [31] Mastihuba, V., Greifová, M.: Svetový deň mlieka na Fakulte Chemickej a Potravinárskej Technológie STU. World

Dairy Day at the Faculty of Chemical and Food Technology of Slovak University of Technology in Bratislava Infoservis v potravinárstve č.39, 15 (2003)

[32] Traubnerová, K., Hojerová, J.: Kozmetické prostriedky pre zimné obdobie. Cosmetics for the winter seasion. Derma Revue,1,(4), 10-11, (2003)

B. Conferences [1] Greifová, M.*, Greif, G., Lešková, E.: Growth and production of tyramine by Enterococcus faecium 106. In: 55.

zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 791, 2003. [2] Hudecová*, D., Ditteová, P., Valigura, D., Augustín, J., Melník, M.: Some new salicylatocopper (II.) complexex and

their biological properties. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 650, (2003).

[3] Karovičová, J., Kohajdová, Z., Lukáčová, D., Bršelová, I., Kukurová, K., Plevková, I.: Authentication of orange juices. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97 (8), 788, (2003).

[4] Kohajdová, Z., Karovičová, J., Lukáčová, D., Kukurová, K.: Fermentation of cabbage-garlic juices. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97 (8), 789, (2003).

[5] Lukáčová, D., Kohajdová, Z., Karovičová, J., Greifová, M., Kukurová, K., Greif, G., Plevková, I.: Fermentation of cabbage juices with inulin addition. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97 (8), 788, (2003).

[6] Bilaničová, D., Mastihuba, V., Kaufmanová, J., Mastihubová, M., Schmidt, Š.: Enzymatic synthesis of alkyl glycosides. In: 55. zjazd chemických spoločností, 8. - 12. september 2003, Košice, Chem. Listy 2003, 97(8) 784. (Pr).

[7] Hrčková, M., Zemanovič, J., Schmidt, Š*.: Influence of extrusion on hydrolysis of potato proteins. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 2003, 97 (8) 779. Pr.

[8] Kopecký,J*, Dandár, A., Bubník, Z., Pawlowski, B.: Mikrobiologická kontrola extrakcie sacharózy, kontrola inkrustácie v odparke a proces kontinuálnej iónovej separácie ISEP Microbiology Control of Sucrose Extraction, Incrustation Control of Evaporation and Continuous Ionic Separation Process ISEP. In: Comp. Rend. 22th General Assembleé C.I.T.S Madrid, May 18.-22. 2003, Verlag Dr.A. Bartens, KG., Berlin 2003, s. 228-234 ISBN

[9] Lauková, D., Valík, Ľ., Görner, F., Schmidt, Š*.: Quantitative analysis of acid tolerance Candida maltosa YP1 In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 2003, 97 (8) 794. Pr.

[10] Sekretár, S*., Schmidt, Š., Šardzíková, I.: Computer aided monitoring of fat interesterification. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 2003, 97 (8) 784. Pr.

[11] Sekretár, S*., Schmidt, Š., Šardzíková, I.: Oxidative stability of vegetable oils stored in various packaging materials. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 2003, 97 (8) 783. Pr.


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[12] Schmidt, Š*., Sekretár, S., Vajdák, M.: Possible health benefits of natural lycopene. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 2003, 97 (8) 782-783. Pr.

[13] Staruch, L., Volanský, P., Budajová, J., Pipek, P., Greif, G., Mastihuba, V.: Polyphosphates in meat products In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy, 97(8), 780 (2003). (Pr)

[14] Bilaničová, D., Garajová, E., Schmidt, Š., Mastihubová, M., Mastihuba, V.: Enzýmové modifikácie laktózy. Enzymatic modifications of lactose. In.: Zborník prednášok zo semináru Mléko a sýry 2003, Praha, 21.-22. januára 2003, ISBN 80-86238-31-8, KAN 978-80-86238-31-9, s. 107-112

[15] Božiková, K., Darnetová, L., Mastihuba, V.: Vývoj biosenzora pre stanovenie laktulózy. Development of biosensor for estimation of lactulose. In.: Zborník prednášok zo semináru Mléko a sýry 2003, Praha, 21.-22. januára 2003, ISBN 80-86238-31-8, KAN 978-80-86238-31-9, s. 118-123

[16] Dandár, A.*,Kostičová, M., Hybenová, E: Stanovenie mikrobiálnej aktivity v extraktore cukrovaru Determination of Microbial Activity in Extraktor of Sugar Factory. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97 (8), 791 (2003).

[17] Karovičová, J., Kohajdová, Z.*, Bršelová, I., Kukurová, K.: Using of isotachophoresis for authentication of orange juices. In: 15. Int. Conf. Chromatogr. Methods and Human Health. Piešťany november 2003. s. 79-80 ISBN 1335-5236

[18] Augustín, J.*, Patoprstá, I., Hudecová D.: Senzorické hodnotenie fermentovaných, polofermentovaných a opakovane fermentovaných listov čajovníkok (Camelia sinensis). Sensory evaluation of the fermentation, poly- and repeated fermentation of the tea leaves (Camellia sinensis). In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97(8), 793 (2003).

[19] Augustín, J., Hudecová, D., Patoprstá, I.: Stanovenie kofeínu a ťažkých kovov v listoch čajovníka (Camellia sinensis). Determination of cofein and heavy metals contents in tea leaves (Camellia sinensis). In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 2003, 97 (8) 792.

[20] Augustín, J., Hudecová, D.: "Fungálny beta-1,3-D-glukán ako potravinový doplnok, izolát z hlivy ustricovitej (Pleurotus ostreatus); chemická štruktúra, zdroje a niektoré farmakologické účinky. " "Fungal ß-1,3-D-glucan as a food supplement isolated from mushroom (Pleurotus ostreatus); chemical structur, sources and some farmacological effects. " In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97 (8),781-782 (2003).

[21] Kohajdová, Z.*, Karovičová, J., Greifová, M., Greif, G., Lukáčová, D.: Using of isotachophoresis for analysis of various lactic acid fermented vegetable juices. In: 15. Int. Conf. Chromatogr. Methods and Human Health. Piešťany november 2003. s. 39-40 ISBN 1335-5236.

[22] Pokorný, J*., Schmidt, Š.: Antioxidanty a jejich význam v potravinařské technologii a ve výživě. Antioxidant and their importance in food technology and nutrition. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 2003, 97 (8) 781. Pr.

[23] Šimon, P.*, Cvengroš, J., Schmidt, Š.: Study of Edible Oil Oxidation by DSC. Study of Edible Oil Oxidation by DSC. "In: Proc. Int. Conf. ""Food Safety and Quality in Transition Countries"", 23.-27.3.2003, Nitra, 4 pgs."

[24] Sekretár, S., Kuniak, Ľ., Schmidt, Š., Štefániková, Z*.: Hliva ustricovitá - významný zdroj imunomodulačného beta-1,3-glukanu. Oyster mushroom - significant source of beta-1,3-glucan. In: Zborník z konferencie Životné podmienky a zdravie, Štrbské pleso 11.-13.9.2002, ŠFZÚ SR, Bratislava 2003. CD verzia s. ISBN 80 - 7159 - 138 - 6, EAN 9788071591382. (Po).

[25] Sekretár, S., Schmidt, Š., Niklová, I., Štefániková, Z*.: Ochranný účinok obalov pri skladovaní jedlých olejov. Protetcive effect of packages during storage of edible oils. In: Zborník z konferencie Životné podmienky a zdravie, Štrbské pleso 11.-13.9.2002, ŠFZÚ SR, Bratislava 2003. CD verzia s.136-138. ISBN 80 - 7159 - 138 - 6, EAN 9788071591382. (Po).

[26] Sekretár, S., Schmidt, Š., Niklová, I., Štefániková, Z*.: Výživové aspekty oxidácie tukov. Nutrition aspects of fat oxidation. In: Zborník z konferencie Životné podmienky a zdravie, Štrbské pleso 11.-13.9.2002, ŠFZÚ SR, Bratislava 2003. CD verzia s. 126-129. ISBN 80 - 7159 - 138 - 6, EAN 9788071591382. (Po).

[27] Bilaničová, D., Mastihuba, V., Kaufmanová, J., Schmidt, Š.: Enzýmová príprava alkylglykozidov Enzymatic preparation of alkyl glycosides. In: XXXVI. Seminář o tenzidech a detergetech, Lázně Bohdaneč, 3.-5. 11. 2003, str. 15-22, ISBN 80-7194-595-1

[28] Bilaničová, D., Mastihuba, V., Lauková, D., Kaufmanová, J., Schmidt, Š.: Prírodné povrchovoaktívne látky. Natural surfactants. In.: Zborník zo 41. Medzinárodnej konferencie z technológie a analytiky tukov, 14.-16. mája 2003, Trenčianske Teplice, Vyd. Palma-Tumys 2003, s. 147-150. ISBN80-86238-32-6.

[29] Lauková, D.*, Valík Ľ., Görner, F., Schmidt, Š.: Dynamika rastu Candida maltosa v mlieku a smotane. Growth Dynamics of C. maltosa YP1 in milk and cream. "In: Celostátní přehlídky sýrů 2003. Výsledky přehlídek a sborník přednášek semináře Mléko a sýry 2003. Ed.: Štětina a kol., Česká společnost chemická, Praha, 2003, s.89-95. ISBN 80-86238-31-8; EAN 978-80-86238-31-9 (Pr)"

[30] Lauková, D.*, Valík, Ľ., Filip, V., Pokorná, I., Plocková, M., Schmidt, Š.: Dynamika rastu Candida maltosa YP1 v emulziách olej vo vode. Growth Dynamics of C. maltosa YP1 in O/W emulsions. In.: Zborník zo 41. Medzinárodnej konferencie z technológie a analytiky tukov, 14.-16. mája 2003, Trenčianske Teplice. Vyd. Palma-Tumys 2003, s. 134-139. ISBN80-86238-32-6.

[31] Lauková, D.*, Valík, Ľ., Görner, F., Leskovská, L., Martinická, L.: Dynamika rastu Bacillus cereus v mlieku a smotane. Growth Dynamics of B.cereus in milk and cream. "In: Celostátní přehlídky sýrů 2003. Výsledky přehlídek a sborník přednášek semináře Mléko a sýry 2003. Ed.: Štětina a kol., Česká společnost chemická, Praha, 2003, s.143-147. ISBN 80-86238-21-0; EAN 978-80-86238-21 (Pr)"

[32] Lauková, D., Valík, Ľ.*, Görner, F.: Vplyv teploty na dynamiku B. cereus v mlieku a smotane. Effect of temperature on growth dynamics of B. cereus in milk and cream. "In: Životné podmienky a zdravie. Zborník vedeckých prác. Ed.: Prof. Ághová, Štátny fakultný zdravotný ústav SR, Bratislava, 2003, s.144-147. ISBN 80-7159-138-6; EAN 978-80-71591382 "


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[33] Sekretár, S*., Földešiová, L., Schmidt, Š., Zemanovič, J.: Potravinárske emulgátory. Food emulsifiers. In XXXVI. seminář o tenzidech a detergentech. Sborník přednášek. Lázně Bohdaneč 3. - 5. 11. 2003. Universita Pardubice. str. 93-100. ISBN 80-7194-595-1. (Pr).

[34] Štefániková, Z*., Jurkovičová, J., Ševčíková, Ľ., Sekretár, S., Ághová, Ľ.: K problematike merania a hodnotenia depotného telesného tuku. On the problem of depot body fat measurement. In: Zborník z konferencie Životné podmienky a zdravie, Štrbské pleso 11.-13.9.2002, ŠFZÚ SR, Bratislava 2003. CD verzia s. ISBN 80 - 7159 - 138 - 6, EAN 9788071591382. (Pr).

[35] Abulgasem, F. M. A., Dodok, L., Trubač, K., Buchtová, V. Hozová, B., Starúch, L., Gajdošová, J.: Možnosti uplatnenia stabilizátora S 1 v pekárskej technológii. Utilization of S 1 stabiliser in baking technology. In: Zborník prednášok z XIV. Medzinárodnej konferencie o analytických metódach v potravinárstve „Laboralim 2003“. Banská Bystrica 18. – 19. februára 2003. Slovenská spoločnosť pre poľnohospodárske, lesnícke, potravinárske a veterinárske vedy pri SAV, Bratislava 2003. s.94-97, ISBN 80-227-1887-4.

[36] Abulgasem, F.M.A., Dodok, L.*: Aspekty trvanlivosti pekárskych výrobkov. Durability of bakery products. "In: Zborník prednášok zo XIV. Medzinárodnej konferencie o analytických metódach v potravinárstve, 18.-19.február 2003 B.Bystrica,""Laboralim 2003"", STU Bratislava, 2003,s.98 -101, ISBN 80 -227 - 1887 - 4"

[37] Augustín, J.*, Sűli, J., Patoprstá, I., Škrovánková, S.: Analytické a senzorické hodnotenie čajovníkových listov (Camellia sinensis). Analytical and sensory evaluation of the quality of tealeaves (Camellia sinensis). In: Laboralim 2003, Zborník prednášok z XIV. Medzinár. Konf. O anal. Metódach v potrav. 18. a 19.2.2003 v B. Bystrici, STU Bratislava, s. 107-114. ISBN 80-227-1887-4

[38] Bilaničová, D., Mastihubová, M., Kaufmanová, J., Schmidt, Š., Mastihuba, V.: Enzýmová príprava alkylglukozidov. Enzymatic preparation of alkyl glycosides. In.: Laboralim 2003, Banská Bystrica, 18. a 19. februára 2003, ISBN 80-227-1887-4, s. 115-118 (poster)

[39] Buchtová, V.*, Dodok, L., Jelušová, M.: Štúdium aminokyselinového zloženia v zmesi korenín používaných pri príprave kurčiat. Study of amino acids composition in the spice mixture for roasted chicken. In: Zborník prednášok z XIV. Medzinárodnej konferencie o analytických metódach v potravinárstve „Laboralim 2003“. Banská Bystrica 18. – 19. februára 2003. Slovenská spoločnosť pre poľnohospodárske, lesnícke, potravinárske a veterinárske vedy pri SAV, Bratislava 2003. s.126-128, ISBN 80-227-1887-4.

[40] Dandár, A., Dandár, R., Kostičová, M.*, Szabová,D.: Príspevok k hodnoteniu ICUMSA metód na stanovenie invertu v cukrovarníckych produktoch Report about the Evaluation of ICUMSA Methods of Invert Determination in Sugar Products. "In: Zborník prednášok zo XIV. Medzinárodnej konferencie o analytických metódach v potravinárstve, 18.-19.február 2003 B.Bystrica,""Laboralim 2003"", STU Bratislava, 2003,s.137-141, ISBN 80 -227 - 1887 - 4"

[41] Dandár, A.,Kostičová, M.*, Dolníková, M: Stanovenie stupňa kontaminácie počas extrakcie v cukrovare Determination of Contamination Degree during Extraction in Sugar Factory. "In: Zborník prednášok zo XIV. Medzinárodnej konferencie o analytických metódach v potravinárstve, 18.-19.február 2003 B.Bystrica,""Laboralim 2003"", STU Bratislava, 2003,s.142-147, ISBN 80 -227 - 1887 - 4"

[42] Dodok, L.*, Abulgasem, F.M.A., Trubač, K., Buchtová, V., Hozová, B., Staruch, L., Gajdošová, J.: Porovnanie dvoch spôsobov aplikácie emulgátora pri výrobe bežného pečiva. Comparison of two applications of emulsifier in production of cookies. "In: Zborník prednášok zo XIV. Medzinárodnej konferencie o analytických metódach v potravinárstve, 18.-19.február 2003 B.Bystrica,""Laboralim 2003"", STU Bratislava, 2003,s. 148 -151, ISBN 80 -227 - 1887 - 4"

[43] Dodok, L.*, Hozová B., Buchtová, V., Staruch L., Halabuková V.: Aplikácia transglutaminázy v cereálnej technológii. In: Zb. z XXXIV. Symposia o nových směrech výroby a hodnocení potravin. Skalský Dvur, 26.-28.5.2003,307-313. ISBN 80-902671-6-5. (Po)

[44] Francisciová, E., Hojerová, J. *, Purgelová, M.: Validácia HPLC metódy pre dôkaz fenolických antioxidantov. Validation of the HPLC method for the proof of the fenolic antioxidants. In: Zborník Medzinárodnej konferencie o analytických metódach v potravinárstve, Laboralim 2003, (Slovenská republika), Banská Bystrica, 3.-5. Február (2003), Vyd.: ,s.163-166, ISBN 80227-1887-4 (Po)

[45] Greifová, M.*, Greif, G., Kukurová, I., Karovičová, J., Kohajdová, Z.: Vplyv modelových podmienok na rast a produkciu biogénnych amínov mliekarensky významnými mikroorganizmami. Effect of model conditions on growth dairy-related mikroorganisms and their production of biogenic amines. "In: Zborník ""Mléko a sýry 2003"". Praha (ČR), január 2003, s. 134-138. ISBN 80-86238-31-8, EAN 978-80-86238-31-9"

[46] Hojerová, J. *,Francisciová, E., Rácová, J.: Bezpečnosť kozmetických prostriedkov. Stanovenie vybraných konzervačných látok. Safety of cosmetics - determination some of the preservatives. In: Sborník Mezinárodní kozmetologické konference (Česká republika), České Budejovice, 3.-5. Novembr (2003), Vyd.: Kosmetologická společnost České republiky, s.54-57, ISBN 80-239-1834-6 (Po)

[47] Hozová, B., *Staruch, L., Buchtová, V. , Dodok, L. : Zlepšenie akosti cereálnych výrobkov prídavkom mikrobiálnej transglutaminázy. In: Zborník prednášok z XIV. Medzinárodnej konferencie o analytických metódach v potravinárstve „Laboralim 2003“. Banská Bystrica 18. – 19. februára 2003. Slovenská spoločnosť pre poľnohospodárske, lesnícke, potravinárske a veterinárske vedy pri SAV, Bratislava 2003. s.192-196, ISBN 80-227-1887-4.

[48] Karovičová, J.*, Kohajdová, Z., Lukáčová, D., Bršelová, I., Plevková, I., Machárová, L.: Autentifikácia citrusových štiav ITP.In: Laboralim 2003, Zborník prednášok z XIV. Medzinár. Konf. O anal. Metódach v potrav. 18. a 19.2.2003 v B. Bystrici, STU Bratislava, s. 214-217. ISBN 80-227-1887-4

[49] Karovičová, J.*, Polonský, J., Kohajdová, Z., Lukáčová, D.: Využitie kapilárnej izotachoforézy na stanovenie cudzorodých látok. In: Laboralim 2003, Zborník prednášok z XIV. Medzinár. Konf. O anal. Metódach v potrav. 18. a 19.2.2003 v B. Bystrici, STU Bratislava, s. 210-213. ISBN 80-227-1887-4

[50] Koréneková, B., Kottfer, L., Skalická, M., Kottferová, J.,- *Staruch, L. : Bod mrznutia – dôležitý faktor v kvalite mlieka. In: Zborník prednášok z XIV. Medzinárodnej konferencie o analytických metódach v potravinárstve


- 93 -

„Laboralim 2003“. Banská Bystrica 18. – 19. februára 2003. Slovenská spoločnosť pre poľnohospodárske, lesnícke, potravinárske a veterinárske vedy pri SAV, Bratislava 2003. s.218-220, ISBN 80-227-1887-4.

[51] Kottferová, J., Pipová, H., Ondrašovič, M., Hvozdík, A., *Staruch, L. :Využitie ATP bioluminiscenčnej metódy pri kontrole mikrobiálnej kontaminácie výrobne. In: Zborník prednášok z XIV. Medzinárodnej konferencie o analytických metódach v potravinárstve „Laboralim 2003“. Banská Bystrica 18. – 19. februára 2003. Slovenská spoločnosť pre poľnohospodárske, lesnícke, potravinárske a veterinárske vedy pri SAV, Bratislava 2003. s.221-224, ISBN 80-227-1887-4.

[52] Kukurová, K.*, Karovičová, J.: Falšovanie vybraných potravinárskych výrobkov. In: Laboralim 2003, Zborník prednášok z XIV. Medzinár. Konf. O anal. Metódach v potrav. 18. a 19.2.2003 v B. Bystrici, STU Bratislava, s. 243-246. ISBN 80-227-1887-4

[53] Kukurová, K.*, Kohajdová, Z., Karovičová, J., Lukáčová, D., Greif, G.: Príprava zeleninových štiav a ich hodnotenie. In: Laboralim 2003, Zborník prednášok z XIV. Medzinár. Konf. O anal. Metódach v potrav. 18. a 19.2.2003 v B. Bystrici, STU Bratislava, s. 239-242. ISBN 80-227-1887-4

[54] Lukáčová, D.*, Karovičová, J.: Charakterizácia inulínu a jeho využitie. In: Laboralim 2003, Zborník prednášok z XIV. Medzinár. Konf. O anal. Metódach v potrav. 18. a 19.2.2003 v B. Bystrici, STU Bratislava, s. 259-262. ISBN 80-227-1887-4

[55] Lukáčová, D.*, Karovičová, J.: Netradičné druhy zeleniny ako zdroj funkčnej zložky potravín. In: Laboralim 2003, Zborník prednášok z XIV. Medzinár. Konf. O anal. Metódach v potrav. 18. a 19.2.2003 v B. Bystrici, STU Bratislava, s. 255-258. ISBN 80-227-1887-4

[56] Pipek, P., Sarnovský, L., Jeleníková, J., *Staruch, L.: Stanovení intramuskulárního tuku pomocí analyzy obrazu. In: Zborník prednášok z XIV. Medzinárodnej konferencie o analytických metódach v potravinárstve „Laboralim 2003“. Banská Bystrica 18. – 19. februára 2003. Slovenská spoločnosť pre poľnohospodárske, lesnícke, potravinárske a veterinárske vedy pri SAV, Bratislava 2003. s.281-286, ISBN 80-227-1887-4.

[57] Staruch, L.*, Cejpek, K., Dandár, A. : Wplyw BSE na spozycie miesa wolowego na Slovacji Žywność regionalna, Krakow, 16 – 17 czerwca 2003, TTŽ OM, 2003, s.74, ISBN 83-907553-5-1.

[58] Staruch, L.*, Achejev, V., Budajová, J., Vranková, R., Štullerová, Ľ.:Sledovanie obsahu bielkovín v morčacej šunke v rôznych regiónoch Slovenska. In: Sborník příspěvků XXXVI . Symposia o nových směrech výroby a hodnocení

[59] Augustín, J*: Biopolyméry polysacharidov ako aktívne zložky, vhodné pre kozmetiku. Biopolymers of the polysaccharides as active compounds available in the cosmetics. In: Zborník prednášok z Medzinárodnej kozmetologickej konferencie, Piešťany 9. – 11. 9. 2002

[60] Augustín, J.*, Sűli, J., Hudecová, D.: Stanovenie obsahu ťažkých kovov v čajovníkových listoch (Camellia sinensis) metódou AAS. Determination of heavy metals content in the tealeaves (Camellia simensis) by AAS method. In: Laboralim 2003, Zborník prednášok z XIV. Medzinár. Konf. O anal. Metódach v potrav. 18. a 19.2.2003 v B. Bystrici, STU Bratislava, s. 102-106. ISBN 80-227-1887-4

[61] Augustín, J.: Nové nealko nápoje zo skupiny ladových (instantných), bylinných, ovocných a čajových (Camellia sinensis) nápojov. New soft-drinks from the group of ice (instant), herbal, fruit and tea (Camellia sinensis) drinks. In: 2. ročník SOFT DRINK FORUM 2003, Medzinár. konferencia FÓRUM Nealko-priemyslu, Bratislava 20.3.2003

[62] Cejpek, K., *Staruch, L., Vajcíková, Z. : Regionalne produkty spožywcze na Slowacji. Žywność regionalna,Krakow, 16 – 17 czerwca 2003, TTŽ OM, 2003, s.21, ISBN 83-907553-5-1.

[63] Greif, G.*, Greifová, M., Karovičová, J., Kohajdová, Z.: Význam biogénnych amínov a ich obsah vo vybraných mliečnych produktoch. Importance of biogenic amines and their levels in selected milk products. "In: Zborník ""Mléko a sýry 2003"". Praha (ČR), január 2003, s. 66-70. ISBN 80-86238-31-8, EAN 978-80-86238-31-9"

[64] Greifová, M.*, Horáková, K.: Zohľadnenie rizík výskytu listérií v oblasti výroby syrov. Risk evaluation of Listeria sp. in cheese technology. "In: Zborník prednášok ""Zabezpečenie kvality syrov a ich kontroly v súlade s požiadavkami EÚ"". Rajecké Teplice, marec 2003, s. 11-18."

[65] Gullová, L.*,Dandár, A., Kopecký, J., Paulenová, Ľ.: Kontrola inkrustácie odparky a riadenie mikrobiálnej aktivity extrakcie prístrojom Microzym L a prípravkami Sucazur Comprehensive Scaling Control in Evaporation and Microbiological Control in Sucrose Extraction with the Microzym-L Enzymatic Device and SUCAZUR Agents. "In: Zborník prednášok zo XIV. Medzinárodnej konferencie o analytických metódach v potravinárstve, 18.-19.február 2003 B.Bystrica,""Laboralim 2003"", STU Bratislava, 2003,s.83 -93, ISBN 80 -227 - 1887 - 4"

[67] Ondrejka, J., *Staruch, L. : Nutnosť aplikácie systému HACCP v lahôdkárskej výrobe. In: Zborník prednášok z XIV. Medzinárodnej konferencie o analytických metódach v potravinárstve „Laboralim 2003“. Banská Bystrica 18. – 19. februára 2003. Slovenská spoločnosť pre poľnohospodárske, lesnícke, potravinárske a veterinárske vedy pri SAV, Bratislava 2003. s. 56-60, ISBN 80-227-1887-4.

[68] Sekretár, S., Schmidt, Š*.: Ochrana tukov obalom. Protection of fats with packaging. In: Zborník z XIV. Medzinárodnej konferencie Laboralim, B. Bystrica 18.-19.2. 2003, Staruch, L., Dandar, A. editori, Vydavateľstvo STU Bratislava 2003, s. 295-298. ISBN 80-227-1887-4. (Pr).

[69] Schmidt, Š*., Šardzíková, I., Vajdák, M., Sekretár, S.: Antioxidačná aktivita fenolických látok z pupalky dvojročnej (Oenothera Biennis L.). Antioxidant activity of phenolic compounds from evening primrose (Oenothera Biennis L.). In: Zborník z XIV. Medzinárodnej konferencie Laboralim, B. Bystrica 18.-19.2. 2003, Staruch, L., Dandar, A. editori, Vydavateľstvo STU Bratislava 2003, s. 35-41. ISBN 80-227-1887-4. (Pr).

[70] Staruch, L.*, Volanský, P., Lederleitnerová, J., Pipek, P., Jeleníková, J., Golián, J., Ondrejka, J. Analytické sledovanie najvyššie prípustného množstva polyfosfátov v mäsových výrobkoch. In: Zborník prednášok z XIV. Medzinárodnej konferencie o analytických metódach v potravinárstve „Laboralim 2003“. Banská Bystrica 18. – 19. februára 2003. Slovenská spoločnosť pre poľnohospodárske, lesnícke, potravinárske a veterinárske vedy pri SAV, Bratislava 2003. s.309-314, ISBN 80-227-1887-4.

[71] Kremnický, Ľ., Mastihuba, V., Côté, G. L.: T. reesei acetyl esterase catalyzed transesterification in water. T. reesei acetyl esterase catalyzed transesterification in water. In: BIOTRANS Olomouc 2003. 6th International Symposium on Biocatalysis and Biotransformations together with COST D25 Workshop, Olomouc, Czech Republic, June 28 -


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July 3 2003, poster P141, Chem. Listy 97, 443 (2003) [72] Buchtová, V.*, Dodok, L., Jelušová, M.: Štúdium aminokyselinového zloženia v zmesi korenín na prípravu kurčiat.

Study of amino acids composition in the spice mixture for roasted chicken. In: Sborník příspěvku XXXIV. Symposium o nových směrech výroby a hodnocení potravín. Skalský Dvúr, 26. –28. 5. 2003, ČR, VUP, Praha, s. 254 - 256, ISBN 80 - 902671 - 6 - 5.

[73] Buchtová, V.*, Dodok, L., Jelušová, M.: Štúdium aminokyselinového zloženia v zmesi korenín na ražnenie a na prípravu steikov a pečenie. In: Sborník příspěvku XXXIV. Symposium o nových směrech výroby a hodnocení potravín. Skalský Dvúr, 26. –28. 5. 2003, ČR, VUP, Praha, s. 252 - 254, ISBN 80 - 902671 - 6 - 5.

[74] Dodok, L.*, Hozová B., Buchtová, V., Staruch L., Halabuková V.: Aplikácia transglutaminázy v cereálnej technológii. In: Sborník souhrnu sdělení XXXIV. Symposium o nových směrech výroby a hodnocení potravín. Skalský Dvúr, 26. –28. 5. 2003, ČR, VUP, Praha , s.38.

[75] Hozová, B., Dodok,L*.: Senzorické hodnotenie pečiva vyrobeného z mraziarensky skladovaného cesta s prídavkom vybraných enzýmov. In : Sborník příspěvku XXXIV. Symposium o nových směrech výroby a hodnocení potravín. Skalský Dvúr, 26. –28. 5. 2003, ČR, VUP, Praha, s. 201- 203, ISBN 80 - 902671 - 6 - 5s

[76] Gullová, L.*,Dandár, A., Kopecký, J.,Paulenová, Ľ.: Prípravky SUCAZUR a globálny servis v cukrovare Trnava v kampani 2002/2003. SUCAZUR Agents and Global Service in Sugar Factory Trnava in 2002/2003 Cukrovarnícka konferencia2003,Luhačovice18.-19.3.2003

DEPARTMENT OF GRAPHIC ARTS TECHNOLOGY AND APPLIED PHOTOCHEMISTRY


Head of Department: Telephone: ++421252495276 Assoc. Prof. Michal Čeppan, PhD Fax: ++421252493198


I. STAFF Associate Professors: Michal Čeppan, PhD; Milan Mikula, PhD; Ján Panák, PhD; Assistant Professors : Vladimír Dvonka; Bohuslava Havlínová, PhD; Viera Jančovičová, PhD; Research Fellows: Zuzana Jakubíková; Juraj Kindernay, PhD; Milena Reháková, PhD; PhD Students: František Belányi (till 30. 11. 2003); Erika Hrehorová; Ivana Lörinczová; Branislav Prosnan (since 1. 10. 2003); Technical staff: Mária Bardúnová; Martin Kovalčík (till 11. 11. 2003);


A. Teaching laboratories: Laboratory of Printing Technology Laboratory of Photochemistry and Photography Laboratory of Optical Spectroscopy and Photometry Laboratory of Thin Films and Plasma Technology Laboratory of Rheology

B. Research laboratories: Laboratory of Absorption Spectroscopy and Colorimetry

III. TEACHING

A. Undergraduate Study: 6. semester (Bc) Paper and Print, Graphic Arts 2/2 Krkoška, Panák Term Project

0/4 Mikula and other members of

academic staff 1. semester (MSc) Colloids Systems and Interfaces 2/1/0 Bakoš, Mikula, Reháková Polymer and Paper Physics 0/2/0 Jančovičová Photochemistry and Photography I. 2/1/0 Čeppan, Reháková Surface and Thin Film Technology 2/0/0 Mikula 1. semester (MSc) Advanced Laboratory Course I. 0/0/9 Havlínová, Jančovičová, Mikula,

Reháková Typography and Text Processing 0/2/0 Dvonka 2. semester (MSc) Photochemistry and photography II. 2/0/0 Čeppan Printing Technology I. 2/0/0 Panák Advanced laboratory Course II. 0/0/7 Čeppan, Dvonka, Havlínová,

Jančovičová Planning for Printing Production 0/2/0 Panák, Dvonka 2. semester (MSc) Text and Image Processing 1/1/0 Čeppan, Dvonka 3. semester (MSc) Printing Technology II. 2/0/0 Panák Repronic 1/3/0 Mikula, Dvonka Advanced Laboratory Course III: 0/0/10 Panák, Dvonka 4. semester (MSc) Diploma Thesis 0/0/27 members of the academic staff


96


A. 5th Framework Program of European Commission: High Productivity and Low Cost for the Encapsulation of Thin Film Solar Cells (NAS-HIPROLOCO) (M. Mikula).

Development of new, material saving, energy saving, automated and cost effective encapsulation systems and processes for thin film solar cells.

Structural analysis of multilayer system based on polymer foil substrate and inorganic and polymeric layers. The quality of interfaces and their role in adhesion and long tem stability of the system.

The study of the barrier properties against the permeation of oxygen and water vapour, the permeation mechanism water through inorganic and organic barrier layers. Aging of the barrier properties. Detailed physical and chemical analysis of the high barrier layer system.

Project duration: from 01. 09. 2002 to 31. 08. 2004 B. VEGA Project No 1/9146/02 Preparation and modification of thin surface layer properties of image-

generating structures and their substrates (Milan Mikula). New type of atmospheric surface discharge treatment of polymer foil substrates considering printability, metalization, lamination, adhesion, mechanical and optical properties of this system in comparison with still-in-use barrier discharge ("corona").

New polymers and copolymers preparation by means of photoinitiated polymerization in thin layers with wanted physical and chemical properties. New information about photochemical reactions of selected photopolymer systems. Photochemical modification of water-soluble based polymers layers, changing their hydrophilic, optical and permeation properties with reference to the imaging technology.


C. VEGA Project No 2/1119/21 (SAV) Study of optical, structural and electric properties of amorphous (a-Si:H, a-SiGe:H) semiconductors after their interactions with plasma particles and/or ion beams (E. Pinčík, SAV, Milan Mikula, STU).

Experimental and theoretical study. Optical absorption properties of semiconductor layers with different defects in bandgap. Thin dielectric blocking layers of SiO2, Si3N4 and interfaces, their properties towards the effective solar cell production on the base of amorphous silicon


D. 5th Framework Programme of EU: Thematic Network /EVK4-CT-2002-20010 Transitional Metals in Paper (MIP), (Michal Čeppan).

Transitional metals may course an accelerated ageing of historic paper documents, drawings and other cellulose cointaining objects. The aim of the network MIP is to exchange present knowledge related to the effects and on how to reduce the effects of transitional metals in paper and how to fit in these results to innovative conservation strategies consisting of assesments methods and treatment technologies.


E. Vega Project No 1/9145/02 Properties of Materials, Constituents and Structures of Printed Images on Polymeric Sustrates (Michal Čeppan).

Development and implementation of the methods of imaging photometry and image analysis of printed images structures on polymeric. Development of method for accelerated light ageing of paper, printing inks, and prints using metal-halogen and fluorescent lamps. Construction of laboratory system for accelerated light ageing using metal-halogen and fluorescent lamps, its basic characterization and calibration. Evaluation of methods and mechanism of printing inks conservation against ageing and attaining new knowledge about relation between various types of paper and inks during ageing of graphic structures on polymeric substrates. Study of influence of fountain solution composition and amount of emulsified fountain solution on rheological properties of offset printing inks. Explaining the influence of printing inks on the emulsions printing ink – fountain solution



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VI. COOPERATION



Duration

Purgina Investigation and evaluation of printing colouring for different printing technologies

Krchňavý Rastislav, technologist, Pri Šajbách 1, 831 06 Bratislava

01. 10. 2003 -

Slovak National Archives Study of ageing of printed documents

Hanus Jozef, head of the Department of archival preservation, Drotárska cesta 42, 817 01 Bratislava

01. 01. 2000 -

Institute of Physics SAS

Amorphous a-Si:H structures for solar cells (VEGA project) Study of barrier layers (EC project)

Pinčík Emil, Dúbravska cesta 9, 845 11 Bratislava 01. 01. 2001 -

Faculty of Mathematics, Physics and Informatics, CU, Bratislava

Polymer surface treatment by atmospheric discharges

Černák Miroslav, Mlynská dolina, 842 48 Bratislava 01. 09. 2000 -



Duration

Departement de Photochimie Generale, Université de Haute Alsace, Mulhouse, France

UV curing reaction of waterbased clearcoats

Decker Christian, professor, 3 rue Alfred Werner, Mulhouse Cedex, France

01. 09. 2002 -

Fraunhofer Institute process Engineering and Packaging (IVV), Freising, Germany

Research of barrier layers on flexible foils (EC project)

Noller Klaus, dr., Fraunhofer Inst. IVV, 853 54 Freising

01. 09. 2002 -

Fraunhofer Institute for Silicate Research, Wurzburg, Germany

Properties of Ormocer lacquer layers (EC project)

Amberg-Schwab Sabine, dr., Fraunhofer Inst. ISC, 970 82 Wurzburg

01. 09. 2002

Faculty of Chemistry, Technical University Brno, Czech Republic

Photochemical properties of light sensitive layers

Michal Veselý, vice-dean, Purkyňova 118, 612 00 Brno 01. 09. 2001 -

Printing House Model Opava, Opava, Czech Republic

Investigation and quality evaluation of offset printing

Matýsek Jiří, Těšínska 101, 74601 Opava, Czech Republic

01. 04. 2002 - 31. 01. 2003

State Central Archives in Prague, Czech Republic

Longlasting measurements of nonaged and aged papers

Ďurovič Michal, head of department, Archivní 4, 149 01 Praha 4 - Chodovec

01. 01. 2001 -

X-Rite Pardubice, Czech Republic Hue colour ink computer formulation Černý Jan, S. K. Neumanna

1316, 53207 Pardubice 01. 09. 2002 - 30.

06. 2003 C. Membership in Domestic Organizations and Societies


Valid date

Čeppan Michal Slovak Union for IndustrialChemistry member 1980 -

Dvonka Vladimír Slovak Union for Industrial Chemistry member 1996 -

Havlínová Bohuslava Slovak Union for Industrial Chemistry member 1980 -

Jančovičová Viera Slovak nion for Industrial Chemistry member 1999 -


98

Kindernay Juraj Slovak Union for Industrial Chemistry member 1999 -

Mikula Milan Slovak Union for Industrial Chemistry member 1980 - Panák Ján Slovak Union for Industrial Chemistry member 1978 - Reháková Milena Slovak Union for Industrial Chemistry member 2001 -



Valid date

Čeppan Michal European Photochemistry Association member 1990 -

Čeppan Michal

International Society of Imaging Science and Technology, Springfield, USA member 1985 -

Michal Čeppan Graphic Arts Technical Foundation, Sewickley, USA member 1988 -



Date / Duration

Kaplanová, M. University of Pardubice, Pardubice Czech Republic January 2003 (1 day)

Pekař, M. Brno University of Technology, Brno Czech republic January 2003 (1 day)

Lapčík, L. Tomas Bata University, Zlín Czech Republic January 2003 (1 day)

Lapčík, L. Tomas Bata University, Zlín Czech Republic June 2003 (2 days)

Veselý, M. Brno University of Technology, Brno Czech Republic June 2003 (2 days)

Holická, H. University of Pardubice, Pardubice Czech Republic




Date / Duration

Jakubíková, Z. Brno University of Technology, Brno Czech Republic

February 2003 (3 days)

Čeppan, M., Reháková,M. Model Obaly, a.s. Opava, Czech

Republic February (1 day)

Mikula, M. Fraunhofer Institute Process Engineering and Packaging, Freising Germany February (2 days)

Čeppan, M., Belányi, F., Dvonka, V., Havlínová, B., Hrehorová, E., Jakubíková, Z., Jančovičová, V.,

Seminar Print Media, Heidelberg Germany March (5 days)

Kindernay, J., kovalčík, M., Lörinczová, I., Reháková, M.

Seminar Print Media, Heidelberg Germany March (5 days)

Havlínová, B. State Central Archives, Prague Czech Republic March (4 days)

Jančovičová, V. Brno University of Technology Czech Republic April (3 days)

Čeppan, M., Mikula, M. Isovolta AG, Werndorf Austria April (2 days)

Jančovičová, V. X-Rite, Pardubice Czech Republic May (1 day)


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Čeppan, M., Belányi, F., Dvonka, V., Jakubíková, Z., Jančovičová, V., kindernay, J., Mikula, M.,

22th International fair EMBAX Czech Republic May (1 day)

Panák, J., Reháková, M. 22th International fair EMBAX Czech

Republic May (1 day)

Hrehorová, E. 22th International fair EMBAX Czech Republic May (2 days)

Čeppan, M. TNO Industrial Technology and the University of Northumbria, Amsterdam, New Castke Holland, UK May (3 days)

Čeppan, M. University of Pardubice, Pardubice Czech Republic Jun (3 days)

Čeppan, M. Brno University of Technology Czech republic June (3 days) Čeppan, M., Belányi, F., Dvonka, V., Havlínová, B., Jakubíková, Z., Jančovičová, V., Mikula M.,

6th Seminar of Graphic Arts, Pardubice Czech republic September (3 days)

Panák, J. 6th Seminar of Graphic Arts, Pardubice Czech republic September (3 days) Čeppan, M. 12th Seminar of Restorers and Historians, Prague Czech republic October (2 days) Reháková, M. 12th Seminar of Restorers and Historians, Prague Czech republic October (4 days) Čeppan, M., Mikula, M.

Centre for solar energy and hydrogen resear Baden Wuttenberg, Stuttgart Germany October (3 days)



Čepcová, K. Modulation transfer function measurement of printed flexible foils Dvonka, V. Grachová, L. Study of thin polymer film properties on paper substrate Reháková, M. Hodál, M. Influence of radiation intensity and layer thickness on UV varnish curing Jančovičová, V. Hoferíková, A. Study of light stability of aryl-methane dyes in solution Jančovičová, V. Iždinská, Z. Characterization of modern writing tools using UV VIS spectroscopy Jančovičová, V. Košová, J. Influence of external factors on stability of digital printing Reháková, M. Múková, J. Study of accelerated light ageing of flexographic inks on board LENETA Havlínová, B.

Perašinová, L. Monitoring of water, pastel and oil colours stability influenced by germicide Havlínová, B.

Polončanová, P. Study of printing quality according to evaluated parameters Dvonka, V. Popovičová, H. Study of acrylate UV varnish polymerization Jančovičová, V. Rehák, P. Study of photoinitiated polymerizatin of acrylates Blažková, A. Šubrtová, M. Study of paper gloss angle dependance according to its smoothness Mikula, M. Trnovec, B. Study of relation of gloss angle dependence on paper surface Mikula, M.

Uherová, A. Study of ink-jet and laser prints stability effected by accelerated wet aging Havlínová, B.

Voltemarová, V. Experimental evaluation of colour management system Čeppan, M. B. Graduate Theses (MS Degree) for state examinations after five years of study

Name Title of Thesis Supervisor Černáková, H. Study of accelerated ageing of prints Reháková, M. Debnárová, Z. Damping and quality of offset printing Panák, J.

Fialkovič, J. Study of historical documents ageing processes - corrosion of iron-gall inks Čeppan, M.

Horáčiková, K. Study of surface and adhesion properties of PP foils treated by barrier discharge Mikula, M.

Hricková, J. Reoviscosimetry of offset printing inks Panák, J. Janatová, Z. Study of ink-jet and laser colour prints stability Havlínová, B. Moricová, P. Photochemically initiated polymerization of urethane-acrylates Jančovičová, V.

Mrlláková, I. Preparation and photochemical modification of polymeric layers based on water-soluble polymer derivates Jančovičová, V.


100

Paulínyová, Z. Options of hue colour ink computer formulation with respect to printed substrate variability Jančovičová, V.

Prosnan, B. Study of SiOx layer properties on polymeric substrate Mikula, M. Studnička, M. Study of printing stability of packages Čeppan, M. Ščambová, I. Image quality in ink-jet printing Čeppan, M. Švorcová, L. Investigation of modification of modern printing matters after ageing Havlínová, B. Tomášová, D. Factors of printed flexible foils colour stability Mikula, M. Vyšná, M. Influence of variable parameters on offset printing stability Reháková, M.


Kindernay, J. Studing and controling methods of UV photopolymeric composition curing Mikula, M.


Panák, J. Rheology study of offset inks and damping in offset printing Marcinčin,A.

VIII. PUBLICATIONS A. Journals [1] Čeppan, M., Fedák, J., Dvonka, V., Veselý, M., Zmeškal, O.: Fractal Spaces of Spectra Sets of Color Prints. J. Imag. Sci.

Technol. 47(2), 171-184 (2003). [2] Lörinczová, I., Jančovičová, V., Čeppan, M.: Hydrofobizácia povrchových polymérnych vrstiev UV žiarením.

Hydrophobization of surface polymer layers using UV light. Chem. Listy 97 (5), 265–268 (2003). [3] Mikula, M., Čeppan, M., Vaško, K.: Gloss and goniocolorimetry of printed materials. Color Research and Application 28 (5),

335-342 (2003). [4] Mikula, M., Jakubíková, Z., Zahoranová, A.: Surface and adhesion changes of atmospheric barrier discharge treated

polypropylene in air and nitrogen. J. Adhesion Sci. Technol. 17 (15), 2097-2110 (2003). [5] Reháková, M., Mikula, M., Čeppan, M., Malec, B.: Proces starnutia a hodnotenia stability grafických zobrazení. Aging process

and stability evaluation of graphic images. Chem. Listy 97, 140-145 (2003). [6] Lörinczová, I., Jančovičová, V., Čeppan, M.: Prijímacie vrstvy ink-jetových médií. Recieving polymerlayers of ink-jet media.

Papír a celulóza 58 (1), 22–24, (2003). [7] Vizárová K., Cedzová M., Reháková M., Šutý Š.: Vplyv svetelnej expozície na zmeny vlastností súčasných papierov v

priebehu urýchleného starnutia. The influence of light exposition on changes of contemporary papers properties in accelerated ageing. Papír a celulóza 58 (9), 264-267 (2003).

B. Conferences [1] Lörinczová, I.*, Decker, C.: Waterbased UV-curable urethane-acrylate clearcoats for offset prints. In: Proc. Int. Conference

on Chemical Technology of Wood, Pulp and Paper, WPP2003. Bratislava (Slovak Republic), Sept. 17-19, 2003. Ed. by Baudin G., Fellegi J., Gellerstedt G., Katuscak S., Pikulik J., Paris J., pp. 487–490 (2003). ISBN 80-227-1942-0. (Po)

[2] Reháková, M.*, Čeppan, M., Černáková, H., Dvonka, V., Hrehorová, E., Kindernay, J.: Light stability of ink-jet prints. In: Proc. Int. Conference on Chemical Technology of Wood, Pulp and Paper, WPP2003. Bratislava (Slovak Republic), Sept. 17-19, 2003. Ed. by Baudin G., Fellegi J., Gellerstedt G., Katuscak S., Pikulik J., Paris J., pp. 440–443 (2003). ISBN 80-227-1942-0. (Po)

[3] Reháková, M.*, Vizárová, K., Hrehorová, E., Račková, K.: The influence of internal and external factors on the ink-jet print quality in the ageing process. In: Proc. Int. Conference on Chemical Technology of Wood, Pulp and Paper, WPP2003. Bratislava (Slovak Republic), Sept. 17-19, 2003. Ed. by Baudin G., Fellegi J., Gellerstedt G., Katuscak S., Pikulik J., Paris J., pp. 417–421 (2003). ISBN 80-227-1942-0. (Po)

[4] Vizárová, K.*, Reháková, M., Hrehorová, E., Jančovičová, V., Jakubíková, Z.: Preparing and properties of polymer protective films on the paper substrate. Preparing and properties of polymer protective films on the paper substrate. In: Proc. Int. Conference on Chemical Technology of Wood, Pulp and Paper, WPP2003. Bratislava (Slovak Republic), Sept. 17-19, 2003. Ed. by Baudin G., Fellegi J., Gellerstedt G., Katuscak S., Pikulik J., Paris J., pp. 412–416 (2003). ISBN 80-227-1942-0. (Po)

[5] Belányi, F.*, Havlínová, B., Brezová, V., Čeppan, M., Novotná, M., Jakubíková, Z.: The stability of offset inks on paper upon ageing. The stability of offset inks on paper upon ageing. In: Proc. Int. Conference on Chemical Technology of Wood, Pulp and Paper, WPP2003. Bratislava (Slovak Republic), Sept. 17-19, 2003. Ed. by Baudin G., Fellegi J., Gellerstedt G., Katuscak S., Pikulik J., Paris J., pp. 462–467 (2003). ISBN 80-227-1942-0. (Pr)

[6] Brezová, V.*, Pigošová, J., Havlínová, B., Dvoranová, D., Ďurovič, M.: The photodegradation of dyes studied by EPR spectroscopy. In: Proc. Int. Conference on Chemical Technology of Wood, Pulp and Paper, WPP2003. Bratislava (Slovak Republic), Sept. 17-19, 2003. Ed. by Baudin G., Fellegi J., Gellerstedt G., Katuscak S., Pikulik J., Paris J., pp. 348-353 (2003). ISBN 80-227-1942-0. (Pr)

[7] Csomorová, M.*, Havlínová, B., Brezová, V., Ďurovič, M., Mináriková, J.: Degradation resistance of three-layer corrugated board printed by flexographic inks. In: Proc. Int. Conference on Chemical Technology of Wood, Pulp and Paper, WPP2003. Bratislava (Slovak Republic), Sept. 17-19, 2003. Ed. by Baudin G., Fellegi J., Gellerstedt G., Katuscak S., Pikulik J., Paris J., pp. 482–486 (2003). ISBN 80-227-1942-0. (Pr)

[8] Decker, C.*, Lörinczová, I.: UV- radiation curing of waterbased acrylate coatings. In: Proc. RadTech Europe Conf , Berlin (Germany), November 3-5 , 2003. Ed. by Vincentz, Hannover (Germany),Vol. 2, pp. 669-678 (2003). (Pr)


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[9] Hanus, J.*, Havlínová, B., Janatová, Z., Mináriková, J., Hanusová, E., Ďurovič, M: Permanence evaluation of colour records made by ink-jet and laser printers. In: Proc. Int. Conference on Chemical Technology of Wood, Pulp and Paper, WPP2003. Bratislava (Slovak Republic), Sept. 17-19, 2003. Ed. by Baudin G., Fellegi J., Gellerstedt G., Katuscak S., Pikulik J., Paris J., pp. 366–373 (2003). ISBN 80-227-1942-0. (Pr)

[10] Mikula, M.*, Čeppan, M., Vaško, K., Jakubíková, Z.: Gloss and multiangle colorimetry of printed materials. In: Proc. Int. Conference on Chemical Technology of Wood, Pulp and Paper, WPP2003. Bratislava (Slovak Republic), Sept. 17-19, 2003. Ed. by Baudin G., Fellegi J., Gellerstedt G., Katuscak S., Pikulik J., Paris J., pp. 468–472 (2003). ISBN 80-227-1942-0. (Pr)

[11] Belányi, F.*, Janatová, Z., Havlínová, B., Hanus, J., Lörinzová, I.: Vyhodnotenie stálosti farebných záznamov ink-jetových a laserových tlačiarní. Stability evaluation of colour image of ink-jet and laser printers. In: Sborník přednášek VI. polygrafický seminář. Pardubice (Czech Republic), Sept 23.-24., 2003, pp. 51-57 (2003). ISBN 80-7194-561-7. (Pr)

[12] Csomorová, M.*, Havlínová, B., Brezová, V., Belányi, F.: Vlnitá lepenka potlačená flexotlačovými farbami a zmeny jej správania sa počas urýchleného starnutia. Paper boards printed with flexographic inks and changes during accelerated ageing. In: Sborník přednášek VI. polygrafický seminář. Pardubice (Czech Republic), Sept 23.-24., 2003, pp. 58-62 (2003). ISBN 80-7194-561-7. (Pr)

[13] Dvonka, V.*, Ščambová, I., Čeppan, M.: Hodnotenie kvality zobrazenia inkjetovej tlače. Quality image evaluation of ink-jet printing. In: Sborník přednášek VI. polygrafický seminář. Pardubice (Czech Republic), Sept 23.-24., 2003, pp. 117-123 (2003). ISBN 80-7194-561-7. (Pr)

[15] Jakubíková, Z.*, Mikula, M., Šutý, Š., Trnovec, B.: Uhlová závislosť lesku vo vzťahu k hladkosti papiera. Angular dependence of gloss related to the paper smoothness. In: Sborník přednášek VI. polygrafický seminář. Pardubice (Czech Republic), Sept 23.-24., 2003, pp. 9-14 (2003). ISBN 80-7194-561-7. (Pr)

[16] Jakucewicz, S.*,. Panák, J.: Štúdium kvality tlače plnofarebných výtlačkov z hárkového ofsetového stroja na nenatieraných papieroch. Study of printing quality of full-colour prints of sheet-fed press on uncoated papers. In: Sborník přednášek VI. polygrafický seminář. Pardubice (Czech Republic), Sept 23.-24., 2003, pp. 15-24 (2003). ISBN 80-7194-561-7. (Pr)

[17] Jančovičová, V.*, Hodál, M., Kindernay, J., Popovičová, H., Kotková, M.: Monitorovanie vytvrdzovania UV lakov na báze akrylátov. UV curing monitoring of acrylate based varnishes. In: Sborník přednášek VI. polygrafický seminář. Pardubice (Czech Republic), Sept 23.-24., 2003, pp. 124-128 (2003). ISBN 80-7194-561-7. (Pr)

[18] Panák, J.*, Jakucewicz, S.: Nároky digitálnych tlačových techník na vlastnosti papierov. Demands of digital printing technics on paper quality. In: Sborník přednášek VI. polygrafický seminář. Pardubice (Czech Republic), Sept 23.-24., 2003, pp. 5-8 (2003). ISBN 80-7194-561-7. (Pr)

[19] Šulla, S.*, Černý, J., Jančovičová, V., Paulínyová, Z.: Možnosti počítačového receptúrování tiskových barev při tisku na hliníkovou fólii. Computer formulation possibilities of printing inks printed on Al foil. In: Sborník přednášek VI. polygrafický seminář. Pardubice (Czech Republic), Sept 23.-24., 2003, pp. 47-50 (2003). ISBN 80-7194-561-7. (Pr)

[20] Brezová, V*., Pigošová, J., Havlínová, B., Dvoranová, D., Ďurovič, M.: Štúdium fotodegradácie arylmetanových farieb EPR spektroskopiou. Photodegradation of arylmethane inks using EPR spectrocsopy. XII Seminář restaurátorů a historiků. Praha (Czech Republic), Oct. 7-10, 2003 (Pr).

[21] Hanus, J.*, Havlínová, B., Janatová, Z., Mináriková, J., Hanusová, E., Ďurovič, M.: Vyhodnotenie stálosti farebných záznamov vyhotovených niektorými ink-jetovými a laserovými tlačiarňami. Stability evaluation of colour images printed on some ink-jet and laser printers. XII Seminář restaurátorů a historiků. Praha (Czech Republic), Oct. 7-10, 2003 (Pr).

[22] Mináriková, J.*, Havlínová, B., Hanus, J., Švorcová, L., Brezová, V.: Sledovanie zmien novodobých písacích látok pri starnutí. Modification monitoring of modern writing substances during ageing. XII Seminář restaurátorů a historiků. Praha (Czech Republic), Oct. 7-10, 2003 (Pr).

[23] Vizárová, K.*, Reháková, M, Cedzová, M.: Vplyv svetelnej predhistórie na stálosť a trvanlivosť novodobých papierov. Influence of light pre-history on stability and durability of modern papers. XII Seminář restaurátorů a historiků. Praha (Czech Republic), Oct. 7-10, 2003 (Pr).

DEPARTMENT OF INFORMATION ENGINEERING AND PROCESS CONTROL

102


Head of Department: Telephone: ++421252495269 Assoc. Prof. Miroslav Fikar, PhD Fax: ++421252496469


I. STAFF Full Professors: Ján Mikleš, PhD, DSc; Associate Professors: Monika Bakošová, PhD; Ján Danko, PhD; Ján Dvoran, PhD; Miroslav Fikar, PhD; Alojz Mészáros, PhD; Assistant Professors : Ľuboš Čirka; František Jelenčiak; Mária Karšaiová, PhD; Magdaléna Ondrovičová; Anna Vasičkaninová; PhD Students: Karol Calík; Lukáš Dermíšek; Tomáš Hirmajer; Ľubomír Šperka; Technical staff: Eva Fuseková; Andrea Kalmárová; Stanislav Vagač;


A. Teaching laboratories: Laboratory of Process Control Laboratory of Control Systems Laboratory of Measuring Instruments and Techniques Computer Laboratory (PC - Windows, Linux) Computer Laboratory (Solaris) B. Research laboratories: Laboratory of Control Theory Laboratory of Modelling and Simulation Laboratory of Identification Laboratory of Optimisation Laboratory of Neural Networks Laboratory of Fuzzy Control and Expert Systems Laboratory of Chemical Reactor Analysis and Control Laboratory of Biochemical Process Analysis and Control Laboratory of Distillation Column Analysis and Control Laboratory of Computer Aided Design (Siemens – SIMATIC S-7 300)

III. TEACHING

A. Undergraduate Study: 2. semester (Bc) Informatics 1/0/2 Ondrovičová, Šperka, Vasičkaninová 5. semester (Bc) Computer Based Data Processing 0/0/2 Jelenčiak, Ondrovičová,

Vasičkaninová 6. semester (Bc) Automatic Control Fundamentals 2/0/0 Bakošová, Fikar Laboratory Exercises of Automatic

Control Fundamentals 0/0/2 Bakošová, Danko, Fikar, Jelenčiak,

Karšaiová, Mészáros, Laboratory Exercises of Automatic

Control Fundamentals 0/0/2 Ondrovičová, Vasičkaninová

Bachelor projects 0/0/4 Bakošová, Čirka, Danko, Dvoran, Fikar, Jelenčiak,

6. semester (Bc) Bachelor projects 0/0/4 Mikleš, Ondrovičová, Vasičkaninová 1. semester (MSc) Process Control 1/0/2 Bakošová, Karšaiová Process Dynamics 2/0/0 Bakošová Operating Systems 1/0/1 Fikar Control Devices and Systems 2/0/1 Danko 1. semester (MSc) Computer Programs 1/0/2 Fikar Laboratory Projects 0/0/8 Bakošová, Čirka, Karšaiová, Šperka,


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Vasičkaninová 2. semester (MSc) Optimisation 2/0/1 Dvoran Control Theory I 2/0/2 Čirka, Mikleš Laboratory Exercises of Control

Theory I 0/0/2 Čirka, Mikleš

Experimental Identification 2/0/0 Fikar 2. semester (MSc) Laboratory Project II 0/0/6 Čirka, Danko, Dvoran, Mészáros Modelling and Control of

Polymerisation Processes 2/0/2 Dvoran, Jelenčiak

Process Dynamics 2/0/0 Bakošová Laboratory Exercises of Process

Dynamics 0/0/1 Bakošová

3. semester (MSc) Control Theory II 2/0/0 Mikleš Laboratory Exercises of Control

Theory II 0/0/2 Čirka

Intelligent Control Systems 2/0/0 Dvoran Semestral Project 0/0/10 Čirka, Dvoran, Karšaiová, Mikleš,

Ondrovičová 3. semester (MSc) CAD systems 2/0/0 Karšaiová Industrial Applications of Process

Control 2/0/0 Mikleš, Ondrovičová

Control of Technological Processes 1/0/2 Bakošová, Čirka, Vasičkaninová 4. semester (MSc) Diploma Theses 0/0/27 Bakošová, Čirka, Fikar, Karšaiová,

Mészáros, Diploma Theses 0/0/27 Ondrovičová


A. VEGA Project No 1/8108/01 Adaptive and Intelligent Control Strategies for Processes of Chemical/Biochemical Technology (Alojz Mészáros)

The scientific project is focused on development of new strategies of adaptive, robust and intelligent control with respect to potential applications to the processes of chemical/biochemical technology. The main goal is to make further progress in the field of artificial neural network (ANN) based identification and control. New adaptive, predictive and robust control structures are designed and tested by both, computer simulations and laboratory control experiments. An original adaptive tuning of discrete PID controller is proposed. Control strategy based on adaptive lambda-tracking policy is also proposed for linear systems with higher relative degree as well as with varying sampling rate for systems with discretely measured outputs. The new methods introduced are tested on computer control of laboratory distillation column and laboratory biochemical reactor. Results achieved will be offered for industrial application in collaboration with the ProCS Ltd. company.

Project duration: from 01.01.2001 to 31.12.2003 B. VEGA Project No 1/0135/03 Development of optimal and supervisory control methods for mass

transfer processes (Miroslav Fikar) The project deals with development of modern control methods and focuses into mass transfer processes: chemical reactors, distillation columns, waste-water treatment plants, and other processes of chemical and food technologies. Involves static and dynamic methods, two level control where supervision and dynamic optimisation will be investigated at the higher level and feedback control at the lower level. Developed algorithms, controllers, and control structures will be tested by simulations and in laboratory conditions.

Project duration: from 01.01.2003 to 31.12.2005 C. Project of Slovak – Czech Scientific Cooperation No 112/189 Advanced Control Methods for

Processes of Chemical and Food Technologies (Ján Mikleš) The aim of the project is to develop new methods of adaptive, robust and intelligent control and to implement obtained control algorithms for processes of chemical and food technologies.



A. Leonardo da Vinci Project No. RO/00/B/F/PP141028 Eurocompetencies Transfer in Vocational Guidance for Young Specialists in Bioscience Field (Alojz Mészáros)

The aim of the project is organising of training courses in various biochemical and biotechnological branches for students, graduate students, young scientists and young specialists form praxes. Project duration: from 01.11.2000 to 01.11.2003


104

VI. COOPERATION



Duration

ProCS, Ltd., Šaľa Processing of graphical displays for RS Centum CS 3000.

Bartošovič Štefan, director, Dolná 16, Šaľa 01.10.2003 -

Department of Automatic Control Systems, FEEI STU, Bratislava

Robust control, control of real processes. Veselý Vojtech, professor, Ilkovičova 3, Bratislava 01.01.2001 -

Department of Automation and Measurement, FME STU, Bratislava

Automatic control, predictive control. Rohaľ-Ilkiv Boris, associate professor, Nám. Slobody 17, Bratislava

01.01.2000 -

Siemens, Inc., Bratislava Industrial control systems. Pätoprstý Radomír, Siemens,

Bratislava 01.01.2001 -



Duration

Department of Process Control and Computer Techniques, FCT, University of Pardubice, Czech Republic

Advanced control methods for processes of chemical and food technologies.

Taufer Ivan, professor, Nám. Čs. legií 565, Pardubice, Czech Republic

01.01.2000 - 31.12.2003

LSGC-CNRS, Ecole Nationale Superieure des Industries Chimiques (ENSIC), Nancy, France

Dynamic optimisation of distillation columns, waste-water treatment plants.

Latifi Mohamed Abderrazak, professor, 1 rue Grandville, Nancy, France

01.01.1997 -

Control Engineering Laboratory, FEIS, Ruhr University, Bochum, Germany

Closed-loop identification, predictive control.

Unbehauen H., professor, Universitätstr. 150, Bochum, Germany

01.01.1998 -

Control Engineering Laboratory, FEIS, Ruhr University, Bochum, Germany

E-learning in control.

Schmid Christian, professor, Universitätstr. 150, Bochum, Germany

01.01.2003 -

Institute of Information Technologies, Tomas Bata University, Zlín, Czech Republic

Adaptive control, decentralized control, robust control.

Dostál Petr, professor, Nám. T. G. Masaryka 275, Zlín, Czech Republic

01.01.1998 -

Institut für Verfahrenstechnik, Brennstoff- und Umwelttechnik, TU Wien, Austria

Optimisation of combustion processes. Hofbauer Hermann, professor, Getreidemarkt 7, Austria

01.01.1999 -30.06.2003

Department of Chemical Engineering,TU Budapest, Hungary

Modelling of chemical processes, Mizsey Peter, Mülgzetem rkp. 3, Budapest, Hungary 01.01.1996 -

Faculty of Electrical Engineering, Czech Technical University, Prague, Czech Republic

Adaptive control, polynomial synthesis. Šebek Michael, Technická 2, Prague, Czech Republic 01.01.1998 -


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Valid date

Bakošová Monika Slovak Society of Chemical Engineering member 03.05.1995 -

Bakošová Monika Slovak Society of Industrial Chemistry member 01.01.1983 -

Čirka Ľuboš Slovak Society of Industrial Chemistry member 01.01.1998 - Danko Ján Slovak Society of Industrial Chemistry member 01.01.1975 - Dvoran Ján Slovak Society of Industrial Chemistry member 01.01.1975 - Fikar Miroslav Slovak Society of Industrial Chemistry member 01.01.1990 - Karšaiová Mária Slovak Society of Industrial Chemistry member 01.01.1975 -

Mészáros Alojz Slovak Society of Industrial Chemistry member 01.01.1981 -

Mikleš Ján Slovak Society of Industrial Chemistry member 01.01.1975 -

Ondrovičová Magdaléna Slovak Society of Industrial Chemistry member 01.01.1991 -

Vasičkaninová Anna Slovak Society of Industrial Chemistry member 01.01.1985 -

Jelenčiak František Slovak Society of Industrial Chemistry member 01.01.2000 -

Dermíšek Lukáš Slovak Society of Industrial Chemistry member 01.01.2003 -

Šperka Ľubomír Slovak Society of Industrial Chemistry member 01.01.2003 -

Mikleš Ján Scientific Grant Agency VEGA MŠSR a SAV - Comission for Elektrotechnics and Informatics member 30.04.2002 -

Mikleš Ján Commission for defence of dissertations (DSc) at science 28-30-9 Chemical Engineering and Process Control

member 01.11.1998 -

Mikleš Ján Commission for defence of dissertations (DSc) at science 38-01-9 Automation and Control chairmann 01.01.1998 -

Mikleš Ján Common branch commission for PhD study at science 28-30-9 Chemical Engineering and Process Control

member 01.01.1998 -

Danko Ján Common branch commission for PhD study at science 28-30-9 Chemical Engineering and Process Control

member 01.01.1998 -

Dvoran Ján Common branch commission for PhD study at science 28-30-9 Chemical Engineering and Process Control

member 01.01.1998 -

Mészáros Alojz

Common branch commission for PhD study at science 28-30-9 Chemical Engineering and Process Control

member 01.01.1998 -

Mikleš Ján Common branch commission for PhD study at science 38-01-9 Automation and Control member 09.09.1997 -

Mikleš Ján Slovak Society for Cybernetics and Informatics member 01.01.1992 - Mészáros Alojz Slovak Society for Cybernetics and Informatics member 01.01.1992 -

Mikleš Ján Editorial board of AT&P Journal member 01.01.1993 - Dvoran Ján Editorial board of AT&P Journal member 01.01.1993 - Mészáros Alojz Editorial board of AT&P Journal member 01.01.1993 -

Mikleš Ján Editorial board of Cybernetics and Informatics member 01.01.1993 - D. Membership in International Organisations and Societies


Valid date

Mikleš Ján International Federation of Automatic Control, Technical Committee on Control Design member 01.01.1996 -

Mikleš Ján International Federation of Automatic Control (IFAC), Slovak National Member Organisation (Slovak NMO) other 01.01.1997 -


106



Date / Duration

Taufer, I. Faculty of Chemical Technology, University of Pardubice, Pardubice


Dostál, P. Institute of Information Technologies, Tomas Bata University, Zlín

Czech Republic June 2003 (1 day)


Czech Republic



Czech Republic



Czech Republic

December 2003

(3 days)

Latifi, M. A. LSGC-CNRS, Ecole Nationale Superieure des Industries Chimiques (ENSIC), Nancy France June 2003 (5 days)



Date / Duration

Mikleš, J. 11th Mediterranean Conference on Control and Automation. Rhodos. Greece June 2003 (7 days)

Mészáros, A. 11th Mediterranean Conference on Control and Automation. Rhodos. Greece June 2003 (7 days)

Fikar, M. European Control Conference 2003. Cambridge. Great Britain September 2003 (6 days)

Bakošová, M. Institute of Information Technologies, Tomas Bata University, Zlín


Bakošová, M. Faculty of Chemical Technology, University of Pardubice, Pardubice

Czech Republic


Bakošová, M. Conference Principia Cybernetica'03, Liberec Czech Republic


Dvoran, J. Faculty of Chemical Technology, University of Pardubice, Pardubice

Czech Republic


Dvoran, J. Conference Principia Cybernetica'03, Liberec Czech Republic


Mészáros, A. Department of Chemical Engineering, University of Technology and Economy, Budapest Hungary August 2003 (2 days)

Mészáros, A. Universität von Hohenheim, Stuttgart Germany September 2003 (6 days)

Mészáros, A. University of Trontheim, Trontheim Norway October 2003 (5 days)

Fikar, M. Faculty of Electrical Engineering, Czech Technical University, Prague

Czech Republic


Mikleš, J. Faculty of Electrical Engineering, Czech Technical University, Prague

Czech Republic


Bakošová, M. Institute of Information Technologies, Tomas Bata University, Zlín

Czech Republic October 2003 (1 day)

Fikar, M. Institute of Information Technologies, Tomas Bata University, Zlín

Czech Republic October 2003 (1 day)

Fikar, M. Faculty of Chemical Technology, University of Pardubice, Pardubice

Czech Republic


Čirka, Ľ. Faculty of Chemical Technology, University of Pardubice, Pardubice

Czech Republic




Borkovič, P. Robust control of a time-delay system. Vasičkaninová, A. Burian, P. Control design for a concentration system. Vasičkaninová, A.


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Cebuľa, M. Design of an adaptive lambda-tracker for control of a distillation column. Bakošová, M. Hudec, P. Development of an publication information systems for the department. Čirka, Ľ. Palacka, O. Computer control of a laboratory distillation column. Bakošová, M. Pastoreková, L. Control of pressure tanks. Danko, J. Prček, T. Design of an adaptive lambda-tracker for control of a chemical reactor. Bakošová, M. Rybárová, K. Testing of an optimisation method in MATLAB. Dvoran, J. Škultéty, M. Identification fo physical parameters of a chemical reactor. Ondrovičová, M.

Valo, R. New methods for PID controllers tuning for control of chemical technological processes. Bakošová, M.

Závacká, J. Internet processing of measured data using MATLAB. Čirka, Ľ. Klačko, M. Internet simulation of dynamic systems using MATLAB. Čirka, Ľ. B. Graduate Theses (MS Degree) for state examinations after five years of study

Name Title of Thesis Supervisor Čáran, M. Using of control system SIMATIC for control of a distillation column. Ondrovičová, M. Čokinová, A. Mathematical model of a process of mixture homogenisation. Bakošová, M. Hirmajer, T. Design of a library information system for the DEEPC. Fikar, M.

Chalupová, K. Control design for a distillation column for separation of methanol-water mixture. Ondrovičová, M.

Jančovič, P. Design of an information system for the PROCESS CONTROL conference. Čirka, Ľ.

Kostendová, M. Application of adaptive lambda-tracking method for control of technological processes. Bakošová, M.

Murínová, M. Design of a control stucture for a technological process. Karšaiová, M. Oláh, A. Methodology design for an application of visualisation systems. Mészáros, A. Smetana, S. Hybrid modelling of a biotechnological process. Mészáros, A.


Čirka, Ľ. Adaptive LQ control. Youla-Kučera parametrisation of controllers and process models. Mikleš, J.

Rusnák, A. Intelligent control of biotechnological processes, Mészáros, A.


[1] Kožka, Š., Mikleš, J., Fikar, M.: An iterative identification based on the Youla-Kucera parameterisation without model reduction. Archives of Control Sciences 13 (1), 5-17 (2003).

[2] Kožka, Š., Mikleš, J.: An iterative identification and control design of a chemical reactor. Chemical Papers 57 (5), 335-341 (2003).

[3] Kožka, Š., Zemanovičová, A., Bachmann, G., Hofbauer, H.: An application of identification and control design to the experimental calorimeter. Chemical Papers 57 (4), 229-236 (2003).

[4] Andrášik, A., Mészáros, A., Šperka, Ľ.: daptívny neurónový regulátor založený na hybridnom modelovaní. Adaptive neural controller based on hybrid modelling. AT&P Journal, 10 (4), 69-72 (2003).

[5] Bakošová, M., Fikar, M., Čirka, Ľ.: Nové prístupy k vyučovaniu základov automatizácie a riadenia procesov. New trends in teaching process control fundamentals. AT&P Journal, 10 (11), 17-19 (2003).

[6] Bakošová, M., Ondrovičová, M., Karšaiová, M.: Riadenie mnohorozmerových chemickotechnologických procesov metódou adaptívneho lambda-sledovania. Control of MIMO processes in chemical technology using adaptive lambda-tracking. AT&P Journal, 10 (4), 73-75 (2003).

[7] Mészáros, A., Andrášik, A., Illeová, V., Šperka, Ľ.: Riadenie laboratórneho fermentora pomocou neurónového regulátora. Control of a laboratory fermenter using neural controller. AT&P Journal, 10 (4), 66-68 (2003).

[8] Mikleš, J., Čirka, Ľ., Fikar, M.: H2 optimálne riadenie chemického reaktora. H2 optimal control of a chemical reactor. AT&P Journal, 10 (11), 92-94 (2003).

B. Conferences [1] Andrášik, A., Mészáros, A.*, Bakošová, M., Šperka, Ľ.: DO concentration control in a laboratory fermenter using neural

networks. In: Proc. 30. Int. Conf. SSCHE. Tatranské Matliare (Slovakia), May 26– 30 2003. SSCHE Bratislava, CD ROM P239 (2003), ISBN 80-227-1889-0. (Po)

[2] Andrášik, A., Mészáros, A.*, Šperka, Ľ.: Neural control of a continuous yeast fermenter. Neural control of a continuous yeast fermenter. In: Proc. 14. Int. Conference Process Control’03. Štrbské Pleso, High Tatras (Slovakia), June 8-11, 2003. KIRP FCHPT STU Bratislava, Slovakia, CD ROM 220 (2003). ISBN 80-227-1902-1. (Po)

[3] Bakošová, M.*, Kostendová, M., Karšaiová, M., Ondrovičová, M.: Adaptive lambda-tracking of a laboaratory fan heater. In: Proc. 14. Int. Conference Process Control’03. Štrbské Pleso, High Tatras (Slovakia), June 8-11, 2003. KIRP FCHPT STU Bratislava, Slovakia, CD ROM 219 (2003). ISBN 80-227-1902-1. (Po)

[4] Bakošová, M., Mészáros, A.*: Control of nonlinear chemical processes by an adaptive lambda-tracker with variable sampling rate. In: Proc. 30. Int. Conf. SSCHE. Tatranské Matliare (Slovakia), May 26– 30 2003. SSCHE Bratislava, CD ROM P142 (2003), ISBN 80-227-1889-0. (Po)


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[5] Danko, J., Veselý, V., Ondrovičová, M.*: PID controller design for uncertain affine SISO systems. In: Proc. 14. Int. Conference Process Control’03. Štrbské Pleso, High Tatras (Slovakia), June 8-11, 2003. KIRP FCHPT STU Bratislava, Slovakia, CD ROM 224 (2003). ISBN 80-227-1902-1. (Po)

[6] Dermíšek, L., Jelenčiak, F.*, Mikleš, J.: Dynamic model of a reactor. In: Proc. 30. Int. Conf. SSCHE. Tatranské Matliare (Slovakia), May 26 – 30 2003. SSCHE Bratislava, CD ROM P115 (2003), ISBN 80-227-1889-0. (Po)

[7] Fikar, M.*, Chachuat, B., Latifi, M. A.: Dynamic optimisation of alternating activated sludge processes. Dynamic optimisation of alternating activated sludge processes. In: Proc. ECC 2003. Cambridge (UK), Sept. 1-4 2003. University of Cambridge, CDROM 536 (2003). (Po)

[8] Karšaiová, M.*, Bakošová, M., Ondrovičová, M.: Optimal control based on simplified mathematical model. Optimal control based on simplified mathematical model. In: Proc. 14. Int. Conference Process Control’03. Štrbské Pleso, High Tatras (Slovakia), June 8-11, 2003. KIRP FCHPT STU Bratislava, Slovakia, CD ROM 218 (2003). ISBN 80-227-1902-1. (Po)

[9] Mikleš, J., Čirka, Ľ.*, Fikar, M.: Youla-Kučera parametrisation in self-tuning LQ control of a chemical reactor. Youla-Kučera parametrisation in self-tuning LQ control of a chemical reactor. In: Proc. 14. Int. Conference Process Control’03. Štrbské Pleso, High Tatras (Slovakia), June 8-11, 2003. KIRP FCHPT STU Bratislava, Slovakia, CD ROM 217 (2003). ISBN 80-227-1902-1. (Po)

[10] Ondrovičová, M.*, Bakošová, M., Karšaiová, M., Čáran, M., Dermíšek, L.: Distillation column control by SIMATIC 300. Distillation column control by SIMATIC 300. In: Proc. 14. Int. Conference Process Control’03. Štrbské Pleso, High Tatras (Slovakia), June 8-11, 2003. KIRP FCHPT STU Bratislava, Slovakia, CD ROM 225 (2003). ISBN 80-227-1902-1. (Po)

[11] Svetíková, M., Annus, J., Čirka, Ľ., Fikar, M.*: Real time control of a laboratory fan heater using dSPACE tools. Real time control of a laboratory fan heater using dSPACE tools. In: Proc. 14. Int. Conference Process Control’03. Štrbské Pleso, High Tatras (Slovakia), June 8-11, 2003. KIRP FCHPT STU Bratislava, Slovakia, CD ROM 211 (2003). ISBN 80-227-1902-1. (Po)

[12] Šperka, Ľ., Andrášik, A., Mészáros, A.*, Smetana, S.: Identification od a fermentation process – hybrid modelling vs. recursive LSM. Identification od a fermentation process – hybrid modelling vs. recursive LSM. In: Proc. 14. Int. Conference Process Control’03. Štrbské Pleso, High Tatras (Slovakia), June 8-11, 2003. KIRP FCHPT STU Bratislava, Slovakia, CD ROM 221 (2003). ISBN 80-227-1902-1. (Po)

[13] Vasičkaninová, A., Zemanovičová, A.: Control design of a multi-kilogram capacity calorimeter. In: Proc. 14. Int. Conference Process Control’03. Štrbské Pleso, High Tatras (Slovakia), June 8-11, 2003. KIRP FCHPT STU Bratislava, Slovakia, CD ROM 213 (2003). ISBN 80-227-1902-1. (Po)

[14] Andrášik, A. Mészáros, A.*, Azevedo, F. S.: Hybrid modelling based adaptive neural controller. In: Proc. 11. Mediterranean Conference on Control and Automation. Rhodos (Greece), June 18-20 2003. NTU Athens, CD ROM T3-030 (2003). ISBN 960-87706-0-2. (Pr)

[15] Dermíšek, L.*, Jelenčiak, F., Mikleš J.: Dynamic model and optimal control of a reactor. In: Proc. 14. Int. Conference Process Control’03. Štrbské Pleso, High Tatras (Slovakia), June 8-11, 2003. KIRP FCHPT STU Bratislava, Slovakia, CD ROM 216 (2003). ISBN 80-227-1902-1. (Pr)

[16] Fikar, M.*, Unbehauen, H., Mikleš, J.: Using controller knowledge in predictive control. In: Proc. 2. IFAC Conference CSD 2003. Bratislava (SK), Sept. 7-10 2003. Ed. STU Bratislava, CDROM 054-31-34 (2003). (Pr)

[17] Mikleš, J.*, Čirka, Ľ., Fikar, M.: H2 Optimal Control of a Chemical Reactor. In: Proc. 11. Mediterranean Conference on Control and Automation. Rhodos (Greece), June 18-20 2003. NTU Athens, CD ROM IV05-01 (2003). ISBN 960-87706-0-2. (Pr)

[18] Latifi, M. A., Fikar, M. Chachuat, M.*: DYNO : un code d'optimisation dynamique des procedes. DYNO : a programm for dynamic optimisation of processes. 9eme Congres Francais de Genie des Procedes, Saint-Nazaire (France), Sept. 9-11 2003. (Po)

[19] Latifi, M. A., Fikar, M., Chachuat, B., Roche, N.*: Regles simples pour la mise en oeuvre en boucle fermee de l'optimisation dynamique des stations d'epuration de petite taille. Sipmle rules for dynamic opimisation of sludge processes. 9eme Congres Francais de Genie des Procedes, Saint-Nazaire (France), Sept. 9-11 2003. (Po)

C. Books and Textbooks [1] Báleš, V., Mészáros, A., Munteam, O., Polakovič, M., Štefuca, V.: Biochemické technológie. Biochemical technologies. AB-

ART, Bratislava. 128 s. (2003). ISBN 80-89006-75-2. [2] Fikar, M.: Decoupling control. Decoupling control. In: Encyclopedia of Life Support Systems (EOLSS), Part 6.43: Control

Systems, Robotics and Automation (Automation (Editors: N. G. Basov and others), EOLSS Publishers, Oxford, 28s. (2003). [3] Mikleš, J.: Automation and control in process industries. In: Encyclopedia of Life Support Systems (EOLSS), Part 6.43:

Control Systems, Robotics and Automation (Automation (Editors: N. G. Basov and others), EOLSS Publishers, Oxford (2003).

[4] Bakošová, M., Fikar, M., Čirka, Ľ.: Základy automatizácie. Laboratórne cvičenia zo základov automatizácie. Automatic contro fundamentals. Laboaratory exercises from automatic control fundamentals. STU, Bratislava, 153s. (2003). ISBN 80-227-1831-9.

DEPARTMENT OF INORGANIC CHEMISTRY

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Head of Department: Telephone: ++421252495257 Prof. Milan Melník, DSc Fax: ++421252493198


I. STAFF Full Professors: Roman Boča, PhD, DSc; Marian Koman, PhD, DSc; Milan Melník, PhD, DSc; Gregor Ondrejovič, PhD, DSc; Jozef Šima, PhD, DSc; Associate Professors: Michal Dunaj-Jurčo, PhD; Adela Kotočová, PhD; Anna Mašlejová, PhD; Iveta Ondrejkovičová, PhD; Peter Segľa, PhD; Dušan Valigura, PhD; Assistant Professors : Mário Izakovič, PhD; Vladimír Jorík, PhD; Ľubov Macášková, PhD; Blažena Papánková, PhD; Anton Sirota, PhD; Miroslav Tatarko, PhD; Research Fellows: Ľubor Dlháň, PhD; Dušan Mikloš, PhD; Milan Ružička; PhD Students: Radovan Herchel (since 1.10.2002); Radoslava Ivaniková (since 1.10.2002); Jana Jašková (since 1.10.2002); Marcela Múdra (since 1.10.2002); Petra Stachová (since 1.10.2002); Katarína Šintalová (since 1.10.2002); Jozef Švorec (since 1.10.2002); Technical staff: Viera Blažová, Andrea Bočová, Marta Danková, Valéria Habudová, Leonard Kováč, Helena Križanová, Silvia Markusová, Marta Polláková, Marta Sprušanská, Klára Valúchová


A. Teaching laboratories: Laboratories of Practical Exercises

B. Research laboratories: Laboratory of Electrochemistry Laboratory of Photochemistry Laboratory of Magnetochemistry Laboratory of Thermal Processing Laboratory of Spectroscopy Laboratory of X-ray Analysis Laboratory of Powder Diffraction

III. TEACHING

A. Undergraduate Study: 1. semester (Bc) Inorganic Chemistry I 3/2/0 Boča, Šima, Kotočová,

Ondrejkovičová, Valigura Inorganic Chemistry I (Laboratory) 0/0/3 2. semester (Bc) Inorganic Chemistry II 2/2/0 Melník, Ondrejovič, Koman, Segľa Inorganic Chemistry II (Laboratory) 0/0/4 1. semester (MSc) Chemical Bond and Chemical

Structure 2/0/0 Boča

Chemistry of Coordination and Organometallic Compounds

2/0/0 Ondrejovič

Inorganic Syntheses 2/0/0 Valigura Inorganic Photochemistry 2/0/0 Šima 1. semester (MSc) Laboratory Practice in the Major

I 0/0/10 Boča, Kotočová, Ondrejkovičová,

Ondrejovič, Růžička Laboratory Practice in the Major

I 0/0/10 Segľa, Valigura

2. semester (MSc) Indirect Methods of Research of 2/2/0 Mašlejová


110

Inorganic Compounds Crystallochemistry 2/0/0 Mikloš Laboratory Practice in the Major II 0/0/6 Jorík, Mašlejová, Mikloš Spectral Methods of Control

Technological Processes 2/2/0 Segľa

2. semester (Bc) Reaction mechanisms of Inorganic Compounds

2/0/0 Šima

3. semester (Bc) Inorganic Materials 2/1/0 Koman Bioinorganic Chemistry 2/1/0 Melník Laboratory of Speciality 0/0/10 3. semester (Bc) Inorganic Biopharmacs 2/0/0 Melník Catalysis 2/0/0 Ondrejkovičová Engineering of Inorganic Substances 2/0/0 Ondrejovič 4. semester (Bc) Diploma Thesis 0/0/27 supervisors


A. VEGA Project No 1/9252/02 Magnetoactive Coordination Compounds (Roman Boča). A rational design of the zero-field splitting parameter in metal complexes lies at the centre of focus. An extensive series of the Ni(II) complexes with a variable coordination sphere (unidentate, bidentate and polydentate ligands) has been synthesized and the recorded magnetic response (the temperature variation of the isothermal magnetic susceptibility and the field dependence of the magnetization) has been analyzed by the developed software. At this stage the sign and magnitude of the zero-field splitting parameter (the axial magnetic anisotropy parameter) can be predicted. New program that handles the complete space spanning by the crystal-field multiplets and Zeeman levels has been outlined. At present the project concentrates to the understanding of the magnetic anisotropy in binuclear complexes. See: Chem. Phys. Lett. 373 (2003) 402-410.

Project duration: from 01. 01. 2002 to 31. 12. 2004 B. DAAD Project No 6/2002 New Crystal, Molecular, Electronic and Magnetic Structures with Functional

Properties (Roman Boča). Molecule-based magnets containing Ni(II) and Co(II) centers have been synthesized and their magnetism was studied extensively by the contemporary battle of the magneto-chemical-physical hardware. See: Inorg. Chem. 42 (2003) 6965-6967.


C. MVTS Project No NEM/Slov/DAAD/CH New Magnetic Materials (Roman Boča). Spin crossover phenomenon was studied by six experimental techniques: magnetic susceptibility measurement, variable-temperature powder diffraction, variable-temperature EXAFS measurements, variable-temperature Moessbauer spectroscopy, variable-temperature infrared spectroscopy and the differential scanning calorimetry. New theoretical insight into the cooperativeness in the solid state has been proposed based upon the concept of the chemical hardness. See: Chem. Phys. 293 (2003) 375-395.


D. MVTS Project No NEM/Slov/DFG/CH Molecular Electronic Multistability (Roman Boča). Multinuclear coordination compounds of iron(III) with cyanide bridges were synthesized where several close-lying electronic states could be stabilized. The effect of the magnetic field to the induced stabilization is investigated. See: Solid State Phenom. 90 (2003) 147-152.


E. APVT Project No 20-009902 Low-Dimensional Magnetic Materials (Roman Boča). Molecular (0D) and chain (1D) coordination compounds were synthesized and their magnetic properties recorded and analyzed. See: Inorg. Chem. 42 (2003) 5801-5803.


F. VEGA Project No 1/9251/02 Preparation and study of novel non-steroid coordination antiflogistics and antituberculotics (Milan Melník).

Synthesis of novel coordination compounds disposing properties of coordination chemotherapeutics which can be applied in human and veterinary medicine represents one of the most perspective fields of bioinorganic chemistry. The synthesis and study of novel nonsteroid coordination antiflogistics and antituberculotics are consistent with these properties. Thus, a search for new types of chemotherapeutics is a great challenge for bioinorganic chemistry. The biocomplexes of copper and iron with various ligands, namely with derivatives of nicotine, salicylic and propionic acids as well as with fenamates are the object of our study in connection


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with the search for coordination antiflogistics. The biocomplexes of copper and magnesium with other group of ligands, namely derivatives of 4-oxoquinolinate are considered to have properties of the potential antituberculotics are also the object of our study. A specific theoretical and experimental procedure characterising the construction of coordination polymers was elaborated. Crystal structure determination of some copper and magnesium complexes contributed to the optimisation of favourable conditions for reactions of ligands forming new compounds in the coordination sphere. The basic factors influencing the relation between the wavelength of irradiation and the photoredox efficiency of iron complexes were formulated. It was found that by photolysis of copper complexes generated hydroxyl radical in solutions participates in photodegradation of some pollutants. The results can be applied to improve ecology. Project duration: from 01. 01. 2002 to 31. 12. 2004


A. Project No 301/02 Picking out of talented students and their motivation in new conditions of social development with respect to the needs of the Faculty of Chemical and Food Technology of the Slovak Technical University (Anton Sirota).

A special questionnaire has been elaborated for research of students' motivation in their choice to study chemistry and their evaluation of the study organisation and the level at the Faculty of Chemical and Food Technology. The questionnaire has been applied to a sample of 178 students of the first course of the Faculty. Their responses have been evaluated and the results obtained are prepared for publishing in a special journal. The results have been compared with those obtained with a similar questionnaire in 1984. The results show that evaluation of students in 2003 differ in many significant aspects from those obtained in the year 1984. It will probably be necessary to adapt the pedagogical process at the Faculty as well as methods how to gain students for study of chemistry to a new situation in the secondary schools education as well as in social life. The similar questionnaire has been elaborated and adapted to the needs of the Faculty of Sciences of the Comenius University in Bratislava. It is supposed to be applied in 2004. The members of the research team organised a special seminar for secondary school teachers in August 2003 with the aim to enhance the quality of chemistry teaching at the schools. Two members of the research team presented their lectures at the seminar. Two members of the research team are chairman and vice-chairman in the club Socrates. The club activates such activities which are in favour of selected talented students of the Faculty. Some members of the research team were involved in a preparation of the national team of the best four secondary school pupils who attended the 35th International Chemistry Olympiad in Greece and were awarded with 2 silver and 2 bronze medals. The members of the research team published 18 papers in journals (in Slovak), presented three lectures at the conferences and two of them published a text book for secondary school pupils on nomenclature of inorganic substances. Project duration: from 01. 01. 2002 to 31. 12. 2004

VI. COOPERATION



Duration

Pharmaceutical Faculty, Comenius University, Bratislava

Synthesis and spectral properties of Schiff base with Cu(II) complexes

Valent Aladár, Assoc. professor, Kalinčiakova 8, 832 32 Bratislava

2002 -

Medical Faculty, Comenius University, Bratislava

Cu(II) Schiff-base complexes as perspective antidotes

Čársky Jozef, professor, Sasinkova 10, 813 72 Bratislava

2000 -



Duration

Materials Science, University of Technology, Darmstadt, Germany

New Crystal, Molecular, Electronic and Magnetic Structures with Functional Properties

Fuess Hartmut, professor, Petersenstrasse 23, 64287 Darmstadt, Germany

1994 -

Institute of Inorganic Chemistry, Johannes-Guttenberg-University, Mainz, Germany

Molecular Electronic Multistability Renz Franz, Dr., Staudinger Weg 9, D-55099 Mainz, Germany

2002 -


112

Institute of Applied Synthetic Chemistry, Vienna University of Technology, Vienna, Austria

Coordination Compounds with Interesting Magnetic Properties

Linert Wolfgang, professor, A-1060 Vienna, Austria 1998 -

Institute of Inorganic and Physical Chemistry, University of Technology, Darmstadt, Germany

New Crystal, Molecular, Electronic and Magnetic Structures with Functional Properties

Haase Wolfgang, professor, Petersenstrasse 23, 64287 Darmstadt, Germany

1994 -

Department of Chemistry, University of Puerto Rico, San Juan, USA

Magnetism of Multinuclear Coordination Compounds and Clusters

Raptis Raphael, professor, San Juan, PR 00931-3346, USA 1994 -

Institute of Solid State Chemistry, Faculty of Chemical Technology, Prague, Czech Republic

RTG analysis of monocrystals and powders

Kratochvíl Bohumil, professor, Technická 5, 16628 Prague 6, Czech Republic

2004 - 2005

York University, Toronto, Canada

X-ray analysis of transition and non-transition metal atoms

Holloway Clive Eduard, director, 4700 Keele Street, North York M3J 1P3, Toronto, Ontario, Canada

1976 -

University of Helsinki, Helsinki, Finland

X-ray analysis of solid compounds Sundberg Markku, professor, A. I. Virtasen aukio 1, P.O. Box 55, Helsinki, Finland

1968 -

Department of Chemistry, University of Jyväskylä, Yyveskilää, Finland

X-ray analysis of solid compounds Sillanpää Reijo, professor, FIN-40351 Jyväskylä, Finland

2003 -

Wroclaw University, Wroclaw, Poland Magnetic properties of solid compounds

Mrozinski Jerzy, professor, 14, F. Joliot-Curie str, 50-383 Wroclaw, Poland

1972 -

Okayama University, Okayama, Japan

Synthesis and magnetic properties of solid compounds

Kojima Masaaki, professor, Tsushima, Okayama, 700-8530 Japan

2003 -

Aoyama Gakuin University, Tokyo Japan

Schiff bases and chemistry of copper complexes

Hasegawa Miki, professor, 6-16-1 Chitosedai Setagaya-ku, Tokyo, 157-8572 Japan

2003 -

Kwansei Gakuin University, Osaka, Japan

Magnetic and spectral properties solid compounds

Mikuriya Masahiro, professor, 2-1 Gakuen, Sanda 669-1337, Japan

2003 -

Ochanomizu University, Tokyo, Japan

PhD students exchange

Fukuda Yutaka, professor, Ochanomizu University,2-1-1 Otsuka, Bunkyo-ku 112-8610, Tokyo, Japan

2003 -



Valid date

Koman Marian Slovak Expert Group of Solid State Chemistry and Physics chairmann 01. 06. 1985 -

Koman Marian Regional Committee of Czech and Slovak Crystallographers vice-president 01. 01. 1992 -

Koman Marian Czech and Slovak Association for Crystal Growth member 01. 02. 1994 - Koman Marian Slovak Society for Industrial Chemistry member 01. 01. 1985 - Moncoľ Ján Czech & Slovak Crystallographic Association member 01. 07. 2001 - Ružička Milan The Czechoslovak Association for Crystal Growth vice-president 1991 -

Ružička Milan Slovak Expert Group of Solid Chemistry and Physics other 1975 -



Valid date

Koman Marian Slovak Expert Group of Solid State Chemistry and Physics chairmann 01. 06. 1985 -


- 113 -

Koman Marian Regional Committee of Czech and Slovak Crystallographers vice-president 01. 01. 1992 - Koman Marian Czech and Slovak Association for Crystal Growth member 01. 02. 1994 - Moncoľ Ján Czech & Slovak Crystallographic Association member 01. 07. 2001 - Ružička Milan The Czechoslovak Association for Crystal Growth vice-president 1991 - Ružička Milan Slovak Expert Group of Solid Chemistry and Physics other 1975 - Melník Milan American Chemical Society member 1998 - Melník Milan Finnish Chemical Society member 1974 - Melník Milan Editioral board MGMC member 1998 - Izakovič Mário European Photochemistry Association member 01. 01. 1997 Tatarko Miroslav European Photochemistry Association member 01. 01. 1996



Date / Duration

Fuess, H. Materials Science, Darmstadt University of Technology, Darmstadt Germany March 2003 (6 days)

Svoboda, I. Materials Science, Darmstadt University of Technology, Darmstadt Germany June 2003 (8 days)



Date / Duration

Jorík, V. Institute of Macromolecular Chemistry, Prague Czech Republic February 2003 (1 day)

Boča, R. Institute of Chemistry, University of Wroclaw, Wroclaw Poland February 2003 (10 days)

Ružička, M. Institute of Physics, Czech Academy of Sciences, Prague

Czech Republic March 2003 (2 days)

Melník, M. Department of Chemistry, University of Helsinki, Helsinki Finland April 2003 (6 days)

Šima, J. Vienna University of Technology, Vienna Austria April 2003 (1 day)

Boča, R. Materials Science, Darmstadt University of Technology, Darmstadt Germany May 2003 (14 days)

Herchel, R. Materials Science, Darmstadt University of Technology, Darmstadt Germany June 2003 (22 days)

Boča, R. Materials Science, Darmstadt University of Technology, Darmstadt Germany June 2003 (22 days)

Papánková, B. Materials Science, Darmstadt University of Technology, Darmstadt Germany June 2003 (14 days)

Mašlejová, A. Materials Science, Darmstadt University of Technology, Darmstadt Germany July 2003 (12 days)

Sirota, A. National and Kapodistrian University, Athens Greece July 2003 (10 days)

Mašlejová, A. ICM 2003 - International Conference on Magnetism, Roma Italy July 2003 (8 days)

Boča, R. ICM 2003 - International Conference on Magnetism, Roma Italy July 2003 (8 days)

Dlháň, Ľ. ICM 2003 - International Conference on Magnetism, Roma Italy July 2003 (8 days)

Herchel, R. Materials Science, Darmstadt University of Technology, Darmstadt Germany August 2003

(21 days)

Dlháň, Ľ. Materials Science, Darmstadt University of Technology, Darmstadt Germany August 2003

(21 days) Boča, R. Johannes-Guttenberg-University, Mainz Germany August 2003 (8 days)

Jorík, V. Structure Solution from Powder Diffraction Data, Stará Lesná Slovakia September 2003

(6 days)

Šima, J. Institute of Chemistry, Hungarian Academy of Sciences, Budapest Hungary October 2003 (1 day)

Melník, M. Institute of Chemistry, Hungarian Academy of Sciences, Budapest Hungary October 2003 (1 day)

Boča, R. Vienna University of Technology, Vienna Austria November 2003 (1 day)

Sirota, A. Christian-Albrechts-University, Kiel Germany December 2003 (4 days)


114



Púčeková, Z. Methyl- and methoxy-salicylatocopper(II) complexes with some biologically active ligands. Valigura, D.

Šípoš, R. Study of equilibria of iron(III) complexes with some kojic acid derivatives. Izakovič, M.

Vasková, Z. Properties of 4-nitrobenzoatocopper(II) complexes with ligands showing biological activity. Valigura, D.


Horváthová, L. Photoredox properties of iron(III) complexes with azidoligands. Šima, J.

Ivaniková, R. Preparation and characterisation of carboxylatonickel(II) complexes with imidazole derivatives. Mašlejová, A.

Jašková, J. Preparation and physical-chemical properties of copper(II) and cobalt(II) complexes with pyridinecarboxylic acids. Segľa, P.

Maťhová, M. Spin transitions in iron complexes. Boča, R.

Šintalová, K. Synthesis and study of physical properties of carboxylate-based coordination compounds. Papánková, B.

VIII. PUBLICATIONS A. Journals [1] Blanáriková-Hlobilová, I., Fišera, Ľ., Pronayová, N., Koman, M.: 1,3-Dipolar Cycloadditions of D-Erythrose- and D-Threose-

derived Alkenes with Nitrones. Collect. Czech. Chem. Commun. 68, 951 – 964, (2003). [2] Boča, M., Boča, R.: Effect of the crystal solvent on magnetic properties of iron(II) complexes. Solid State Phenom. 90-91,

135-140, (2003). [3] Boča, R., Boča, M., Ehrenberg, H., Fuess, H., Linert, W., Renz, F., Svoboda, I.: Spin Crossover in Iron(II) Tris(2-(2-

pyridyl)benzimidazole) Complex Monitored by Variable Temperature Methods: Synchrotron Powder Diffraction, DSC, IR Spectra, Mössbauer Spectra, and Magnetic Susceptibility. Chem. Phys. 293, 375-395, (2003).

[4] Boča, R., Dlháň, L., Mezei, G., Ortiz-Pérez, T., Raptis, R. G., Telser J.: Triangular, Ferromagnetically-Coupled CuII3-Pyrazolato Complexes as Possible Models of Particulate Methane Monooxygenase (pMMO). Inorg. Chem. 42, 5801-5803, (2003).

[5] Boča, R., Dlháň, Ľ.,. Haase, W, Herchel, R., Mašlejová, A.,. Papánková, B.: Limiting negative zero-field splitting in tetrakis(imidazole)bis(acetate)nickel(II) complex. Chem. Phys. Lett. 373, 402-410, (2003).

[6] Boča, R., Gembický, M., Herchel, R., Haase, W., Jager, L., Wagner, C., Ehrenberg, H., Fuess, H.: Ferromagnetism in a dinuclear nickel(II) complex containing triethylenetetramine and tricyanomethanide. Inorg. Chem. 42, 6965-6967, (2003).

[7] Boča, R., Linert, W.: Is there a need for new models of the spin crossover? Monats. Chemie 134, 199-216, (2003). [8] Boča, R.: A tuning of the spin crossover in Fe(II) complexes. Solid State Phenom. 90-91, 141-146, (2003). [9] Dlháň, Ľ., Gembický, M., Herchel, R., Boča, R., Renz, F.: A field induced high-spin molecule: {Fe(II)-Fe(III)6} cluster. A field

induced high-spin molecule: {Fe(II)-Fe(III)6} cluster. Solid State Phenom. 90-91, 147-152, (2003). [10] Hvastijová, M., Boča, R., Kohout, J., Jäger, L., Císařová, I., Kožíšek, J.: Cyanamidonitrate-cobalt (II) complexes of pyrazole

and imidazole ligands. X-ray structure of [Co(NO2NCN)2(pyrazole)4] and [Co(2-methylimidazole)4](NO2NCN)2. Inorg. Chim. Acta 343, 217-223, (2003).

[11] Jorík, V., Ondrejkovičová, I., von Dreele, R.B., Ehrenberg, H.: X-ray powder diffraction structural characterization of iron(III) chloro- and bromo- complexes of triphenylphosphine oxide. Cryst. Res. Technol. 2, 14-1871, (2003).

[12] Koman, M., Martiška, L., Valigura, D., Glowiak T.: 1H-Nicotinamidium 3,5-dinitrosalicylate. Acta Crystallogr. E59, o441–o442, (2003).

[14] Kráľová, K., Masarovičová, E., Štroffeková, O., Ondrejkovičová, I: Effect of cadmium compounds on growth and metal accumulation in Zea mays L. in the presence of hydroxyphenyl-b-cyclodextrin. Fresenius Environment. Bull. 12, 852-856, (2003).

[15] Langer, V., Gyepesová, D., Koman, M., Kapitán, P., Babjak, M., Gracza, T., Koóš, M.: Preparation and crystal structure of (1S, 5S, 7S, 8R)-8-hydroxy-7-phenyl-2,6-dioxabicyclo[3.3.0]octan-3-one. Molecules 8, 599-606, (2003).

[16] Mašlejová, A., Gembický, M., Svoboda, I., Boča, R.: Magnetic Anisotropy in Nickel(II) Complexes. Solid State Phenom. 90-91, 171-176, (2003).

[17] Mojumdar, S. C., Martiška, L., Valigura, D., Melník, M.: Thermal and Spectral Properties of Halogenosalicylato-Cu(II) Complexes. J. Therm. Anal. Cal. 74, 904–914, (2003).

[18] Múdra, M., Monco,ľ J., Švorec, J., Melník, M., Lönnecke, P., Glowiak, T., Kirmsee, R.: Crystal structures and spectroscopic behavoiur of polymeric copper(II) chloroacetate adducts with 3- and 4-pyridylmethanol. Inorg. Chem. Commun. 6, 1259-1265, (2003).

[19] Paharová, J., Černák, J., Boča, R., Žák, Z.: Cyano Bridged One-dimensional Tetracyanonickellate Ni(dien)(mea)Ni(CN)4 : Preparation, Structure and Magnetic Properties. Inorg. Chim. Acta 346, 25-31, (2003).

[20] Papánková, B., Šimon, P., Boča, R.: Fitting The Heat Capacity For Spin Crossover Systems. Solid State Phenom. 90-91, 177-182, (2003).

[21] Šima, J., Horváthová, L., Izakovič, M.: Photoredox reactions occurring in methanolic solutions of iron(III) azido complexes with N,N'-ethylenebis(salicylaldiminato) Schiff base derivatives. Monatsh. Chem., 134, 1 – 8, (2003).


- 115 -

[22] Šima, J., Horváthová, L.: Bell-shaped dependence of the quantum yield of Fe(II) formation in irradiated methanolic solutions of iron(III) azido complexes with N,N'-ethylenebis(benzoylacetoneiminato) Schiff base derivatives. Pol. J. Chem. 77, 1857-1866, (2003).

[23] Wiliams, Ch., Morris, H., Švorec, J., Valková, M., Valko, M., Moncoľ, J., Mazúr, M., Valach, F., Melník M.: A study of copper(II) carboxylato complexes with the biological ligands nocotinamide and papaverine. J. Mol. Struct. 659, 53-60, (2003).

[24] Mojumdar, S., C., Lebrušková, K., Valigura, D.: Thermal Stability and Spectral Properties of Pyrazine-2,3-dicarboxylatocopper(II) Complexes with Ronicol. Chem. Pap. 57(3), 245–249, (2003).

B. Conferences [1] Hudecová*, D., Ditteová, P., Valigura, D., Augustín, J., Melník, M.: Some new salicylatocopper(II) complexes and their

biological properties. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 650, (2003). [2] Ondrušová*, D., Jóna, E., Koman, M., Šimon, P.: Structural study of metal N-ethyl-N-phenyl-dithiocarbamates and their

influence on the properties of vulcanizates. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 659, (2003).

[3] Melník, M.*: Copper(II) complexes – perspective antiinflammatory drugs. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 636, (2003).

[4] Boča, R.*: Magnetism of Multi-Term Systems. In: Monograph Series of the International Conferences on Coordination Chemistry held periodically at Smolenice in Slovakia: Progress in Coordination and Bioinorganic Chemistry, Bratislava 2003. Ed. M. Melnik, A. Sirota, STU Press, pp. 227-232 (2003). ISBN 80-227-1891-2

[5] Dlháň* Ľ., Boča R., Gembický M., Falk K., Haase W., Jäger L., Wagner C.: Ferromagnetic Exchange And Ferromagnetism Of A Nickel(II) Tricyanomethanide-Triethylenetetramine Dinuclear Complex. In: Monograph Series of the International Conferences on Coordination Chemistry held periodically at Smolenice in Slovakia: Progress in Coordination and Bioinorganic Chemistry, Bratislava 2003. Ed. M. Melnik, A. Sirota, STU Press, pp. 239-244 (2003). ISBN 80-227-1891-2

[6] Fargašová* A., A. Mašlejová, I. Ondrejkovičová, E. Havránek: Environmental risk assessment of copper(II) cyanato-complexes with imidazole ligands to alga scenedesmus quadricauda. In: Monograph Series of the International Conferences on Coordination Chemistry held periodically at Smolenice in Slovakia: Progress in Coordination and Bioinorganic Chemistry, Bratislava 2003. Ed. M. Melnik, A. Sirota, STU Press, pp. 401-406. (2003). ISBN 80-227-1891-2.

[7] Fargašová*, A., Mašlejová, A., Ondrejkovičová, I.: Influence of Cu(II) complexes with imidazole ligands on alga scenedesmus quadricauda physiology. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 803-804, (2003).

[8] Herchel, R.*, Boča, R., Baran, P., Raptis, R.: Exchange Interactions In Octanuclear Complexes. In: Monograph Series of the International Conferences on Coordination Chemistry held periodically at Smolenice in Slovakia: Progress in Coordination and Bioinorganic Chemistry, Bratislava 2003. Ed. M. Melnik, A. Sirota, STU Press, pp. 245-250 (2003). ISBN 80-227-1891-2

[9] Koman*, M., Melník, M., Moncoľ, J., Lörinc, Š., Glowiak, T.: Structural study of copper(II) aminobenzoates with pyridine and its some derivatives. In: Monograph Series of the International Conferences on Coordination Chemistry held periodically at Smolenice in Slovakia: Progress in Coordination and Bioinorganic Chemistry, Bratislava 2003. Ed. M. Melnik, A. Sirota, STU Press, pp. 121-126 (2003).

[10] Koman*, M., Melník, M., Moncoľ, J.: Structural aspects of Cu(II) complexes with bio-active ligand. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97 641-642, (2003).

[11] Kráľová, K., Masarovičová*, E., Ondrejkovičová, I., Štrofeková I.: Uptake accumulation and effects of zinc(II) compounds on young maize plants. In: Monograph Series of the International Conferences on Coordination Chemistry held periodically at Smolenice in Slovakia: Progress in Coordination and Bioinorganic Chemistry, Bratislava 2003. Ed. M. Melnik, A. Sirota, STU Press, pp. 407-412 (2003). ISBN 80-227-1891-2

[12] Mašlejová, A.*, Ivaniková, R., Svoboda, I.: Synthesis, Spectral Properties and Structure of Nickel (II) Formatocomplexes with Imidazole Ligands. In: Monograph Series of the International Conferences on Coordination Chemistry held periodically at Smolenice in Slovakia: Progress in Coordination and Bioinorganic Chemistry, Bratislava 2003. Ed. M. Melnik, A. Sirota, STU Press, pp. 133-138 (2003). ISBN 80-227-1891-2.

[13] Mazúr, M.*, Stachová, P., Kleinová, M., Valko, M.: Mn(II) EPR spectroscopy of sol-gel process. In: Monograph Series of the International Conferences on Coordination Chemistry held periodically at Smolenice in Slovakia: Progress in Coordination and Bioinorganic Chemistry, Bratislava 2003. Ed. M. Melnik, A. Sirota, STU Press, pp. 311-316 (2003). ISBN 80-227-1891-2

[14] Mazúr, M., Švorec, J., Kleinová, M., Valko*, M.: Cu(II) ESR spectroscopy of sol-gel progres. In: Monograph Series of the International Conferences on Coordination Chemistry held periodically at Smolenice in Slovakia: Progress in Coordination and Bioinorganic Chemistry, Bratislava 2003. Ed. M. Melnik, A. Sirota, STU Press, pp. 317-322 (2003). ISBN 80-227-1891-2

[15] Mikloš*, D., Segľa, P.,Melník, M., Sundberg, M.R., Lönecke, P.: Crystallographic study of Cu(II) pyridinecarboxylate complexes – Structure of [Cu(II) (2-MeSnic)2(CH3OH)]2 and [Cu(II)(2-MeSnic)2(py)2(H2O)2]. In: Monograph Series of the International Conferences on Coordination Chemistry held periodically at Smolenice in Slovakia: Progress in Coordination and Bioinorganic Chemistry, Bratislava 2003. Ed. M. Melnik, A. Sirota, STU Press, pp. 139-144 (2003). ISBN 80-227-1891-2

[16] Mojumdar, S. C., Martiška, L., Valigura, D.: Thermal, Elemental and Spectral Analysis of Cu(II) Complexes with Halogenosalicylates. NATAS (North American Thermal Analysis Society) 31, 1811–1820, (2003). – full paper.

[17] Moncoľ*, J., Koman, M., Múdra, M., Melník, M., Lörinc, Š., Glowiak, T., Lönnecke, P.: Coordination polymers of copper(II) carboxylate with 3-pyridylmethanol and N,N-diethylnicotinamide. In: Monograph Series of the International Conferences on Coordination Chemistry held periodically at Smolenice in Slovakia: Progress in Coordination and Bioinorganic Chemistry, Bratislava 2003. Ed. M. Melnik, A. Sirota, STU Press, pp. 219-224 (2003). ISBN 80-227-1891-2

[18] Múdra, M.*, Moncoľ, J., Lönnecke, P. Melník, M.: Synthesis, spectral properties and crystal structure of trans- Cu(2-bromopropionate)2(2-pyridylmethanol)2. In: Monograph Series of the International Conferences on Coordination Chemistry held periodically at Smolenice in Slovakia: Progress in Coordination and Bioinorganic Chemistry, Bratislava 2003. Ed. M. Melnik, A. Sirota, STU Press, pp. 151-156 (2003). ISBN 80-227-1891-2

[19] Ondrejkovičová*, I., Melník, M.: Structural aspects of mononuclear Iron coordination compounds. In: Monograph Series of the International Conferences on Coordination Chemistry held periodically at Smolenice in Slovakia: Progress in Coordination and Bioinorganic Chemistry, Bratislava 2003. Ed. M. Melnik, A. Sirota, STU Press, pp. 157-162 (2003). ISBN 80-227-1891-2

[20] Ondrejovič*, G., Kotočová, A.: Electronic spectra and electrochemistry of distorted mono and tetranuclear pentacoordinate


116

copper(II) complexes. In: Monograph Series of the International Conferences on Coordination Chemistry held periodically at Smolenice in Slovakia: Progress in Coordination and Bioinorganic Chemistry, Bratislava 2003. Ed. M. Melnik, A. Sirota, STU Press, pp. 273-278 (2003). ISBN 80-227-1891-2

[21] Papánková, B.*, Boča, R., Chnápková, V., Dlháň, Ľ., Svoboda, I.: Synthesis, Crystal Structure and Magnetic Properties of Cobalt (II) Complex with Pyridine - 2-Carboxylic Acid. In: Monograph Series of the International Conferences on Coordination Chemistry held periodically at Smolenice in Slovakia: Progress in Coordination and Bioinorganic Chemistry, Bratislava 2003. Ed. M. Melnik, A. Sirota, STU Press, pp. 279-284 (2003). ISBN 80-227-1891-2

[22] Rudinská, E., Sirota*, A., Kubranová, M., Jóna, E.: 4-R-derivatives (R = H, Me, Et, OH) and their interactions with Co- exchanged montmorillonite. In: Monograph Series of the International Conferences on Coordination Chemistry held periodically at Smolenice in Slovakia: Progress in Coordination and Bioinorganic Chemistry, Bratislava 2003. Ed. M. Melnik, A. Sirota, STU Press, pp. 323-328 (2003). ISBN 80-227-1891-2

[23] Segľa, P.*, Mikloš, D., Jašková, J., Palicová, M., Švorec, J., Fischer, A., Melník, M.: Synthesis, spectral properties and crystal structures of copper(II) pyridinecarboxylates. In: Monograph Series of the International Conferences on Coordination Chemistry held periodically at Smolenice in Slovakia: Progress in Coordination and Bioinorganic Chemistry, Bratislava 2003. Ed. M. Melnik, A. Sirota, STU Press, pp. 163-168 (2003). ISBN 80-227-1891-2

[24] Stachová, P.*, Valigura, D., Melník, M., Valko, M., Mazúr, M.: Spectral properties of Cu(II) 2-nitrobenzoate and crystal structure of [Cu2(2-NO2bz)4(H2O)2].2H2O. In: Monograph Series of the International Conferences on Coordination Chemistry held periodically at Smolenice in Slovakia: Progress in Coordination and Bioinorganic Chemistry, Bratislava 2003. Ed. M. Melnik, A. Sirota, STU Press, pp. 169-174 (2003). ISBN 80-227-1891-2

[25] Šima, J.*: Photoredox chemistryof coordination compounds chalenges and limitations. In: Monograph Series of the International Conferences on Coordination Chemistry held periodically at Smolenice in Slovakia: Progress in Coordination and Bioinorganic Chemistry, Bratislava 2003. Ed. M. Melnik, A. Sirota, STU Press, pp. 291-296 (2003). ISBN 80-227-1891-2

[26] Švorec, J.*, Kleinová, M., Valko, M., Mazúr, M., Melník, M., Wiliams, C.J., Morris, H., Birdsall, W.J.: Copper(II) chloride complexes with the biologically important ligands creatinine, kinetin, xantine and guanine : an EPR and electronic spectroscopy. In: Monograph Series of the International Conferences on Coordination Chemistry held periodically at Smolenice in Slovakia: Progress in Coordination and Bioinorganic Chemistry, Bratislava 2003. Ed. M. Melnik, A. Sirota, STU Press, pp. 393-398 (2003). ISBN 80-227-1891-2

[27] Tatarko*, M., Boča, R., Dlháň, L., Makáňová, D., Ondrejovič, G., Mrozinski, J.: Magnetic Exchange In Hexahalide Tetrakis (Piperidine/ Triphenylphospineoxide)Tetracopper(Ii) Complexes. In: Monograph Series of the International Conferences on Coordination Chemistry held periodically at Smolenice in Slovakia: Progress in Coordination and Bioinorganic Chemistry, Bratislava 2003. Ed. M. Melnik, A. Sirota, STU Press, pp. 297-302. (2003). ISBN 80-227-1891-2

[28] Valigura, D.*, Hudecová, D., Melník, M., Cibíčková, D., Martiška, L.: Halogenosalicylato copper(II) complexes – characterization and antimicrobial activity. In: Monograph Series of the International Conferences on Coordination Chemistry held periodically at Smolenice in Slovakia: Progress in Coordination and Bioinorganic Chemistry, Bratislava 2003. Ed. M. Melnik, A. Sirota, STU Press, pp. 425-430 (2003). ISBN 80-227-1891-2

[29] Dudová, B., Ditteová, P., Hudecová, D., Palicová, M., Segľa, P., Melník, M.: Effects of N-heterocyclic copper carboxylates on the growth and morphology of flamenous fungi. In: Colloquium Fungi as Model Organisms in Research and Biotechnology II. Olomouc 5. - 6. 9. 2002. Czech Mycol. 55, 106 (2003).

[30] Fargašová, A., Ondrejkovičová, I.: Cd(II) complexes inhibitory effects on green alga scenedesmus quadricauda. Industrial Toxicology 2003, Proceedings, Bratislava, June 18-20. 2003, p. 117-119 ISBN 80-968011-5-5

[31] Hudecová, D., Cibičková, D., Dudov,á B., Valigura, D., Martiška, L., Melník, M.: Some biological properties of new copper(II) halogenosalicylates. In: Colloquium Fungi as Model Organisms in Research and Biotechnology II. Olomouc 5. - 6. 9. 2002. Czech Mycol. 55, 109-110 (2003).

[32] Valent, A.*, Kohútová, M., Melník, M., Hudecová, D., Dudová, D.: Antimikróbna aktivita meďnatých komplexov. Antimicrobial activity of coppercomplexes. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 651-652, (2003).

[33] Dlhaň*, Ľ., Boča, R., Gembický, M., Herchel, R.: Ferromagnetism in a dinuclear Ni(II) complex. In: Development of materials science in research and education, Račkova dolina, Sept. 15-19 2003. NOI Press, Bratislava 2003, pp. 21-22. ISBN 80-89088-16-3

[34] Koman*, M., Melník, M., Moncoľ, J.: Effect of anionic ligands on coordination ability of neutral ligands in the structure of coordination compounds of Cu(II). In: Development of Materials Science in Research and Education, Sept. 15-19, 2003, Račkova dolina, pp. 27-28, (2003). ISBN 80-89088-16-3

[35] Mikloš*, D., Segľa P., Jašková, J., Melník M., Silanpää, R.: Structure and properties of some Co(II) pyridinecarboxylate complexes. In: Development of Materials Science in Research and Education, Sept. 15-19, 2003, Račkova dolina, p. 42-43 (2003). ISBN 80-89088-16-3

[36] Ondrejovič*, G., Kotočová, A.: Koordinačné supermolekuly Cu4OX6L4. Coordination supermolecules Cu4OX6L4. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 644-645 (2003).

[37] Papánková, B.*: Molecule - based magnets - crystal engineering. In: Development of materials science in research and education, Račkova dolina, Sept. 15-19 2003. NOI Press, Bratislava 2003, pp. 55-56. ISBN 80-89088-16-3

[38] Boča, R.*: A Solid-State Cooperativeness In Iron(II) Complexes Exhibiting The Spin Crossover. International Conference on Magnetism, ICM2003, Roma, Italy, July 27-August 1, 2003. Abstract 5Q-pm-23, p. 697.

[39] Dlháň*, Ľ., Boča, R., Gembický, M., Herchel, R., Renz, F.: Field-Induced Level Crossing Stabilizing A High-Spin State In A Heptanuclear Iron(II)-Iron(III)6 Cluster. International Conference on Magnetism, ICM2003, Roma, Italy, July 27-August 1, 2003. Abstract 5Q-pm-24, p. 697.

[40] Mašlejová, A.*, Boča, R., Dlháň, Ľ., Herchel, R.: Magnetic Anisotropy In Nickel Complexes As Determined By Combined Magnetic Susceptibility/ Magnetization/ Theoretical Studies. International Conference on Magnetism, ICM2003, Roma, Italy, July 27-August 1, 2003. Abstract pm, 2S-am-14, p.200.

[41] Svoboda, I., Papánková, B., Chnápková, V., Fuess, H.: Trans- Diaquabis(pyridine-2carboxylatoN,O)cobalt(II) dihydrate. Zeitschrift für Kristallographie, Supplement Issue No.20, 2003, 58, 10.-13. 3. 2003. ISBN 3 - 486 - 64273 - 1

[42] Mojumdar, S. C.*, Martiška, L., Valigura, D.: Thermal, Elemental and Spectral Analysis of Cu(II) Complexes with


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Halogenosalicylates. In: 31st Annual Conference of NATAS (North American Thermal Analysis Society) p. 182, (2003). [43] Jorík, V., Von Dreele, R.B.: X-ray and neutron powder diffraction study of sodium cation distribution in hydrated Na-Y zeolite.

X-ray and neutron powder diffraction study of sodium cation distribution in hydrated Na-Y zeolite. Structure Solution from Powder Diffraction Data, SSPD 03, Book of Abstracts, Sept. 14-19, 2003, Stará Lesná,CCA, Slovakia, p.37

[44] Izakovič, M.*: I. Test z výpočtov - jednoduché stechiometrické výpočty. II. Riešenie a hodnotenie úloh testu. Calculation test - simple stoichometric calculations. “XVII. Seminár pre sredoškolských učiteľov cjémie ‘Príprava študentov stredných škôl na vysokoškolské štúdium chémie.’", 27.8 - 28.8. 2003, FCHPT STU, Bratislava."

[45] Jašková, J.*, Segľa, P., Mikloš, D., Melník, M.: Štúdium pyridínkarboxylátomeďnatých komplexov s chelátovými N-heterocyklickými ligandami. Study of pyridinecarboxylate copper(II) complexes with chelate N-heterocycle ligands In: Študentská vedecká konferencia, 9-10.4.2003, Bratislava, pp. 220

[46] Ondrejkovičová*, I.: I. Test z názvoslovia koordinačných zlúčenín. II. Riešenie a hodnotenie úloh testu. I. Test - Naming of coordination compounds. II. Solutions and evaluating of test excercises. "XVII. Seminár pre sredoškolských učiteľov cjémie ‘Príprava študentov stredných škôl na vysokoškolské štúdium chémie.’", 27.8 - 28.8. 2003, FCHPT STU, Bratislava."

[47] Ondrejkovičová*, I.: Názvoslovie koordinačných zlúčenín. Naming of coordination compounds. "XVII. Seminár pre sredoškolských učiteľov cjémie ‘Príprava študentov stredných škôl na vysokoškolské štúdium chémie.’", 27.8 - 28.8. 2003, FCHPT STU, Bratislava."

[48] Valigura, D.*: Jednoduché stechiometrické výpočty. Simple stoichometric calculations. "XVII. Seminár pre sredoškolských učiteľov chémie ‘Príprava študentov stredných škôl na vysokoškolské štúdium chémie.’”, 27.8 - 28.8. 2003, FCHPT STU, Bratislava."

E. Others [1] Ondrejkovičová, I.: a) Úlohy študijnej časti školského kola, b) Riešenie úloh študijnej časti školského kola, c) Zadania úloh

školského kola, d) Riešenia úloh školského kola, e) Zadania úloh regionálneho kola, f) Riešenia úloh regionálneho kola. a) Study part of school circle - problems. b) Study part of school circle - solutions of problems. c) School circle - problems. d) School circle – solutions of problems. e) Regional circle – problems. f) Regional circle – solutions of problems. "Chemická olympiáda, 40. ročník, 2003/2004, kategória E a F, IUVENTA, Bratislava, (2003). ISBN 80-8072-011-8; EAN 9788080720117, ISBN 80-8072-012-6; EAN 9788080720124"

DEPARTMENT OF INORGANIC TECHNOLOGY

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Head of Department: Telephone: ++421252963637 Prof. Pavel Fellner, PhD, DSc Fax: ++421252 92 01 71


I. STAFF Full Professors: Prof. Pavel Fellner, PhD, DSc Associate Professors: Jana Gabčová, PhD; Ján Híveš, PhD; Marta Chovancová, PhD; Ján Valtýni, PhD Assistant Professors : .Anna Žúžiová, PhD Research Fellows: Peter Adamčík; Vladimír Danielik, PhD; Vladimír Khandl; Matilda Zemanová, PhD PhD Students: Marta Ambrová; Michaela Benová; Zuzana Gáliková; Jana Jurišová; Michaela Nemčeková. Technical staff: Viliam Cauner; Daniela Dančová; František Kollár.


A. Teaching laboratories: Molten Salt Chemistry Laboratories Laboratories of Chemical Inorganic Syntheses and Industrial Inorganic Chemistry

B. Research laboratories: Molten Salt Chemistry and Electrochemistry Laboratories Technical Electrochemistry Laboratories Electroplating, Special Coatings and Corrosion Laboratories

III. TEACHING

A. Undergraduate Study: 3. semester (Bc) Fundamental Principles of Inorganic

Technology 2/2/0 Gabčová, Valtýni

5. semester (Bc) Corrosion and Material Surface Treatment

2/0/2 Chovancová

1. semester (MSc) Phase Equilibria 1/2/0 Gabčová Corrosion and Material Protection 2/1/0 Chovancová, Zemanová Applied Thermodynamics 2/2/0 Fellner, Danielik Laboratories I. 0/0/8 Gabčová, Híveš, Chovancová,

Žúžiová 2. semester (MSc) Chemical Reaction Engineering 2/2/0 Valtýni, Híveš Applied Electrochemistry 2/2/0 Híveš Laboratories II. 0/0/8 Gabčová, Híveš, Chovancová,

Žúžiová 3. semester (MSc) Fertilizers 2/0/0 Žúžiová, Gabčová Electrochemical Engineering 1/1/0 Híveš, Fellner Elements of System Engineering 1/1/0 Valtýni, Danielik Laboratories III. 0/0/10 Danielik, Fellner, Gabčová, Híveš,

Chovancová, Valtýni, 4. semester (MSc) Diploma work 0/0/27 Danielik, Fellner, Gabčová, Híveš,

Chovancová, Valtýni,


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A. VEGA Project No 1/9425/02 Preparation and Properties of Composite and Alloy Layers on Metal Substrates (Marta Chovancová)

Corrosion resistance of teflon sealed anodized aluminium was investigated by standard test and impedance spectroscopy. PTFE dip coating on anodized aluminium belongs to the new way of material preparation. Sealing quality and compactness of the prepared materials is the best one for PTFE sealing after anodic oxidation in the phosphoric acid electrolyte.

The combined two steps sealing method of anodic oxide coatings on aluminium has been designed. This sealing method is able to substitute classical hydrothermal sealing.

The preparation of electrochemical composite coatings with nickel matrix and Si dispersion particles has been studied. The influence of electrode position on the silicon content in the coatings has been tested. The participation of solid Cu and A2O3 powder particles in the transfer of charge through the heterogeneous system consisting of an electrolyte and both conducting and non-conducting powder particles was studied by means of EIS.

The corrosion resistance and mechanical properties of Ni – W alloy coatings electrodeposited from the water solutions has been investigated by the standard tests and anodic polarisation curves.

Basic physical and chemical features of insulation layers of pipeline materials were verified by the laboratory tests. The samples were exposed to QUV-tester in order to define the influence of UV radiation on degradation of insulation materials. Insulation features were assessed on the base of cathodic polarisation curves. The test of endurance against the loss of cohesion was evaluated according to the standard.

Corrosion under stress of steel pipe samples in modelled environment of sand and clay has been laboratory tested. For each soil, there were performed four variants of steel sample exposition. The influence oíf cathode protection on corrosion of monitored steel samples is discussed.

Project duration: from January 2002 to December 2004 B. VEGA Project No 1/9426/02 Thermodynamics and kinetics of the chemical and electrochemical

reactions in the electrolyte at the phase boundary aluminium- melt (Pavel Fellner) Impurities are introduced to the electrolyte for aluminium smelting with raw materials or they originate from the reactions of construction materials of the electrolytic cells and/or electrodes with the electrolyte.

They are responsible for contamination of aluminium, but they can also participate in the reactions responsible for the decrease of current efficiency or they can escape from the cell and to pollute environment. Importance of research of impurities will be stressed when the inert anodes (which are now tested in an industrial trial) are introduced.

Aim of the project is investigation of the reactions of aluminium dissolved in cryolite-based melts with impurities like sulphates using electrochemical methods (linear and cyclic voltametry, chronopotentiometry, impedance methods). There is no generally accepted theory explaining behavior of impurities in the aluminium electrolyte and they role in decreasing of current efficiency. Aim of the project is to supply experimental data for a new theory of the back reactions of dissolved aluminium.

The electrolyte will consist of the molten system NaF - AlF3. We will start to investigate the reactions in molten NaF at the temperature of 1000 °C. The addition of AlF3 will make it possible to decrease the temperature to the range of 700 – 750 °C.

In the second stage (1.5 years from beginning of the project) we plan to investigate behavior of the impurities originating from dissolution (corrosion) of the inert anodes.

The proposed project is demanding because of high reactivity of aluminium dissolved in the melt at the temperatures of 750 – 1050 °C. Investigation of fast electrochemical reactions requires suitable experimental technique. The proposed research team is skilled enough for the work with molten salts. We have the electrochemical analyzer Autolab which is suitable for the electrochemical measurements in molten salts.

Project duration: from January 2002 to December 2004

C. E 02.02.01 Concept of twosteps transmutation (Pavel Fellner) Phase equilibria and electrochemical properties of the lanthanide and actinide fluorides, literature rewiev and experimental meassurements

Project duration: from October 2003 to December 2006


120


VI. COOPERATION



Duration

Boge Slovakia, a.s. Trnava The analysis of anodic layer Ing. Karol Mečár 14.1. - 31.7.2003

Thermosolar Žiar, s.r.o. 3.2. - 31.10.2003

SHMÚ Balance of green house emissions Ing. Janka Szemesova 16.6. - 31.10.2003



Duration

Soil and Water Ltd. Finland 7.11.2002 -

30.4.2003 NTNU Trondheim, Norway Sulphur in cryolitic melt Prof. Jomar Thonstad January -

December 2003 C. Membership in Domestic Organizations and Societies


Valid date

M. Chovancová

Slovak Society for Surface Tretment and Technology other from 1995

M. Chovancová Slovak Chemical Society member from 1987

M. Chovancová Slovak Cleaner Production Centre member from 1993

M. Chovancová

Union of Slovak Scientific and Technological Societies member from 1972

J. Híveš Slovak Society for Surface Tretment and Technology member from 1987

J. Híveš Slovak Chemical Society member from 2000

J. Híveš Union of Slovak Scientific and Technological Societies member from 1987

A. Žúžiová Slovak Chemical Society member from 1993

A. Žúžiová Union of Slovak Scientific and Technological Societies member from 1972

J. Gabčová Slovak Chemical Society member from 1972

J. Gabčová Union of Slovak Scientific and Technological Societies member from 1972

J. Valtýni Union of Slovak Scientific and Technological Societies member from 1972

V. Khandl Union of Slovak Scientific and Technological Societies member from 1972

V. Danielik Slovak Chemical Society member from 1992 M. Zemanová Slovak Chemical Society member from 1992

M. Zemanová Slovak Society for Surface Tretment and Technology member from 1995

P. Fellner Slovak Chemical Society member from 1972

P. Fellner Union of Slovak Scientific and Technological Societies member from 1972

P. Fellner Slovak Society for Surface Tretment and Technology member from 1995

P. Fellner Scientific Board of UACH SAV member 2003 P. Fellner Editorial Board of Chemical Papers member 2003

P. Fellner Scientific Board of Faculty of Technology of University of Trenčín member 2003


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Valid date

P. Fellner EFCE, group Electrochemical Engineering member from 1999 J. Híveš International Society of Electrochemistry member from 2000

E. Visitors from abroad


Date / Duration

Prof. J. Thonstad NTNU, Trondheim Norway March 2003 (3 days)

Prof. J. Thonstad NTNU, Trondheim Norway September 2003 (3 days)

Prof. J. Thonstad NTNU, Trondheim Norway November 2003 (4 days)

Dr. C. Bessada + 2 PhD Students CNRS, Orleans France November 2003

(1 day)

Dr. D. Schröterová VŠCHT, Prague Czech Republic June 2003 (1 day)

Prof. V. Sharma Florida Institute, Melbourne USA May 2003 (1 day)

Prof. V. Sharma Florida Institute, Melbourne USA November 2003 (1 day)

Dr. K. Bouzek VŠCHT, Prague Czech Republic May 2003 (1 day)

Dr. K. Bouzek VŠCHT, Prague Czech Republic

November 2003 (1 day)



Date / Duration

P. Fellner Symposium on Ionic Liquids France June 2003 (4 days)

P. Fellner VŠCHT, Prague Czech Republic June 2003 (1 day)

M. Zemanová BRD FZ Karlsruhe Germany October - December 2003 (3 month)

M. Ambrová NTNU, Trondheim Norway April – June 2003 (3 months)

M. Chovancová AKI Czech Republic October 2003(3 days)

M. Chovancová Progresívni a netradiční technológie povrchových úprav Czech Republic


Z. Gáliková Progresívni a netradiční technológie povrchových úprav Czech Republic




Báchor, M. Composite coatings I. Zemanová, M. Čech, J. Thermal analysis Gabčová, J. Kamenár, J. Combined sealing of anodically oxidized aluminium Chovancová, M. Kováč, L. Trends in the Treatment of Spent Nuclear Fuels Fellner, P. Mikulášová, M. Preparation of Ni(II) complexes Adamčík, P. Obžerová, L. Magnesium ammonia sulphates as N-S-Mg Fertilizers Žúžiová, A. Onderčin, M. Protection of pipelines in gas industry Híveš, J. Pentrák, M. Emissions of greenhouse gases in ZSNP Žiar Danielik, V. Podzimek, F. Differential thermal analysis Gabčová, J.


Benová, M. Electrical conductivity of suspenses Híveš, J. Ivanová, Z. Phase diagram of the system KF - K2TaF7 - Ta2O5 Boča, M. Jurišová, J. Methods of utilization of Slovak dolomites Fellner, P.


122

Makovíniová, D. Deposition of Ni-W Alloy Coatings from Aqueous Electrolytes. Quality of coatings Chovancová, M.

Nemčeková, M. Reactions of sulphur compounds in aluminium electrolytic cell Gabčová, J. Pachingerová, D. Characterization of pigmented anodically oxided coatings Zemanová, M. Tóthová, M. Phase equilibria in the system NaF - KF - AlF3 Danielik, V.


Korenko, M. Relationship between the content of sodium in aluminium and cathodic overvoltage during electrolysis and solubility of some sulphides in cryolite-base

Fellner, P.

VIII. PUBLICATIONS A. Journals [1] Chrenkova M., Danielik V., Kubikova B., Daněk V.: Phase diagram of the system LiF-NaF-K2NbF7. Calphad 27 (1), 19 - 26

(2003). [2] Zemanová, M., Híveš, J., Chovancová, M.: Study of Anodic Oxide Layers by Electrochemical Impedance Spectroskopy

(EIS). Solid State Phenomena, 90 - 91, 455 - 460 (2003). [3] Zemanová, M., Chovancová M.: Sol-Gel Method for Sealing Anodized Aluminium. Metal Finishing 101(12), 14 - 16 (2003). [4] Fellner P., Danielik V.: Inconsistency of the Thermodinamic Model of Molten Salt Mixtures Based on the Ion Equivalent

Fractions. Chem. Pap. 57(4), 237 - 239 (2003). [5] Gáliková Z., Chovancová M.: Vlastnosti zliatinových povlakov Ni - W vylúčených z vodných elektrolytov. Properties of the Ni-

W alloy layers deposited from aqueous solutions. Acta Mechanica Slovaca 4 - A/2003, 51 - 56 (2003). [6] Chovancová M., Híveš J., Fellner P., Zemanová M.: Testovanie izolačných vrstiev potrubných materiálov - I. časť. Testing of

the isolation layers on pipeline materials. Part I. Slovgas 2, 22 - 24 (2003). [7] Chovancová M., Híveš J., Fellner P., Zemanová M.: Testovanie izolačných vrstiev potrubných materiálov - II.časť. Testing of

the isolation layers on pipeline materials. Part II. Slovgas 3, 13 - 15 (2003). [8] Chovancová M., Híveš J., Zemanová M., Fellner P.: Korózia pod napätím v prostredí piesku a ílu. Corrosion under stress in

the environment of sand and clay. Slovgas 12(6), 7 - 10 (2003). B. Conferences [1] Ambrová, M., Gabčová, J.*: Reakcie zlúčenín síry pri elektrolytickej výrobe hliníka. Reactions of sulphur speciec at the

electrolytic production of aluminium. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97(8), 856 (2003).

[2] Danielik, V., Gabčová, J.*: Phase Diagram of the system NaF - KF - AlF3. In: Zborník z XVI. medzinárodnej konferencie o termickej analýze a kalorimetrii TERMANAL 2003, Vysoké Tatry-Stará Lesná 8. 10. - 11. 10. 2003, s. PO – 12 (2003). (Po)

[3] Ambrová, M.*, Fellner, P., Gabčová, J., Thonstad, J.: Chemical Reactions o Sulphur Species in Cryolite - Based Melts. Zborník The 12th International Al Symposium, Bratislava, September 7. - 10. 2003. pp. 131 - 140 (2003). (Pr)

[4] Fellner, P.*, Korenko, M., Ambrová, M., Danielik, V., Thonstad, J.: Reactions of sulphides in molten cryolite. Reactions of sulphides in molten cryolite. Zborník z International Symposium on Ionic Liquids, Carry de Rouet, France, June 26. - 28. 2003, pp. 75 - 81 (2003). (Pr)

[5] Fellner, P.*, Korenko, M., Danielik, V., Thonstad, J.: Solubility and Activity of Sodium in Molten Aluminium. Solubility and Activity of Sodium in Molten Aluminium. Zborník The 12th International Al Symposium, Bratislava, September 7. - 10. 2003. pp. 21 - 29 (2003). (Pr)

[6] Gál, M., Híveš, J.*, Benová, M.: Sledovanie prenosu náboja v heterogénnom systéme pomocou impedančnej spektroskopie. Investigation of the charge transfer in heterogeneous systems using the impedance spectroscopy. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 850 (2003).

[7] Híveš, J.*, Ambrová, M., Fellner, P.: Behaviour of Sulphur in Aluminium Cells - Electrochemical Reactions. Zborník The 12th International Al Symposium, Bratislava, September 7. - 10. 2003. pp. 36 - 42 (2003). (Pr)

[8] Híveš, J.*, Thonstad, J.: Electrical Conductivity of Low - Melting Electrolytes. Zborník The 12th International Al Symposium, Bratislava, September 7. - 10. 2003. pp. 64 - 71 (2003). (Pr)

[9] Korenko, M.*, Fellner, P., Thonstad, J.: The Phase Diagram of the System Na3AlF6 - Al2S3. In: Zborník The 12th International Al Symposium, Bratislava, September 7. - 10. 2003. pp. 141 - 143 (2003). (Pr)

[10] Gáliková, Z.*, Chovancová, M., Makovíniová, D., Zemanová, M.: Vylučovanie zliatinových povlakov Ni - W z vodných elektrolytov. Deposition of Ni-W alloy layers from aqueous electrolytes. Zborník prednášok zo 44. medzinárodnej galvanickej konferencie, Bratislava 24. - 25. jún 2003, s. 29 - 35 (2003). ISBN 80-227-1916-1. (Pr)

[11] Gáliková, Z.*, Chovancová, M.: Vylučovanie zliatinových povlakov Ni - W z vodných elektrolytov. Deposition of Ni-W layers from aqueous electrolytes. Zborník z 20. Konferencie Progresívni a netradiční technológie povrchových úprav, Praha 25. - 26. 11. 2003, s. 50 – 52 (2003). (Pr)

[12] Híveš, J.*, Benová, M., Gál, M.: Elektrická vodivosť elektródy s fluidným lôžkom. Electrical conductivity of the fuid bed electrode. Zborník prednášok zo 44. medzinárodnej galvanickej konferencie, Bratislava 24. - 25. jún 2003, s. 101 - 107 (2003). ISBN 80-227-1916-1. (Pr)

[13] Híveš, J.*, Chovancová, M., Fellner, P., Zemanová, M.: Testovanie odolnosti izolačných vrstiev potrubných materiálov voči podkorodovaniu. Testing of corrosion resistens of izolation layers on pipeline materials. Zborník z 13. konferencie Korózia úložných materiálov 2003, Košice 27. - 28. máj 2003, s. 41 – 46 (2003). ISBN 80-7099-251-4. (Pr)

[14] Gáliková Z., Chovancová, M.: Vlastnosti zliatinových povlakov Ni – W vylúčených z vodných elektrolytov. Properties of Ni-W layers deposited from aqueous electrolytes. 2. medzinárodná vedecká konferencia Povrchové inžinierstvo 2003, Košice 6. - 7. 11. 2003 (2003). (Po)

DEPARTMENT OF LANGUAGES

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Head of Department: Telephone:++421252496708 Alžbeta Oreská Fax: ++421252493198


I. STAFF Assistant Professors : Marta Harmanová; Magdaléna Horáková; Ľubica Kachničová; Viera Kuželová, PhD; Veronika Polóniová; Zuzana Štefanovičová; Technical staff: Katarína Vépyová;


A. Teaching laboratories: English language classroom German language classroom Computer-operated Data Video Projector Room

III. TEACHING

A. Undergraduate Study: 1. semester (Bc) Technical English I. 0/2/0 Horáková, Kachničová, Oreská,

Polóniová, Štefanovičová Technical German I. 0/2/0 Kuželová English language I. 0/2/0 Harmanová, Horáková, Kachničová,

Oreská, Polóniová Slovak language I. (for foreign

students) /0/4/0 Kuželová

1. semester (Bc) Russian language 0/2/0 Harmanová German language 0/2/0 Kuželová English conversation 0/2/0 Kachničová 2. semester (Bc) Technical English II. 0/2/0 Harmanová, Horáková, Oreská,

Polóniová, Štefanovičová Technical German II. 0/2/0 Kuželová English language II. 0/2/0 Harmanová, Horáková, Kachničová,

Oreská, Polóniová Slovak language II. (for foreign

students) /0/40 Kuželová

2. semester (Bc) Russian language 0/2/0 Harmanová German language 0/2/0 Kuželová English conversation 0/2/0 Kachničová 3. semester (Bc) Technical English I. 0/2/0 Harmanová, Horáková, Oreská,

Polóniová, Štefanovičová Technical English II. 0/2/0 Harmanová, Horáková, Kachničová,

Oreská, Polóniová English language I. 0/2/0 Harmanová, Horáková, Oreská,

Polóniová, Štefanovičová English language II. 0/2/0 Harmanová, Horáková, Oreská,

Polóniová, Štefanovičová 3. semester (Bc) Russian Language 0/2/0 Harmanová German Language 0/2/0 Kuželová English konversation 0/2/0 Kachničová 4. semester (Bc) Technical English I. 0/2/0 Harmanová, Horáková, Oreská,

Polóniová, Štefanovičová Technical English II. 0/2/0 Harmanová, Horáková, Kachničová,

Oreská, Polóniová English language I. 0/2/0 Harmanová, Horáková, Oreská,

Polóniová, Štefanovičová English language II. 0/2/0 Horáková, Kachničová,Oreská,


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Polóniová, Štefanovičová 4. semester (Bc) Russian Language 0/2/0 Harmanová German Language 0/2/0 Kuželová English conversation 0/2/0 Kachničová 5. semester (Bc) Technical English I. 0/2/0 Harmanová, Horáková, Oreská,

Polóniová, Štefanovičová Technical English II. 0/2/0 Harmanová, Horáková, Oreská,

Polóniová, Štefanovičová English language I. 0/2/0 Horáková, Kachničová,Oreská,


Polóniová, Štefanovičová 5. semester (Bc) Russian Language 0/2/0 Harmanová German Language 0/2/0 Kuželová English conversation 0/2/0 Kachničová 6. semester (Bc) Technical English I. 0/2/0 Harmanová, Horáková, Oreská,

Polóniová, Štefanovičová Technical English II.. 0/2/0 Harmanová, Horáková, Oreská,

Polóniová, Štefanovičová English language I. 0/2/0 Horáková, Kachničová,Oreská,


Polóniová, Štefanovičová


A.Pedagogical project No 304/03 Aspects of Teaching Foreign Languages for Specific Purposes at the University of Technology (Veronika Polóniová)

Aims of the project are : to realise teaching of foreign languages in distant form of study; to prepare innovative material suitable for on-line study of foreign languages at FCHPT; to teach basics of ESP and GSP for the needs of profession.

Project duration: from 01.012003 to 31.12.2005

VI. COOPERATION



Duration

Language departments of STU, Bratislava

Preparing syllabuses for EU exam courses UNICERT introducing besides the general language also the area of professional language

Polóniová Veronika,assistant professor, FCHPT STU, Radlinského 9, 812 37 Bratislava

01.01.2000 -

IASTE Bratislava Oral interviews with applicants for mobility abroad

Oreská Alžbeta, head of Language Department, FCHPT STU, Radlinského 9, 812 37 Bratislava

01.01.2001 -

Specialist departments of FCHPT STU, Bratislava

Language section of the annual "Students´Scientific and Research Activity" competition - advisers Zálupský Peter, Štefuca Vladimír


01.01.1994 -

Slovak Association of Translators and Interpreters, Bratislava

Multimedia and Translation

Polóniová Veronika,assistant professor, FCHPT STU, Radlinského 9, 812 37 Bratislava

01.01.1998 -

University of Third Age, STU, Bratislava Language course


1. 9. 2003 -

Language Centre, Rectorate of STU, Bratislava

Language courses: ZoD 1/2003, ZoD 94/2003

Kuželová Viera, head of Language Centre STU, Laurinská 14, 810 00 Bratislava

01.01.1994 -


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Publishing House "Príroda", Bratislava

Review of a series of textbooks of English language

Horáková Magdaléna, assistant professor, FCHPT STU

01.09.2003 - 31.12.2003



Duration

CASAJC, Bratislava

Slovak and Czech Association of Language Centres in Higher Education- preparing materials for Portfolio and Unicert


01.02.2003 -

Leonardo da Vinci Community

EU Vocational Action Programme - practical placements for Slovak University students 2 (cooperation with Civil Engineering Faculty STU

Horáková Magdaléna, assistant professor, FCHPT STU 12.122003 -



Valid date

Polóniová Veronika

Slovak Association of Translators and Interpreters, Bratislava member 01.01.1998 -



Valid date

Horáková Magdaléna British Council - Resource Centre, Bratislava member 01.09.1996 -

Horáková, Kachničová, Oreská,Polóniová,Štefanovičová

CERCLES/CASAJC, Slovak Republic member 11.02.2003 -

VIII. PUBLICATIONS B. Conferences (*international conferences)

[1] Kuželová, V.: Prečo Unicert. Why Unicert. CD-konf.Nitra September 03, výuč.CJ C. Books and Textbooks

[1] Recenzia série učebnícLacinová,Kadlecová,Zahálková,Balcarová [2] Horáková, M.: Angličtina pre 4.-9.roč. zákl. školy

DEPARTMENT OF MANAGEMENT

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Head of Department: Telephone: 00421-7/2495246 Assoc. Prof. Dušan Baran, PhD Fax: 00421-7-52493198


Associate Professors: Agáta Ďurkovičová, PhD; Pavel Herzka, PhD.; Marta Šostroneková, PhD; Dušan Špirko, PhD Assistant Professors : Štefan György, PhD; Milan Majerník PhD.; Martin Jozefček, Jana Kajanová, Martina Kuperová; Jana Plchová; Monika Zatrochová. Technical staff: Martin Mikloš, Katarína Macušková.


A. Teaching laboratories: Laboratory of Computerized Technique

III. TEACHING

A. Undergraduate Study: 1. semester (Bc) Economics (2-0 h) Majerník 2. semester (Bc) Fundamentals of Environmental

Philosophy(2-0 h) Špirko

5. semester (Bc) Fundamentals of Manag. of Chem.andFood-Proc.Enterprises

(2-2 h) Šostroneková

5. semester (Bc) Marketing (2-2 h) Špirko, Ďurkovičová 6. semester (Bc) Introduction to Law (2-0 h) György Semester Project (0-4 h) Baran Accounting (2-2 h) Šostroneková 1. semester (MSc) Corporate Economics (2-2 h) Herzka Operations Research (3-2 h) Kuperová Strategic Management (3-2 h) Herzka, Jozefček Calculations and Prices (2-2 h) Plchová, Kajanová 2. semester (MSc) Capital Market and Corporation

Finances (2-0 h) Baran

Marketing (2-0 h) Špirko, Ďurkovičová Decision-Making in Business (2-3 h) Herzka Human Resource Management (2-2 h) Herzka 2. semester (MSc) Production Management (2-3 h) Kuperová 3. semester (MSc) Financial Management (3-2 h) Baran, Zatrochová Analysis of Business Economics (3-2 h) Baran Logistics (2-2 h) Kuperová Fundamentals of Mercantile and

Financial Law (2-0 h) György

3. semester (MSc) International Marketing (2-2 h) Špirko, Ďurkovičová Annual Project (0-4 h) Baran


A. Project A-162/2003 Application of modern management methods in chemical and food-processing enterprises. (Dušan Baran)

Leader of the project: Dušan Baran. Project participants: Agáta Ďurkovičová, Pavel Herzka, Marta Šostroneková, Dušan Špirko, Štefan György, Martina Kuperová, Milan Majerník, Jana Plchová, Martin Jozefček, Jana Kajanová, Martina Svítková, Monika Zatrochová, Martin Mikloš, Katarína Macušková. Parts of the project: A. Environmental management in conditions of the chemical and food-processing enterprises. (Leader of the part A: Dušan Špirko. Participants: Štefan György, Ing. Jana Plchová.)


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B. Financial management of chemical and food-processing enterprises in Slovakia. (Leader of the part B: Dušan Baran. Participants: Martina Kuperová, Milan Majerník, Martina Svítková, Monika Zatrochová, Katarína Macušková.) C. Modern trends in the management of a firm. (Leader of the part C: Pavel Herzka. Participants: Agáta Ďurkovičová, Marta Šostroneková, Martin Jozefček, Jana Kajanová, Martin Mikloš.) Project duration: from 1 January 2003 to 31 December2005


VI. COOPERATION



Duration

Frucona Košice, Inc. Material-technical cooperation

Ing. Ján Király, general manager and chairman of the Board of directors

CCW, Ltd. Bratislava Pedagogic cooperation Dipl.Ing. Magdaléna Sulanová, marketing manager

Slovak association of small enterprises Scientific-technical cooperation Ing. Vladimír Sirotka, PhD.

Stock exchange, Inc. in Bratislava Pedagogic cooperation Ing. Barbora Lazorová

TENTO, Inc. Žilina Material-technical cooperation Ing. Marián Majtán, financial director

Chemosvit, Inc. Svit Material-technical cooperation Ing. Ján Olekšák Matej Bel University, Faculty of Economics, Banská Bystrica

Pedagogic cooperation

Assoc. Prof. Jaroslav Ďaďo Prof. Ľubica Lesáková Assoc. Prof. Marková Assoc.Prof. František Lipták

University of Economy, Bratislava Pedagogic cooperation

Assoc. Prof. Šubertová Prof. Július Alexy Assoc.Prof.Alena Chodasová

University of Žilina, Faculty of Economics, Transport and Communication


Prof. Štefan Cisko Assoc. Prof. Štefan Hittmar Assoc. Prof. Jozef Strišš Assoc. Prof. Szilágyi

Slovak University of Technology, Faculty of Materials Science and Technology, Trnava


Prof. Jozef Sáblik Assoc.Prof. Alexander Štrbka Assoc. Prof. Peter Sakál Assoc. Prof. Miloš Čambal

Slovak University of Technology,Faculty of Mechanical Engineering

Pedagogic cooperation Assoc. Prof. Štepka Prof. Dita Hekelová

Slovak University of Technology,Faculty of Civil Engineering

Pedagogic cooperation Prof. Koloman Ivanička Assoc. Prof. Mária Zúbková Prof. Trávnik

Alexander Dubček University, Faculty of Social-Economic Relations, Trenčín

Pedagogic cooperation Prof. Baránik Assoc. Prof. Sergej Vojtovič

Comenius University Bratislava, Faculty of Management

Pedagogic cooperation Assoc.Prof.Ľubica Bajzíková Assoc. Prof. Cibáková


128



Duration

BORSOD CHEM Moravian Chemical Plants, Ostrava Czech Republic

Material-technical and pedagogic cooperation

Ing. Alexander Pálffy, general manager

University of Economics, Faculty of Business Administration, Prague, Czech Republic

Pedagogic cooperation Prof. Eduard Stehlík

Institute of Chemical Technology, Faculty of Chemical Engineering, Prague, Czech Republic

Pedagogic cooperation Prof. Ivan Gros Assoc. Prof. Stanislava Grosová

Karol Adamiecki University of Economics in Katowice, Faculty of Management, Poland

Pedagogic cooperation Prof. Kornelia Karcz Prof. Žofia Kedzior

University of Economics in Krakow, Faculty of Management, Poland

Pedagogic cooperation Prof. Jan W. Wiktor Prof. Jerzy Altkorn

Vilnius University, Faculty of Humanities in Kaunas, Lithuania

Pedagogic cooperation Assoc. Prof. Jogaila Mačerinskas

Masaryk University Brno, Faculty of Economics and Administration, Czech Republic

Pedagogic cooperation Prof. Blažek Dr. Viliam Záthurecký

Lvov Polytechnic National University, Institute of Economics and Management, Ukraine

Pedagogic cooperation Assoc. Prof. Natalia Čuchraj

Kiev National Economic University, Ukraine

Pedagogic cooperation I.L. Reshetnikova

University of Pardubice, Faculty of Chemical Technology, Czech Republic

Pedagogic cooperation Assoc. Prof. Hana Lošťáková

VIII. PUBLICATIONS A. Journals [1] Baran, D.: Komunikacija samovrjaduvanija z gromadskisťju i marketing. Self-government Communication with Public and

Marketing Visnik Logistika. Vydáva: Nacionalni univerzitet „Ľvivskaja politechnika“, Ľvov, Ukrajina, 2003, č. 472/2003, s. 3–6. ISSN 0321 – 0499

[2] Baran, D.: Management kvality a benchmarking. Management of quality and benchmarking Marketing a komunikace. Vydáva Česká marketingová spoločnosť, Praha. 2003. Roč. XlV, č. 3/03, s.21-22. ISSN 1211 – 5622

[3] Baran, D.: Controlling pohľadávok v praxi. Controlling of Debts in Practice. Ekonomika a spoločnosť, roč.3, č. 2/2002, Banská Bystrica, s. 158 – 166. ISSN 1335 – 7069

[4] Šostroneková, M.: Nové podvojné účtovníctvo pre podnikateľov. New double-entry accounting for entrepreneurs Účtovníctvo a poradenstvo. Ročník II, č.11/2003, s. 3-23. ISSN 1335-9509


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B. Conferences [1] Baran, D.* – Ďurkovičová, A.: Strategy of Entering of Slovak Firm into Foreign Market. In: Marketing of the companies in V4

countries one step before the entry to european union. Text book of international scientific conference. Faculty of Economics of Matej Bel University in Banská Bystrica, 17.– 19. 09. 2003, Nízke Tatry - Krpáčovo. UMB Banská Bystrica 2003, s. 24–30. ISBN–80–8055–815–9

[2] Baran, D.: Efficiency of Support Programmes Financed from the State Budget and Phare Programme for Development of the Small- and Medium-sized Enterprising in 2002 in the Slovak Republic. CO–MAT–TECH 2003: Zborník z 11. medzinárodnej vedeckej konferencie, MTF STU v Trnave, 16. – 17. 10. 2003. STU Bratislava 2003, s. 59. Zborník na CD. ISBN 80–227–1949–8

[3] Baran, D.: International Financial Market and Worldwide Globalization. Globalizácia a jej sociálno-ekonomické dôsledky ´03. Zborník z 3. medzinárodnej vedeckej konferencie, ŽU Žilina, FPEDAS, 7.-8. 10. 2003, Rajecké Teplice. EDIS Žilina 2003, s. 9–11. ISBN–80–8070–134–2

[4] Baran, D.: Quality Function Deployment ( QFD ), Method of Management of Quality. In: Nové trendy v manažmente kvality. Zborník z vedeckého seminára s medzinárodnou účasťou. Materiálovotechnologická fakulta STU v Trnave, apríl 2003. STU Bratislava 2003, s.12–15. ISBN 80–227–1894–7

[5] Zatrochová, M.* - Ivanička, K.: Benefits and the risk factors of construction and management of factory outlets. Ekonomické a riadiace procesy v stavebníctve a v investičných projektoch. Zborník z 4. vedeckého sympózia s medzinárodnou účasťou, SVF STU Bratislava, 16-17. september 2003. STU Bratislava 2003, s. 160-163. ISBN 80-227-19293

[6] Baran, D: Daňová reforma v SR po 1.1.2004. Tax reform in Slovakia after 1st January, 2004. Nové trendy rozvoje průmyslu. Zborník z medzinárodnej konferencie, Fakulta podnikání VUT Brno, 26.– 27. 11. 2003. Brno 2003. Zborník na CD. ISBN 80–214–2518–0

[7] Baran, D: Management kvality a benchmarking. Multidimenziálne aspekty kvality QVI. Zborník z vedeckej konferencie s medzinárodnou účasťou, EF UMB Banská Bystrica, 6. mája 2003. UMB Banská Bystrica 2003, s. 10–13. ISBN 80–8055–767–5

[8] Baran, D: Možnosti riešenia nedostatkov kapitálového trhu v podnikateľskom prostredí SR. Possibilities of solving some deficiencies in the capital market in the busines environment in Slovakia. Podnikateľské prostredie v Slovenskej republike – súčasný stav a perspektívy V. Zborník z medzinárodnej konferencie. EU FPM Bratislava, Modra–Harmónia, 15.–16. máj 2003. Ekonóm Bratislava 2003, s. 14–18. ISBN 80–225–1734–8

[9] Baran, D: Návrh systému prevencie a vymáhania pohľadávok v modelovom podniku. Proposal of the preventive and enforceable system of debts in the model firm. Marketing a obchod 2003. Zborník z medzinárodnej vedeckej konferencie, Drevárska fakulta TU vo Zvolene, 6. – 7. 11. 2003. TU Zvolen, s. 309–314. ISBN 80–969033–0–6

[10] Baran, D: Problémy slovenského kapitálového trhu, príčiny ich vzniku a ochrana práv investorov. Problems of the Slovak capital market, reasons of their emergence and the law protection of investors Etika v ekonomickom prostredí II. Zborník z medzinárodnej vedeckej konferencie, EF UMB Banská Bystrica, 6.–7. februára 2003. UMB Banská Bystrica 2003, s. 90–94. ISBN 80–8055–798–5

[11] Baran, D: Rozvoj a výsledky malého a stredného podnikania v roku 2002. Ekonomické a riadiace procesy v stavebníctve a v investičných projektoch. Zborník zo 4. medzinárodného sympózia SvF STU Bratislava, 16.– 17. september 2003. STU Bratislava 2003, s. 64–67. ISBN 80–227–1929–3

[12] Baran, D: Výskum a výuka v oblasti podnikového manažmentu z pohľadu novokoncipovaného študijného odboru pre prvý stupeň vysokoškolského štúdia. Research and instruction in the sphere of the corporate management from the aspect of the newly-designed field of study for the first grade of the university study. Zborník z medzinárodnej pedagogickej konferencie: Výuka a výzkum v odvětvových ekonomikách a podnikovém managementu na vysokých školách, Katedra ekonomiky a managementu chemického a potravinářského průmyslu, FCHT UP, ČR. Lázně Bohdaněč, 21.–22. 10. 2003. Univerzita Pardubice 2003, s. 276-279. ISBN 80-7194-623-0

[13] György, Š.: Niektoré otázky uplatňovania environmentálnych zákonov v SR a európske normy. Some questions of applying environmental laws in the Slovak Republic and European standards Humanizácia a životné prostredie. Zborník vedeckých prác z medzinárodnej vedeckej konferencie na SvF STU v Bratislave, 11. a 12. 9. 2003. STU Bratislava 2003, s. 59-63. ISBN 80-227-1920-X

[14] Herzka, P.: Riadenie ľudských zdrojov z aspektu manažmentu kvality. Human resource management from the aspect of the management of quality. Nové trendy v manažmente kvality. Zborník z vedeckého seminára s medzinárodnou účasťou. Materiálovotechnologická fakulta STU v Trnave, apríl 2003. STU Bratislava 2003, s. 38–43. ISBN 80-227-1894-7

[15] Herzka, P.: Systém hmotnej zainteresovanosti zamestnancov. System of the material interest of employees. Nové trendy rozvoje průmyslu. Zborník z medzinárodnej konferencie. Fakulta podnikatelská VUT v Brne, ČR, 26.-27.11.2003. Brno 2003. Zborník na CD. ISBN 80-214-2518-0

[16] Herzka, P.: Zamestnávanie telesne postihnutých – handicapovaných ľudí v podmienkach trhovej ekonomiky. Employment of physically handicapped people in conditions of the market economy. Uplatnenie nezamestnaných starších ľudí na slovenskom trhu práce: Zborník z vedeckého seminára, konaného dňa 28. apríla 2003. Výskumný ústav práce, sociálnych vecí a rodiny v Bratislave. Bratislava 2003, s. 55–58

[17] Jozefček, M.: E-marketing malých a stredných podnikov. E-marketing of the small- and medium-sized enterprises. Nové trendy rozvoje průmyslu. Zborník s medzinárodnej konferencie, Fakulta podnikatelská, Vysoké učení technické Brno, ČR, 26.-27.11.2003. Brno 2003, zborník na CD. ISBN 80-214-2518-0

[18] Jozefček, M.: Identifikácia obalov ako súčasť kvality v logistike. Identification of packages as a component of the quality in logistics. Nové trendy v manažérstve kvality. Zborník z vedeckého seminára s medzinárodnou účasťou. Materiálovotechnologická fakulta STU v Trnave, apríl 2003. STU Bratislava, s.62. ISBN 80-227-1894-7

[19] Jozefček, M.: Marketingové stratégie malých a stredných podnikov. Marketing strategies of the small- and medium-sized enterprises. Podnikateľské prostredie v Slovenskej republike – súčasný stav a perspektívy V. Zborník z vedeckej konferencie, Fakulta podnikového manažmentu, Ekonomická univerzita Bratislava, 15.-16. 5. 2003 Modra-Harmónia. Ekonóm Bratislava 2003, s. 52-53. ISBN 80-225-1734-8

[20] Jozefček, M.: Využitie čiarových kódov a informačných technológií v logistike. Application of bar codes and information


130

technologies in logistics. Diagnostika podniku, controlling a logistika. Zborník z 1. medzinárodnej vedeckej konferencie, Fakulta prevádzky a ekonomiky dopravy a spojov Žilinskej univerzity v Žiline, 16. 4 .2002. EDIS Žilina 2002, s. 128-133. ISBN 80-7100-951-2

[21] Kajanová, J.: Výnosy – ekonomická kategória predstavujúca významného nositeľa informácií. Revenues – economic category and significant carrier of information. Nové trendy rozvoje průmyslu. Zborník z medzinárodnej konferencie, Fakulta podnikatelská, Vysoké učení technické Brno, ČR, 26.-27.11.2003. Brno 2003, zborník na CD. ISBN 80-214-2518-0

[22] Kuperová, M.: Informačné systémy v logistike. Information systems in logistics. Nové trendy rozvoje průmyslu. Zborník s medzinárodnej konferencie, Fakulta podnikatelská, Vysoké učení technické Brno, ČR, 26.-27.11.2003. Brno 2003, zborník na CD. ISBN 80-214-2518-0

[23] Kuperová, M.: Stratégia KAIZEN v riadení kvality. Strategy of KAZEIN in managing the quality. Nové trendy v manažmente kvality. Zborník z vedeckého seminára s medzinárodnou účasťou. Materiálovotechnologická fakulta STU v Trnave, apríl 2003. STU Bratislava 2003, str. 88–94. ISBN 80-227-1894-7

[24] Majerník, M.: Finančné prostriedky Európskej únie pre rozvoj podniku. EU finances for the development of a firm Nové trendy rozvoje průmyslu. Zborník s medzinárodnej konferencie, Fakulta podnikatelská, Vysoké učení technické Brno, ČR, 26.-27.11.2003. Brno 2003, zborník na CD. ISBN 80-214-2518-0

[25] Piatrik, M., - Plchová, J.*: Systémy podpory proaktívneho správania podnikov k ochrane životného prostredia. Support Systems of Proactive Behaviour of Enterprises to the Protection of an Environment . Humanizácia a životné prostredie. Zborník vedeckých prác z medzinárodnej vedeckej konferencie na SvF STU v Bratislave, 11. a 12. 9. 2003. STU Bratislava 2003, s. 199-202. ISBN 80-227-1920-X

[26] Plchová, J.: Environmentálne manažérstvo podľa noriem radu ISI 14 000. Management of environment according to ISI 14 000. Nové trendy v manažmente kvality. Zborník z vedeckého seminára s medzinárodnou účasťou.

Materiálovotechnologická fakulta STU v Trnave, apríl 2003. STU Bratislava 2003, str.118-122. ISBN 80-227-1894-7 [27] Plchová, J.: Starostlivosť o životné prostredie v kontexte manažmentu kvality. Care about environment in conjunction with the

management of quality Nové trendy rozvoje průmyslu. Zborník s medzinárodnej konferencie. Fakulta podnikatelská, Vysoké učení technické Brno, ČR, 26.-27.11.2003. Brno 2003, zborník na CD. ISBN 80-214-2518-0

[28] Svítková, M.: Benchmarking – Riadenie kvality. Benchmarking – management of quality. Nové trendy v manažmente kvality. Zborník z vedeckého seminára s medzinárodnou účasťou. Materiálovotechnologická fakulta STU v Trnave, apríl 2003. STU Bratislava 2003, s.161-164. ISBN 80-227-1894-7

[29] Svítková, M.: Investovanie v súčasných podmienkach slovenských podnikov. Investment in the present-day conditions of Slovak enterprises. Zborník z medzinárodnej vedeckej konferencie TU vo Zvolene, Drevárska fak., 6.-7. 11. 2003, Zvolen. TU Zvolen 2003, s. 61- 63. ISBN 80-969033-0-6

[30] Šostroneková, M. - Kajanová, J.*: Proces zavádzania systému manažmentu kvality vo firme. Process of introducing the quality management system in the firm Zborník z vedeckého seminára s medzinárodnou účasťou, Materiálovotechnologická fakulta v Trnave apríl 2003. STU Bratislava 2003, str. 154–163. ISBN 80-227-1894-7

[31] Šostroneková, M.: K problémom vo výučbe ekonomiky a manažmentu na FCHPT STU v Bratislave. Problems of the instruction of economics and management at the Faculty of Chemical and Food Technology STU in Bratislava. Zborník z medzinárodnej pedagogickej konferencie : Výuka a výzkum v odvětvových ekonomikách a podnikovém managementu na vysokých školách, Katedra ekonomiky a managementu chemického a potravinářského průmyslu, FCHT UP, ČR. Lázně Bohdaněč, 21.–22. 10. 2003. Univerzita Pardubice 2003, s. 276-279. ISBN 80-7194-623-0

[32] Špirko, D.: Environmentálny problém ako dôsledok modernistického konceptu vzťahu kultúry a prírody. Environmental Problem as a Consequence of the Relation of Modernistic Concept of Culture to Nature Hodnotové aspekty súčasného sveta. Zborník príspevkov z interdisciplinárnej konferencie vedeckej s medzinárodnou účasťou konanej v rámci 5. stretnutia SFZ v dňoch 18.-19. septembra. 2003 v Nitre. IRIS Bratislava 2003, s. 238-243. ISBN 80-89018-57-2

[33] Špirko, D.: Environmentálna etika a súčasné ekonomické myslenie. Environmental ethics and present-day economic thinking. Humanizácia a životné prostredie. Zborník vedeckých prác z medzinárodnej vedeckej konferencie na SvF STU v Bratislave, 11. a 12. 9. 2003. STU Bratislava 2003, s. 239-246. ISBN 80-227-1920-X

[34] Špirko, D.: Zodpovednosť, kvalita ľudskosti? Responsibility – Quality of Humanity? Philosophica XXXIII. Filozofia v škole, filozofia v živote. Zborník Filozofickej fakulty Univerzity Komenského (materiály z konferencie Filozofia v škole, filozofia v živote, ktorá sa konala 8. 2. 2001). Vydavateľstvo UK Bratislava 2002, s. 77-82. ISBN 80-223-1665-2

[35] Zatrochová, M.: Multiobchod ako súčasť marketingu. Multi-business as a marketing component. Nové trendy rozvoje průmyslu. Zborník s medzinárodnej konferencie, Fakulta podnikatelská, Vysoké učení technické Brno, ČR, 26.-27.11.2003. Brno 2003, zborník na CD. ISBN 80-214-2518-0

[36] Zatrochová, M.: Procesy kvality ako súčasť normy ISO 9001:2000. Processes of the quality as a component of the standard ISO 9001:2000 Nové trendy v manažmente kvality. Zborník z vedeckého seminára s medzinárodnou účasťou. Materiálovotechnologická fakulta STU v Trnave, apríl 2003. STU Bratislava 2003, s. 195–200. ISBN 80-227-1894-7

C. Books and Textbooks [1] Baran, D.: Kapitálový trh a podnikové financie. Fundamentals of the capital market STU Bratislava 2003, 169 s. ISBN 80–

227–1856–4 [2] Šostroneková, M. a kol.: Nové podvojné účtovníctvo pre podnikateľov s príkladmi. New double-entry accounting for

entrepreneurs with examples EPOS Bratislava 2003, 526 s. ISBN 80-8057-542-8

DEPARTMENT OF MATHEMATICS

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Head of Department: Telephone:++421252495177 Assoc. Prof. Štefan Varga, PhD Fax: ++421252495177


I. STAFF Full Professors: Vladimír Kvasnička, PhD, DSc Associate Professors: Vladimír Baláž, PhD; Anna Kolesárová, PhD; Jiří Pospíchal, PhD; Michal Šabo, PhD; Štefan Varga, PhD Assistant Professors : Jozef Antoni, PhD; Július Bánki, PhD; Štefan Boor, MSc; Ivan Garaj, PhD; Viera Grusková, PhD; Eva Hainzlová, MSc; Vladimír Haluška, PhD; Ľubomíra Horanská, PhD; Milan Jasem, PhD; PhD Students: Štefan Babinec, Ing., Jozef Babjak, Ing., Peter Sarkoci, Ing.

II. TEACHING AND RESEARCH LABORATORIES A. Teaching laboratories:

Laboratory equipped by personal computers for the Basics of Computer Science B. Research laboratories:


1. semester (Bc) Calculus I 3/3/0 Baláž, Grusková, Jasem, Kolesárová, Šabo

Calculus I (external study) 2/2/0 Kvasnička Basics of Computer Science 1/0/2 Antoni, Bánki, Boor, Heinzlová,

Pospíchal 2. semester (Bc) Calculus II 4/4/0 Baláž, Grusková, Jasem, Kolesárová,

Šabo 5. semester (Bc) Calculus III 2/0/2 Antoni, Garaj, Varga 1. semester (MSc) Discrete mathematics 2/1/0 Kolesárová Programming and algorithms 2/0/1 Pospíchal Numerical mathematics 2/0/1 Šabo Computer architecture 2/0/1 Antoni 1. semester (MSc) Laboratory of specialization 2/0/1 Boor, Sarkoci 2. semester (MSc) Artificial intelligence in chemistry 2/0/1 Kvasnička Statistics 2/0/1 Varga, Šabo Laboratory of specialization II 0/0/6 Sarkoci 3. semester (MSc) Database systems 2/0/1 Antoni Laboratory of specialization 0/0/10 Babinec, Babjak, Bánki, Heinzlová,

Pospíchal 2. semester (MSc) Evolutionary algorithms (FMFI UK) 2/0/0 Pospíchal Evolutionary algorithms (FEI STU) 2/2/0 Kvasnička 1. semester (Bc) Basics of Computer Science (FSEV

UK) 2/1/0 Kvasnička, Pospíchal


A. VEGA Project No 1/0085/03 Mathematical vague information processing and its applications (Anna Kolesárová)

Quantification of uncertainty related to vagueness of studied objects. Extension of the theory of aggregation operators, new constructions methods for aggregation operators, in particular, construction of stable aggregation operators, clarifying their structure and uniqueness. Ordinal aggregation operators for aggregation of data of qualitative nature. The study of possible applications of different types of aggregation operators in inference process in fuzzy logic and construction of new operators for this purpose.


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Fuzzy preference modelling and decision making. Mixed fuzzy-stochastic models.

Project duration: from (01/01/2003 to 31/12/2005 B. EU Project COST ACTION 274/2 : Theory and Applications of Relational Structures as Knowledge

Instruments (TARSKI) (Kolesárová Anna) The main objective of the Action COST 274 is to advance the understanding and use of relational structures in applicable object domains. The researchers of FCHFT STU are involved in the working group WG3 for the development of non-invasive scaling methods for the prediction of relational data and comparing, and possibly, integrating, a nominal scaling approach with numerical methods such as fuzzy relations, etc. The aim is also the improvement of methods and procedures for gaining information from everyday relational situations such as, e.g., preference models.

Project duration: from 06/2001 to 05/2005

C. VEGA Project No 1/8107/01 Computational simulations with multiagent systems (Jiří Pospíchal) The goal of the project is a study of multiagent systems using evolutionary algorithms and neural networks in order to observe a possible emergence of a coordinated communication, cooperation and social structures. For a study of emergence of a coordinated communication the agents are endowed with a cognitive organ, which is represented by a simple recurrent neural network. An agent has its randomly chosen internal state and with its cognitive organ it will code it and send as a message to another agent. This agent will decode the received message by its cognitive organ to an internal state representation. Emergence of cooperation and development of social structures between agents is studied by a prisoners dilemma game. Each agent of a population is represented by a strategy (coded by a binary vector), which will determine its interaction with other agents. Evolution of strategies is simulated by simple evolutionary algorithms. The evolutionary stability of emerging strategies is studied in detail.

Project duration: from 01/01/2001 to 31/12/2003

D. VEGA Project No 1/0062/03 Artificial chemistry and molecular evolution (Vladimír Kvasnička) Biotic and abiotic molecular systems with kinetics determined by Eigen's replicator system are studied by methods of artificial chemistry. Molecules are represented by strings of tokens over a finite alphabet. These molecules are capable of a physical process called "folding" (an analogy with biomacromolecules RNA). Each molecule is evaluated by a fitness on the basis of its particular folding. Molecules are placed in a chemical-reaction system, where they take part in a reproduction process (with probabilities proportional to their fitness) consisting in a simple copying accompanied by mutations. Such a simple reaction system corresponds to biomacromolecular systems that are capable of Darwinian evolution on molecular level. A goal of evolution specified in this way is an emergency of strings with required folding (required phenotype or a goal phenotype). The present in-silico approach offers a conceptual and notional machinery for a deeper theoretical interpretation and description of molecular Darwinian evolution.



A. KEGA Project No 3./100603 Mathematics on-line: An internet course (Dobrakovová Jana/ Kolesárová Anna)

The aim of the project is to propose and create the framework for a dynamical mathematical electronic education using XML documents, with respect to new pedagogical methods. The electronic net course will be addressed to the students of all faculties at STU in the first year of their study.


VI. COOPERATION



Duration

FSEV UK Project of development of Cognitive Science Ing. E. Gál, CSc. 1.9.2002-

FMFI UK Project of development of Cognitive Science

Doc. PhDr. J. Šefránek, CSc., Doc. PhDr. J. Rybár, CSc. 1.9.1999-

FEI TU Košice Organization of a conference about Computational Intelligence Prof. Ing. P. Sinčák, CSc. 1.1.2003-

17.5.2003

SjF STU Bratislava New trends in teaching mathematics RNDr. V. Záhonová, PhD., Mgr. M. Kováčová, PhD., Doc. J. Dobrakovová

1.1.2003-31.12.2005


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FEI STU New trends in teaching mathematics RNDr. Ľ. Marko, PhD. 1.1.2003-31.12.2003



Duration

FFP UO, Opava Organization of a seminar on Artificial Life and Cognition Prof. RNDr. J. Kelemen, DrSc. 1.5.2000-

University of Alcalá de Henares, Madrid COST TARSKI cooperation Prof. Tomasa Calvo, Enriqueta

Muel 2002-2005

J. Kepler University, Linz CEEPUS cooperation Prof. E.P. Klement 2003-2004



Valid date

Kvasnička Vladimír Slovak Academic Society member zakladajúci člen,

1997 Kvasnička Vladimír Slovak Artificial Intelligence Society chairmann 29.8.2000-

Kvasnička Vladimír Slovak Computer Science Society member 1.1.1996-

Kvasnička Vladimír Slovak Society for Mathematicions and Physicists member 1980-1992

Kvasnička Vladimír Scientific Commity of FCHPT STU member 1.9.2002-

Kvasnička Vladimír Scientific Commity of FIIT STU member 1.10.2003-

Kvasnička Vladimír

Joint Commission for PhD study in Applied Informatics member 1.1.1998-


Joint Commission for PhD study in Artificial Intelligence member 1.1.2000-

Šabo Michal Joint Commission for PhD study in Applied Mathematics member 1.1.1998-


Commission for defence of DrSc. dissertations in Chemical Physics member 1.1.1998-

Garaj Ivan Technical commission TK71 Applications of statistical methods in quality control member 1.1.2003

Garaj Ivan Committee of Slovak Statistical and Demographic Society member 1.1.2000

Kolesárová Anna Slovak Society for Mathematiciants and Physicists member 1974-

Kolesárová Anna Editorial Board of Tatra Mountains Math. Publ. member 1998

Šabo Michal Slovak Society for Mathematicians and Physicists member 1968- Pospíchal Jiří Slovak Computer Science Society member 1.1.1996- Pospíchal Jiří Slovak Artificial Science Society member 29.8.2000- Antoni Jozef Slovak Society for Mathematicians and Physicists member 1968- Baláž Vladimír Slovak Society for Mathematicians and Physicists member 1978- Jasem Milan Slovak Society for Mathematicians and Physicists member 1978- Varga Štefan Slovak Society for Mathematicians and Physicists member 1968-



Valid date

Kvasnička Vladimír MATCH Communications in Mathematical Chemistry member of advisory 1.1.1998-

Kvasnička Vladimír Neural Network World member of advisory 1.1.2001-

Kvasnička Vladimír Croatica Chimica Acta member of advisory 1.1.2002-

Kolesárová Anna

European Society for Fuzzy Logic and Technology (EUSFLAT) member 1998-

Šabo Michal European Society for Fuzzy Logic and Technology (EUSFLAT) member 1998-


134

Šabo Michal SEFI - Mathematical Working Group member 1994-

Pospíchal Jiří EURO Working group on fuzzy sets (EUROFUSE) (http://allserv.rug.ac.be/~bdebaets/members.html#SlovakRepublic)

member 1999-



Date / Duration

Kvasnička Vladimír Santa-Fe seminar on Evolutionary theory Czech

Republic 10.6.2003/3 days

Pospíchal Jiří Conference Mendel 2003 Czech Republic 4.6.2003-6.6.2003

Šabo Michal Conference Cost Action 274 TARSKI Belgium 3.12-6.12.2003

Kolesárová Anna Conference Principles of Fuzzy Preference Modelling and Decision Making Belgium 30.11-2.12.2003

Kolesárová Anna Conference COST Action 274 TARSKI Belgium 3.12.2003-6.12.2003 Kolesárová Anna Conference EUSFLAT' 2003 Germany 10.-12.9.2003 Kolesárová Anna Cracow Technical University Poland 9.6.2003-23.6.2003 Šabo Michal Conference EUSFLAT' 2003 Germany 10.-12.9.2003



Gall, M. Cooperation in strategies of a spacially distributed game with and without memory Pospíchal, J.

Hisira, M. Application of a system of nonlinear equations in chemistry Baláž, V. Kubovičová, D. Evolution of cooperation in a spacially distributed game Pospíchal, J. Mišiaková, S. Prediction of properties of chemical compounds by neural networks Pospíchal, J.


[1] Kolesárová, A.: 1-Lipschitz aggregation operators and quasi-copulas. Kybernetika 39, 615-629 (2003). [2] Kvasnička, V., Pospíchal, J.: Artificial Chemistry and Molecular Darwinian Evolution in silico. Collection of Czechoslovak

Chemical Communications 68 (2003) 139-177. [3] Jasem, M.: On Lattice-Ordered Monoids. Discussiones Mathematicae, General Algebra and Applications 23, 101-114 (2003). [4] Kvasnička, V.: Replicator theory of coevolution of genes and memes. Neural Network World 13 (3) (2003) 255-266. [5] Pospíchal, J., Kvasnička, V.: Simulated annealing construction of shortest paths on incomplete graphs. Neural Network World

13 (3) (2003) 277-290. Neural Network World 13 (3) (2003) 277-290. [6] Garaj, I., Janiga, I.: Exaktný výpočet dvojstranných tolerančných medzí normálnych rozdelení s neznámymi strednými

hodnotami a s neznámym spoločným rozptylom, Exact calculation of two-sided tolerance limits of normal distributions with unknown mean and unknown common variance. Statistika 4/2003, pp. 29-35

[7] Janiga, I, Garaj, I.: Two-sided Tolerance Limits of Normal Distributions with Unknown Means an Unknown Common Variability. MEASUREMENT SCIENCE REVIEW, Volume 3, Section 1, 2003, pp. 75-78

[8] Kvasnička, V: Konekcionistické modelovanie v kognitívnych vedách. Connectionist modelling in cognitive sciences Filozofia 58(1) (2003) 35-43.

B. Conferences [1] Kolesárová, A., Mordelová, J., Muel, E.: A review of binary kernel aggregation operators. Proc. AGOP ' 2003, Alcalá

de Henares, Spain ( ISBN: 84-8138-570-0), 97-102 (2003). [2] Kolesárová, A.: On the operator equation A+B=sum. Proc. of Third Int. Conference EUSFLAT ' 2003, Zittau, Germany(

ISBN: 3-9808089-4-7), 285-289 (2003) [3] Kvasnička, V: "Memetics ""in silico""" In: J. Kelemen (ed.): Kognice a umělý život III. Ediční středisko FPF SU, Ostrava, 2003,

ISBN 80-7248-186-8, pp. 109-120. [4] Pospíchal, J.: Adaptive fitness and the seceeder model of group formation. In R. Matoušek, P. Ošmera: MENDEL 2003,

Proceedings of 9th International Conference on Soft Computing, VUT Brno Press, 2003, ISBN 80-214-2411-7, pp. 76-84 [5] Šabo, M., Sarkoci, P.: The History and Role of Relevancy Transformation Operators. Proc. Uncertainty Modeling'2003, STU

Bratislava, Slovakia, 1-5(2003) [6] Šabo, M.: Fuzzy Modeling Inference Process "Proc.of Third Sem.""Fuzzy Sets and Quantum Structures, Vyhne'2002,

Slovakia, 42-50(2003)" [7] Šabo, M.: The role and properties of rule relevancy in fuzzy inference process. Proc.of Third Int.Confference EUSFLAT'2003,

Zittau, Germany, 259-262 (2003) [8] Šabo, M.: The Role of T-Reversible T-Norms in Fuzzy Preference Structures. Proc.of Second Int. Conference

APLIMAT'2003, Bratislava, Slovakia,659-664 (2003)


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[9] Janiga, I*., Garaj, I.: Two-sided Tolerance Limits of Normal Distributions with Unknown Means an Unknown Common Variability. MEASUREMENT 2003. 4nd International Conference on Measurement., pp.75-78, Smolenice , June 15-19, 2003.

[10] Janiga, I, Garaj* I.: Two-sided Tolerance Limits of Normal Distributions with Unknown Parameters. International Conference. Managment, Economic and Business in new Europe, pp. 107-112, Brno,April 25, 2003.

[11] Kolesárová, A.: On extensions of crisp utility functions. Proc. of The Third Seminar: Fuzzy Sets and Quantum Structures, STU Bratislava, 34-41 (2003).

[12] Kolesárová, A.: On ordinal weighted means. Proc. of Second Int. Conference APLIMAT ' 2003, Bratislava, Slovakia (ISBN: 80-277-1813-0), 441-445 (2003).

[13] Kolesárová, A.: Some new results on quasi-copulas. Proc. Uncertainty Modelling ' 2003, STU Bratislava, 14-19 (2003). [14] Kvasnička, V., Pospíchal, J.: Evolúcia jazyka a univerzálny darwinizmus. Evolution of language and universal darwinizm. In:

J. Kelemen (ed.): Kognice a umělý život III. Ediční středisko FPF SU, Ostrava, 2003, ISBN 80-7248-186-8, pp. 121-150. [15] Kvasnička, V: "Memetika ""in silico""" "Memetics ""in silico""" In: P. Sinčák, V. Kvasnička, J. Pospíchal, J. Kelemen, P. Návrat:

Slovensko-České rozpravy o umelej inteligencii. elfa publishing, ISBN 80-89066-64-X, Košice, 2003, pp. 61-72. [16] Pospíchal, J.: Simulácie vzniku druhov s modelom odpadlíka. Simulation of emergence of species with a seceeder model. In:

J. Kelemen (ed.): Kognice a umělý život III. FPF SU Publishing, Ostrava, 2003 ISBN 80-7248-186-8, pp. 165-174. [17] Pospíchal, J.: Vznik druhov, adaptívny fitnes a model odpadlíka. Emergence of species, adaptive fitness and the seceder

model. In: P. Sinčák, V. Kvasnička, J. Pospíchal, J. Kelemen, P. Návrat: Slovensko-České rozpravy o umelej inteligencii. elfa publishing, ISBN 80-89066-64-X, Košice, 2003, pp. 95-102.

[18] Garaj, I*., Janiga, I.: Dvojstranné tolerančné medze normálnych rozdelení s neznámymi strednými hodnotami a s neznámym spoločným rozptylom. Two sided tolerance limits of normal distributions with unknown means and unknown common variability. 2nd International Conference APLIMAT 2003, pp. 127-131, February 5-7, 2003 Bratislava.

[19] Garaj, I..: Numerický výpočet kvantilov normovaného normálneho rozdelenia v programovom systéme Mathematica s presnosťou na 16 desatinných miest. Numerical calculation of quantiles of normal distribution in the Mathematica programming system with a precision on 16 decimal numbers. 12. Medzinárodný seminár VÝPOČTOVÁ ŠTATISTIKA, pp. 28-31, 4.-5. 12. 2003 Bratislava

[20] Janiga, I, Garaj* I.: Exaktné tolerančné intervaly pre normálne rozdelené znaky kvality. Exact Tolerance Intervals for Normaly Distributed Quality Characteristics. 12nd International Conference – Quality 2003, pp. 20-22, May 13-15, 2003, Ostrava.

[21] Janiga, I*., Garaj, I.: Dvojstranné tolerančné intervaly normálneho rozdelenia s neznámymi parametrami. Two-sided Tolerance Limits of Normal Distributions with Unknown Parameters. STAKAN III, 23.-25. května, Bystřica pod Hostýnem.

[22] Kolesárová, A.: 1-Lipschitz aggregation operators. Lecture at the Conference: Principles of Fuzzy Preference Modelling. Bilateral Scientific and Technological Cooperation Flanders-Hungary, Gent, Belgium (2003).

DEPARTMENT OF NUTRITION AND FOOD ASSESSMENT

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Head of Department: Telephone: ++421-2-59325491 Assoc. Prof. Ernest Šturdík, PhD Fax: ++421-2-52493198


I. STAFF Associate Professors: Vladimír Frank, PhD; Mária Takácsová, PhD; Ľubomír Valík, PhD Assistant Professors : Eva Hybenová, PhD; Mária Kováčová, PhD; Vlasta Kuklišová, MSc.; Soňa Škrovánková, MSc; Research Fellows: Bernadette Hozová, PhD; Viola Buchtová; Anna Mikulajová, MSc. PhD Students: Silvia Vojteková, MSc; Iveta Kukurová, MSc; Kitti Németh, MSc; Denisa Lauková, MSc; Iveta Együdová, MSc; Alena Gajdošová, Mgr Technical staff: Žofia Fórová; Edita Kovačičová; Eva Vosátková;

II. TEACHING AND RESEARCH LABORATORIES A. Teaching laboratories:

Laboratory of Food Microbiology and Hygiene Laboratory of Food Analysis and Assessment

B. Research laboratories: Laboratory of Food Microbiology and Hygiene Laboratory of Food Analysis and Assessment Laboratory of Food Chemistry


5. semester (Bc) Food Chemistry I. (2 h) Takácsová 6. semester (Bc) Food Analysis (2 h) Kováčová Laboratory of Food Analysis (4 h) Kováčová Semestral Project (0-4 h) All Department Staff 1. semester (MSc) Food Microbiology (2 h) Valík Laboratory of Food Microbiology (3 h) Valík, Frank, Hozová, Kuklišová Food Additives and Contaminants (2-0 h) Hybenová Laboratory Practice Food Additives

and Contaminants (0-2 h) Hybenová

1. semester (MSc) Physiology and Pathophysiology of Human Nutrition

(2-2 h) Bukovský

Semestral Project I. (0-5 h) All Department Staff 2. semester (MSc) Food Hygiene (2-1 h) Valík Food Chemistry II. (2 h) Takácsová Diethology (2 h) Kajaba Semestral Project II. (0-5 h) All Department Staff 2. semester (MSc) Laboratory of Food Chemistry (1 h) Takácsová Food Analysis II. (2 h) Prachár Laboratory of Food Analysis II (4 h) Prachár Food Toxicology (2 h) Piecková 2. semester (Bc) Laboratory Practices (0-4 h) All Department Staff 3. semester (MSc) Food Additives and Contaminants (0-2 h) Hybenová Food Evaluation (2 h) Škrovánková Laboratory of Food Evaluation (0-2 h) Škrovánková Laboratory Practice Food Additives

and Contaminants (0-2 h) Hybenová

3. semester (MSc) Food Ecohygiene (2-0 h) Frank Semestral Project III. (0-5 h) All Department Staff


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4. semester (MSc) Diploma Project (0-27 h) All Department staff

IV. CURRENT RESEARCH PROJECTS A. Governmental project 2003 SP 27/028 0E 02/028 0E 02 Quality, safety and functionality of primary

food resources“ (Eva Hybenová) The project is coordinated by Research Institute of Plant Production where some tasks of the project are carried out in our Faculty. Objectives of these tasks are focused on a) Enhancement of nutritional value of various types of cereals by polyunsaturated fatty acids, b) Evaluation and selection of primary food resources and preparation of functional foods with preventive-medical properties, c) Study of genotype dependance on lipid profile in oil seeds, d) Identification of essential fatty acids donors in cereals. Project duration: from 2003 to 2005

B. COMmon dataBASE on microbial responses to food environments generated in EU (in cooperation with IFR; contact person of STU Bratislava - Ľubomír Valík)

Important advances to develop such a database structure were made by the Institute of Food Research (IFR, Norwich, UK) in the 90’s. The IFR database format is utilised in a project, called ComBase, being jointly run by the U.S. Department of Agriculture - Agricultural Research Service (USDA/ARS), Institute of Food Research (IFR) and Food Standard Agency of the UK (FSA). ComBase will store the raw data of the USDA Pathogen Modeling Programme, which is one of the largest databases of its kind. FSA is supporting ComBase by releasing data and computer programs developed at IFR and funded by the FSA. The project has attracted the interest of many universities and industrial partners. Some of them (first of all University of Complutense Madrid, UCM) has already submitted large amount of suitable data to ComBase. Project duration: from 2002 to 2004

C. VEGA Project No 1/9133/02 Development, optimising and control of new food products with the aim to increase the food quality using biological active substances and modern technologies (Alexander Dandár)

Research activity was focused on selection, analysis and utilization of antioxidants of natural sources namely of plant origin, applied in edible plant oil. Antioxidative activity of ethanol extracts from oil seeds /corn, amaranth, soy, rapeseed, and cultivated flax/ as well as from legumes /pea, lens, bean, chickpea, French bean/ was studied.Positive antioxidant effects on lipid stability were established e.g. in the samples of heat-treated pork with lens. Antioxidative activity of ethanol extracts of some spices as green and black tee and coffee drinks. Volatile compounds of silica and the extracts from selected herbs and tees as well as its sensory properties were analysed too.Chemical parameters of sensory properties of fermented natural juices /cabbage, celery and beetroot/ were evaluated. Effect of NaCl content and an initial pH value as well as the effect of bacteria on biogenic amines and organic acids production were observed in evaluated juice samples. Decrease of vitamins B in heat-treated confectionery samples within an optimazing of technology was studied. Soy flavonoids / genistein, daidzein and their glukozides / in term of their antioxidative properties were studied.The influence of polyphosphate content on sensory and physico-chemical properties in selected meat products was observed. Nutritive parameters as well as the additives, mainly amino acids composition were analysed. An effect of lactic acid addition applied on the surface of butcher`s meat with the aim to extend its shelf life was evaluated. Project duration: from 2002 to 2004

D. Development of Good Hygiene Practices in the Slovak Food Industry; Development of the standard approach for codes to hygiene practice (in cooperation with STOAS Netherlands and Ministry of Agriculture of the SR; national expert - Ľubomír Valík)

The Netherlands and Slovak task force will develop a standard approach for the development, implementation and verification of codes to hygiene practice. The standard approach must be based on best practices from the Netherlands and/or from other EU sources. The standard approach must include all principles of HACCP according to Codex Alimentarius, the documentation on the hazard and risk analyses for future reference and a general structure according which to develop common codes to hygiene practice. The standard approach must be approved by the official inspection institutes (task international consultants (I.C.): initially a workshop should be held to train task force members and to develop a common understanding of (content and budget is task of I.C., organisation is task of T.L.); the background of food safety including legislation, hygiene, food safety hazards, historical and future food safety developments in the international food market; the principles of HACCP and the approach to risk analyses; the development, implementation and verification of HACCP-systems and hygiene codes; the programs, methods and material to train the workforce on good hygiene practice in relation to HACCP systems and hygiene codes. A course was be made on the developed approach, methods and techniques to be able to train project teams, which undertake to develop specific codes. This course will include the development-, the implementation- and the verification phase. Subjects were:- legislation; food safety hazards determination; risk assessment; control measures; documentation; validation; verification and registration (task of I.C.). Project duration: from 2003 to 2004

E. Study of the influence environmental factors on behaviour of technological and health relevant microflora in foods and food production areas (in cooperation with Institute of Food research Bratislava - Ľubomír Valík).

Principles of predictive microbiology in the evaluation of hygienic safety of food were used. Mathematical modelling of growth of hygienically relevant microorganisms in model systems, in food and in emulsion systems was worked out. Prediction of shelf-life and dynamics of microbial deterioration of foods was studied. Influence of external and internal environmental determinants on food micro flora.


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V. CURRENT EDUCATION PROJECTS A. Nutrition and health in training and education - V. Frank; M. Takácsová Preparation of variable training and educational moduls for various groups. Preparation of conceptual framework and subjects for whole-life education in nutrition, health and food safety in cooperation with the EAEA - European Association for the Education of Adults (http://www.eaea.org/slovak/eaea.html) and Institute of whole-life education at Slovak University of Technology (http://www.stuba.sk/svk1/icv/slovak.html). Establishing of the Educational centre STU in co-operation with College of Education of the Trnava university. Development of programmes for pre-sschool and school nutrition recommendations. Project duration: from 2003 to 2005

B. Implementation of the BSP Food Safety Action (FSA) in cooperation with CIAA as a national expert - Ľubomír Valík

The experts have been provided with a well crafted methodology to carry out their job and have been provided with specific tools to achieve the expected results. Monitoring of the activities and evaluation of the results - by CIAA and the E. Commission - will be done according to the scheme provided: there is no place for “creative” interpretation or reporting. Project duration: from 2003 to 2004

VI. COOPERATION A. Cooperation in Slovakia


Duration

Rajo, S.A., Bratisl. Experimental and consult. project Ľ. Valík All the year Palma Tumys S.A. Experimental project Ľ. Valík Two months Institute of Food Research Experimental project Ľ. Valik All the years

Agrifood , accredited testing laboratory s.r.o., Prievidza

Microbiological analysis V. Frank 1998-2004

Research Institute of Plant Production

Cooperation on governmental project "Quality, safety and functionality of primary food resources"

E. Hybenová 2003-2005



Duration

Institute of Food Research

Support for database on predictive food microbiology Ľ. Valík All the year

STOAS Netherlands Consultancy and experimental in hygiene and HACCP Ľ. Valik All the year

CIAA Brussels Expert's cooperation Ľ. Valík A month in 2003 C. Membership in Domestic Organizations and Societies


Valid date

B. Hozová Expert of the Slovak National Accreditation Service – Technical Commission TVA-L4 member

E. Hybenová, Ľ. Valík Member of Committee of the Food Section SCHS member

V. Frank, B. Hozová Slovak Chemical Society (SCHS' member

E. Hybenová Slovak Society of Forestry, Agricultural, Food and Veterinary Sciences at Slovak Academy of Sciences

member

K. Nemeth Slovak Society of Forestry, Agricultural, Food and Veterinary Sciences at Slovak Academy of Scieces, Bratislava

member


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A. Mikulajova Slovak Society of Forestry, Agricultural, Food and Veterinary Sciences at Slovak Academy of Sciences, Bratislava

member

S. Škrovánková

Slovak Society of Forestry, Agricultural, Food and Veterinary Sciences at Slovak Academy of Sciences

member

V. Frank, E. Šturdík

Slovak Society of Forestry, Agricultural, Food and Veterinary Sciences at Slovak Academy of Sciences

member 1995

E. Šturdík Scientific board of the Institute of Preventive and Clinical Medicine member 2003

E. Šturdík Scientific board of the Chemical Institute (Slovak Academy of Science) member 2003

E. Šturdík Academic board of the Slovak Nuclear Society member 2003 E. Šturdík Scientific board of the UCM University Trnava member 2003 E. Šturdík Editorial Board of the Bulletin of Food Research member 2003 M. Takácsová Editorial Board- Czech Journal of Food Sciences member 2003



Valid date

B. Hozová, V. Frank, Ľ. Valík Czechoslovak Society for Microbiology member

B. Hozová Expert of Certikom, Ltd. Deutsche Akkreditierungssystem member F. Visits of Staff Members and Postgraduate Students in Foreign Institutions


Date / Duration

Ľ. Valík University of Chemical Technology, Prague CZ January 2003 (2 days) Ľ. Valík Institute of Food Research, Norwich UK April 2003 (a week)

Kitti Nemeth Institute of Animal Reproduction and Food Research of the Polish Academy of Sciences Poland 8 months

Anna Mikulajova Agricultural University of Wroclaw Poland 1 month

VII. THESES AND DISSERTATIONS A. Graduate Theses (Bc Degree) for state examinations after three years of study

Name Title of Thesis Supervisor B. Bancíková Unconventional sources of flavonoids S. Vojteková E. Baxová Fresh cheese in human nutrition. V. Kuklišová N. Hudjec Mycotoxins E. Hybenová G. Galajdová Study of antioxidative activity and stability of selected flavonoids S. Vojteková L. Sekerešová Bacterial toxins E. Hybenová L. Šindelková Sensoric methods with mathemathic-statistical evaluation S. Škrovánková S. Špaldová Analysis of flavourous spice and herbal compounds S. Škrovánková E. Malinová Use of citrus flavonoids as the source of natural antioxidants M. Kováčová N. Bordash The relations between aditives and healthy nutrition requirements V. Frank

Segíňová, L. Effectt of free Radicals of Lipids on Foods Quality and their Prevention by natural Materials M. Takácsová

Kobzová, J. Effect of natural Antioxidants on Formation of oxidative Products of Lipids M. Takácsová


Miriama Bohucká Antioxidative properties of selected agricultural raw materials. M. Takácsová Jozef Fedor Examination of amno acid concentration in soya products. V. Buchtová

Jana Gulánová Study of free amino acids in cow and goat milk at simulated digestive conditions V.Kuklišová; V.Boroš

Mária Havasiová Microbiological control of yoghurt production. Ľ. Valík Jana Janecová Study of antioxidative effects of apples. M. Kováčová Michaela Keslérová Sensoric evaluation of various kinds of tea S. Škrovánková

Marcela Malová Evaluation of fermented vegetable juices E. Hybenová Nadežda Matičová Application of selected proteolytic enzymes in dough B. Hozová


140

Monika Morochovičová-Fundáková

Microbiology properties of spices and taste additives V. Frank

Ľudmila Mošková Isolation and stabilisation of buckwheat flavonoids M. Kováčová Natália Rašová Effect of selected by-product on lipid stability in foods A. Mikulajová Mária Stracová Sensoric evaluation of selected herbs and herbal tea S. Škrovánková Matej Pokrievka Microbiological relations of lactic acid fermentations D. Lauková, Ľ. Valík Knapčíková Denisa The effect of storage on microbial quality of selected foods V. Frank


Lauková D. Stability of food emulsions. Š. Schmidt, Ľ. Valík Kukurová I. Interactions of antibiotics in milk in the determination of detection limits. B. Hozová Németh K. Onion flavonoids: Content, absorption, metabolism. M. Takácsová

Petríková J. Quantitative analysis of mutual relationships among microorganisms in foods. Ľ. Valík

Együdová I. Valuation and selection cereals for development foods with minimal contents unfavourable substances. V. Frank

Gajdošová A. Valuation and selection cereals for development foods with preventive medicinal properties. V. Frank

Mikulajová A. Effect of addition of some raw materials and secondary raw materials on food lipids stability. M. Takácsová

Škrovánková S. Isolation and Identification of sensory effective natural Materials of Plant Origin M. Takácsová

Vojteková S. Study of flavonoids in term of stability and antioxidant effects in selected raw materials. M. Takácsová

Ďuračíková A. Development of rapid methods for the diagnostic of microorganisms. B. Hozová


[1] Hozová, B., Kukurová, I., Dodok, L.: Application of transglutaminase and fermizyme for sensory quality improvement of pastry. NAHRUNG 47 (3): 171-175 JUN 2003

[2] Kukurová, I., Hozová, B.: "Interactions of antimicrobials in milk and their detection by the disk diffusion method and Delvotest SP. " J AOAC INT 86 (3): 529-533 MAY-JUN 2003

[3] Németh, K., Plumb, G.W., Berrin, J.-G., Juge, N., Jacob, R., Naim, H.Y., Williamson, G., Swallow, D.M., Kroon P.A.: Deglycosylation by small intestinal epithelial cell beta-glucosidases is a critical step in the absorption and metabolism of dietary flavonoid glycosides in humans. Eur. J. Nutr. 42 (1), 29-42 (2003).

[4] Mikulajová, A., Takácsova, M., Nemeth, K.,Rasova, S., Vojtekova: Antioxidant activity of wheat bran extract in rapeseed oil. Źywwność.Nauka. Technologija. Jakość, 2003, 2,(35),124-128.

[5] Németh, K., Piskuła, M.K.: Effect of cooking on yellow onion quercetin. Pol. J. Food Nutr. Sci. 12/53 (SI 1), 175-179 (2003). [6] Németh, K., Takácsová, M., Piskula,M.K.: Flavonoid metabolism in human. Źywność. Nauka. Technologija. Jakość, 2003, 2

(35), 129-133. [4] Wiczkowski W., Németh, K., Bucinski A., Piskuła, M.K.: Bioavailability of quercetin from fresh scales and dry skin of onion in

rats. Pol. J. Food Nutr. Sci. 12/53 (SI 1), 100-104 (2003). [5] Lauková, D., Valík Ľ., Görner, F.: Effect of lactic acid on the growth dynamics of Candida maltosa YP1. Czech J. Food Sci.,

21, 2003: 43-49. [6] Valík, Ľ., Görner, F., Lauková, D.: Growth Dynamics of Bacillus cereus and Shelf-life of Pasteurised Milk. Growth Dynamics

of Bacillus cereus and Shelf-life of Pasteurised Milk. Czech. J. Food Sci., 21, 6, 2003. s. 195-202 [7] Lauková, D., Valík. Ľ.: Kvantitatívna analýza vplyvu substrátu a teploty na rast kvasinky Candida maltosa YP1 Quantitative

analysis of growth Candida maltosa YP1 in dependance on substratum and temperature Bulletin potravinárskeho výskumu, 42, 2003, č. 4, s. xxx.

[8] Lauková, D., Valík Ľ., Görner, F.: Heat Resistance of vegetative cells of Candida maltosa YP1. Agriculture Agriculture (Poľnohospodárstvo), 49 (7), 2003: 375-380.

[9] Piecková, E., Valík, Ľ., Görner, F.: Mikroskopické vláknité huby v jogurtoch. Filament Funfi in Yoghurts. Bulletin potravinárskeho výskumu, 41, 2002, č. 4, s. 291-301.

[10] Pišteková, P., Maďarič, A., Šturdík, E.: Biologické účinky flavonoidov. Biological effect of flavonoides. Farmakologický obzor, 72, 2003, s. 170-179.

[11] Gajdošová, A., Múčková, M., Šturdík, E.: Produkcia taxánov kalusovými kultúrami tisu. Production of taxans by calus culture of yew-tree. Nova Biotechnol., 3, 2003, s.52-63

[12] Kokindová, M., Kraic, J.: DNA polymorfizmus pšeníc druhu Triticum turgidum L. Nova Biotechnol., 3, 2003, s.81-91 B. Conferences (*international conferences)

[1] Hybenová, E., Malová, M.: Lactic acid fermented vegetable juices inoculated with Lactobacillus plantarum and Saccharomyces cerevisiae. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy, 97 (8), 797-798 (2003).

[2] Mikulajová, A., Takácsová M., Vojteková, S., Rašová, N.: Stabilization of rapeseed oil with wheat bran and buckwheat hulls.


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In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97 (8), 789 (2003). [3] Škrovánková, S., Hybenová, E.*: The flavour, aroma and health aspects of herbal teas. In: 55. zjazd chemických spoločností,

Košice, 8.9.-12.9.2003, Chem. Listy 97 (8), 790 (2003). [4] Vojteková, S.*, Takácsová, M., Kováčová, M., Mikulajová, A.: Stability of flavonols isolated from onion scales. In: 55. zjazd

chemických spoločností, Košice, 8.9.-12.9.2003, Chem. listy,97, 2003,č.8,s. 789-790. [5] Hybenová, E., Šmeringová, K.: Inhibition properties of Lactobacilli and their survival at low pH-value In: 55. zjazd

chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy, 97 (8), 783-784 (2003). [6] Lauková, D., Valík, Ľ., Görner, F., Schmidt, Š*.: Quantitative analysis of acid tolerance Candida maltosa YP1 In: 55. zjazd

chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 2003, 97 (8) 794. Pr. [7] Dandár, A.*,Kostičová, M., Hybenová, E: Stanovenie mikrobiálnej aktivity v extraktore cukrovaru Determination of microbial

activity in extractor of sugar factory. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy, 97 (8), 791 (2003).

[8] Kováčová, M., Takácsová, M., Vojteková, S., Fodorová, M.: Štúdium antioxidačných účinkov izoflavónov sóje. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy,97, 2003,č.8, s.790-791.

[9] Škrovánková, S., Takácsová, M.: Zdravotné aspekty bylinných čajov In: Zborník prednášok z XIV.medz. konf. o analytických metódach v potravinárstve. 18 a 19.2.2003 B. Bystrica, 2003, s. 338-340. ISBN 80-227-1887-4.

[10] Takácsová, M., Kováčová, M., Sova, M.: Antioxidačný účinok extraktov repky a sóje. In: Zborník prednášok z XIV. medz.konf. io analytických metódach v potravinárstve. 18. a 19.2.2003 B. Bystrica, 2003, s. 347. ISBN 80-227-1887-4.

[11] Vojteková, S., Kováčová, M.*, Takácsová, M.: Vplyv žiarenia na stabilitu flavonoidov izolovných zo šupiek cibule. Effect of irradiation on the stability of flavonoids isolated from onion scales. In: Zborník prednášok z XIV. medz.konf. o analytických metódach v potravinárstve. 18. a 19.2.2003 B.Bystrica, 2003, s. 352 -355. ISBN 80-227-1887-4.

[12] Lauková, D.*, Valík Ľ., Görner, F., Schmidt, Š.: Dynamika rastu Candida maltosa v mlieku a smotane. Growth Dynamics of C. maltosa YP1 in milk and cream. "In: Celostátní přehlídky sýrů 2003. Výsledky přehlídek a sborník přednášek semináře Mléko a sýry 2003. Ed.: Štětina a kol., Česká společnost chemická, Praha, 2003, s.89-95. ISBN 80-86238-31-8; EAN 978-80-86238-31-9 (Pr)"

[13] Lauková, D.*, Valík, Ľ., Filip, V., Pokorná, I., Plocková, M., Schmidt, Š.: Dynamika rastu Candida maltosa YP1 v emulziách olej vo vode. Growth Dynamics of C. maltosa YP1 in O/W emulsions. In.: Zborník zo 41. Medzinárodnej konferencie z technológie a analytiky tukov, 14.-16. mája 2003, Trenčianske Teplice. Vyd. Palma-Tumys 2003, s. 134-139. ISBN80-86238-32-6.

[14] Lauková, D.*, Valík, Ľ., Görner, F., Leskovská, L., Martinická, L.: Dynamika rastu Bacillus cereus v mlieku a smotane. Growth Dynamics of B.cereus in milk and cream. "In: Celostátní přehlídky sýrů 2003. Výsledky přehlídek a sborník přednášek semináře Mléko a sýry 2003. Ed.: Štětina a kol., Česká společnost chemická, Praha, 2003, s.143-147. ISBN 80-86238-21-0; EAN 978-80-86238-21 (Pr)"

[15] Lauková, D., Valík, Ľ.*, Görner, F.: Vplyv teploty na dynamiku B. cereus v mlieku a smotane. Effect of temperature on growth dynamics of B. cereus in milk and cream. "In: Životné podmienky a zdravie. Zborník vedeckých prác. Ed.: Prof. Ághová, Štátny fakultný zdravotný ústav SR, Bratislava, 2003, s.144-147. ISBN 80-7159-138-6; EAN 978-80-71591382 "

[16] Valík, Ľ.*, Görner, F., Lauková, D.: Kvantitatívna charakterizácia acidotolerancie kvasinky Candida maltosa YP1. Quantitative characteristic of acid-tolerance of Candida maltosa YP1. In: Mikrobiologie potravin. Sborník ze semináře, Ed.: Demnerová, K., Jenč, P., Vysoká škola chemicko-technologická, Československá společnost mikrobiologická, Komise potravinářské mikrobiologie, 2003, s. 65-70. ISBN 80-7080-519-6

[17] Valík, Ľ.*, Görner, F.: K trvanlivosti a hygienickej bezchybnosti pasterizovaného mlieka. Notes to the safety and shelf-life of pasteurised milk."In: Životné podmienky a zdravie. Zborník vedeckých prác. Ed.: Prof. Ághová, Štátny fakultný zdravotný ústav SR, Bratislava, 2003, s.139-143. ISBN 80-7159-138-6; EAN 978-80-71591382 (Pr)"

[18] Abulgasem, F. M. A., Dodok, L., Trubač, K., Buchtová, V. Hozová, B., Starúch, L., Gajdošová, J.: Možnosti uplatnenia stabilizátora S 1 v pekárskej technológii.Utilization of S 1 stabiliser in baking technology. "In:z XIV. Medz. Konferencie "" LABORALIM 2003 "" o analytických metódach v potravinách. Slovenská spoločnosť SAV, Bratislava, s. 94 -97, ISBN 80 - 227 -1887 -4."

[19] Augustín, J.*, Sűli, J., Patoprstá, I., Škrovánková, S.: Analytické a senzorické hodnotenie čajovníkových listov (Camellia sinensis) Analytical and sensory evaluation of the quality of tealeaves (Camellia sinensis). In: Laboralim 2003, Zborník prednášok z XIV. Medzinár. Konf. O anal. Metódach v potrav. 18. a 19.2.2003 v B. Bystrici, STU Bratislava, s. 107-114. ISBN 80-227-1887-4

[20] Buchtová, V.*, Dodok, L., Jelušová, M.: Štúdium aminokyselinového zloženia v zmesi korenín používaných pri príprave kurčiat. Study of amino acids composition in the spice mixture for roasted chicken. In: Zborník prednášok z XIV. Medzinárodnej konferencie o analytických metódach v potravinárstve „Laboralim 2003“. Banská Bystrica 18. – 19. februára 2003. Slovenská spoločnosť pre poľnohospodárske, lesnícke, potravinárske a veterinárske vedy pri SAV, Bratislava 2003. s.126-128, ISBN 80-227-1887-4.

[21] Dodok, L.*, Abulgasem, F.M.A., Trubač, K., Buchtová, V., Hozová, B., Staruch, L., Gajdošová, J.: Porovnanie dvoch spôsobov aplikácie emulgátora pri výrobe bežného pečiva. "In:z XIV. Medz. Konferencie "" LABORALIM 2003 "" o analytických metódach v potravinách. Slovenská spoločnosť SAV, Bratislava, s. 148 - 151, ISBN 80 - 227 -1887 -4."

[22] Dodok, L.*, Hozová B., Buchtová, V., Staruch L., Halabuková V.: Aplikácia transglutaminázy v cereálnej technológii. In: Zb. z XXXIV. Symposia o nových směrech výroby a hodnocení potravin. Skalský Dvur, 26.-28.5.2003,307-313. ISBN 80-902671-6-5. (Po)

[23] Frank, V., Machalcová, T., Škvareková, Z.: Mikrobiologická kvalita niektorých parených syrov. Microbiological Quality of steamed cheese. "In: Zborník prednášok z XIV. Medzinár. konferencie o analytických metódach v potravinách, ""LABORALIM ´03"", Slovenská spoločnosť SSPLPV SAV, Bratislava 2003, s. 171-174, ISBN 80-227-1887-4"

[24] Frank,V., Machalcová, T., Žemberová, J.: Rozbor mikrobiologických vlastností vybraných mrazených výrobkov. Microbiological Analysis of selected frozen food products. "In: Zborník prednášok z XIV. Medzinár. konferencie o analytických metódach v potravinách, ""LABORALIM ´03"", Slovenská spoločnosť SSPLPV SAV, Bratislava 2003, s. 167-170, ISBN 80-227-1887-4"


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[25] Hozová, B., *Staruch, L., Buchtová, V. , Dodok, L. : Zlepšenie akosti cereálnych výrobkov prídavkom mikrobiálnej transglutaminázy. "In"" Zb. prednášok z XIV. Medzinárodnej konferencie o analytických metódach v potravinárstve Laboralim 2003,B.Bystrica 18.-19.2.2003,192-196. ISBN 80-227-1887-4.(Po)"

[26] Kováčová, M.*, Takácsová, M., Vojteková, S. Fodorová, M.: Synergický účinok flavonoidov sóje a kyseliny askorbovej na inhibíciu oxidácie nenasýtených mastných kyselín. a kyseliny askorbovej na inhibíciu oxi In: Laboralim 2003,Zborník prednášok zo XIV. Medzinárodnej konferencie o analytických metódach v potravinárstve. Banská Bystrica, 18.-19.2.2003. Vydavateľstvo STU Bratislava, s.225-228 (2003). ISBN 80-227-1887-4. (Po)

[27] Kováčová, M.*, Takácsová, M., Vojteková, S., Žemličková, Z.: Zvýšenie stability karotenoidov na svetle prídavkom rutínu a kyseliny askorbovej. In: Sborník příspěvku XXXIV.Symposium o nových směrech výroby a hodnocení potravin. Skalský Dvur, 26.-28.5.2003. VÚPP Praha, s.263-266 (2003). ISBN 80-902671-5-6. (Po)

[28] Kováčová, M.*, Vojteková, S., Takácsová, M., Fodorová, M.: Vplyv enzýmovej hydrolýzy na zvýšenie antioxidačnej aktivity flavonoidov sóje. In: Laboralim 2003,Zborník prednášok zo XIV. Medzinárodnej konferencie o analytických metódach v potravinárstve. Banská Bystrica, 18.-19.2.2003. Vydavateľstvo STU Bratislava, s.230-234 (2003). ISBN 80-227-1887-4. (Po)

[29] Kováčová, M., Takácsová, M., Vojteková, S., Fodorová, M.: Synergický účinok flavonoidov sóje a kyseliny askorbovej na inhibíciu oxidáćie nenasýtených mastných kyselín In: Laboralim 2003. Zborník prednášok z XIV. Medz. konf. o analytických metódach v potravinárstve. 18. a 19. 2.2003 B. Bystrica 2003, s. 225-229. ISBN 80-227-1887-4.

[30] Kováčová, M., Vojteková, S., Takácsová, M., Fodorová, M.: Vplyv enzýmovej hydrolýzy na zvýšenie antioxidačnej aktivity flavonoidov sóje. In: Laboralim 2003. Zborník prednášok z XIV. Medz. konf. o analytických metódach v potravinárstve. 18. a 19. 2.2003 B. Bystrica 2003, s. 230-234. ISBN 80-227-1887-4.

[31] Mikulajová, A., Takácsová, M., Škrovánková, S.*: Oxidačná stabilita majonéz. Oxidative stability of mayonnaise. In: „Laboralim 2003“. Zborník prednášok z XIV. Medzinárodnej konferencie o analytických metódach v potravinárstve . Banská Bystrica (SK), 18.-19. február, 2003. STU, Bratislava, s. 271-274 (2003). ISBN 80-227-1887-4. (Po)

[32] Škrovánková, S.*, Takácsová, M., Galdunová, L.: Horká a trpká chuť bylinných čajov. The bitter and astringent taste of herbal teas. In: Zborník prednášok z XIV. Medzinárodnej konferencie o analytických metódach v potravinárstve Laboralim 2003. Banská Bystrica, 18.-19.2.2003. STU Bratislava, 2003, 334-337. ISBN 80-227-1887-4. (Po)

[33] Škrovánková, S.*, Takácsová, M., Galdunová, L.: Chutnosť a obľúbenosť bylinných čajov. The flavour and favour of herbal teas. In: Zborník prednášok z XIV. Medzinárodnej konferencie o analytických metódach v potravinárstve Laboralim 2003. Banská Bystrica, 18.-19.2.2003. STU Bratislava, 2003, 331-333. ISBN 80-227-1887-4. (Po)

[34] Škrovánková, S.*, Takácsová, M.: Zdravotné aspekty bylinných čajov. The health aspects of herbal teas. In: Zborník prednášok z XIV. Medzinárodnej konferencie o analytických metódach v potravinárstve Laboralim 2003. Banská Bystrica, 18.-19.2.2003. STU Bratislava, 2003, 338-340. ISBN 80-227-1887-4. (Po)

[35] Vojteková, S., Kováčová, M.*, Takácsová, M.: Vplyv spracovania na stabilitu flavonoidov cibule. Effect of processing on the stability of onion flavonoids. In: Sborník, XXXIV. Symposium o novych směrech výroby a hodnocení potravin,Skalský Dvor (ČR), Febr.26 –29., 2003, s.283-285. ISBN 80-902671-6-5.(Po)

[36] Mikulajová, A., Takácsová, M., Németh, K.*, Rašová, N., Vojteková, S.: Antioxidant activity of wheat bran extract in rapeseed oil. Antioxidant activity of wheat bran extract in rapeseed oil. In: Bezpieczna Żywność. VIII Sesja Sekcji Młodej Kadry Naukowej Polskiego Towarzystwa Technologów Żywności. Olsztyn (Poland), May 29-29, 2003. pp. 84-85 (2003). (Po)

[37] Németh, K., Wiczkowski, W., Piskuła, M.K.: Onion processing and bioavailability of quercetin in humans. Onion processing and bioavailability of quercetin in humans. In: Abstract books. First international conference on polyphenols and health, Vichy. 172 s. (2003) (Po)

[38] Takácsová, M., Kováčová, M., Kravec, J.: Vplyv čajových extraktov na stabilitu oleja. Influence of tea extract on stability oil In: Sborník souhrnu sdělení XXX.semináře o jakosti potravin a potravin.surovin. MZLU Brno 2003, s.14. ISBN 80-7157-648-4.

[39] Vojteková, S., Kováčová, M., Takácsová, M.: Vplyv spracovania na stabilitu flavonoidov cibule. In: Sborník souhrnu sdělení XXXIV. Symposium o nových směrech výroby a hodnocení potravin. 26.-28.5.2003 Skalský Dvur, VÚPP Praha,2003, s.38.

[40] Vojteková, S., Takácsová, M., Kováčová, M., Németh, K.*, Mikulajová, A.: Stability of flavonoids in onion scales. Stability of flavonoids in onion scales. In: Bezpieczna Żywność, VIII Sesja Sekcji Młodej Kadry Naukowej Polskiego Towarzystwa Technologów Żywności. Olsztyn (Poľsko), Máj 28.–29. 2003, s. 86.(Po)

[41] Buchtová, V.*, Dodok, L., Jelušová, M.: Štúdium aminokyselinového zloženia v zmesi korenín na prípravu kurčiat. Study of amino acids composition in the spice mixture for roasted chicken. In: Sborník příspěvku XXXIV. Symposium o nových směrech výroby a hodnocení potravín. Skalský Dvúr, 26. –28. 5. 2003, ČR, VUP, Praha, s. 254 - 256, ISBN 80 - 902671 - 6 - 5.

[42] Buchtová, V.*, Dodok, L., Jelušová, M.: Štúdium aminokyselinového zloženia v zmesi korenín na ražnenie a na prípravu steikov a pečenie. In: Sborník příspěvku XXXIV. Symposium o nových směrech výroby a hodnocení potravín. Skalský Dvúr, 26. –28. 5. 2003, ČR, VUP, Praha, s. 252 - 254, ISBN 80 - 902671 - 6 - 5.

[43] Dodok, L.*, Hozová B., Buchtová, V., Staruch L., Halabuková V Aplikácia transglutaminázy v cereálnej technológii. In: Sborník souhrnu sdělení XXXIV. Symposium o nových směrech výroby a hodnocení potravin. Skalský Dvur 26.-28.5.2003, 16. (Po)

[44] Hozová, B., Dodok, L.: Senzorické hodnotenie pečiva vyrobeného z mraziarensky skladovaného cesta s prídavkom vybraných enzýmov. In: Zb. z XXXIV. Symposia o nových směrech výroby a hodnocení potravin. Skalský Dvur, 26.-28.5.2003,307-313.ISBN 80-902671-6-5. (Po)

[45] Kováčová, M.*, Takácsová, M., Vojteková, S., Žemličková, Z.: Zvýšenie stability karotenoidov na svetle prídavkom rutínu a kyseliny askorbovej. In: Sbornik souhrnu sdělení XXXIV. Symposium o nových směrech výroby a hodnocení potravin. Skalský Dvur, 26.-28.5.2003. VÚPP Praha, s.35-36 (2003). (Po)

[46] Németh, K., Piskuła, M.: Evaluation of the technology‘s influence on onion flavonoids. In: Ethical and Methodological Aspects of Phytochemicals Biological Activity Estimation, Olsztyn, Poland 12-14.6.2003. (Po)

[47] Wiczkowski, W., Németh, K., Buciński, A., Piskuła, M.: Bioavailability a new tool for food evaluation. In: Methodology of the novel food evaluation, Olsztyn, Poľsko 24-25.4.2003. (Po)

[48] Németh, K., Piskuła, M.K.: Flavonoid metabolism in human. In: Bezpieczna żywność, Olsztyn, Poland 29.5.2003. (Pr)


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[49] Valík, Ľ.*, Görner, F., Lauková, D.: Shelf-life prediction and growth of Bacillus cereus in pasteurised milk. In: “Food Safety and Quality in Transition Countries“, Nitra, Slovakia, 23-27 March 2003.

[50] Valík, Ľ.: Introduction to hazards, hazard analysis. Workshop „Systém HACCP pre cukrársku výrobu“. Ministerstvo pôdohospodárstva, Výskumný ústav potravinársky Bratislava, Štátny inštitút odborného vzdelávania Bratislava. Biocentrum Modra, 3. až 7. november 2003.

[51] Valík, Ľ.: Stanovovanie aktivity vody av s praktickými ukážkami. Water activity determination: a practice Seminár fmy Ilabo, Katedry potravinárskej technológie FCHPT STU a firmou „eagle lab`s Nemecko, FCHPT STU Bratislava, 28. 10. 2003.

DEPARTMENT OF ORGANIC CHEMISTRY

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Head of Department: Telephone:+421252968560 Prof. Ľubor Fišera, PhD, DSc Fax: +421252968560


I. STAFF Full Professors: Ľubor Fišera, PhD, DSc; Tibor Gracza, PhD, DSc; Štefan Marchalín, PhD, DSc; Michal Uher, PhD, DSc; Associate Professors: Dušan Berkeš, PhD; Ľubomír Floch, PhD; Viktor Milata, PhD; František Považanec, PhD; Štefan Stankovský, PhD; Katarína Špirková, PhD; Ladislav Štibrányi, PhD; Assistant Professors : Mária Bobošíková, PhD; Eva Jedlovská, PhD; Anna Koreňová, PhD; Angelika Lásiková PhD; Peter Szolcsányi PhD; Peter Šafař, PhD; Jarmila Štetinová, PhD; Research Fellows: Matej Babjak; Iva Blanáriková-Hlobilová, PhD; Daniel Végh, PhD, DSc; Peter Zálupský, PhD; Jozefína Žúžiová, PhD; PhD Students: Barbora Baumlová (since 1. 10. 2003); Petra Černuchová; Branislav Dugovič; Róbert Fischer; Eva Hýrošová (since 1. 10. 2003); Mária Gardiánová; Katarína Hrnčáriková; Pavol Jakubec; Peter Kapitán; Peter Koóš (since 1. 10. 2003); Zita Puterová (since 1. 10. 2003); Technical staff: Miroslava Caňová; Eva Kaisová; Mária Nemcová; Antón Pavlíček; Stanislav Tomek; Iva Viskupičová; Andrea Volentičová; Kveta Wiesingerová;


A. Teaching laboratories: Basic Skills in Organic Chemistry Laboratory I, II. Organic Synthesis Laboratory B. Research laboratories: Laboratory of Organic Synthesis Laboratory of Chiral Cycloaddition Reactions Laboratory of Heterocyclic Chemistry Laboratory of Stereoselective Synthesis Laboratory of Applied Organic Synthesis Laboratory of Natural Compounds Laboratory of Nuclear Magnetic Resonance Spectroscopy Laboratory of IR and UV Spectroscopy Laboratory of Gas Chromatography

III. TEACHING

A. Undergraduate Study: 3. semester (Bc) Organic Chemistry 2/2/0 Marchalín, Gracza Organic Chemistry Laboratory 0/0/4 all teachers and research workers 4. semester (Bc) Organic Chemistry 2/2/0 Fišera, Považanec Organic Chemistry Laboratory 0/0/4 all teachers and research workers 5. semester (Bc) Chemical Information 1/1/0 Uher 6. semester (Bc) Chemical Specialities 2/2/0 Mravec, Štibrányi Semestral Project 0/0/4 Fišera, Gracza, Marchalín, Štibrányi,

Végh 1. semester (MSc) Organometallic Compounds 1/1/0 Gracza Mechanisms of Organic Reactions

I 3/1/0 Fišera

Bioorganic Chemistry 2/0/0 Uher Laboratory Project I 0/0/10 Šafař


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1. semester (MSc) Organic Chemistry III 1/1/0 Považanec 2. semester (MSc) Organic Synthesis 2/1/0 Floch Asymmetric Synthesis 2/1/0 Gracza Stereochemistry 0/2/0 Štibrányi Spectroscopic Methods in the Control

of Technology

2/2/0 Milata, Segľa

2. semester (MSc) Laboratory Project II 0/0/6 Šafař, Štibrányi Training at Industrial Production Floor 15 d Berkeš Fišera, Považanec,

Stankovský, Šafář 3. semester (MSc) Mechanisms of Organic Reactions II 1/1/0 Marchalín Applied Organic Synthesis 1/1/0 Považanec Chemistry of Heterocyclic

Compounds 2/0/0 Stankovský

Chemistry of Natural Substances and Drugs

2/0/0 Berkeš

3. semester (MSc) Laboratory Project 0/0/10 Berkeš, Fišera, Považanec, Stankovský, Šafář

4. semester (MSc) Diploma Seminar Považanec Diploma Thesis Project Fišera, Gracza, Jedlovská,

Marchalín, Považanec, Špirk


A. VEGA Project No 1/0057/03 The Application of Stereoselective Cycloaddition, Cyclization and Oxycarbonylation Reactions in the Total Syntheses of Natural Products and Its Analogues (Lubor Fišera)

The syntheses of natural products and their analogues, especially polyhydroxylated derivatives of pyrrolidines, piperidines, pyrrolizidines and indolizidines via asymmetric palladium(II)-catalyzed oxy-/amino-/amidocarbonylation of unsaturated polyols and/or aminopolyols and 1,3-dipolar cycloaddition of nitrones. The study of the effect of substituent/Lewis acids to influence diastereoselectivity of nitrone cycloaddition reactions. Modeling and synthesis of chiral palladium(II)-complexes for kinetic resolution of racemic mixtures in Pd(II)-catalyzed cyclization and carbonylation reactions of unsaturated polyols and aminopolyols. The application of these reactions as a key step in the total asymmetric synthesis.

Project duration: from 01.01.2003 to 31.12.2005 B. APVT Project No 20-010702 Synthesis of optically pure buildings blocks for syntheses of biologicaly

active natural compounds and their analogues as potential chemoterapeutics (Tibor Gracza) Development and optimization of new synthetic ways - chiral pool approaches - in the syntheses of optically pure alkenitols derived from cheap and commercially avaiable monosaccharides in laboratory grams and multigrams scale. Study of chemo-, regio- and stereoselectivity of palladium(II)-catalyzed oxy-/amino-/amidocarbonylation and cyclization of unsaturated polyols and aminopolyols. Evolution of asymmetric version of the transformations using chiral palladium(II)-complexes. The study of stereoselectivity of 1,3-dipolar cycloaddition of nitrile oxides and nitrones with chiral alkenes. The study of the effect of substituent/Lewis acids to influence the diastereoselectivity of the cycloadditions. The new type of cross-coupling reaction with contributing neighbouring group and finding of the reaction conditions for kinetic resolution of racemic polyols and aminopolyols.

Project duration: from 01.10.2002 to 30.09.2005 C. VEGA Project No 1/9249/02 Stereoselective syntheses, reactivity and properties of hydroxylated

indolizidines and substituted indolizines (Štefan Marchalín) Basic research in the chemistry of heterocyclic compounds, in organic synthesis aiming at elucidation of structure of products and of reaction mechanisms, as well as at search for novel synthetic procedures.The objective of this project is to develop new general synthetic methodologies for the synthesis of diastereo- and enantiopure polyhydroxyindolizidines, dihydroindolizines and tricylic heterocycles with 1,4-dihydropyridine ring. The project is divided in two parts. All parts of project are synergistically connected and leverage each other. The first part explores new synthetic approach for the synthesis of chiral polyhydroxylated indolizidines starting from enantiopure tetrahydrohetero[f]indolizinediones. The second part is based on our previous research in the chemistry of 1,4-dihydropyridines and is focused in the utilization of easily obtainable 2-formyl-1,4-dihydropyridines for the preparation of new chiral dihydroindolizines and tricylic heterocycles containing 1,4-dihydropyridine ring by means of diastereoselective intramolecular cyclization reactions.

Project duration: from 01.01.2002 to 31.12.2004 D. VEGA Project No 1/0058/03 Benzazines and Their Condensed Analogues; Preparation, Properties

and Utilisation (Štefan Stankovský) The objective of the proposed research project lies in preparation of novel condensed aromatic heterocycles – derivatives of


146

benzazines mainly of the quinazoline and quinoline type fused with another ring containing O, S, N as heteroatoms. Special attention will be paid to use of non-traditional precursors leading to desired skeletons carrying desired functionality, or such that allow to preserve the original skeleton and introduce desired substituents. Such modifications are expected to streamline structures of target compounds to achieve significant bioactivity, mainly antimicrobial, antifungal and cytostatic. Structural and spectral characteristics of novel compounds will be studied, including the x-ray analysis and study of supramolecular parameters by computational methods.

Project duration: from 01.01.2003 to 31.12.2005 E. VEGA Project No 1/1379/04 Syntheses directed towards novel heterocyclic compounds such that

show opto-electronic properties, specific bioactivity, and apoptosis (Daniel Végh) Design of syntheses of novel compounds supported by modern trends gleaned from theoretical studies. Synthesis of novel heterocyclic compounds from the furan, thiophene, pyrrole, imidazole, pyrazine, �- and �-pyrone series a modeling of their biological activity. Study of controlled di- and trimerization of the prepared �-conjugated heterocyclic compounds aiming at preparation of molecular and supramolecular functional units and nano-structures. Modeling of supramolecular structures and potential �-conjugated antennae systems for molecular recognition and self-organization by theoretical calculations a combination of building blocks. Utilization of perfluoroaromatics for molecular recognition. Structure modeling of compounds with cancerostatic effects and those capable of initiating apoptosis.

Project duration: from 01.01.2004 to 31.12.2006 F. VEGA Project No 1/9250/02 Crystallization-induced dynamic resolution in the synthesis of

enantiomerically pure amino acids and their derivatives (Dušan Berkeš) Conjugated addition of chiral amino derivatives on electron-deficient unsaturated carboxylic acids followed by crystallization-induced dynamic resolution of primary adducts as key steps in a methodology of asymmetric transformation leading to pure enantiomers. Also stereoselective transformations of prepared adducts, synthesis of optically pure hydroxyamino- and diaminocarboxylic acids.

Project duration: from 01.01.2002 to 31.12.2004 G. VEGA Project No 1/9254/02 Preparation, properties and reactivity of the nitrogen heterocycles with

fused ring containing O, S, Se or N atoms (Viktor Milata) The preparation of new aromatic polyazaheterocycles on the basis of quinoline, quinazoline and benzoazoles with other fused aromatic or saturated heterocycle containing O, S, Se or N, is the subject of this proposed project. In the first period of this project the greatest attention will be aimed at the preparation of new precursors of the mentioned heterocycles. In the next part these precursors of nitroquinazolines, nitrobenzimidazoles, nitroselenodiazoles, imidoylhalogenides, cyanoacetamides, quinazolones and their thioanalogues will be used for the synthesis of the target compounds in the cyclization and cyclocondensation reactions. Derivatisation of the newly synthetized heterocycles by incorporation of saccharide or other hydrophilic component, an increased solubility of compounds in water and thus better biological application will be pursued. Attention will be given to physico-chemical and spectral parameters, e.g. X-Ray analysis and supramolecular chemistry will be confronted with calculated models.


VI. COOPERATION



Duration

Slovakofarma, Hlohovec Research and teaching

Gattnar Ondřej, director, Nitrianska 100, 920 27 Hlohovec

01.01.1970-01.07.2003

Synkola, Bratislava Seminars and conferences Karvaš Milan, director, Mlynská dolina, 842 15 Bratislava 4 01.01.1992-

Duslo, Šaľa The synthesis of heterocyclic compounds.

Lehocký Peter, director, Duslo, a. s. 927 03 Šaľa

01.01.1990-

Slovak Academy of Sciences, Bratislava

The synthesis of heterocyclic compounds.

Hirsch Ján, director, Dubravská cesta 9, 841 04 Bratislava 4 01.01.1970

Tau-Chem, Bratislava


Žvak Vladimír, director, Nobelova 34, 836 05 Bratislava 3

01.01.1996

Institute of Drugs Research, Modra


Šmahovský Vendelín, director, Horná 36, 900 01 Modra 01.01.1980-

Tatra Trade, Prievidza


IKlínovský Ján, director, Matice slovenskej 10, 971 01 Prievidza 01.01.2000-

Institute of Preventive Medicines, Bratislava


Sedlák Ján, Dr., Vlárska 1, 833 91 Bratislava 37

01.01.2000-


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National Center of Onkology, Bratislava


Chalupa Ivan, Dr, Vlárska 7, 831 01 Bratislava 37 01.01.2000-

Georganics, Bratislava


Ďuriš Juraj, director, Koreničova 1, 811 03 Bratislava 1

01.01.2000-

CMS, Bratislava The synthesis of heterocyclic compounds.

Toman Jaromír, director, Nobelova 34, 836 03 Bratislava 3

01.01.2000-

Zentiva a.s., Hlohovec Research and teaching

Jaroslav Chylik, API prod. manager, Nitrianska cesta 100, 920 27 Hlohovec

01.07.2003-



Duration

Inst. für Angewandte Synthese Chemie TU Vienna, Austria

The synthesis of heterocyclic compoundsFröhlich Hannes, professor, Getreide Markt 9, A-1060 Vienna, Austria

01. 01. 1991-

Inst. für Organische Chemie Univ. Stuttgart, Germany

Stereoselective dipolar cycloaddition and oxycarbonylation reactions

Jäger Volker, professor, Pfaffenwaldring 55, D-70569 Stuttgart, Germany

01. 01. 1989-

Max Plank Institute, Stuttgart, Germany

The synthesis of heterocyclic compounds for nanotubes

Roth Siegmar, Dr., Helsenbergerstr. 1, D-70569 Stuttgart, Germany

01.01.2002-

Inst. für Organische Chemie Univ. Berlin, Germany

Stereoselective reactions of chiral nitrones

Reissig Hans-Ulrich, professor, Takustr. 3, D-14195 Berlin, Germany

01. 01. 2002-

Inst. de Chimie Moleculaire d´Orsay, France

Resau formation recherche

Basch E. H., professor, IUT d'Orsay Université de Paris-Sud (XI) Département Chimie Plateau du Moulon 91400 ORSAY, France

01.01.1976-

Institute de Chimie Moleculaire, Orsay, Univ. Paris-Sud, France

NMR study of chiral compounds and cooperation in exchange of students

Loupy, A. , professor, Institut of Molecular Chemistry, ICMO, University Paris – South, Orsay, France

01.01.2000-

URCOM, Univ. Le Havre, France

The synthesis of condensed heterocyclic compounds

DECROIX B., DAICH A., professors Laboratoire de Chimie URCOM, EA 3221 Faculté des Sciences et Techniques Université du Havre 25, r

01.01.1990

Inst. für Festkörperphysik der Univ. Vienna, Austria

New materials for microelectronics

Kauffmann H. F. professor, University of Vienna, Intitut fur Physikalische chemie, Währingerstrasse 42, Wien, Austria.

01.010.2001-

Laboratorium für Org. Chem, ETH, Zürich, Switzerland

The total synthesis of natural products Vasella Andrea, professor ETH Hoenggerberg, HCI H315 CH-8093, Zürich, Switzerland

01.01.1990-

Institute of Organic Chemistry, TU Wroclaw, Poland

The synthesis of heterocyclic compounds

Mlochowski Jacek, professor, Technical University of Wroclaw, 50-370 Wroclaw, Poland

01.01.1986-

Institute of Organic Chemistry, Univ. Debrecen, Hungary

The synthesis of heterocyclic compoundsLevai Albert, professor, H-4010 Debrecen, P.O.Box 20, Hungary

01.01.1995-

Institute of Organic Chemistry, U Warsaw, Poland

The synthesis of heterocyclic compounds Cyranski, M. K., professor, 02 093 Warsaw, Poland 01.01.1996-

Institute of Organic Chemistry, AU Krakow, Poland

The synthesis of heterocyclic compoundsTomasik Piotr, professor, Mickiewicz Ave. 21 31 120 Krakow, Poland

01.01.1975-


148

Department of Organic Chem. and Biology UNED, Madrid, Spain

The synthesis of heterocyclic compounds, NMR spectroscopy

Claramunt, R. M., Cabildo, P., Lopéz G., professors, UNED, Madrid, Spain

01.01.1998-

Instituto de Quimica Medica (CSIC), Madrid, Spain

Physical organic chemistry Elguerro, J. B., professor, Madrid, Spain 01.01.1998-

Institute of Organic Chemistry, Panon Univ. Mosonmagyaróvár, Hungary

The synthesis of heterocyclic compounds. Utilization in Agriculture

Schmiedt Rudolf, professor, Mosonmagyaróvár, Hungary 01.01.1997-

Department of Chemistry, Univ. Puerto Rico, USA

Structure determination of amino acids and peptides

Baran Peter, Dr, Department of Chemistry, Univ. of Puerto Rico, Rio Pedras, PO Box 23346, San Juan 00931-3346, Puerto Rico, USA

2002

Department of Chemistry, Keele University, United Kigdom

The synthesis of heterocyclic compoundsRamsden Christopher, professor, Keele, Staffordshire ST55BG, United Kigdom

1980



Valid date

Fišera Ľubor Academic board of STU member 2003 Fišera Ľubor Academic board of FCHPT member 1997 Fišera Ľubor Scientific Grant Agency chairmann 2000 Fišera Ľubor Chemical Papers member 1994 member Berkeš Dušan Slovak Chemical Society member 1984 Bobošíková Mária Slovak Chemical Society member 1993

Fišera Ľubor Slovak Chemical Society chairmann 1971 Floch Lubomír Slovak Chemical Society member 1972 Gracza Tibor Slovak Chemical Society member 1984 Hlobilová Iva Slovak Chemical Society member 1997 Jedlovská Eva Slovak Chemical Society member 2003 Koreňová Anna Slovak Chemical Society member 1983

Milata Viktor Slovak Chemical Society member of advisory board 1977 Považanec František Slovak Chemical Society member 1983

Stankovský Štefan Slovak Chemical Society member 1971

Šafař Peter Slovak Chemical Society member 2000 Špirková Katarína Slovak Chemical Society member 1983

Štetinová Jarmila Slovak Chemical Society member 1973

Uher Michal Slovak Chemical Society member 1965 Végh Daniel Slovak Chemical Society member 1972 Žúžiová Jozefína Slovak Chemical Society member 1989

Černuchová Petra Slovak Chemical Society member 2001

Gardianová Mária Slovak Chemical Society member 2002

Hrnčáriková Katarína Slovak Chemical Society member 2002

Lasíková Angelika Slovak Chemical Society member 1996

Berkeš Dušan Slovak Society of Industrial Chemistry member 1995 Bobošíková Mária Slovak Society of Industrial Chemistry member 1995

Fišera Ľubor Slovak Society of Industrial Chemistry member 1993 Floch Lubomír Slovak Society of Industrial Chemistry member 1995


- 149 -

Gracza Tibor Slovak Society of Industrial Chemistry member 1996 Hlobilová Iva Slovak Society of Industrial Chemistry member 1998 Jedlovská Eva Slovak Society of Industrial Chemistry member 1993 Koreňová Anna Slovak Society of Industrial Chemistry member 1995

Milata Viktor Slovak Society of Industrial Chemistry member 1993 Považanec František Slovak Society of Industrial Chemistry member 1995

Stankovský Štefan Slovak Society of Industrial Chemistry member 1995

Šafař Peter Slovak Society of Industrial Chemistry member 1998 Špirková Katarína Slovak Society of Industrial Chemistry member 1993

Štetinová Jarmila Slovak Society of Industrial Chemistry member 1993

Uher Michal Slovak Society of Industrial Chemistry member 1995 Végh Daniel Slovak Society of Industrial Chemistry member 1993 Žúžiová Jozefína Slovak Society of Industrial Chemistry member 1995

Černuchová Petra Slovak Society of Industrial Chemistry member 2002

Gardianová Mária Slovak Society of Industrial Chemistry member 2003

Hrnčáriková Katarína Slovak Society of Industrial Chemistry member 2001

Lasíková Angelika Slovak Society of Industrial Chemistry member 1996

Marchalín Štefan Slovak Society of Industrial Chemistry member 1996

Zálupský Peter Slovak Society of Industrial Chemistry member 1996

Štibrányi Ladislav Slovak Society of Industrial Chemistry member 1995

Dugovič Branislav Slovak Society of Industrial Chemistry member 2003

Babjak Matej Slovak Society of Industrial Chemistry member 2000 D. Membership in International Organisations and Societies


Valid date

Fišera Ľubor ARKIVOC member 2000 Fišera Ľubor American Chemical Society member 1994 Fišera Ľubor German Chemical Society member 1994 Fišera Ľubor Czech Chemical Society member 1994 Gracza Tibor German Chemical Society member 1994 Gracza Tibor Czech Chemical Society member 1997 Marchalín Štefan Czech Chemical Society member 1980

Milata Viktor Czech Chemical Society member 2002 Milata Viktor ARKIVOC member 2000 Végh Daniel Magyar Tudomanos Akademia member 2001 Gracza Tibor Advisory Board of EUROCAT member 2002 Milata Viktor Molecules member 2000 Milata Viktor Eur. J. Org. Chem. member 2002 Fišera Ľubor Eur. J. Org. Chem. member 2002



Date / Duration

Walter, H. SYNGENTA Basel Switzerland April 2003 (1 day) Spitzner, D. Univ. Stuttgart Germany May 2003 (2 days) Bach, T. T. Univ, München Germany May 2003 (1 day) Sauter, F. T. Univ, München Austria May 2003 (1 day)

Radulič, V. Univ. Beograd Serbia and Montenegro

March-May 2003 (90 days)


150

Demanze, S. IUT Orsay, Univ. Paris-Sud France May-June 2003 (60 days)

Le Liepvre, M. IUT Orsay, Univ. Paris-Sud France May-June 2003 (60 days)

Vera, F. IUT Orsay, Univ. Paris-Sud France May-June 2003 (60 days)

Ernst, B. Univ. Basel Switzerland November 2003 (1 day)

Kos, A. MDL Germany November 2003 (1 day)



Date / Duration

Babjak, M. 10th BDSHC, Vienna Austria September 2003 (4 days)

Berkeš, D. 10th BDSHC, Vienna Austria September 2003 (4 days)

Berkeš, D. Univ. Le Havre France March 2003 (7 days)

Černuchová, P. 10th BDSHC, Vienna Austria September 2003 (4 days)

Černuchová, P. Univ. Paris-Sud, Orsay France 2003 (180 days)

Dugovič, B. 10th BDSHC, Vienna Austria September 2003 (4 days)

Fišera, Ľ. 10th BDSHC, Vienna, T. Univ. Vienna Austria September 2003 (4+6 days)

Fišera, Ľ. Univ. Dallas, Denton, Gainesville, USA March 2003 (14 days)

Fišera, Ľ. FU Berlin Germany November 2003 (14 days)

Gracza, T. 10th BDSHC, Vienna, T. Univ. Vienna Austria September 2003 (4+2 days)

Hrnčáriková, K. 10th BDSHC, Vienna Austria September 2003 (4 days)

Hrnčáriková, K. Univ. Stuttgart Germany 2003 (35 days)

Jedlovská, E. 10th BDSHC, Vienna Austria September 2003 (4 days)

Kapitán, P. T. Univ. Vienna Austria 2003 (270 days) Lásiková, A. Univ. France 2003 (365 days) Hlobilová, I. FU Berlin Germany 2003 (365 days) Marchalín, Š. Univ. Le Havre, Univ. Strasbourg, France March 2003 (14 days)

Marchalín, Š. 10th BDSHC, Vienna Austria September 2003 (4 days)

Milata, V. 10th BDSHC, Vienna, T. Univ. Vienna Austria September 2003 (4+11 days)

Stankovský, Š. 10th BDSHC, Vienna Austria September 2003 (4 days)

Špirková, K. 10th BDSHC, Vienna Austria September 2003 (4 days)

Štetinová, J. 10th BDSHC, Vienna Austria September 2003 (4 days)

Uher, M. Univ. Krakow, Univ. Lublin Poland September 2003 (10 days)

Végh, D. 10th BDSHC, Vienna Austria September 2003 (4 days)

Végh, D. Univ. Mosonmagyaróvár Hungary 2003 (15 days)

Zálupský, P. 10th BDSHC, Vienna Austria September 2003 (4 days)



Baleja, J. The influence of Lewis acids on the stereoselectivity of 1,3-dipolar cycloadditions of nitrones with electronrich alkenes Fišera, Ľ.

Andicsová, A. Synthesis of potentional angiotensin II receptor antagonists. Végh, D.


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Solčán, T. Synthetic utilization of pentafluorobenzaldehyde for preparation of biologically active compounds and novel materials. Végh, D.

Rehák, J. Pd(II)-Catalysed alkoxycarbonylations of unsaturated aminolpolyols Gracza, T. Kubizna, P. PdCl2/CuX2 - catalysed halocyclizations of unsaturated aminopolyols Gracza, T.


Adamenko, I. Study of quinazoline ring linearly annelation. Špirková, K. Balážová, K. Synthesis and reaction of 2-amino-4-phenylbutanoic acid. Považanec, F. Csusz , B. Enantioselective synthesis of jatrofam and its epimer. Fišera, Ľ. Hýrošová, E. Stereoselective synthesis of isoxazolidinyl spironucleosides. Fišera, Ľ. Koóš, P. Asymmetric Pd(II)catalysed oxycarbonylations of unsaturated polyols. Gracza, T. Obranec, M. Stereoselectivity of chiral nitrone cycloadditions. Fišera, Ľ.

Šilhár, P. Preparation 2-aryl-3-methylidentetrahydrofurans and their use in synthesis of spiroheterocyclic compounds.

Jedlovská, E.


Kadlečíková, K. Synthesis o the novel benzo- and heteroanalogues of the hydroxylated indolizidine alkaloids.

Marchalín, Š.

Kakalík, I. Synthesis of new inhibitors of biosynthesis of cholesterol Fišera, Ľ

Kolarovič, A. Crystallization – Induced Asymmetric Transformation in the Synthesis of Amino Acids Považanec, F.

VIII. PUBLICATIONS A. Journals [1] Berkeš, D., Lopuch J., Proksa B., Považanec F.: Optical resolution of Ethyl 2-(benzylamino)-4-oxo-4-phenylbutanoate with

Tartaric Acid. A Practical Synthesis of d-Homophenylalanine. Chem Pap. 57, 350-354 (2003). [2] Blanáriková-Hlobilová, I., Fišera, L., Prónayová, N., Koman, M.: 1,3-Dipolar cycloadditions of D-erythrose and D-threose

derived alkenes with nitrones. Coll. Czech. Chem. Commun. 2003, 68, 951. [3] Blanáriková-Hlobilová, I., Kopaničáková, Z., Fišera, L., Cyrański ,M. K., Salanski, P., Jurczak, J., Prónayová, N.:

Stereoselectivity of 1,3-Dipolar Cycloadditions of L-Valine Derived Nitrones with Methyl Acrylate. Tetrahedron 2003, 59, 3333. [4] Boduszek B., Koreňová A., Uher M., Végh, D.: Synthesis and Cleavage of Pyridone-4-aminophosphonic Acids. Phosphorus,

Sulfur and Silicon. 178, 1047-1053 (2003). [5] Carrión Carmen M., Guerrero A., Jalón F.A., Manzano B.R., de la Hoz A., Claramunt R.M., Milata, V., Elguero J.: Five

Different Fluxional Processes in Polyfluorophenyl Palladium(II)Complexes with 2,4,6-Tris(3,5-dimethylpyrazol-1-yl)-1,3,5-triazine. The Driving Effect of the Solvent.Inorg. Chem. 885-895, 42 (2003).

[6] Cul, A., Chihab-Eddine, A., Pesquet, A., Marchalín, Š., Daich, A.: Evaluation of N-hydroxymethylphthalimide in alkaline medium: Novel entry to the tricyclic [1,3]-oxazepine core via an intramolecular π- and O-cationic cyclization. J. Heterocycl. Chem. 40, 499-505 (2003).

[7] Fischer, R., Hýrošová, E., Drucková, A., Fišera, L., Hametner, C., Cyrański, M. K.: Isoxazolinyl Spironucleosides: Stereoselectivity of 1,3-Dipolar Cycloadditions of 7 -Methylenepyrrolo[1,2-c]pyrimidin-1(5H)-ones. Synlett. 2003, 2364.

[8] Guerrero, A., Jalón F.A., Manzano B.R., Rodríguez A., Claramunt R.M., Cornago P., Milata, V., Elguero J.: Apparent Allyl Rotation in New Allylpalladium(II) Complexes with Pyrazolyl-N-Donor Ligands Eur. J. Inorg. Chem. 2004, DOI: ejic.200300359

[9] Langer V., Gyepesova D., Koman M., Kapitan P., Babjak M., Gracza, T., Koóš M.: Preparation and Crystal Structure of (1S, 5S, 7S, 8R)-8-Hydroxy-7-phenyl-2,6-dioxabicyclo[3.3.0]octan-3-one“. Molecules 2003, 8, 599-606.

[10] Milata, V., Kada R., Lokaj J.: Carbazol-9-yl-methanol. Molecules/Molbank, http://www.mdpi.net/molbank/molb200300106 [11] Novotný L., Abdel-amid M., Rauko P., Uher M., Brtko J.: Stability of the new antileukemic 4-pyranone derivative, BTMP, using

HPLC and LC-MS analyses. Pharmazie, 57, 252-255 (2002). [12] Rohdahl, L., Uher M., Brtko J.: Syntheses and structure determinations of some selenocyanato-kojic acid derivatives.

Heterocycl. Commun., 9, 257-258 (2003). [13] Saloň, J., Milata, V., Chudík M., Prónayová N., Leško J., Seman M., Belicová A.: Synthesis, Properties, and Reactions of 5-

Substituted Derivatives of 2,3-Diphenylquinoxaline Synthesis, Properties, and Reactions of 5-Substituted Derivatives of 2,3-Diphenylquinoxaline Monath. Chem. 2003, DOI: 10.1007/s00706-003-0058-5

[14] Szemes, F., Jr., Marchalín, Š., Prónayová ,N., Szemes F., Daich A.: A facile access to 2-ethynyl-1,4-dihydropyridines via Hantzsch three-component reaction. Heterocycles 59, 779-783 (2003).

[15] Vrábel, V., Kožíšek, J., Marchalín, Š.: Diethyl 2-methyl-6-(2-thiazolidinyl)-4-(2-thienyl)-1,4-dihydropyridine-3,5-dicarboxylate. Acta Cryst. E59, 376-377 (2003).

[16] Vrábel, V., Marchalín, Š., Kožíšek, J.: Diethyl (2´R,4R,4´R)-2-(4’-ethoxycarbonyl-2’-thiazolidinyl)-6-methyl-4-(2’’-thienyl)-1,4-dihydropyridine-3,5-dicarboxylate. Acta Cryst. E59, 1964-1966 (2003).

[17] Vrábel, V., Marchalín, Š., Kožíšek, J.: Isopropyl 2-Methyl-4-(3-nitrophenyl)-5,7-dioxo-4,5,6,7-tetrahydro-1H-pyrrolo[3,4-b]-pyri-dine-3-carboxylate. Acta Cryst. E59, 1570-1571 (2003).

[18] Vrábel, V., Oktavec, D., Marchalín, Š.: 2,3-Dimethyl 5-isopropyl 1-ethoxymethyl-6-methyl-4-(3-nitrophenyl)-1,4-dihydropyridine-2,3,5-tricarboxylate. Acta Cryst. E59, 306-307 (2003).


152

[19] Wojtowicz, H., Chojnacka, M., Mlochowski, J., Palus, J., Syper, L., Hudecova, D., Uher, M., Piasecki, E., Rybka, M. Functionalized alkyl and aryl diselenides as antimicrobial and antiviral agents: synthesis and properties. Functionalized alkyl and aryl diselenides as antimicrobial and antiviral agents: synthesis and properties. Farmaco 58(12), 1235-42, (2003)

[20] Zieba, A., Masłankiewicz A., Milata, V., Sitkowski J.: N-15 NMR spectra of some 3-substituted 4(1H)-quinolinones and their 1-methyl derivatives. Magn. Reson. Chem. 41 (8), 639-640 (2003).

[21] Uher, M., Wojtowicz H.: Naturalne I synteticzne niecukrowe substancje slodkie. Wiadomosci Chemiczne, 57, 505-546 (2003). [22] Dugovič, B., Fišera, L., Hametner, C., Prónayová, N.: Diastereoselectivity of Nitrone 1,3-Dipolar Cycloaddition to Baylis-

Hillman Adducts. ARKIVOC 2003, xiv, 162 [23] Štibrányi, L., Milata, V.: Vzťah chémie a životného prostredia – trvalo udržateľný rozvoj. Relationship Chemistry And

Surroundings - Sustainable Development. Chemické rozhľady, 3(3-4), 211-216, 2003. IUVENTA, Bratislava 2003, ISSN 1335-8391.

[24] Milata, V., Zubek M.: Green chemistry ? Bulletin SCHS, 48, 23-29, 2003. SCHS, Bratislava 2003. [25] Sališová, M., Milata, V.: Ocenenia Dusľa Šaľa a Slovenskej chemickej spoločnosti za rok 2003. Dusľo Šaľa and Slovak

Chemical Society Awards for 2003. Bulletin SCHS, 49, 64-67, 2003. SCHS, Bratislava 2003. B. Conferences [1] Bobošíková, M.*, Ramsden, C. A.: Syntéza 2,4-disubstituovaných chinazolínov. Synthesis of 2,4-disubstituted chinazolines. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 766 (2003). (Po) [2] Černuchová, P.,* Milata, V., Vo-Thanh G., Loupy A.: Syntéza chinolónových derivátov v tuhej fáze s využitím mikrovlnného

žiarenia. Synthesis of quinolone derivatives in solid phase under microwave irradiation. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 755 (2003) (Po).

[3] Hritzová, O., Černák J., Csoregh I., Frohlichová Z., Šafář, P.: Furanové deriváty substituovaných fenyltiomočovín: porovnanie výsledkov štruktúrnej analýzy, spektrálnych a kvantovo-chemických metód. Furan derivatives of substituted phenylthioureas: comparison of results of structural analysis, spectral and quantum chemical methods. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 2003, 97, 757.

[4] Koreňová A.*, Berkeš, D., Prónayová N.: Kryštalizáciou indukovaná asymetrická transformácia (CIAT) v konjugovanej adícii na deriváty kyseliny 4-(indolyl)-4-oxo-2-buténovej. Crystallization-Induced Asymmetric Transformation (CIAT) in the Conjugate Addition on 4-(Indol-3-yl)-4-oxo-2-butenoic Acid Derivatives. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 2003, 97, 759.

[5] Milata, V.,* Kada R., Lokaj J., Goljer I., Štetinová, J., Hammetner Ch., Belicová A.: Príprava, spektrálne a biologické vlastnosti sulfónov 2-heteroarylpropénnitrilov. Preparation, spectral and biological properties of 2-hetarylpropenenitrile sulfones. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 761 (2003). (Po).

[6] Milata, V.,* Zubek M.: Green Chemistry - Zelená chémia, áno či nie ? Green Chemistry - yes or no ? In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 816 (2003). (Po).

[7] Stankovský, Š.,* Špirková K.: Analógy chinazolínových alkaloidov. Analogs of quinazoline alkaloids. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 763 (2003).

[8] Šafář, P.*, Berkeš, D., Prónayová N.: 4-(1-Benzénsulfonyl-1H-pyrrol-3-yl, resp. 1H-indol-3-yl)-4-oxobut-2-énová kyselina v syntéze aminokyselín. 4-(1-Benzenesulfonyl-1H-pyrrol-3-yl, resp. 1H-indol-3-yl)-4-oxobut-2-enoic Acid in the Synthesis of Amino Acids. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 2003, 97, 761-762.

[9] Špirková, K.,* Stankovský Š.: Lineárne anelované azepinochinazolínové deriváty Linearly annellated azepinoqionazoline derivatives In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 762 (2003). (Po).

[10] Štetinová, J.,* Milata, V., Prónayová N., Leško J., Petrov O.: Syntéza a vlastnosti niektorých 1,2,4-trisubstituovaných pyrolov. Synthesis and properties of some 1,2,4-trisubstituted pyrroles. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 770 (2003). (Po).

[11] Šturdíková M., Koreňová A., Végh, D., Boduszek B., Kravcová A, Uher M.*: Inaktivácia elastázy a katepsínu B β-tienyl a furyl derivátmi kyseliny aminometylfosfónovej. Inactivation of elastase and cathepsin B by β-thienyl and furyl derivatives of aminomethylphosphonic acid In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 2003, 97, 764.

[12] Babjak M., Gracza, T., Zálupský P.: New Transformations of Unsaturated Polyols Catalysed with PdCl2. 10th Blue Danube Symposium on Heterocyclic Chemistry,

[13] Carrión C.M.,* Guerrero A., Jalón F.A., Manzano B.R., de la Hoz A., Claramunt R.M., Milata, V., Elguero J.: Cinco procesos fluxionales diferentes en complejos polifluorofenilo de paladio(II). XXIX Reunion Bienal de la Real Sociedad Espanola de Química, Madrid 2003, Espana, S207 (p. 306).(Po).

[14] Černuchová, P.,* Milata, V., Vo-Thanh G., Loupy A.: Solvent-Free Synthesis Of Quinolone Derivatives Using Microwave Irradiation. 10th Blue Danube Symposium on Heterocyclic Chemistry, September 3rd-6th, 2003, Vienna, Austria. Ed. By J. Fröhlich, ISBN 80-227-1938-2. (Po)

[15] Dugovič, B., Obranec, M., Fišera, L., Hametner, C.: Stereoselectivity of D-erythrose derived nitrone cycloadditions in the presence of Lewis acids. In: 10th Blue Danube Symposium on Heterocyclic Chemistry, Vienna / Austria, September 03-06, 2003. Edited by Fröhlich, J. p. 124 (2003), ISBN 80-227-1938-2 (Po)

[16] Fischer, R., Hýrošová, E., Drucková, A., Fišera, L., Hametner, C., Cyrański, M. K.: Isoxazolinyl Spironucleosides: 1,3-Dipolar Cycloadditions of 7 Methylenepyrrolo[1,2-c]pyrimidin-1(5H)-ones. 10th Blue Danube Symposium on Heterocyclic Chemistry,

Vienna / Austria, September 03-06, 2003. Edited by Fröhlich, J. p. x (2003), ISBN 80-227-1938-2 (Po) [17] Jakubec P., Šiška R., Berkeš, D.*, and Považanec F.: Crystallization-induced Asymmetric Transformations. The Synthesis of

Furoylalanines. 10th Blue Danube Symposium on Heterocyclic Chemistry, 16.-20. sept. 2003, Vienna, Austria. Book of Abstracts, p. 88, ISBN 80-227-1705-3.

[18] Koreňová A., Berkeš, D., Uher M.*, Prónayová N.: Crystallization-induced asymmetric transformations. Applications to the synthesis of analogues of homotryptophane. Zborník XLVI Zjazd naukowy polskiego towarzystwa chemicznego i stowarzyszenia inžynierów i techników przemyslu chemicznego. Lublin 15 - 18 wrzesnia 2003, s. 128, ISBN 83-901844-7-8.

[19] Marchalín, Š.*, Cvopová, K., Daïch, A., Kríž, M.: A new convenient synthesis of indolizines and bipyridinyls from 2-formyl-1,4-dihydropyridines. Book of Abstracts, 10th Blue Danube Symposium on Heterocyclic Chemistry. Wien (Austria), Sept. 03-06, 2003. Vydavateľstvo STU, Vazovova 5, Bratislava PO-122 (2003). ISBN 80-227-1938-2. (Po)


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[20] Marchalín, Š., Cvopová ,K., Oulyadi, H., Daich, A.*: New resolution of 2-formyl-1,4-DHPs derivatives using CIDR methodology. A facile access to new chiral bicyclic thiolactam. Book of Abstracts, IIIrd PPG-Sipsy Symposium on New frontiers in asymmetric synthesis. Angers (France), Sept. 03-04, 2003. (Po)

[22] Milata, V.,* Kada R., Lokaj J., Goljer I., Štetinová, J., Hammetner Ch., Belicová A.: Preparation, Spectral And Biological Properties Of Sulfones Of 2-Heteroarylcinnamonitriles. In: 10th Blue Danube Symposium on Heterocyclic Chemistry, September 3rd-6th, 2003, Vienna, Austria. Ed. By J. Fröhlich, ISBN 80-227-1938-2. (Po)

[23] Stankovský, Š.,* Špirková K.: Azepinoquinazolines-analogs of quinazoline alkaloids. 10th Blue Danube Symposium on Heterocyclic Chemistry, September 3rd-6th, 2003, Vienna, Austria. Ed. By J. Fröhlich, ISBN 80-227-1938-2. (Po)

[24] Špirková, K.,* Stankovský Š.: Preparation of some linearly annellated azepinoquinazolines. 10th Blue Danube Symposium on Heterocyclic Chemistry, September 3rd-6th, 2003, Vienna, Austria. Ed. By J. Fröhlich, ISBN 80-227-1938-2. (Po)

[25] Štetinová, J.,* Milata, V., Prónayová N., Leško J., Petrov O.: Synthesis and properties of some 1,2,4 trisubstituted pyrroles. 10th Blue Danube Symposium on Heterocyclic Chemistry, September 3rd-6th, 2003, Vienna, Austria. Ed. By J. Fröhlich, ISBN 80-227-1938-2. (Po)

[26] Zborowski, K.*, Koreňová A., M. Uher M., Proniewicz L.M.: Quantum chemical studies on the tautomeric equilibria in chlorokojic and azidokojic acids. Zborník XLVI Zjazd naukowy polskiego towarzystwa chemicznego i stowarzyszenia inžynierów i techników przemyslu chemicznego. Lublin 15 - 18 wrzesnia 2003, s. 814, ISBN 83-901844-7-8.

[27] Fišera, L.: Stereoselective 1,3-Dipolar Cycloadditions of chiral nitrones. 10th Blue Danube Symposium on Heterocyclic Chemistry, Vienna / Austria, September 03-06, 2003. Edited by Fröhlich, J. p. 44 (2003), ISBN 80-227-1938-2 (PPr)

[28] Marko, M.,* Milata, V.: The utilization of higher 1,3-cycloalkanediones in the synthesis of 1,4-dihydropyridine ring. 7th International Electronic Conference on Synthetic Organic Chemistry (ECSOC-7), http://www.mdpi.net/ecsoc-7, 1-30 November 2003, A032, http://www.mdpi.net/ec/ec_article.php?id=102&file=papers/ecsoc-7/a032/a032.htm (Po).

[29] Milata, V.,* Bella M.: Preparation of selectively N-methylated X-nitro-1,2-phenylenediamines. 7th International Electronic Conference on Synthetic Organic Chemistry (ECSOC-7), http://www.mdpi.net/ecsoc-7, 1-30 November 2003, A030, http://www.mdpi.net/ec/ec_article.php?id=102&file=papers/ecsoc-7/a030/a030.htm (Po).

[30] Gracza, T.: Stereocontrolled Palladium(II)-catalyzed Oxycarbonylation of Unsaturated Polyols and Aminopolyols. GOCh lecture, 23. 1. 2003, TU Wiena, Austria, invited lecture

[31] Berkeš, D.: Chémia liečiv - Antibakteriálne látky. Medicinal Chemistry - Antibacterial substances. In: XVII. Seminár pre stredoškolských učiteľov chémie., Bratislava 27.8.-28.8. 2003 (pr)

C. Books and Textbooks [1] Uher, M.: Natural and Synthetic Non-saccharide Sweeteners. "In book ""Chemical and Functional Properties of Food

Saccharides."" Ed. Tomasik P., CRC Press, 2003, ISBN: 0849314860, 30pp." [2] Lesný, J., Simon G., Végh, D.: Všeobecná chémia 290str.. Általános kémia 290 str. Vydavateľstvo Univerzity Istvana

Széchenyiho, Universitas Győr KHT, Tetx-Print 2003 E. Others:

[1] Fišera, L.: Chiral 1,3-Dipolar Cycloadditions of Nitrones and Nitrile Oxides. University of Florida, Gainesville, 2003, USA

[2] Fišera, L.: Stereoselective 1,3-Dipolar Cycloadditions of Nitrones and Nitrile Oxides. Southern Methodist University, Dallas, 2003, USA

[3] Fišera, L.: Stereoselective 1,3-Dipolar Cycloadditions of Nitrones and Nitrile Oxides. Christian University, Dallas Fort Worth, 2003, USA

[4] Fišera, L.: Stereoselective 1,3-Dipolar Cycloadditions of Nitrones and Nitrile Oxides. University of Texas at Dallas, Richardson, 2003, USA

[5] Fišera, L.: Stereoselective 1,3-Dipolar Cycloadditions of Nitrones, The University of Texas, Arlington, 2003, USA [6] Fišera, L.: Stereoselective Chiral 1,3-Dipolar Cycloadditions of Nitrones. Stereoselective Chiral 1,3-Dipolar Cycloadditions of

Nitrones University of North Texas, Denton, 2003, USA

DEPARTMENT OF ORGANIC TECHNOLOGY

154


Head of Department: Telephone: ++421252495242 Assoc. Prof. Alexander Kaszonyi, Phd Fax: ++421252493198


I. STAFF Full Professors: Milan Hronec, PhD, DSc, Dusan Mravec, PhD Associate Professors: Alexander Kaszonyi, PhD, Jan Vojtko, PhD Assistant Professors : Dana Gašparovicová Research Fellows: Michal Báhidský, Zuzana Cvengrošová, PhD., Blažej Horváth, Magdaléna Štolcová, PhD PhD Students: Erik Juhás, Katarína Klepáčová, Miroslav Mrzula, Zuzana Vallušová Technical staff: Eva Šuleková, Gabriel Mikeš, Jozef Tánczos, Ľudmila Tvarožková


A. Teaching laboratories: Technological laboratory 1, 2, 3, 4

B. Research laboratories: Laboratory of catalytic processes Laboratory of reactor technique Laboratory of separation (chromatographic) methods Laboratory of spectroscopic methods


4. semester (Bc) Organic Technology and Petrochemistry (3-l h) Hronec, Kaszonyi

6. semester (Bc) Fine Chemicals (2-2 h) Mravec 6. semester (Bc) Semestral project (0-4 h) Cvengrošová, Gašparovičová,

Hronec, Kaszonyi, Králik, Mravec, Štolcová 1. semester (MSc) Chemical-Engineering

Thermodynamics (0-2 h) Vojtko

Catalysis (2-0 h) Hronec Engineering Calculations on a

Computer (1-2 h) Kaszonyi

Processes of Organic Technology

(2-1 h)

Králik

1. semester (MSc) Laboratory Practise I (0-8 h) Báhidský, Cvengrošová, Gašparovičová,Horváth,

Hronec, Juhás, Kaszonyi, Mravec, Štolcová 2. semester (MSc) Kinetics and Reactors (0-2 h) Kaszonyi Process Design (2-1 h) Hronec, Králik Technology and Monomers and

Polymers (2-0 h) Vojtko

Special Organic Products (2-0 h) Mravec 2. semester (MSc) Analysis of Complex Organic

Systems (0-2 h) Štolcová, Cvengrošová

Laboratory Practise II (0-7 h) Cvengrošová,Hronec,


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Gašparovičová,Kaszonyi, Mravec, Štolcová 3. semester (MSc) Coating Materials (2-0 h) Kramár Manufacturing of Pharmaceuticals (2-1 h) Mravec Laboratory Practise III (0-14 h) Cvengrošová, Hronec, Kaszonyi,

Gašparovičová, Mravec, Štolcová 4. semester (MSc) Seminar to Masters Theses (0-3 h) Cvengrošová, Hronec, Kaszonyi,

Králik, Mravec, Štolcová 4. semester (MSc) Catalysis ( PhD) (2 h) Hronec


A. VEGA Project No 1/9242/02 Ecofriendly options for the production of nitrogen compounds and their precursors (Milan Hronec)

A simultaneous hydrogenation of nitro group and hydrogenation of chlorine in chloroanilines was studied over palladium catalysts on resins and inorganic materials. Beta zeolites with defined acid strength and the type of Broensted and Lewis sites were prepared and tested for condensation of aniline to diphenylamine. Metal phosphates were discovered as selective catalyst for gas-phase oxidation of benzene to phenol. In the progress is the research of partial oxidation of methane to formaldehyde, selective oxidation of cyclohexylamine to cyclohexanone oxime, oxidation of propylene to propylene oxide and synthesis of pyridine from ethanol, formaldehyde and ammonia.

Project duration: from january 2002 to december 2004 B. VEGA Project No 1/9143/02 Zeolites as catalysts for fine chemicals intermediates ( Dusan Mravec,

Martin Bajus ) Tert-butylation of toluene: Preparation of shape-selective zeolite catalysts for alkylation of toluene by deactivation of outer surface of basic zeolites. Study of tert-butylation of toluene in the liquid phase over basic and modified zeolite catalysts (H-MOR and H-BEA).

Etherification of glycerol: Study of reaction conditions for oxygenates to fuels preparation by etherification of glycerol with tert-butanol, isobutylene and C4 –fraction over different acid catalysts.

Project duration: from january 2003 to december 2004

VI. COOPERATION



Duration

DETOX, a. s. Banská Bystrica Kaszonyi from 1996

DUSLO, a. s., Šaľa Hronec FERMAS, s. r. o., Slovenská Ľupča Kaszonyi from 2003

NCHZ, a. s., Nováky Kaszonyi from 1995 PlasticOmnium, s. r. o., Lozorno Kaszonyi from 2002

SLOVNAFT VURUP, a. s., Bratislava Kaszonyi, Hronec from 1990

VUCHT, Bratislava Hronec from 1990 CHEMZA, a. s., Strážske Vojtko from 2003

CarCode, Bratislava Kaszonyi from 2001 SLOVAKOFARMA, a.s,Hlohovec Mravec from 1995



Duration

ENSCM, Montpellier, France

- zeolite catalysts, - physico-chemical characterisation of solid catalysts

Mravec, Hronec 1992


156

Universita di Padova, Italy

ad hoc projects on polymer supported catalysts, characterisation Kralik, Hronec 1991

Italian National Centre of research, Padova - Legnaro, Italy

ad hoc project on preparation of organic supports for catalysts Kralik, Hronec 1993

CNRS, Lyon, France Oxidation of organic matreials Hronec, Horvath 2002 C. Membership in Domestic Organizations and Societies


Valid date

Hronec M. SAIV (Slovak Academy of Engineering Sciences) chairmann 2001 Hronec M. SSPCH (Slovak Society for Industrial Chemistry chairmann 1990 Hronec M., Kaszonyi A., Mravec D.

SCHS (Slovak chemical Society) member 1990

Hronec M. Editorial Board of Journal: Petroleum and Coal member 1992 D. Membership in International Organisations and Societies


Valid date

Hronec M. National representative of the European Federation of catalysis Societes (EFCATS) member 1992

Hronec M. Member of the European Academy of Sciences and Arts member 1995 E. Visitors from Abroad


Date / Duration

Červený L. VŠCHT Praha Czech Republic 6. 6. 2003

Sugi Y. Faculty of Engineering, Gifu University Japan 28. - 29. 8. 2003 Corain B., Centomo P., Canton P., Prati L.

University of Padova Italy 5. - 7. 10. 2003



Date / Duration

Hronec M. VŠCHT Praha ČZ 28. - 29. 1. 2003

Horváth B. 6. Int. symposium on catalysis applied to fine chemical, Delft Netherlands 6. - 10. 4. 2003

Hronec M. ŠZS VŠCHT Praha ČZ 2. - 3. 6. 2003 Hronec M., Kaszonyi A., Štolcová M., Báhidský M.

EuropaCat IV., Innsbruck Austria 31. 8. - 4. 9. 2003

Hronec M., Báhidský M., Vallušová Z.

Symposium on catalysis, Praha ČZ 2. - 4. 11. 2003

Hronec M. VR, Praha ČZ 10. - 11. 11. 2003 Horváth B. IRC - CNRS Lyon France 3. 7. 2003 - 2. 1. 2004 Hronec M. VŠCHT, Pardubice ČZ 27. - 28. 11. 2003



Krejčová Barbora Toluén - výroba a použitie Toluene - production and utilization

Cvengrošová Zuzana


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Rovenský Peter Cyklohexán, jeho získavanie a využitie Cyclohexane - production

Cvengrošová Zuzana

Bieliková Lenka Výroba kyseliny benzoovej Benzoic acid production

Hronec Milan

Kerekeš Ladislav Zeolitové katalyzátory, príprava a použitie Zeolite catalysts, preparation and application

Hronec Milan

Pavlík Juraj Ekologické technológie výroby dusíkatých zlúčenín Nitrogen compounds production by ecological processes

Hronec Milan

Ondrejkovič Matúš Nitrácia toluénu Toluene nitration Hronec Milan

Csányi Marián Výroba a použitie difenylamínu Manufacture and utilization of diphenylamine Kaszonyi Alexander

Foltín Tomáš Výroba a využitie dusíkatých antioxidantov Manufacture and utilization of N containing antioxidants Kaszonyi Alexander

Sulačeková Jana Príprava a použitie cyklohexanónoxímu Preparation and utilization of cyclohexanone oxime Kaszonyi Alexander

Bartoš Kristián Výroba a využitie fenolu Manufacture and utilization of phenol Štolcová Magdaléna


Ďuračková Andrea Preparation of precursors for substituted aromatic amines Štolcová M. Foldesová Zuzana Synthesis of pyridine from ethanol, formaldehyde and ammonia Cvengročová Z.

Holecová Miroslava

A comparison of the activity and selectvity od Pd-Cu catalysts sported onup polymer and inorganic support in the process of the catalytic liquid phase

Králik M.

Klepáčová Katarína Ětherification of glycerol Mravec D.

Kucharovičová Sona

The effect of the support on the catalytic hydrogenation of chloronitrobenezene Králik M

Mrzula Miroslav Catalytic condensation of 2-mercaptobenzothiazole with alkylamines Štolcová M. Múčková Katarína Alkylation of toluene over zeolite catalysts Mravec D. Olejník Pavol Gas phase epoxidation of propylene Hronec M. Páleš Michal The synthesis of carbazole from diphenylamine Cvengrošová Z. Šimo Peter Amination of benzene by ammonia Kaszonyi A. Šmidt Michal Oxidation of cyclohexylamine in vapor phase Kaszonyi A.

VIII. PUBLICATIONS A. Journals [1] Artuso, F., D`Archovio A.A., Lora S., Jerabek K., Kráik M., Corain B.: Nanomorphology of Polymer Framworks and their Role

as templates for Ganeration Size-Controlled Metal Nanoclusters. Chem. Eur. J. 9, 5292-5296 (2003) [2] Corain, B., Centomo P., Lora S., Kralik M.: Functional resins as innovative supports for catalytically active metal nanoclusters

Journal of Molecular Catalysis A: Chemical 204–205 (2003) 755–762 [3] Hronec, M., Cvengrošová Z., Čejka J.: Synthesis of diphenylamine catalyzed by zeolites. Appl. Catal. A. General 255, 197-

202 (2003) [4] Kralik, M., Kratky V, Centomo P, Guerriero P, Lora S, Corain B.: Polymer frameworks as templates for generating size-

controlled metal nanoclusters. Active and reusable metal catalysts based on organic resins and on organic/inorganic composites. JOURNAL OF MOLECULAR CATALYSIS A-CHEMICAL 195 (1-2): 219-223 MAR 18 2003

[5] Kralik, M., Kratky V, De Rosso M, Tonelli M, Lora S, Corain B.: Metal catalysis inside polymer frameworks: Evaluation of catalyst stability and reusability. CHEMISTRY-A EUROPEAN JOURNAL 9 (1): 209-214 JAN 3 2003

[6] Krátky, V. Králik M.,Kaszonyi, A., Štolcová M.,Zalibera L., Mečárová M. , Hronec, M.: Reaction pathway and the role of solvent in the hydrogenation of chloronitrobenzenes. Coll.Czech.Chem.Comm. 68, 1819-1832, (2003)

[7] Mravec, D.,Zavadan P., Kaszonyi, A., Joffre J., Moreau P.: Tert-butylation of toluene over zeolite catalysts. Appl. Catal. A: General 257(2004) 49 - 55

[8] Kaszonyi, A., Cvengrošová Z., Hronec, M.: Oxidation of Cyclohexylamine over H4[Si(W3O10)4].xH2O / γ-Al2O3 . Petroleum and Coal, 44,195-97 (2002)

[9] Klepáčová, K., Mravec, D., Hájeková, E., Bajus, M.: Etherification of glycerol. Petroleum and Coal 45, 1-2, 2003 B. Conferences [1] Cvengrošová, Z., P. Michalica, A. Kaszonyi, M.Hronec: Condensation reaction of ethanol, formaldehyde and ammonia. 41st

International Petroleum Conference October 6th – 8th, 2003 Bratislava, Slovak Republic [2] Horváth, B., M.Hronec: Gas-phase exopxidation of propylene. 41st International Petroleum Conference October 6th – 8th,

2003 Bratislava, Slovak Republic


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[3] Kaszonyi, A.*, Hronec, M. : Determination of V5+ and V4+ in Polyoxometalate Catalysts. EuropaCat-VI, August 31 – September 04, 2003 in Innsbruck/Austria

[4] Kaszonyi, A.*, Hronec, M. : Direct Amination of Benzene over Heterogeneous Catalysts. EuropaCat-VI, August 31 – September 04, 2003 in Innsbruck/Austria

[5] Kaszonyi, A., Cvengrošová Z., Hronec, M.: Oxidation of Cyclohexylamine over Solid Acids . EuropaCat-VI, August 31 – September 04, 2003 in Innsbruck/Austria

[6] Sá, J., Gašparovičová, D., Kinger, G., Vinek, H.: Degradation of nitrates by hydrogenation over a bimetallic catalyst. Europa Cat-VI, Innsbruck Austria, Aug. 31- Sept. 04, 2003 (B3.075)

[7] Štolcova, M*., Juhás, E., Hronec, M.: Effect of structure on the catalytic activity of Ca-Fe phosphates in the partial oxidation of methane to formaldehyde. EuropaCat-VI, Aug. 31-Sept.4, 2003, Insbruck, Austria

[8] Vallušová, Z., Hronec, M., Jorik V., Králik M.: Hydrogenation of chloronitrobenzenes over Pt/beta zeolite catalysts. XXXV Symposium on Catalysis, Prague, November 3-5, 2003

[9] Bahidsky, M.*, Hronec, M.: Direct hydroxylation of aromatics over copper containing phosphate catalyst. 35th Symposium on Catalysis, 3 - 5 November 2003, Prague, Czech Republic

[10] Bahidsky, M.*, Hronec, M.: Direct hydroxylation of benzene over phosphate catalysts in the gas phase. ISO 2003 - EUROPACAT VI, Innsbruck (Austria), September 1-3, 2003

[11] Bahidsky, M.*, Hronec, M.: Direct hydroxylation of benzene to phenol. 41st International Petroleum Conference October 6th – 8th, 2003 Bratislava, Slovak Republic

[12] Gašparovičová, D., Hronec, M., Jorík, V., Vinek, H., Biffis, A., Zecca, M., Králik, M.: A formation of palladium-copper composites on functional resins and alumina and catalytic properties of these materials. 41st International Petroleum Conference, Bratislava, Oct. 6-8, 2003

[13] Juhás, E*., Hronec, M.: Direct oxidation of methane to formaldehyde over silicalite supported iron catalysts Direct oxidation of methane to formaldehyde over silicalite supported iron catalysts 41st International Petroleum Conference October 6th – 8th, 2003 Bratislava, Slovak Republic

[14] Kaszonyi, A.*, Hronec, M.: State of the Art in the Direct Amination of Benzene. 41st International Petroleum Conference, Bratislava, October 6th –8th, 2003

[15] Štolcova, M*., Hronec, M., Mikula M.: Spectral study of Ca-Fe phosphates useful in the partial oxidation of methane to formaldehyde. 41th International Petroleum Conference, Oct 6th-8th, 2003, Bratislava

[16] Vallušová, Z., Hronec, M., Jorik V., Králik M.: Comparison of palladium catalysts supported on functional resins and Beta-zeolite in the hydrogenation of chloronitrobenzenes. 41st International Petroleum Conference, Bratislava, October 6-8, 2003

[17] Cvengroš, J.*, Cvengrošová, Z: Príprava koncentrátov fitosterolov. Preparation of phytostrerol concentrates. TOP 2002, Technique of Environmental Protection Focused of Waste Treatment,24-25.6.2003, Častá-Papiernička, proceedings str. 145-150

[18] Klepačová K., Mravec D.,Hajekova E., Bajus M.: Priprava oxygenatov do paliv eterifikaciou glycerolu. Preparation of oxygenates to fuels by etherification of glycerol. Konferencia „Ropa v 21.storočí, Bratislava, FCHPT STU, 10.-11.6.2003, 103-111 (0,5/1)

[19] Mravec, D.: Niektore moznosti vyuzitia zeolitov ako katalyzatorov v organickej technologii. Some possibilities of utilisation of zeolites as catalysts in organic technology. Konf.: Prirodne a synteticke zeolity, FCHPT, Bratislava,13. Februar 2003

DEPARTMENT OF PETROLEUM TECHNOLOGY AND PETROCHEMISTRY

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Head of Department: Telephone: ++421252926037 Assoc. Prof. Pavol Daučík, PhD Fax: ++421252493198


I. STAFF Full Professors: Martin Bajus, PhD, DSc; Associate Professors: Pavol Daučík, PhD; Pavol Hudec, PhD; Agáta Smiešková, PhD; Zdenek Židek, PhD; Assistant Professors : Elena Hájeková, PhD; Research Fellows: Jozef Ambro; Beata Liptáková; PhD Students: Jana Danišková; Marek Ladický; Peter Michalica; Andrej Nociar; Technical staff: Marcela Hadvinová; Stanislava Kováčová; Dagmar Machatová; Marta Olleová;


A. Teaching laboratories: Laboratory of Catalysts Characterization Laboratory of High Pressure Reactors Laboratory of Gas and Liquid Chromatography Laboratory of Chemistry and Analysis of Fuels Laboratory of Pyrolysis Laboratory of Rheology of Lubricants Laboratory of Infra-Red Spectroscopy Laboratory of Natural Gas Conversion

B. Research laboratories: Laboratory of Catalysts Characterization Laboratory of High Pressure Reactors Laboratory of Gas and Liquid Chromatography Laboratory of Chemistry and Analysis of Fuels Laboratory of Pyrolysis Laboratory of Rheology of Lubricants Laboratory of Infra-Red Spectroscopy Laboratory of Natural Gas Conversion

III. TEACHING

A. Undergraduate Study: 4. semester (Bc) Organic Technology and

Petrochemistry 3/1/0 Bajus, Smiešková, Liptáková

1. semester (MSc) Catalysis 0/1/0 Hudec Analysis of Petroleum Products 2/0/0 Daučík Technology of Crude Oil 3/0/0 Židek, Smiešková Combustion Processes 1/2/0 Smiešková 1. semester (MSc) Refinery and Petrochemical Plants 1/2/0 Daučík Laboratory exercise 1 0/0/8 Daučík, Liptáková 2. semester (MSc) Alternative Fuels 2/0/0 Bajus Catalytic and Thermal Processes in

Crude Oil Treatment 3/0/0 Židek

Tribology 2/0/0 Hájeková Kinetic and Reactors 0/2/0 Hudec


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2. semester (MSc) Laboratory exercise II 0/8/0 Hudec 3. semester (MSc) Petrochemistry 3/0/0 Bajus Gas Industry 2/0/0 Hudec Laboratory exercise III 0/0/10 Hudec


A. VEGA Project No 1/9143/02 Catalytic and Thermic Conversion of Hydrocarbons from Crude oil and Natural gas to Petrochemicals (Martin Bajus)

The subject of the scientific project is the study of kinetics and mechanism of catalytic and thermal conversions of hydrocarbons from crude oil, natural gas and polymers with the orientation on copyrolysis of primary naphtha with polyethylene, polypropylene, polystyrene, polyvinyl chloride to desired petrochemicals. During the first period of the project we studied: A. solubility of polymers )PE, PP, PVC, PST, PET) in aromatic diluent (xylenes) and in primary naphta B. pyrolysis of individual polymers (PE, PP, PVC, PST, PET) in batch reactor C. thermal decomposition of PE, PP and PS in the system PYRO-GC-MS D. copyrolysis of primary naphtha with polyethylene, polypropylene, polystyrene, polyvinyl chloride in flow tubular reactor Project duration: from 01. 01. 2002 to 31. 12. 2004

B. VEGA Project No 1/9144/02 The Modern Trends in Petroleum Treatment and in Petrochemistry (Pavol Hudec)

The study of physical, physico-chemical and catalytic processes leading to the conversion of petroleum fractions, individual hydrocarbons or natural gas to prepare components of modern and perspective reformulated fuels corresponding to the strict ecologic and economic requirements. Examined topics join to the production of motor fuels in refinery-petrochemical complex Slovnaft on the base of hydrocracking of heavy residues. Solved is influence of the composition on light and oxidizing stability and low-temperature properties of motor fuels. In work, the possibilities of the improving the quality of the products by the modification of classical hydrorefining catalyst by modified Y-type zeolites and by mesoporous molecular sieves of M41S type, and the modification of fluid catalytic cracking catalyst by ZSM-5 zeolite additives will be studied, in direct connection with the composition of industrial feeds in these processes.


VI. COOPERATION



Duration

CHEMZA, j. s. co., Strážske The way of utilization HALS product

Foltín Jozef, director, Priemyselná 720, 07222 Strážske

15. 03. 2003 - 30. 11. 2003

PETROCHEMA, j. s. co., Dubová

Technical support at higher explotation of destilates

Šuráb Jozef, director, 976 97 Nemecká

15. 3. 2003 - 30. 11. 2003

TRANSPETROL, j. s. co., Bratislava

Evaluation of standart methods of quolity of cruide oil and waste water

Polák Peter, technical director, Šumavská 98, 821 08 Bratislava

9. 6. 2003 - 15. 11. 2003

VÚRUP, j. s. co., Bratislava

Determination of polycyclic aromatics in oils

Mikulec Jozef, director, Vlčie hrdlo, 824 12 Brstislava

1. 10. 2002 - 30. 6. 2003

DRON - Sklady, ltd. co. Recyclation of polymeric wastes

Hóka Csaba, director, Gazdovský rad 1587, 931 01 Šamorín

01. 12. 2003 -



Valid date

Ambro Jozef Slovak Society of industrial Chemistry member Bajus Martin Slovak Society of industrial Chemistry member Daučík Pavol Slovak Society of industrial Chemistry member Hájeková Elena Slovak Society of industrial Chemistry member 01. 01. 1994

Hudec Pavol Slovak Society of industrial Chemistry member Liptáková Beata Slovak Society of industrial Chemistry member 01. 01. 2001


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Michalica Peter Slovak Society of industrial Chemistry member

Smiešková Agáta Slovak Society of industrial Chemistry member

Židek Zdenek Slovak Society of industrial Chemistry member Daučík Pavol Slovak institute of technical normalization member 30. 4. 2001 Daučík Pavol Examining board in the field of oils member 29. 11. 2001 Hudec Pavol Slovak zeolite association at SSPCH president 01. 01. 2001

E. Visitors from abroad


Date / Duration

Zanzotto, L. Faculty of Engineering, University of Calgary, Calgary Canada 13. 03. 2003 - 18. 03. 2003



Date / Duration

Bajus, M. The Univeristy of Calgary, Calgary Canada 01. 08. 2003 - 22. 09. 2003

Hájeková, E. International Conference „CARBON 2003“, Oviedo Spain 05. 07. 2003 - 11. 07. 2003

Hudec, P. XXXV. Symposium on Catalysis, Praha Czech Republic

03. 11. 2003 - 05. 11. 2003

Hudec, P. Feza Committee Meeting, Praha Czech Republic 08. 11. 2003

Hudec, P. Europacat - VI, Insbruck Austria 31. 08. 2003 - 04. 09. 2003

Liptáková, B. XXXV. Symposium on Catalysis, Praha Czech Republic

03. 11. 2003 - 05. 11. 2003

Michalica, P. The Univeristy of Calgary, Calgary Canada 28. 09. 2003 - 22. 12. 2003

Michalica, P. X. Zeolite Forum, Tuczno Poland 21. 09. 2003 - 26. 09. 2003

Nociar, A. X. Zeolite Forum, Tuczno Poland 21. 09. 2003 - 26. 09. 2003

Nociar, A. XXXV. Symposium on Catalysis, Praha Czech Republic

03. 11. 2003 - 05. 11. 2003

Smiešková, A. XXXV. Symposium on Catalysis, Praha Czech Republic

03. 11. 2003 - 05. 11. 2003

Smiešková, A. X. Zeolite Forum, Tuczno Poland 21. 09. 2003 - 26. 09. 2003



Bartík, M. Determination of water in cruide oil fraction Daučík, P. Bartková, A. Study of acid properties of zeolites Smiešková, A.

Bokšanský, V. Dehydrogenation of lowmolecular weight hydrocarbons in membrane reactor Ladický, M.

Mlynková, B. The way of recyclation of waste polymers by copyrolysis Hájeková, E. Porkertová, G. Extraction of nitrogen compounds from GO-RHC by metal complexes Smiešková, A. Šándor, M. Preparation and characterization of catalysts for methane aromatization Liptáková, B.


Benkovský, L. Regeneration of waste oils. Daučík, P

Danišková, J. Coke formation during copyrolysis of polyethylene with straight run of naphta. Hájeková, E.

Hochholczer, E. Study of the acid properties of zeolites by TPD of ammonia. Smiešková, A. Kondášová, I. Copyrolysis of polyethylene with straight run of naphta. Bajus, M. Nemčovská, J. Investigation of aditive efects on diesel fuel properties. Daučík, P. Tóth, R. Aditivation FCC catalysts by ZSM-5 zeolites. Hudec, P.


162


Danišková, J. Pyrolysis of polymeric wastes. Bajus, M. Ladický, M. Dehydrogenation of low molecular alkanes. Bajus, M. Michalica, P. Study of conversion of nitrogen compounds in petroleum faction. Smiešková, A. Nociar, A. Alkylation of aromatics by linear alkanes. Hudec, P.

VIII. PUBLICATIONS A. Journals [1] Bajus, M.: Hydrocarbon technologies. Petroleum and Coal, 45 (1-2), 10-18, 2003 [2] Hájeková, E., Bajus, M., Biskupičová, E., Hóka, Cs., Ilkovič, I.: Parametre kvality a chromatografická analýza MERO pri

použití ako paliva. Parameters of quality and chromatographic analysis of FAME at usage as a fuel. Ropa, uhlie, plyn a petrochémia, 44 (2), 29 – 33, 2002

[3] Hájeková, E., Bajus, M.: The Study of Coke Formation During Copyrolysis of Hexadecane, Cyclohexane, and Isooctane. Petroleum and Coal, 45 (1-2), 25-29, 2003

[4] Ilkovič, J., Bajus, M., Vlček, V.: Štúdium polymérnych materiálov pomocou analytickej pyrolýzy. Study of polymeric materials by analytical pyrolysis. Ropa, uhlie, plyn a petrochémia, 44 (2), 41-44, 2002

[5] Klepáčová, K., Mravec, D., Hájeková, E., Bajus, M.: Ethericifaction of glycerol. Petroleum and Coal, 45 (1-2), 54-57, 2003 [6] Ladický, M., Bajus, M.: Izomerizácia C4 frakcie. Isomerisation of C4 fraction. Izomerizácia C4 frakcie. Isomerisation of C4

fraction. Ropa, uhlie, plyn a petrochémia, 44 (2), 34-36, 2002 [7] Michalica, P., Smiešková, A., Hudec, P., Rácová, R., Ambro, J.: Performance Comparison of Conventional and Y-Zeolite

Containing Hydrotreatment Catalysts in Hydrorefining of Middle Fuel Distillates Derived from Different Sources. Petroleum and Coal 45 (1-2), 30-34 (2003)

[8] Bajus, M.: Súčasnosť a budúcnosť alternatívnych palív. Presence and future of alternative fuels Slovgas 11(5-6), 28-31 (2002)

B. Conferences [1] Hájeková, E., Bajus, M.: The Study of Coke Formation During Copyrolysis of Hexadecane, Cyclohexane, and Isooctane. The

Study of Coke Formation During Copyrolysis of Hexadecane, Cyclohexane, and Isooctane. Carbon 2003, An International Conference on Carbon, July 6-10, 2003, Oviedo, Spain, 1-5, ISBN 84-607-8305-7

[2] Hájeková, E., Bajus, M., Špirková, I., Pechová, A., Ilkovič, J.: Feedstock Recycling of Polyethylene by Copyrolysis. Feedstock Recycling of Polyethylene by Copyrolysis. 41th International Petroleum Conference, October 6th – 8th, 2003 Bratislava, Slovensko, H PO 42, ISBN 80-968981-6-7

[3] Liptáková, B., Hudec, P., Smiešková, A.: Methane dehydro-aromatization over Mo/ZSM-5 catalysts. In: XXXV Symposium on catalysis, November 3 - 4, 2003, Praha, ČR, p 54-55

[4] Michalica, P., Smiešková, A., Hudec, P.: Solvent extraction of nitrogen compounds from gas oil derived from residual hydrocracking by metal complexation. In: 41st International Petroleum Conference, Bratislava, October 6-8, 2003, 8 pages, CD-ROM ISSN 1335-888X, ISBN 80-968981-6-7

[5] Nociar, A., Hudec, P., Smiešková, A., Jakubík, T., Židek Z.: Alkylation of benzene by linear 1-olefins C16 over dealuminated Y-zeolites and mordenites. 41st International Petroleum Conference, Bratislava, October 6-8, 2003, 7 pages, CD-ROM ISSN 1335-888X, ISBN 80-968981-6-7

[6] Nociar, A., Hudec, P., Smiešková, A., Jakubík, T., Židek Z.: Alkylation of benzene by linear a-olefin C16 over zeolite catalysts in flow pressure reactor. XXXV Symposium on catalysis, November 3 - 4, 2003, Praha, ČR, p 26-27

[7] Šabo, Ľ., Gábová, V., Hudec, P., Smiešková, A.: Stability of siliceous MCM-41 materials as support for Ni-supported catalyst under incipient wetness method. 41st International Petroleum Conference, Bratislava, October 6-8, 2003, 7 pages, CD-ROM ISSN 1335-888X, ISBN 80-968981-6-7

[8] Hudec, P., Šabo L., Smiešková, A., Židek, Z.: Zeolites and zeolite catalysts in refinery and petrochemistry. 41st International Petroleum Conference, Bratislava, October 6-8, 2003, 12 pages, CD-ROM ISSN 1335-888X, ISBN 80-968981-6-7

[9] Michalica, P., Smiešková, A., Hudec, P., Rácová, R., Ambro, J.: Comparison of conventional and Y-zeolite containing hydrotreatment catalyst in hydrorefining of primary gas oil from residual hydrocracking. In: X Zeolitic forum „Zeolites – synthesis, adsorption and catalysis“, September 21 – 26, 2003, Tuczno, Poland, p.136-142

[10] Nociar, A., Hudec, P., Smiešková, A., Jakubík, T.: Alkylation of benzene by linear alpha-olefins C16 over dealuminated Y-zeolites and mordenites. X Zeolitic forum „Zeolites – synthesis, adsorption and catalysis“, September 21 – 26, 2003, Tuczno, Poland, p.107-112

[11] Ambro, J., Nemčovská J., Daučík, P.: Vplyv prísad na nízkoteplotné vlastnosti Dieselových palív. Influence od additives on low-temperature properties of Diesel fuels. Konferencia „Ropa v 21.storočí, Bratislava, FCHPT STU, 10.-11.6.2003. str. 112-119

[12] Bajus, M.: Hydrocarbon technologies. Konferencia „Ropa v 21.storočí, Bratislava, FCHPT STU, 10.-11.6.2003. 15-38 [13] Hudec, P., A.Smiešková, Z.Židek: Zeolity a zeolitové katalyzátory v spracovaní ropy a v petrochémii Zeolites and zeolite

catalysts in petroleum treatment and petrochemistry. Konferencia „Ropa v 21.storočí, Bratislava, FCHPT STU, 10.-11.6.2003. str. 62-68

[14] Klepáčová, K., Mravec D., Hájeková E., Bajus M.: Príprava oxygenátov do palív éterifikáciou glycerolu Preparation of oxygenates for fuels by eterification of glycerine. Konferencia „Ropa v 21.storočí, Bratislava, FCHPT STU, 10.-11.6.2003, 103-111 (0,5/1)

[15] Michalica, P., Porkertová, G., Smiešková, A.: Odstránenie dusíkatých látok z PO-RHC komplexačnou extrakciou. Removing of nitrogen compounds from gas oil from residue hydrocracking by complexing extraction method. Konferencia „Ropa v 21.storočí, Bratislava, FCHPT STU, 10.-11.6.2003. str.133-141


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[16] Nociar, A., Hudec, P.: Alkylácia benzénu 1-hexadecénom na zeolitových katalyzátoroch. Alkylation of benzene with 1-hexadecene on zeolite catalysts. Konferencia „Ropa v 21.storočí, Bratislava, FCHPT STU, 10.-11.6.2003. str.120-126

[17] Šabo, Ľ., Hudec, P., Gábová, V., Smiešková, A.: Mezopórové molekulové sitá na báze kremíka ako nosiče pre niklový hydrogenačný katalyzátor. Siliceous mesoporous molecular sieves as supports for Ni-hydrogenation catalyst. Konferencia „Ropa v 21.storočí, Bratislava, FCHPT STU, 10.-11.6.2003. str.127-132

[18] Michalica, P., Smiešková, A., Nociar, A.: Zlepšenie katalytickej aktivity zeolitov Y fyzikálno-chemickými úpravami Improving of catalytic activity of Y zeolites by chemical treatment Študentská vedecká konferencia pri príležitosti 50 rokov SAV, Bratislava 9.-10.apríla 2003, str.245

[19] Nociar, A., Hudec, P., Michalica, P.: Alkylácia benzénu 1-hexadecénom na zeolitoch Y Alkylation of benzene by 1-hexadecene over Y zeolites Študentská vedecká konferencia pri príležitosti 50 rokov SAV, Bratislava 9.-10.apríla 2003, str.249

C. Books and Textbooks [1] Baxa, J., Daučík, P., Židek, Z.: Technológia ropy I. Petroleum Technology I. STU v Bratislave, 2003, 257 str., ISBN 80-227-

1825-4 E. Others: [1] Bajus, M.: Návrat do budúcnosti, Automobily bez škodlivých emisií už nie sú chimérou (I.) Back to the future, Cars without

harmfull emissions are not already vision. Stop 23(3), 28-29, 2003

DEPARTMENT OF PHYSICAL CHEMISTRY

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Head of Department: Telephone: ++ 421-2-5292 6032 Prof. Stanislav Biskupič, PhD, DSc Fax: ++ 421-2-5249 3198 E-mail: [email protected]

I. STAFF Full Professors: Stanislav Biskupič, PhD, DSc; Andrej Staško PhD, DSc; Peter Šimon, PhD, DSc Associate Professors: †Jozef Antalík, PhD; Tomáš Bleha, PhD, DSc; Martin Breza, PhD; Vlasta Brezová, PhD, DSc; Ján Cvengroš, PhD, DSc; Anton Gatial, PhD; Pavel Kovařík, PhD; Jozef Kožíšek, PhD; Milan Mazúr, PhD; Jiří Polavka, PhD; Peter Rapta, PhD; Ján Reguli, PhD; Marián Valko, PhD. Assistant Professors : Vladimír Adamčík, PhD; Dana Dvoranová; Erik Klein, PhD; Róbert Klement, PhD; Jozef Polakovič, PhD; Ľubomír Zalibera, PhD Research Fellows: Andrea Kleinová PhD Students: Ingrid Bažányiová; Zuzana Cibulková; Marek Fronc; Teodora Kocsisová; Júlia Pigošová, Martin Polovka; Pavol Skubák. Technical staff: Imrich Csonka, Elena Fabíková, Alžbeta Chochulová, Hana Janošková, Marta Lintnerová, Štefan Miksai, Jarmila Paligová, Milan Štefunko, Mária Šuleková.


A. Teaching laboratories: Laboratory for the Basic Course of Physical Chemistry Laboratory for the Advanced Course of Physical Chemistry Laboratory of Electronics Laboratory of UV-VIS and IR Spectroscopy Computational Laboratory

B. Research laboratories: Laboratory of Thermal Analysis and Calorimetry Laboratory of EPR Spectroscopy Laboratory of IR spectroscopy Laboratory of Molecular Distillation and Alternative Diesel Fuels

III. TEACHING

A. Undergraduate Study: 3. semester (Bc) Physical Chemistry I (3-2 h) S. Biskupič, A. Gatial Physical Chemistry II (3-2 h) P. Rapta Laboratory Practice in Physical

Chemistry I (0-3 h) J. Reguli

4. semester (Bc) Physical Chemistry II (3-2 h) S. Biskupič, P. Kovařík, A. Gatial Laboratory Practice in Physical

Chemistry II (0-3 h) J. Reguli

5. semester (Bc) Physical Fundamentals of Spectroscopic Methods

(2-2 h) A. Staško, V. Brezová

6. semester (Bc) Biophysical Chemistry I (2-2 h) M. Valko 1. semester (MSc) Chemical Physics I (2-1 h) M. Breza Thermodynamics (2-1 h) P. Šimon Kinetics and Catalysis (2-1 h) P. Kovařík Colloid Chemistry (2-0 h) J. Antalík 1. semester (MSc) Statistical Treatment and Evaluation

of Exp. Data (2-0 h) M. Breza

Group Theory and Symmetry (2-0 h) M. Breza, V. Kvasnička


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Special Laboratory Practice I (0-8 h) P. Rapta 2. semester (MSc) Chemical Physics II (2-1 h) S. Biskupič Solid State Physics (2-0 h M. Breza Biophysical Chemistry II (2-0 h) M. Valko Special Laboratory Practice II. (0-6 h) P. Rapta 2. semester (MSc) Traineeship Excursion 3. semester (MSc) Molecular Spectroscopy (2-1 h) A. Staško Chemical Physics III (2-0 h) A. Gatial Physical Chemistry of

Macromolecules (2-0 h) T. Bleha

Special Laboratory Practice III (0-10 h) P. Rapta


A. VEGA Project No 1/0052/03 DEVELOPMENT AND APPLICATION OF COMPUTATIONAL METHODS TO THE STUDY OF ELECTRONIC STRUCTURE OF MOLECULAR SYSTEMS (Stanislav Biskupič)

Within this research project, new theoretical treatments based on quantum-chemical principles are developed and then - with other accessible techniques - used to obtain exact and detailed information on the structure and dynamics of selected molecular sytems. Many-body perturbation and CC formalism of interaction energy evaluation (higher order contributions) has been elaborated and applied to some van der Waals complexes that are important for chemical reactions in upper shells of the Earth atmosphere. Systematic study of the factors causing unusual electronic structure of selected compounds with interesting physico-chemical properties has been oriented to oligothiophenes, cyclophosphazenes, transition metal complexes in unusual oxidation states and blue proteins model compounds.Vibration spectra of new push-pull olephines (as model compounds of pharmacotherapeutics) have been calculated and interpreted.

Project duration: from 2003 to 2005 B. VEGA Project No 1/0053/03 SPECTROSCOPICAL ANALYSIS OF STRUCTURE AND REACTIVITY OF

FREE RADICALS AND TRANSITON METAL COMPLEXES IN CHEMICAL, BIOLOGICAL AND PHOTOCHEMICAL SYSTEMS (Vlasta Brezová)

Research project is focused on the investigation of structure and reactivity of radical intermediates and metal complexes in the chemical, electrochemical, photochemical, and biological systems with the predominant application of spectroscopic methods (EPR, UV/VIS/NIR spectroscopy) and electrochemical techniques (voltammetry). The investigation is oriented especially on the synthesis and physicochemical characterization of new organic materials for LEDs (Light Emitting Devices) systems, and on the study of magnetic, redox and spectroscopic properties of metal complexes. The primary radical intermediates of the photoinduced electron transfer in heterogeneous titanium dioxide systems, as well as reactive species produced upon the photoexcitation of drugs are investigated. Additionally, the attention is paid to research of antioxidant properties of foods and beverages (tea, wine, beer) with the main aim to select foods with the positive health effect. Concerning the experimental methods, the systematical development of combined spectroelectrochemical and spectrophotochemical techniques continued, as well as further analysis of experimental error sources in quantitative EPR spectroscopy is performed.

Project duration: from 01/2003 to 12/2005 C. VEGA Project No 1/0054/03 MATERIALS – physico-chemical methods of their study (Peter

Šimon) The method for the evaluation of kinetic parameters of induction periods has been elaborated. The method enables to estimate the length of nonisothermal induction periods in the processes such as rubber curing, oxidation in condensed phase, freezing of undercooled liquids, oxidation stability of drugs and foods, etc. The method is expected to be applied in the quality management and risk assessment in technological processes.

Theory of model-free isoconversional kinetics is developed and a new incremental isoconversional method has been elaborated. The method enables modeling the processes without deeper insight into their mechanism.

Degradation and stabilisation of PVC is studied both experimentally and theoretically. The attention is paid to the non-hazardous stabiliser mixtures based on tocoferyl acetate.

Project duration: from 2003 to 2005 D. VEGA Project No 1/9255/03 ELECTRON STRUCTURE AND PROPERTIES OF MATERIALS IN SOLID

PHASE (Jozef Kožíšek) The ambition of the solved project is the integrated study of the selected systems in solid state with possible applications in understanding the mechanisms of enzymatic reactions in biological systems. In the experimental area the present possibilities of measurements on the synchrotron equipments in the Europe (Hamburg, Grenoble) are utilized, as well as our collaboration with TU-Darmstadt. The composition of investigators of this project was selected in such way that involves both theoretical (quantum-mechanical) as well as available experimental methods (X-ray analysis, EPR spectroscopy, DSC measurements). So it will be possible to produce the complex results including many aspects of the studied systems. We focus our attention on the study of electronic structure and properties of the model systems of blue proteins. For this purpose we have synthesized monocrystals of the compounds [Cu(bite)(BF4)] and [Cu(bite)(BF4)2] which very well reproduce the active centre of these interesting biological


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catalysers. The electron density of compounds with various characteristic types of coordination sphere are studied experimentally and results are correlated with the physico-chemical properties of these and similar compounds. These measurements will be correlated also with ab-initio quantum-chemical calculations in solid state.

Another object of experimental study is the electron density of stereospecific catalyzers on the base of Ni complexes with Schiff bases, which are reaction centers for the assymetric synthesis of various aminoacids and their analogs.

Project duration: from 2002 to 2004 E. Project APVT-20-014702 Research and development of biogenic ecological fuels and lubricants from

domestic renewable resources (Ján Cvengroš) The research project is focused on the research, development, production and application of esters of higher fatty acids as ecological fuels for diesel engines based on the renewable domestic raw materials with complex utilisation of the by-products. The main results in 2003 are as follows:

1. Oxidation of methyl esters based on rapeseed oil and methyl esters based on frying oils used as the alternative diesel fuels, unstabilized and stabilized by some antioxidants has been studied by differential thermal analysis/thermogravimetry (DTA/TG) under non-isothermal conditions for various heating rates and by Rancimat test under isothermal conditions. Low oxidation stability of the undistilled methyl esters was stated. The induction period increased expressively by the addition of low quantities of selected antioxidants. Especially high stabilising effect was reached for pyrogallol. The results obtained by the both methods are compared and the differences are accounted for by the oxygen diffusion within the samples. The DTA/TG method is suitable for the evaluation of the oxidation stability of the studied esters.

2. The importance of the alternative fuels based on the biomass as reliable domestic and renewable resource is great. The environmental, energetic and economical effects connected with the production and the utilization of biofuels in the transportation were evaluated. The analysis of the biofuels taxation in the tax system of Slovakia was carried out.

3. Glycerol is a valuable by-product used in the production of methyl esters. Its production can positively influence economical balance of the production of methyl esters. The method of refinement of glycerol in vacuum evaporator with wiped film was tested and the parameters of the distilled glycerol were stated. Distilled glycerol meets the requirements of the industrial glycerol according to the standard.

Project duration: from 2002 to 2005 F. VEGA Project No 1/8110/01 Evaporation performance and separation efficiency at molecular

distillation (Ján Cvengroš) The research project is focused on the theory of molecular distillation, the development of the short-path evaporators with wiped film and on the applications of molecular distillation. The main results in 2003 are as follows:

1. In the model study, selected parameters with the effect on the distillation output and composition of outlet streams from the molecular evaporator were investigated in the laminar and turbulent regimes in the film, depending on the evaporator´s liquid load and temperature. In the case of a turbulent film a higher portion of a feed is evaporated at a lower content of the more volatile component in the distillate. There are only small differences in the separation efficiency at both studied regimes. Re-evaporation from the condenser has a small effect on the separation efficiency. The decrease of the separation efficiency is greater in the case of splashing. The qualitative agreement between experimental results and results from the model shows that the model describes well the phenomena that occur within the distillation space of the molecular evaporator.

2. The study of the film wiping with the wiping element having profiled surface shows that there are three different liquid flow regimes on the evaporating cylinder. The conditions for the formation of these regimes and their consequences are discussed. Optimum conditions for distillation can be reached at increased retention of liquid on the evaporator. The increased residence time is a positive factor, which makes efficient evaporation at a lower evaporating temperature.

3. Some technically interesting applications of molecular evaporators were developed (regeneration of used mineral oil, final treatment of methyl esters as alternative diesel fuels, purification of the phytosterols from vegetable oils and others).

Project duration: from 2001 to 2003 G. Project APVT-20-005702 Thermooxidation and photooxidation processes in chemical and biological

systems and their influence on the quality of life (Stanislav Biskupič) The project is oriented towards spectroscopic (EPR, UV/VIS) and thermoanalytical (DSC) characterization of the processes occuring in thermal and photooxidative degradation of food, drugs and newly synthesized pharmaceutical precursors. A great attention is paid to spectroscopic study of antioxidative properties of foods with the aim of selecting the group of beneficial functional food and to monitor and improve their quality. Elaboration of time-saving procedures for the determonation of stability of food and drugs (DSC, EPR). Study of photoinitiated radical transformations of drugs, interpretation of the results by quantum-chemical calculations with the aim of elucidating the mechanisms of their effects and targeted improvement of their quality.

Project duration: from 06/2002 to 06/2005 H. VEGA Project No 1/9256/02 The role of trace metals and light in camptothecin – serum albumin

interactions (NMR and EPR studies) (M. Valko) The anticancer drug camptothecin (CPT) is a plant alkaloid that has recently gained approval for clinical trials as a treatment of gastric, rectum, and bladder tumors. The drug exists in two forms, a lactone form which is biologically active and a carboxylate form which is not. It has been shown that in the presence of human serum albumin (HSA) the drug converts to the biologically inactive form and therefore the liposomal stabilization of the lactone form of the drug is of primary importance. In this connection the high


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resolution NMR study is planned to elucidate the stabilization of the lactone form of the drug and the nature of the binding mode with HSA. It is generally believed that camptothecin activity occurs through a free radical mechanism. We also believe, that the role of trace metals is in particular important. Our preliminary results show that upon irradiation (365 nm light) copper(II)-CPT complex generates free radicals which may cause DNA damage to cancer cells. The aim of the proposed project is to further investigate a radical mechanism of the action of the drug.


VI. COOPERATION



Duration

LikoSpol Bratislava scientific P.Šimon 2003 Research Inst. Food scientific P.Šimon 2003 BEL/Novaman scientific, industrial P.Šimon 2003 Res.Inst.Chem. Technology scientific P.Šimon 2003

Slovak Academy of Science scientific A.Staško 2003

DETOX Banská Bystrica scientific, industrial J.Cvengroš 2003

VÚLM Modra scientific,industrial J.Cvengroš 2003 Q-CHEM Bratislava scientific,industrial J.Cvengroš 2003 Bel/Novamann Bratislava scientific J.Cvengroš 2003

Kovostroj Lučenec scientific, industrial J.Cvengroš 2003 Ekoil Bratislava scientific,industrial J.Cvengroš 2003 Lubocons Stupava scientific J.Cvengroš 2003 DAMT-MDT Martin scientific,industrial J.Cvengroš 2003 Slovnaft VÚRUP Bratislava scientific J.Cvengroš 2003

TU Žilina scientific J.Cvengroš 2003 JAV-AKC Vlčany scientific J.Cvengroš 2003



Duration

DIAS UMIST, Manchester, UK (F.Kvasnik)

scientific P.Šimon 2003

University of Technology, Sydney, Australia (A.Ray, P.Thomas)


Faculty of Chemistry, Technical University, Brno, Czech Republic (L.Omelka)


LUKAS Research, Prague, Czech Republic (R.Lukáš, L.Kalvoda)


Materialwissenschaft, TU Darmstadt, Germany (Prof. Hartmut Fuess)

scientific J. Kožíšek 2003

State University of New York, Buffalo, USA (Prof. Philip Coppens)


Technologic Institute of Morelia, Mexico (Dr. Jesús García Díaz)



168

Technische Universitat Munchen (prof. Nuyken)

scientific A.Staško 2003

Liverpool John Moores University (Dr. Morris)

scientific M. Valko 2003

Roosevelt University, Chicago (Prof. Telser)

scientific M. Valko 2003

TCT Vidče, Czech Republic industrial J. Cvengroš 2003

Energoinvestment Zlín, Czech Republic scientific J. Cvengroš 2003

Ciba Grenzach, Germany scientific J. Cvengroš 2003



Valid date

P.Šimon Slovak Chemical Society other 2003 A.Staško Slovak Chemical Society member 2003 J. Cvengroš Slovak Chemical Society member 2003 J. Cvengroš Slovak Society of Chemical Engineers member 2003 J. Reguli Slovak Commision for Chemistry Olympiad member 1999-



Valid date

P.Šimon International Congress on Thermal Analysis and Calorimetry (ICTAC) other 2003

A.Staško American Chemical Society member 2003

S. Biskupič International Society for Theoretical Chemical Physics (Germany) member 2003

S. Biskupič International ESR Society (USA) member 2003 J. Kožíšek International Union of Crystallography, IUCr member 2003 J. Kožíšek European Crystallographic Committee, EEC member 2003 J. Cvengroš Americal Oil Chemist´s Society member 2003



Date / Duration

Dr. K. Brudíková Brno University of Technology Czech Republic January 28-30/3 days

Dr. K. Brudíková Brno University of Technology Czech Republic May 12-13/2 days

Dr. K. Brudíková Brno University of Technology Czech Republic June 1-6/6 days

Prof. L. Omelka Brno University of Technology Czech Republic Apri 14-15/2 days

Prof. Hartmut Fuess Materialwissenschaft, TU Darmstadt Germany 3 days

Prof. Dylan Jayatilaka University of Western Australia, Nedlands Australia 2 days

Prof. Joshua Telser Roosevelt University USA 7 days



Date / Duration

S. Biskupič CESTC Nové Hrady Czech Republic

September 25-28 4 days

M. Breza CESTC Nové Hrady Czech Republic



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M. Ilčin CESTC Nové Hrady Czech Republic


J. Reguli Ostrava University, Int. Conf. on Chemistry Teachers Education,Rožnov pod Radhoštěm

Czech Republic

May 20-22 3 days

E.Klein Rice University, Houston USA 6 months P. Šimon PIRA, Leatherhead UK May 7-11, 5 days

J.Polavka Lublin, 55.Congress of Polish Chem.Soc. Poland September 14-18, 5 days

P. Šimon Hungarian Acad.Sci., Budapest Hungary October 18-21, 4 days J. Kožíšek Cuarto Congreso Nacional, Morelia Mexico November, 14 days J. Kožíšek Charge Density Meeting, Sandbjerg Denmark June, 5 days J. Kožíšek DESY – Hamburg Germany 8 + 5 days J. Kožíšek TU-Darmstadt Germany 3 + 5 + 5 days M. Fronc TU-Darmstadt Germany 5 + 5 days M. Fronc DESY – Hamburg Germany 8 + 5 days P. Skubák Faculty of Mathematics and Natural Sciences,Leiden Netherland 2 months A.Staško TU Darmstadt Germany 15.5. -15.6.2003 S. Biskupič TU Darmstadt Germany 3 days



Zuzana Belaňová Optical properties and thermostability of indeno-fluorantenes – innovative materials for optoelectronics Peter Rapta

Silvia Galková Isolation of phytosterols from plant oils Ján Cvengroš Katarína Genčanská Investigation of vibronic interaction in the transition metals complexes Martin Breza

Martin Gróf Investigation of conformation analysis of push-pull compounds by means of infrared and Raman spectroscopy and quantum chemical calculations Anton Gatial

Martin Hudák Analytical shape of potential hypersurfaces Stanislav Biskupič Lucia Kurucová Induction periods of polyisoprene oxidation Peter Šimon Jozef Malo Lubricants based on chemically modified fat acids Ján Cvengroš, Helena Švajdlenková

EPR investigation of reactive intermediate formation in the irradiated titanium dioxide suspensions Vlasta Brezová

Michal Zalibera The influence of stress factors on the formation of antioxidants and radical scavengers in microorganisms investigated by EPR and UV-Vis spectroscopy

Peter Rapta


Zuzana Cibulková Termooxidation stability of polymer materials Peter Šimon Jana Hajasová Properties of chemically modified fat acids and their esters Ján Cvengroš Teodora Kocsisová Isolation of phytosterols from deodorization condesates Ján Cvengroš

Júlia Pigošová EPR study of photochemical reactions of arylmethane dyes Vlasta Brezová

Martin Vida Conformation analysis and interpretation of vibration spectra of cyclopropylaminomethylene-propanedinitrile and 1-cyclopropylaminoethylidene-propanedi

Anton Gatial

VIII. PUBLICATIONS A. Journals [1] Boča, M., Valko M., Kickelbick G., Ďurík M., Linert W.: Complexes with the new Schiff Base Ligands as a mono- and bis-

Condensation Products of 2-Pyridinecarboxaldehyde-N-Oxide with Diethylenetriamine. Inorg. Chim. Acta 349, 111-122 (2003).

[2] Breza, M., Biskupič S.: On the stability of hydroxo-dilead(II) complex cations. Collect. Czech. Chem. Commun. 68(12), 2377-2385 (2003)

[3] Breza, M., Biskupič, S., Manová, A.: On the structure of lead(II) complexes in aqueous solutions. IV. Binuclear clusters. Polyhedron 22(20), 2863-2867 (2003)

[4] Breza, M.: On non-planarity of cyclotetraphosphazenes. Polyhedron 22(24), 3243-3248 (2003) [5] Breza, M.: "Some comments on ""Jahn-Teller effect in coronene monoanion: A comparative study with” Chem. Physics

291(2), 207 – 212 (2003) [6] Brezová, V., Tarábek, P., Dvoranová, D., Staško, A., Biskupič, S.: EPR study of photoinduced reduction of nitroso

compounds in titanium dioxide suspensions. J. Photochem. Photobiol. A: Chem. 155, 179-198 (2003).


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[7] Brezová, V., Valko, M., Breza, M., Morris, H., Tesler, J., Dvoranová, D., Kaiserová, K., Varečka, Ľ., Mazúr, M., Leibfritz, D.: Role of Radicals and Singlet Oxygen in Photoactivated DNA Cleavage by the Anticancer Drug Camptothecin: An Electron Paramagnetic Resonance Study. J. Phys. Chem. B 107, 2415-2425 (2003).

[8] Burian, M., Omelka, L., Ondrášová, S., Brezová, V.: Nitroxide radicals of some N-Phenyl substituted 1,4- and 1,2-phenylenediamines. Monatsh. Chem. 134, 501-508 (2003).

[9] Díaz, J.G., Kožíšek, J. & Langer V.: Bis(cyanamidonitrato-N)[tris(3,5-dimethylpyrazole)copper(II). Acta Cryst., E59, m241-m243 (2003).

[10] Dunsch,L., P. Rapta, A. Gromov, A. Staško: Spins in [60]fullerene and its C120, C120O and C120OS dimers. An in situ ESR/UV-Vis-NIR spectroelectrochemical study. J. Electroanal. Chem. 547, 35-43 (2003).

[11] Hvastijová, M., Boča, R., Kohout, J., Jäger, L. Císařová, I. & Kožíšek, J.: Cyanamidonitrate-cobalt (II) complexes of pyrazole and imidazole ligands. X-ray structure of [Co(NO2NCN)2(pyrazole)4] and [Co(2-methylimidazole)4](NO2NCN)2. Inorg. Chim. Acta 343, 217-223, (2003).

[12] Krátky, V., Králik, M., Kaszonyi, A., Štolcová, M., Zalibera, Ľ., Mečárová M., Hronec, M.: Reaction pathways and the role of of solvent in the hydrogenation of chlotronitrobenzenes. Coll.Czech.Chem.Comm. 68, 1819-1832, (2003)

[14] Mazúr, M., Valko M., Morris H.: Influence of the variable wall thickness of the sample tube and a quartz Dewar on an EPR signal intensity in a single TE102 and double TE104 rectangular cavities. Anal. Chim. Acta 482, 229-248 (2003).

[15] Papánková, B., Šimon, P., Boča R.: Fitting the heat capacity for spin crossover systems. Solid State Chemistry V - Solid State Phenomena 90-91 (2003) 177-181

[16] Pelikán, P., Omelka L., Brudíková K., Breza, M.: Quantum chemical study of the preferential ortho-addition of phenoxyl radicals to nitroso spin traps J. Mol. Struct. (Theochem) 2003, 624, 251-255.

[17] Polovka, M., Brezová, V., Staško, A.: Antioxidant properties of tea investigated by EPR spectroscopy. Biophys. Chem. 106, 39-56 (2003).

[18] Scorsone, E., Christie S., Persaud K.C., Šimon, P., Kvasnik F.: Fibre-optic evanescent sensing of gaseous ammonia with two forms of a near-infrared dye in comparison to phenol red Sensors and Actuators B90 (2003) 37-45

[19] Šimon, P., Landl M., Breza, M., Kvasnik F.: New NIR dyes for ammonia sensing. Sensors and Actuators B90 (2003) 9-14 [20] Šimon, P., Thomas P.S., Okuliar J. Ray A.: An incremental integral isoconversional method. Determination of activation

parameters Journal of Thermal Analysis and Calorimetry 72 (2003) 867-874 [21] Thomas, P.S., Šimon, P. Ray A.: The effect of thermal history on the morphology of nickel sulphide. Journal of Thermal

Analysis and Calorimetry 72 (2003) 801-809 [22] Vrábel, V., Kožíšek, J., Marchalín, Š.: Diethyl (2’R,4R,4’R)-2-(’-ethoxycarbonyl-2’-thiazolidinyl)-6-methyl-4-(2’’-thienyl)-1,4-

dihydropyridi-ne-3,5-dicarboxylate. Acta Cryst. E59, 1964-1966 (2003). [23] Vrábel, V., Kožíšek, J., Marchalín, Š.: Diethyl 2-methyl-6-(2-thiazolidinyl)-4-(2-thienyl)-1,4-dihydropyridine-3,5-dicarboxylate.

Acta Cryst. E59, 376-377 (2003). [24] Vrábel, V., Marchalín, Š., Kožíšek, J.: Isopropyl 2-methyl-4-(3-nitrophehyl)-5,7-dioxo-4,5,6,7-tetrahydro-1 H-pyrrolo[3,4-

b]pyridine-3-carboxylate. Acta Cryst. E59, 1570-1571 (2003). [25] Williams, C.J., Morris H., Švorec J., Valko M., Moncoľ J., Mazúr, M., Melník M.: A study of copper(II)-carboxylato complexes

with the biological ligands nicotinamide and papaverine. J. Mol. Struct. 659, 53-60 (2003). [26] Mazúr, M., Valko M.: Error sources in quantitative EPR spectroscopy. EPR Newsletter 13 27-27 (2003). [27] Lukeš, V., Cibulková Z., Vlčková S.: On the structural effects of the Head-to-Tail Coupled oligo (3-alkyloligothiophenes) on

their optical properties. Petroleum and Coal, 1-2, 45-48, (2003). [28] Rapta, P., V. Lukeš, K. Matuszná, P. Végh: Experimental and theoretical study of optical and electrochemical properties of

novel alkyl-substituted 2,3-diaza-1,3-butadiene bithienyls. Petroleum and Coal 45, 63-68 (2003) [29] Reguli, J.: Čo majú spoločné žĺtok a saponáty alebo o schopnosti stredoškolských študentov vysvetľovať situácie a javy

z bežného života. In what way egg yolk and tensides are similar – on the ability of secondary school students to explain situations and phenomena from everyday life. Biológia, ekológia, chémia 8 (3), 15-17 (2003).

[30] Reguli, J.: Príprava chemicky gramotných učiteľov chémie. Education of chemically literate chemistry teachers. "Acta Fac. Paed. Univ. Tyrnaviensis, Ser. D, Suppl. 1, 6, 153-158 (2002); ISBN 80-89074-47-2."

[31] Reguli, J.: Úlohy z fyzikálnej chémie. Riešenie a hodnotenie úloh z fyzikálnej chémie. Školské kolo – študijná časť 40. ročníka CHO v kategórii A. Tasks form physical chemistry. Solution and evaluation of the tasks form physical chemistry. School round - study part of the 39th Chemistry Ollympiad. "Chemické rozhľady 4 (3-4), 165-166, 193-197 (2003); ISSN 1335-8391."

[32] Reguli, J.: Úlohy z fyzikálnej chémie I. Riešenie a hodnotenie úloh z fyzikálnej chémie I. Republikové kolo 39. ročníka CHO v kategórii A. Tasks form physical chemistry I. Solution and evaluation of the tasks form physical chemistry I. National round of the 39th Chemistry Ollympiad. "Chemické rozhľady 4 (1), 10-13, 37-40 (2003); ISSN 1335-8391."

B. Conferences [1] Bírová, A., Fodran, P., Hajasová, J., Stacho, D., Cvengroš, J.: Higher Fatty Acids Based Technical Fluids. In: 55. zjazd

chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, p. 684 (2003). [2] Klein E.*, Kovařík P., Spišák R.: Influence of additives on poly(vinyl chloride) thermal degradation. In: 55. zjazd chemických

spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 684 (2003) (Po) [3] Polovka, M.*, Staško, A., Brezová, V., Kogan, G., Šoltés, L.: Antioxidant properties of (1-3)-beta-D-glucan studied by EPR. In:

55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. listy 97, 685 (2003). [4] Belányi, F.*, Havlínová, B., Brezová, V., Čeppan, M., Novotná, M., Jakubíková, Z.: The stability of offset inks on paper upon

ageing. "In: Proceedings of the International Conference ""Chemical Technology of Wood, Pulp and Paper"", September 17.-19.2003, Bratislava, pp. 462-467."

[5] Breza, M.*, Brudíková K.: Ab initio studies of transition metal complexes with bis(methoxycarbimido) amine ligand and its anion. Progress in Coordination and Bioinorganic Chemistry. Monograph series of the International Conference on Coordination Chemistry. Vol. 6. Eds. M. Melnik, A. Sirota, Slovak Technical University Press, Bratislava, pp. 3-8 (2003), ISBN 80-227-1891-2. (Pr)

[6] Brezová, V.*, Pigošová, J., Havlínová, B., Dvoranová, D., Ďurovič, M.: The photodegradation of dyes studied by EPR spectroscopy. "In: Proceedings of the International Conference ""Chemical Technology of Wood, Pulp and Paper"",


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September 17.-19.2003, Bratislava, pp. 348-353." [7] Csomorová, M.*, Havlínová, B., Brezová, V., Ďurovič, M., Mináriková, J.: Degradation resistance of three-layer corrugated

board pronted by flexographic inks. "In: Proceedings of the International Conference ""Chemical Technology of Wood, Pulp and Paper"", September 17.-19.2003, Bratislava, pp. 482-486."

[8] Černáková, L., Kováčik D., Šimor M., Záhoranová A., Černák M., Mazúr, M., Kúš P.: Atmospheric-pressure plasma activation of PP nonwoven textile followed by acrylic acid grafting. 14th Symposium on Application of Plasma Processes, Symposium Proceedings, Eds. P. Šutta, J. Müllerová, R. Bruner, MFF UK Press Centre, Bratislava, Slovakia, Liptovský Ján, January 13-18, 2003, p. 106-107, ISBN 80-8040-195-0.

[9] Diaz J.G.*, Kožíšek J., Albor A.G. & Potočnák I.: Estudio Cristalografico del Comportamiento de las Pseudohalidas en Complejos de Coordinación de Elementos de trasición 3d. Crystallographic Study of Behavior of Pseudohalides Complexes with 3d –Elements Cuarto Congreso Nacional, Libro des Resumes pp. 110-116, November 2003, Morelia, Mexico.

[10] Dunsch, L.*, P. Rapta, N. Schulte, A. D. Schlüter: In situ spectroelectrochemical studies of radical reactions in ladder type oligomers. "In: Proceedings of 203rd ECS International Conference, Paris (France), April 27 - May 2, 2003, ""Mechanistic and synthetic aspects of organic and biological electrochemistry"" (Ed. D. G. Peters, J. Simonet, H. Tanaka) 201-204 (2003). ISBN 1-56677-392-X."

[11] Fáber, R., *Staško A., Nuyken, O.: Synthesis and characterization of new polymers based on flurenylidene-linked conjugated oligo(P-phenylene)s. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. listy 97, 714 (2003).

[12] Fáber, R., *Staško A., Rapta, P., Nuyken, O.: New crosslinkable polymers for organic light emmitting devices (their physicochemical properties). In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. listy 97, 677 (2003).

[13] Fronc, M.*, Kožíšek, J. , Breza, M., Fuess, H., Wu, G. & Paulmann, C.: Charge Density Studies of the blue Protein Model compound. Proc.19 ICCBC, pp. 9-14, 2003, Smolenice-Bratislava.

[14] Kožíšek, J.*, Skubák, P., Fronc, M., Breza, M., Popkov, A., Paulmann, C. & Fuess, H.: Electronic Structure of Ni(II) Complex of the Schiff Base of (S)-N-Benzylproline(2-benzoylphenyl)amide and Glycine. Proc.19 ICCBC, pp. 15-20, 2003, Smolenice-Bratislava.

[15] Mazúr, M.*, Stachová, P., Kleinová, M., Valko, M.: Mn(II) EPR spectroscopy of sol-gel process. In: Monograph Series of the International Conferences on Coordination Chemistry held periodically at Smolenice in Slovakia: Progress in Coordination and Bioinorganic Chemistry, Bratislava 2003. Ed. M. Melnik, A. Sirota, STU Press, pp. 311-316 (2003). ISBN 80-227-1891-2

[16] Mazúr, M., Švorec J., Kleinová M., Valko M.: Cu(II) EPR spectroscopy of sol-gel process. Prog. Coord. Bioinorg. Chem.,Volume 6, 317-322, (Melník M., Sirota A., Eds.) Slovak Technical University Press, Bratislava, 2003. ISSN 1335-308X, ISBN 80-227-1891-2. (Pr)

[17] Skubák, P.*, Fronc, M., Biskupič, S, Breza, M., Kozisek, J., Paulmann, C. & Fuess, H.: Charge Density Study of Tetrakis[mi-acetato-O:O’] dicopper dihydrate. Proc.19 ICCBC, pp. 33-38, 2003, Smolenice-Bratislava.

[18] Stachová, P., Valigura D., Melník M., Koman M., Valko M., Mazúr, M.: Spectral properties of Cu(II) 2-nitrobenzoate and crystal structure of [Cu2(2-NO2bz)4(H2O2)].2H2O. Prog. Coord. Bioinorg. Chem.,Volume 6, 169-174, (Melník M., Sirota A., Eds.) Slovak Technical University Press, Bratislava, 2003. ISSN 1335-308X, ISBN 80-227-1891-2. (Pr)

[19] Švorec, J.*, Kleinová, M., Valko, M., Mazúr, M., Melník, M., Wiliams, C.J., Morris, H., Birdsall, W.J.: Copper(II) chloride complexis with the biologically important ligands creatinine, kinetin, xanthine, and guanine. And EPR and electronic spectroscopy. Prog. Coord. Bioinorg. Chem.,Volume 6, 393-398, (Melník M., Sirota A., Eds.) Slovak Technical University Press, Bratislava, 2003. ISSN 1335-308X, ISBN 80-227-1891-2. (Pr)

[20] Bírová, A., Radovanović, D., Šimon, P., Cvengroš, J.: Comparison of Methyl Esters Low-Temperature Measurements with CFPP Method. In: Proc. 41th Int. Petrol. Conf., 6.-8.10.2003, Bratislava, 10 pgs.

[21] Cvengroš, J., Bírová, A., Cvengroš, M.: Glycerol Refining. In: Proc. 41th Int. Petrol. Conf., 6.-8.10.2003, Bratislava, 8 pp. [22] Kučerík, J*., Kovář J., Pekař M. & Šimon, P.: Evaluation of lignite humic substances oxidation stability by DSC induction

period measurement. In: XVI. Conference on Thermal Analysis and Calorimetry Termanal 2003. Stará Lesná, 8.-10.10.2003, ISBN 80-227-1955-2

[23] Lisý, M., Cvengroš, J., Lutišan, J.: Vapour Pressure of Pure Liquids: Antione and Extended Antoine Equations. In: Proc. 30th Conf. Slovak Soc. Chem. Eng., Tatranské Matliare, 26.-30.5.2003, 5 pgs.

[24] Polavka, J*., Šimon, P, Cvengroš J.: Study of induction periods of biodiesel fuels oxidation by differential thermal analysis. In: XVI. Conference on Thermal Analysis and Calorimetry Termanal 2003. Stará Lesná, 8.-10.10.2003, ISBN 80-227-1955-2, 2 str.

[25] Bírová, A.*, Fodran, P., Hajasová, J., Stacho, D., Cvengroš, J.: Free Fatty Acids Based Technical Fluids. In: Proc. 41th Int. Petrol. Conf., 6.-8.10.2003, Bratislava, 15 pgs.

[26] Bírová, A.*, Radovanovič D., Šimon, P., Cvengroš J.: DSC measurements and low-temperature properties of methyl esters of fatty acids. In: XVI. Conference on Thermal Analysis and Calorimetry Termanal 2003. Stará Lesná, 8.-10.10.2003, ISBN 80-227-1955-2

[27] Šimon, P*., Cibulková Z., Fratričová M.: Isoconversional description of the lengths of induction periods. In: XVI. Conference on Thermal Analysis and Calorimetry Termanal 2003. Stará Lesná, 8.-10.10.2003, ISBN 80-227-1955-2

[28] Šimon, P.*, Cvengroš, J., Schmidt, Š.: Study of Edible Oil Oxidation by DSC. "In: Proc. Int. Conf. ""Food Safety and Quality in Transition Countries"", 23.-27.3.2003, Nitra, 4 pgs."

[29] Reguli, J.*, Linkešová, M.: Katalýza – alternatívny doplnkový vzdelávací materiál. Catalysis – an alternative additional educational material. Pregraduální příprava a postgraduální vzdělávání učitelů chemie. Sborník přednášek z mezinárodní konference 20.-22.5.2003 v Rožnově pod Radhoštěm, str. 207-210. ISBN 80-7042-960-7.

[30] Cvengroš, J.*, Cvengrošová, Z: Príprava koncentrátov sterolov. Preparation of Sterol Concentrates. In: Proc. Int. Conf. TOP 2003, 24.-25.6.2003, Častá-Papiernička, pp. 145-150.

[31] Čertík, M.*, Rapta, P., Breierová, E., Strhanová, K.: Využitie EPR spektroskopie pri sledovaní účinku karotenoidov ako zhášačov radikálov tvorených kvasinkami v stresových podmienkach. Application of EPR spectroscopy for measurement of ability to quench free radicals by yeast's carotenoids produced by yeasts grown under stress. "In: Proceedings of International Conference ""Laboralim 2003"", Banská Bystrica (2003), pp. 129-132"

[32] Reguli, J.: Rozvíjanie kľúčových kompetencií učiteľov chémie. Development of key competencies of chemistry teachers.


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Pregraduální příprava a postgraduální vzdělávání učitelů chemie. Sborník přednášek z mezinárodní konference 20.-22.5.2003 v Rožnově pod Radhoštěm, str. 125-129. ISBN 80-7042-960-7.

[33] Šimon, P*.: Hodnotenie kryštálovej štruktúry pomocou metód termickej analýzy. Evaluation of crystal structure using thermoanalytical methods 3. Odborná konferecia VÚFB. Praha, 12.-13.11.2003,

[34] Šimon, P*., Šimko P., Mráz I. Bariérové vlastnosti polymérnych obalových materiálov. Barrier properties of polymer packaging materials VI. Mezinárodní konference Obalové dny 2003. Brno 18.-19.11.2003

[35] Bírová, A.*, Cvengroš, J.: Biobased Lubricants. In: Book of Abstracts EUROREGIONALE 2003, Dresden, p.25. [36] Bírová, A.*, Cvengroš, J.: Biobased Lubricants. In: Proc. Int. Symp. Green Cheemistry, May 19-22, 2003, Poitiers (France),

p.2-E. [37] Brudíková K.*, Breza, M.: MP2 studies of bis(methoxycarbimido)amine ligand and its anion. Proc. 19th Conf. Coord. Bioinorg.

Chem., June 2-6, Smolenice, p. 76 (2003). (Po) [38] Čertík, M.*, Breierová, E., Rapta, P., Žitňanová, I. Scavenging and antioxidant properties of carotenoids generating by yeasts

stressed by heavy metals. In: Book of Abstracts. p. 42. XXXI Výročná konferencia o kvasinkách, 19.-21.5.2003, Smolenice. [39] Polovka, M.*, Brezová, V., Staško, A.: Antioxidant properties of teas investigated by EPR spectroscopy. Free Radic. Res. 37,

Suppl. 1, 70 (2003). Society for Free Radical Research Europe Meeting 2003, Ioannina, Greece, 26.6.-29.6.2003. [40] Polovka, M.*, Brezová, V., Staško, A.: Antioxidant properties of teas investigated by EPR. In: Book of Abstracts. pp. 136.

Euroregionale 2003, 5. JCF Spring-Symposium, 27.2.-1.3.2003 Dresden. [41] Polovka, M.*, Brezová, V., Staško, A.: Antioxidants and free radicals investigated by means of Electron Paramagnetic

Resonance (EPR). In: Vitamins 2003. Sborník konference. pp. 142. Pardubice 15.-17.9.2003. [42] Rapta, P.*, J. Lukkari, J. Tarábek, J. Kankare, L. Dunsch: In situ ESR/UV-Vis-NIR spectroelectrochemical study of charge

carriers formed under doping of selfassembled ultrathin polyelectrolyte multilayers. In: Book of Abstracts. p. O37, International Workshop on Electrochemistry of Electroactive Materials, WEEM 2003, Bad Herrenalb, Germany, 22-27 July 2003

[43] Dvoranová, D.*, Brezová, V., Valko, M.: Investigation of photochemical transformation of anticancer drug camptothecin. In: Book of Abstracts. pp. 30. Euroregionale 2003, 5. JCF Spring-Symposium, 27.2.-1.3.2003 Dresden.

[44] Breza, M.*, Brudíková K.: Ab initio studies of transition metal complexes with bis(methoxycarbimido) amine ligand and its anion. Proc. 19th Conf. Coord. Bioinorg. Chem., June 2-6, Smolenice , p. 123 (2003). (Pr)

[45] Cibulková, Z.*, Šimon, P., Fratričová M.: Study of induction periods of polymer oxidation by an integral isoconversional method. In: XLVI Zjazd Naukowy Polskiego Towarzystwa Chemicznego i Stowarzyszenia Inzynierow I Technikow Przemyslu Chemicznego,Lublin, 15-18 Sept. 2003.

[46] Čertík, M.*, E. Berierová, P. Rapta, J. Márová, J. Omelková, K. Strhanová: Enviromenbtal stress and carotenogenic yeasts membrane lipids, carotenoid formation and scavenging radicals. In: Book of Abstracts. p. 18. XXXI Výročná konferencia o kvasinkách, 19.-21.5.2003, Smolenice.

[47] Kožíšek, J.*, Skubák, P., Fronc, M., Breza, M. & Fuess, H.: Electronic Structure of some 3d-Coordination Compounds. Cuarto Congreso Nacional, Libro des Resumes p. 61, November 2003, Morelia, Mexico.

[48] Kožíšek, J.*, Skubák, P., Fronc, M., Breza, M., Popkov, A., Paulmann, C. & Fuess, H.: Electronic Structure of Ni(II) Complex of the Schiff Base of (S)-N-Benzylproline(2-benzoylphenyl)amide and Glycine. Charge Density Meeting, O19, June 2003, Sandbjerg Denmark.

[49] Mazúr, M., Stachová, P., Kleinová M., Valko M.: Mn(II) EPR spectroscopy of sol-gel process. 19th International Conference on Coordination and Bioinorganic Chemistry, Smolenice, Slovak Republic, June, 2-6, 2003.

[50] Mazúr, M., Švorec J., Kleinová M., Valko M.: Cu(II) EPR spectroscopy of sol-gel process. 19th International Conference on Coordination and Bioinorganic Chemistry, Smolenice, Slovak Republic, June, 2-6, 2003.

[51] Mazúr, M.: Positive, Negative and Concurrent Lens Effect in magnetic resonance spectroscopy. 18th NMR Valtice, Central Europan NMR discussion groups, Valtice, Czech Republic, April, 28-30, 2003.

[52] Stachová, P., Valigura D., Melník M., Koman M., Valko M., Mazúr, M.: Spectral properties of Cu(II) 2-nitrobenzoate and crystal structure of [Cu2(2-NO2bz)4(H2O2)].2H2O. 19th International Conference on Coordination and Bioinorganic Chemistry, Smolenice, Slovak Republic, June, 2-6, 2003.

[53] Staško, A.*, Polovka, M., Brezová, V.: Antioxidant properties of wine, beer and tea (EPR study). In: Vitamins 2003. Sborník konference. pp. 121. Pardubice 15.-17.9.2003.

[54] Šimon, P*., Cibulková Z., Fratričová M.: Study of induction periods of polymer oxidation by an integral isoconversional method. 42nd IUPAC Microsymposium on Degradation, Stabilization and Recycling of Polymers, Prague, 14-17 July 2003

[55] Švorec, J., Kleinová M., Valko M., Mazúr, M., Melník M., Williams C.J., Morris H., Birdsall W.J.: Copper(II) chloride complexis with the biologically important ligands creatinine, kinetin, xanthine, and guanine. And EPR and electronic spectroscopy. 19th International Conference on Coordination and Bioinorganic Chemistry, Smolenice, Slovak Republic, June, 2-6, 2003.

[56] Tarábek, J.*, P. Rapta, D. Ferse, H.-J. Adler, M. Maumy, L. Dunsch: Spectroelectrochemical and potentiometric studies of functionalised electroactive Polymers. In: Book of Abstracts. p. V8. Symposium anlässlich des 150. Geburtstages von Wilhelm Ostwald-Elektrochemie im 21. Jahrhundert, 11. September, 2003, Meinsberg

[57] Breza, M.*, Brudíková K.: On electronic structure of bis(methoxycarbimido)amine ligand and its anion. CESTC 2003, Sept. 25-28, 2003. Nové Hrady (Czech Republic) (Pr)

Department of Physical Education

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DEPARTMENT OF PHYSICAL EDUCATION

Head of the Department Telephone:++421-7-52495198 Assoc. Prof. Dr. Miroslav Bobrík, PhD. Fax: ++421-7-52493198 E-mail: [email protected]

I. STAFF Assistant Professors: Mgr. Peter Bartok, Dr. Július Fehér, Mgr. Viliam Lendel, PhD., Mgr. Jiřina Moravcová, Dr. Dalma Sochorová, Mgr. Ľuboš Benko, PhD.; Technical Staff: Gabriela Boršányiová;

II. TEACHING AND RESEARCH LABORATORIES: Gym 14x21 m – ground /volleybal, basketball, football/ Two Body Building rooms 15x5 m and 10x5 m

III. TEACHING: Aerobic (2 h) D. Sochorová Kalanethics (2 h) D. Sochorová Harmonic gymnastics (2 h) D. Sochorová Healing gymnastic (2 h) D. Sochorová Athletic sport (2 h) V. Lendel, Ľ. Benko Basketball (2 h) P. Bartok Football (2 h) P. Bartok Handball (2 h) M. Bobrík Body building (2 h) M. Bobrík, P. Bartok, V. Lendel, Ľ. Benko J. Moravcová Swimming (2 h) J. Fehér, Ľ. Benko Canoeing and kayak (4 h) M. Bobrík Volleyball (2 h) J. Moravcová Winter sports camp /skiing/ M. Bobrík, J. Fehér Summer sports camp / M. Bobrík, J. Fehér

IV. RESEARCH PROJECTS: State of Physical and Motor Development of Undergraduates of FCHFT STU in Bratislava. Proportion of body fat on the total weight of the students of FCHFT STU in Bratislava.

V. COOPERATION IN SLOVAKIA: Faculty Physical Education and Sport of the Comenius University, Bratislava; Research Institute of Physical Culture, Bratislava; Institute of History, Slovak Academy of Sciences, Bratislava.

VI. PUBLICATIONS: A. Journals

[1] Bobrík, M.: Námety ku koncepcii telesnej výchovy a športu na STU pred vstupom do EÚ. Thems to conception of physical education and sport at the STU before an admission in the EU. In: Telesná výchova & šport (Physical Education & Sport), roč. XIII, č. 3/2003, s. 5 – 8. ISSN 1335-2245.

B. Conferences [1] Bobrík, M.*: Nová koncepcia telesnej výchovy a športu na STU pred vstupom do Európskej únie. (New conception of physical

education and sport at the STU before an admission in the EU). In: Súčasný stav a vývojové trendy vysokoškolskej telesnej výchovy a športu pred vstupom do Európskej únie (Present state and trends of development in the physical education and sport at Universities before an admission in the EU). Zborník z vedeckej konferencie s medzinárodnou účasťou, Bratislava 2003, s. 5 – 10. ISBN 80-223-1880-9.

[2] Bobrík, M., Lendel, V., Benko, Ľ.: Podiel tuku na celkovej hmotnosti u poslucháčov FCHPT STU v Bratislave.(Proportion of body fat on the total weight of the students at the FCHPT STU in Bratislava). In: Telesná výchova a šport v súčasnej spoločnosti.(Physical education and sport in today society). Vedecké práce zo seminára, Trenčín 2003, s. 15 – 21. ISBN 80-8075-003-3.

[3] Bobrík, M., Lendel, V., Benko, Ľ.: Vysokoškoláci a problém podielu tuku na celkovej hmotnosti. (Students of University and

Department of Physical Education

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problem of fat proportion on total body weight). In: Telesná výchova, šport, výskum na univerzitách (Physical education, Sport, research at the universities). Zborník referátov z medzinárodnej konferencie, Bratislava, 13.-14.11.2003, s. 38-44. ISBN 80-227-1972-2.

[4] Bobrík, M.*: Koncepcia telesnej výchovy a športu na STU pred vstupom do Európskej únie. (Conception of physical education and sport at the STU before an admission in the EU). In: Telesná výchova a šport

v súčasnej spoločnosti.(Physical education and sport in today society). Vedecké práce zo seminára, Trenčín 2003, s. 22 – 26. ISBN 80-8075-003-3.

[5] Bobrík, M.*: Telovýchovná historiografia na Slovensku – kultúrne dedičstvo od macochy? (Sport Historiography in Slovakia – Cultural Heritage Comming from Stepmother? In: Telesná výchova a šport v kultúre spoločnosti. (Physical education and

sport in the cultur of society. Monografický zborník vedeckých a odborných prác. Medzinárodné vedecké sympózium Bratislava 25.-26.9.2003, s. 13-17. ISBN: 80-89075-20-7.

[6] Benko, Ľ.*: Skáče Štefan Holm – analýza kinogramu 234 cm. (Stefan Holm is high jumping – analysis of kinogram 234 cm). In: Telesná výchova, šport, výskum na univerzitách (Physical education, Sport, research at the universities). Zborník referátov z medzinárodnej konferencie, Bratislava, 13.-14.11.2003, s. 18-21. ISBN 80-227-1972-2.

DEPARTMENT OF PLASTICS AND RUBBER

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Head of Department: Telephone: ++421-2-52926 053 Assoc. Prof. Ivan Hudec, PhD Fax: ++421-2-524 93 198


I. STAFF Full Professors: Dušan Bakoš, PhD, DSc; Associate Professors: Ivan Hudec, PhD; Viera Chrástová, PhD; Gabriela Kyselá, PhD; Eugen Špirk, PhD; Assistant Professors : Pavol Alexy, PhD; Research Fellows: Viera Khunová, PhD (Senior Research Fellow); Ľudmila Černáková, PhD; PhD Students: Silvia Hanzelová (since 1.10.2003); Michal Jaššo (since 1. 10. 2002); Zuzana Kramárová (since 1.10.2003); Miroslav Kršiak (until 30.9.2003); Henrich Krump (until 16.9.2003); Lenka Kukolíková (since 1. 10. 2001); Eva Simigová (since 1.10.2003); Barbora Šimková (since 1. 10. 2002) Technical staff: Mária Dočolomanská; Viera Godályová; Mária Pekarovičová; Anna Tatarková


A. Teaching laboratories: Laboratory of Polymer Synthesis Laboratory of Polymer Solutions Laboratory of Polymer Processing Laboratory of Polymer Testing

B. Research laboratories: Laboratory of Polymer Synthesis Laboratory of Polymer Solutions Laboratory of Polymer Modification Laboratory of Thermal Analysis Laboratory of Polymer Rheology Laboratory of Electron Microscopy Laboratory of Polymer Processing and Estimation of its Properties Laboratory of Biomaterials


5. semester (Bc) Macromolecular Chemistry 2/0/0 Chrástová Corrosion and Material Surface

Treatment 2/0/2 Chovancová, Špirk

6. semester (Bc) Technology of Materials 2/0/0 Hudec, Marcinčin, Majling Semestral Project 0/4/0 Production, Properties and

Processing of Plastics 2/0/0 Hudec (for students of Faculty of

Architecture) 1. semester (MSc) Polymer Physics 2/2/0 Chodák Colloids and Interfaces 2/1/0 Bakoš, Reháková Macromolecular Chemistry II. 2/1/0 Chrástová Production and Processing of

Plastics

3/0/0 Hudec

1. semester (MSc) Production and Processing of Rubber 3/2/0 Kyselá Laboratory from Macromolecular

Chemistry 0/0/8 Černáková


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2. semester (MSc) Additives for Plastics 2/0/0 Hudec Methods of Polymer Characterisation 2/0/0 Černáková Biotechnological Polymers 2/0/0 Bakoš Design of Experiments 1/1/0 Alexy 2. semester (MSc) Laboratory from Production of

Polymers 0/0/8 Alexy, Kyselá

3. semester (MSc) Polymer Processing 3/1/0 Špirk Polymer Blends and Composites 2/0/0 Khunová Polymer Recycling and Waste

Disposal 2/0/0 Hudec, Khunová, Špirk

Polymer Testing 0/2/0 Alexy 3. semester (MSc) Laboratory from Processing of

Polymers 0/0/10 Alexy, Hudec

4. semester (MSc) Diploma work 0/0/27


A. VEGA Project No 1/0059/03, Study of Structure and Properties of Crosslinked Polymers (Gabriela Kyselá).

The project is focused on the curing of polymers and copolymers during their preparation in the presence of multifunctional monomers and using the suitable post-polymerization reactions, too. The curing of elastomers is interesting in the application of non-harmful sulfur curing systems, based on the phosphoric accelerators and their combinations with thiazoles, respectively. The experiments are predominantly oriented on the researching of the optimal composition of accelerate systems, as well as, on the connection of the network structure of crosslinked materials and their age resistance and the level of the retaining of original physical-mechanical properties, too. Also, the crosslinking reactions are studied in the course of two stage seeded semi-continuous starved emulsion polymerization of styrene and butylacrylate in the presence of N-methylol acrylamide. Partially crosslinked latexes with core-shell particles are used for formulation of ecological paints. The influence of polymerization strategy and crosslinking reaction on the film - forming properties of modified dispersions are investigated..

Project duration: from 01.01.2003 to 31.12.2005 B. VEGA Project No 1/0283/03, New Types Blends and Composites Materials Containing Biodegradable

Polymers and Fillers (Ivan Hudec). The project is aimed on the investigation of polymer blends and composite materials based on biodegradable polymers and particulate fillers. The main research and experimental efforts are focused on chemical and physical modification of thermoplastic, elastomeric and crosslinked multy-phase polymer materials by changing morphological structure and interphase interactions on polymer/polymer and polymer/filler interface. The selection of the polymer matrix and modification methods are oriented on the new achievements which enables to reveal relations between composition, structure and properties of studied multiphase polymer blends and composites.


C. GER Project No 17/2001, Modification of Reinforcing Materials for Rubber Articles (Ivan Hudec). Development of new technologies and procedures for surface modification of materials for rubber articles, using applications of plasma-chemical methods. Preparation of new types of biodegradable textile reinforcing materials based on polyvinylalcohol, their chemical and physical modification with the aim to obtain advantageneous physical-mechanical properties and required adhesion to rubber. Preparation of new rubber blends for warp applications in combination with textile and steel cords, including the application of new and advanced types of elastomers.


D. WHEYPOL - Project No GRD 2-2000-30385, Dairy Industry Waste as Source for Sustainable Polymeric Material Production (Dušan Bakoš).

The aim of the European procect is the preparation of biodegradable polyhydroxybuthylene from whey (waste from milk industry) by biotechnological way. The cooperation of STU in this project is focused on investigation of blending PHB with other biodegradable polymers (e.g. polyethylene oxide), and investigation of various modes of compatibilization, as well as investigating the possibility of blending PHB with thermoplastic starch. Determination of ultimate properties of prepared blends with PHB matrix is aimed especially to improved toughness of the material.


E. Project No 2-3-5 CHN, New Biomaterials Based on Chitosan Complexes (Dušan Bakoš). Target of the project is complexation of natural polymers to set-up a new tissue-engineered multi-functional composite products that are successful in three-dimensional tissue regeneration as being biologically active, biodegradable, heterogenous, anisotropic structures. The research activity will be based on highly innovative technological processes and biopolymers (chitosan, hyaluronan and starch). Special nano-technologies for natural polysacharide-based polymers will be used to optimise the materials


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morphological development and consequent mechanical and degradation behaviour and to tailor their in vivo performances.



A. SOCRATES - ERASMUS (Eugen Špirk) Bilateral Agreement for the Academic Year 2001/2006, SOCRATES Program, section for higher education ERASMUS, Between Slovak Technical University Bratislava - Martin Luther University Halle-Wittenberg


VI. COOPERATION



Duration

Rubber Research Institute Matador, a.s., Púchov

Surface modification of reinforcing materials for tire construction by plasma

Rubber Research Institute Matador, a.s. Púchov

Modification of traction properties of tires

Research Institute of Processing and Application of Plastics, VUSAPL a.s., Nitra

New types of fillers and reinforcing materials for plastics

LEONI Slovakia, Ltd., Trenčianska Teplá - Dobrá

PVC blends for cables

VIPOTEST, LtD., Partizánske Rheology of rubbers and rubber mixtures

PLASTIKA, a.s., Nitra Technological centrum for processing of plastics



Duration

Martin Luther University of Halle-Wittenberg, Institute of Materials Science, Halle, Germany

Modification of reinforcing materials for rubber articles

Radusch Hans-Joachim, professor, Gesauer Str., Halle-Wittenberg, D-06099 Halle(Saale), Germany

since 2002

Technical University of Szczecin, Institute of Material Engineering, Szczecin, Poland

Chemical and physical modification of polymers

Tartakowski Zenon, professor,al.Piastow č. 19, Szczecin, Poland

since 1996

Clinica Puerta de Hierro, Cirugia Exoerimental, Madrin, Spain

Chemical modification and biocompatibility, testing of collagen membranes.

Herrero Eduardo, doctor, Hospital Puerto de Hierro, Madrid, Spain

since 1996

Institute of Macromoleculare Chemistry, Academy of Science of the Czech Republic, Prague, Czech Rep.

Polymer nanocomposites Kelnar Ivan, senior research fellow, Academy of Science, Praque, Czech Republic

since 2001

International Clinic for Neo-Organs, Roma, Italy

Biomaterials development. Letič Gavrilovič Anka, professor, International Clinic for Neo-Organs, Roma, Italy

since1999


178

The Manchester Metropolitan University, Faculty of Science and Engineering, Manchester, UK

Reactive processing of particulate polymer composites.

Liauw C.M., senior research fellow, Chester str., Manchester M1 5GD, UK

since 1996

University of Minho, Department of Polymer Engineering, Guimaräes, Portugal

Development of biomaterials, polymer processing.

Reis Rui, professor, University of Minho, Guimaräes, Portugal since 1999

University of Pisa, Department of Chemistry and Industrial Chemistry, Pisa, Italy

Biodegradable polymers Chiellini Emo, professor, Via Risorgimento 35, 56126 Pisa, Italy

since 1999

Department of Macromolecular Science, Fudan University, Shanghai,China

New biomaterials based on chitosan complexes

Wei Zhong, associate professor, 220 Handan Road, Shanghai 200433, P.R. China

since 2002

Institute of Materials Technology, Poznaň University of Technology, Poznaň, Poland

Testing of adhesion properties of reinforcing materials to rubber

Szostak Marek, associate professor, ul. Piotrowo 3, 61-138 Poznaň, Poland

since 2001



Valid date

Bakoš Dušan European Biomaterial Society member 1995 - Špirk Eugen Plasty a kaučuk member 1990



Date / Duration

Ducháček, V. Institute of Chemical Technology, Faculty of Chemical Technology, Department of Polymers, Prague

Czech Republic


Epacher, E. Research Laboratory of Materials and Environmental Chemistry, Chemical Research Center, Hungarian Academy of Sciences, Budapest

Hungary October 2003 (2 days)

Pukánszky, B. Research Laboratory of Material and Environmental Chemistry, Chemical Research Center, Hungarian Academy of Sciences, Budapest

Hungary October 2003 (2 days)

Radusch, H. J. Institute of Material Science Martin-Luther University Halle-Wittenberg, Halle Germany October 2003

(3 days)

Roda, J. Institute of Chemical Technology, Faculty of Chemical Technology, Department of Polymers, Prague

Czech Republic


Roslaniec, Z. Institute of Materials Science and Engineering, Technical University, Szczecin Poland October 2003

(3 days)

Rzymski, W .M. Institute of Polymers, Technical University, Lódž Poland October 2003

(3 days)

Šimoník, J. Faculty of Technology, Tomas Bata University, Zlín Czech Republic


Szostak, M. Institute of Materials Technology, Poznaň University of Technology, Poznaň Poland October 2003

(3 days)

Sperber, V. E. University of Kassel Germany October 2003 (3 days)

Wei, Zhong Department of Macromolecular Science, Fudan University, Shangai China

November - December 2003

(14 days)

Illisch, S. Institute of Material Science, Martin-Luther University Halle-Wittenberg, Halle Germany October 2003

(3 days)

Betchev, Ch. Department of Physics, University of Chemical Technology and Metallurgy, Sofia Bulgaria October 2003

(3 days)


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Date / Duration

Khunova, V. Manchester Metropolitan University, Manchester, Socrates Exchange Teachers Mobility UK June 2003 (10 days)

Khunova, V. International Workshop on Processing and Characterisation of Nanomaterials, Warsaw Poland October 2003

(5 days)

Khunova, V. International Conference NANO 03, Brno Czech Republic


Khunova, V. DSM Scientific Meeting "Functional Coatings", Vaalsbroek Holand December 2003

(3 days)

Hudec, I., Alexy, P. 4th International Symposium on "Materials from Renewable Resources", Erfurt Germany September 2003

(4days) Hudec, I., Krump, H.

International Conference ELASTOMERS 2003, Science for Industry, Poltusk Poland June 2003

(4 days)

Černáková, Ľ. International Conference XXVI ICPIG, Greifswald University, Greifswald Germany July 2003 (6 days)

Šimková, B. International Conference PLASTKO 2003, Tomas Bata University, Zlín


Alexy, P., Krump, H., Špirk, E.

International Conference Deformation and Fracture of Polymers, Martin Luther University Halle -Wittenberg, Merseburg

Germany June 2003 (5 days)

Hudec, I., Jaššo, M.

International Conference Deformation and Fracture of Polymers, Martin Luther University Halle -Wittenberg, Merseburg

Germany June 2003 (4 days)



Amir, I. The surface plasma-chemical treatment of steel reinforcing materials for tire construction Jaššo, M.

Bariaková, L. The study of enzymatic degradation of membranes from biopolymers Kukolíková, L.

Galandová, J. The study of transporte properties of complex membrane from biopolymers Bakoš, D.

Nahálková, A. The influence of fillers on the stability of polyvinyl alcohol Alexy, P. Szabová, R. The plasma chemical treatment of woven textiles for tire construction Krump, H.


Hanzelová, S. Study of polyvinyl alcohol degradation Alexy, P.

Hronkovič, J. The influence of poly-cis- isoprene modification on the properties of its blends and vulcanisates Kyselá, G.

Chlebcová, M. The rheological properties of rubber blends Špirk, E. Keratová, V. Modification and properties of biodegradable polymer blends Chodák, I.

Mulinková, K. The influence of crosslinking on the properties of modified poly styrene/poly(butyl acrylate) dispersions Chrástová, V.

Olejníková, K. The modification of traction properties of treads for sports tires Špirk, E. Ondrušová, P. The influence of modification on the properties of nanocomposites Khunová, V.

Rumanovská, L. The study of properties of polyvinyl alcohol fibres modified with collagene hydrolyzate Alexy, P.

Simigová, E. Magnetic composites for intelligent tires Hudec, I. Srnečková, Z. The grafting of acrylic acid onto polypropylene Černáková, Ľ.

Števiar, M. The influence of surface treatment of reinforcing materials on their adhesion to rubber Hudec, I.

Víghová, A. The study of complexation of biopolymers for advacement of resortable matrix Bakoš, D.


Hanzelová, S. Structure and properties of compex biomaterials for tissue engineering Bakoš, D.

Jaššo, M. Influence of plasma treatment on the properties of reinforcing materials for tire construction Hudec, I.

Kramárová, Z. Utlisation of biopolymers as fillers in rubber blends Spirk, E.


180

Kršiak, M. Utilisation of collagen hydrolysate in polymer blends Bakoš, D. Krump, H.. Surface treatment of reinforcing materials for tire construction Hudec, I.

Kukolíková, L. Biomaterials based on polyelectrolyte complexes focused on chitosan and glycosamino-glycanes Bakoš, D.

Simigová, E. High - loaded composite materials with magnetic active filler Hudec, I. Šimková, B. The study of processing properties of polyvinyl alcohol blends Bakoš, D.


Khunova, V. Modification of composite materials based on polyolefines and particulate inorganic fillers Bakoš, D.


[1] Alexy, P., Bakoš, D., Crkoňová, G.,Kramárová, Z., Hoffmann, J., Julinová, M., Chiellini, E., Cinelli, P.: Poly(vinyl alcohol)-collagen hydrolysate thermoplastic blends:II. Water penetration and biodegradability of melt extruded films. Polymer testing, 22 (7), 2003, p.811-818

[2] Alexy, P., Bakoš, D., Hanzelová, S., Kukolíková, L., Kupec, J., Charvátová, K., Chiellini, E., Cinelli, P.: Poly(vinyl alcohol) - collagen hydrolysate thermoplastic blends: I. Experimental design optimisation and biodegradation behaviour Poly(vinyl alcohol) - collagen hydrolysate thermoplastic blends: I. Experimental design optimisation and biodegradation behaviour. Polymer testing, 22(7), 2003, p.801-809

[3] Hoffmann, J., Řezníčková, I., Kozáková, J., Ružička, J., Alexy, P., Bakoš, D., Precnerová, L.: Assessing biodegradability of plastics based on poly(vinyl alcohol) and protein wastes. Polymer degradation and stability, 79 (3), 2003, pp. 511-519

[4] Chiellini, E., Cinelli, P., Ilieva, V.I., Ceccanti, A., Alexy, P., Bakoš, D.: Biodegradable hybdrid polymer films based on poly (vinyl alcohol) and collagen hydrolyzate. Macromol. Symp., 197(1), 2003,p. 125-132

[5] Košíková, B., Alexy, P., Gregorová, A.: Use of lignin derived from wood pulping as environmentally desirable component of composite rubber materials Wood research, 48 (1/2), 2003, p.62-67

[6] Lacík, I., Šnauková, R., Šimková, B., Hanzelová, S., Alexy, P.: Aqueous phase size exclusion chromatography of polyvinylalcohols of different degrees of hydrolysis. Macromol. Symp., 197(1), 2003, p. 101-114

[7] Liauw, C. M., Khunová, V., Lees, G. C. and Rothon, R. N.: Reactively Processed High Performance Impact Modified Polypropylene/Magnesium Hydroxide Composites:- Interfacial Studies. Macrom. Symp. 194, 191-200, (2003)

[8] Sláma, J., Dosoudil,R., Vicen, R., Grusková, A., Olah, V., Hudec, I.,Ušák, E.: Frequency dispersion of permeability in ferrite polymer composites. Journal of Magnetism and Magnetic Materials, 254-255,(2003), 195-197

[9] Hoffman, J., Řezníčková, I., Rozsypalová, L., Julinová, M., Alexy, P., Bakoš, D.: Biorozložitelnost vodorozpustných plastových folií na bázi polyvinylalkoholu v aerobním vodním prostředí. Aplikace respirometrického a Zahn-Wellensova testu Aerobic biodegradability of water-soluble plastic films based on polyvinyl alcohol. Aplication of respirometric and Zahn-Welles test. Plasty a kaučuk, 10, 2003, s. 295-302

[10] Kyselá, G., Kolláriková, G., Urbanovská, M.: Vplyv bis-diizopropyltiofosforyldisulfidu na štruktúru priečnych väzieb v sírnych vulkanizátoch prírodného kaučuku. Influence of bis(diisopropyl)thiophosphoryl disulfide on network structure of natural rubber sulfur vulcanizates. Plasty a kaučuk 40(11), 327-332 (2003)

[11] Janypka, P., Mlčúch, M., Gažo P., Šuriová, V., Ďuriš, Š., Hudec, I., Szostak, M.: Adhesion properties of steel reinforcement materials. Tire Technology International 03ˇ, (2003), 140-145

[12] Janypka, P., Mlčúch, M., Gažo P., Šuriová, V., Ďuriš, Š., Hudec, I., Szostak, M.: The adhesion properties of steel reinforcement materials. Plasty a kaučuk,40, (2003),100-106

[13] Bakoš, D., Koller, J.: Biosyntetické implantáty pre riadenú rekonštrukciu kože. Biosynthetic skin substitutes for controled skin reconstruction. DERMA, III, 2, 2003, s. 16-23

[14] Hudec, J., Bakoš, D., Brestič, M., Kobida, Ľ.: Polyamide biosynthesis stimulators accelerate accumulation of cadmium in grains of spring barley. Biologia, 58, (2003), No 12, 81-86

[15] Markovičová, L., Chalupová, M., Simigová, E.: Magnetické kompozity s polymérnou matricou. Magnetic Composites with Polymeric Matrix Materiálové inžinierstvo, 10, (2003), No.4, 55-62

B. Conferences [1] Jaššo, M.*, Hudec, I., Krump, H., Kováčik, D., Šimor, M.: Surface Modification of Polyester Monofilaments by Atmospheric -

Pressure Nitrogen Plasma Proceedings of the XIV-thSymposium on Application of Plasma Processes SAPP XIV, January 13-18, 2003, Liptovský Mikuláš, s. 156-159, ISBN 80-8040-195-0 , (Po)

[2] Bakoš, D., Kukolíková, L., Alexy, P.: Chitosan Lactate/Hyaluronan Scaffold for Tissue Engineering. 18th European Conference on Biomaterials, Stuttgard, Germany, October 1-4, 2002, Proceedings (CD), Lecture Section L 17

[3] Černáková, Ľ., Kováčik, D*., Šimor, M., Zahoranová, A., Černák, M., Mazúr, M., Kúš, P.: Atmospheric - Pressure Plasma Activation of PP Nonwoven Textile followed by Acrylic Acid Grafting. Atmospheric - Pressure Plasma Activation of PP Nonwoven Textile followed by Acrylic Acid Grafting Proc.14th Symposium on Application of Plasma Processes, Liptovský Mikuláš (Slovak Republic), January 13-18, (2003). pp.106-107. ISBN 80-8040-195-0. (Pr)

[4] Jaššo, M.*, Hudec, I., Krump, H., Kováčik, D., Černák, M., Janypka, P.: Atmospheric plasma surfacemodifications of polyesters cordsfor improvement of rubber adhesion. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy, 97, 2003, p. 713. (Pr)

[5] Gregorová, A.*, Košíková, B., Alexy, P., Ďuračka, M.: Possibility of thermo-oxidative Stabilization of SBR Blends by Using Lignin as a Natural Filler. International Conference Polymer Materials, oct. 29-30, 2003, Bratislava, proceedings, p. 123-128, ISBN 80-227-1959-5 (Po)

[6] Jaššo, M.*, Hudec, I., Krump, H., Jakubíková, Z.,Kováčik, D., Sťahel, P., Janypka, P., Funke, Z., Široký, J.: Evaluation of


- 181 -

surface properties of reinforcement materials and Rubber blends. International Conference Polymer Materials, oct. 29-30, 2003, Bratislava, Proceedings, p. 46, on CD p. 209-213, ISBN 80-227-1959-5 (Po)

[7] Jaššo, M.*,Hudec, I., Krump, H., Alexy, P., Široký, J.,Kováčik, D., Černák, M.: The influence of plasma grafting on properties of polyester cords. Slovak RubberConference 2003, 21.-22.máj 2003, Púchov, Proceedings, s. 53, on CD- SRC03-PO- 0170, s.1-6, ISBN 80-968099-8-9 (Po)

[8] Julinová,M.*, Řezníčková, I., Hoffman, J., Růžička, J., Alexy, P., Bakoš, D.: New possibilities in Production of Biodegradable Polymers Utilising Dechromated Leather Wastes. "ECCE 4th European Congress of Chemical engineering, ""Chemical Engineering a Tool for Progress, 21-25 sept. 2003, Granada, Spain, Topic 4 Abstracts, 2 pages. ISBN 84-88233-26-4 (Po)"

[9] Khunová, V., Kelnar, I., Jesenák K.: Polypropylene/clay Nanocomposites: Influence of Reactive Modifiers on Structure and Interphase Development. In: International Conference NANO '03, Proceedings, October 21-23, 2003, Brno, Czech Republic, ISBN 80-214-2486-9, pp.115-120

[10] Kramárová, Z.*, Špirk, E., Chodák, I., Hudec, I., Alexy, P., Kršiak, M.: Influence of natural fillers on properties of rubber blends and vulcanizates. 15. ročník medzinárodnej konferencie SRC 2003, 21.-22.máj 2003, Púchov, Zorník prednášok, s. 54, on CD -SRC-PO-0220, s.1-10, ISBN 80-968099-8-9 (Po)

[11] Kukolíková, L.*, Bakoš, D., Alexy, P.: Chitosan-hyaluronan Polymeric Scaffolds for Tissue Engineering. International Conference Polymer Materials, oct. 29-30, 2003, Bratislava, proceedings, p. 130-140, ISBN 80-227-1959-5 (Po)

[12] Šimková, B.*, Hanzelová, S., Alexy, P., Bakoš, D., Nahálková, A., Lacík, I.: Degradation of PVAL during extrusion and possibility of its stabilization. International Conference Polymer Materials, oct. 29-30, 2003, Bratislava, proceedings, p. 199-205, ISBN 80-227-1959-5 (Po)

[13] Šustek, J., Kyselá, G., Kosár, K., Balko, J.: Polyisoprene rubber with improved green strength.Polyisoprene rubber with improved green strength. Proc. 15th International Slovak Rubber Conference 2003 (Púchov), Slovenská republika.May 21-22, 2003. Ed. Matador, a.s. Púchov, p.55 + CD POSTER SRC03-PO-0400. ISBN 80-968099-8-9

[14] Ackerman, E.*, Yanwei, C., Hudec, I.: Intumescent polymeric materials and theirapplication in firestopping. International Conference Polymer Materials, oct. 29-30, 2003, Bratislava, Proceedings, p.19, on CD p. 72 - 20s., ISBN 80-227-1959-5 (Pr)

[15] Bakoš, D.*, Koller, J., Kukolíková, L., Alexy, P.: Úloha polymérov v tkanivovom inžinierstve. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy, 97, 2003, p. 715-716.

[16] Bakoš, D., Kukolíková, L., Harvanová, D.: Bioreactors and bioprocessing for tissue engineering. In: 30th Intern. Conf. Slovak Chemical Engineering, Tatranské Matliare, May 26-30, (2003), pp. 7, ISBN 80-227-1889-0, Plen.predn.

[17] Černáková, Ľ*., Chrástová, V., Volfová, P., Prónayová, P.: Funkcionalizované PS/PBA disperzie s časticami jadro-obal (Functionalized Dispersions with Core-Shell Particles). Functionalized Dispersions with Core-Shell Particles In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 715, (2003). (Pr)

[18] Hanzelová, S.*, Šimková, B., Fuleová, V., Nahálková, A., Alexy, P.: Vplyv stupňa hydrolýzy a koncentrácie octanu sodného na degradáciu polyvinylalkoholu. Influence of degree of hydrolysis and concentration of sodium acetate on degradation of PVAL. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy, 97, 2003, p. 717 (Pr).

[19] Hudec, I.*, Krump, H., Jaššo, M., Dayss, E., Janypka, P., Šuryová, V., Šimor, M.: Surface modification of reinforcing materials by atmospheric-pressure plasma treatment, Elastomers 2003, Science for Industry, 12-13 June 2003, Pultusk, Proceedings on CD, K - 2, s. 29-30, full text 1-16, (Pr)

[20] Hudec, I.*,Krump, H., Szostak, M., Skorel, K., Janypka, P., Šuriová, V.: Comparison of evaluation methods of adhesion of reinforcing materials to rubber. 15. ročník medzinárodnej konferencie SRC 2003, 21.-22.máj 2003, Púchov, Proceedings, s. 41, na CD - SRC03-PA-140, s. 1-7, ISBN 80-968099-8-9 (Pr)

[21] Kelnar, I., Kotek, J., Kaprálková, L., Khunová, V.: Melt Intercalated Polyamide Nanocomposites with Improved Balance of properties. International Conference NANO '03, Proceedings, October 21-23, 2003, Brno, Czech Republic, ISBN 80-214-2486-9, pp.135-140

[22] Khunová, V.: Maleinisation of Polypropylene Waste in Solid Phase New possibilities in Production of Biodegradable Polymers Utilising Dechromated Leather Wastes In: TOP 2003, Technique of Environment Protection Focused on Waste Utilisation, pp. 353-357, June 24-25, Častá - Papiernička, ISBN 80-227-1898-X

[23] Khunová, V., Liauw C.M., Kelnar I.: Reactive Melt Processing of Nano-structured Polyolefine Matrix Composites International Workshop on Processing and Characterisation of Nanomaterials, October 8-10, 2003, Warsaw, Poland, pp. 1-8 on CD

[23] Kolláriková, G.*, Lathová, E., Lath, D., Chorvát, D., Gemeiner, P., Vikartovská, A., Bučko, M., Štrbák, V., Benický, J., Najvirtová, M., Bačová, Z., Alexy, P., Lacík, I.: Príprava a charakterizácia polymérnych mikrokapsúl pre biotechnologické a biolekárske účely. Preparation and characterisation of polymer microcapsules for biotechnological and biomedical applications. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy, 97, 2003, p. 725. (Pr)

[24] Kramárová, Z., Alexy, P.*, Hudec, I., Špirk, E., Chodák, I., Ďuračka, M., Kršiak, M.: Influence of natural cornstarch and collagen hydrolysate on properties of SBR blends and vulcanisates. "In: 4th International Symposium ""Materials from Renewable Resources"", 11.-12. september 2003,Erfurt, Proceeding p. 57, full text on CD - S 2-3, p.1-6 (Pr)"

[25] Kramárová, Z., Kršiak, M.*, Špirk, E., Chodák, I., Alexy, P., Bugaj, P.: Vplyv prírodných plnív na vlastnosti gumárenských zmesí a vulkanizátov. Influence of natural fillers on properties of rubber blends and vulcanisates. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy, 97, 2003, p. 722. (Pr)

[26] Kršiak, M.*, Alexy, P., Hudec, I., Bakoš, D., Chodák, I., Kramárová, Z.: PVAL vlákna modifikované hydrolyzátom kolagénu. PVAL fibres modified with collagen hydrolysate. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy, 97, 2003, p. 712. (Pr)

[27] Liauw, C. M., Khunová, V., Lees, G. C. and Rothon R. N.: Interfacial Effects in Polypropylene Block Copolymer/Magnesium Hydroxide Composites Reactively Processed with 1,3-Phenylene Dimaleimide. Society of Mining Engineers (SME) In: Annual Meeting and Exhibit, February 24-26th, 2003, pp. 121-138, ISBN 0-87335-228-9, Cincinnati Convention Center, Ohio, USA.

[28] Šimková, B.*, Hanzelová, S., Lacík, I., Bakoš, D., Alexy, P.: Možnosti sledovania zmien molekulovej hmotnosti PVAL viskozimetricky v nevodnom prostredí Possibility of measurement of changes in molecular weight of PVAL using nonwater viscosimetry. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy, 97, 2003, p. 712. (Pr)

[29] Kramárová, Z.*, Špirk, E., Chodák, I., Alexy, P., Hudec, I., Kršiak, M., Ďuračka, M.: Natural Polymers as a Fillers for Rubber


182

Blends. International Conference Polymer Materials, oct. 29-30, 2003, Bratislava, proceedings, p. 170-174, ISBN 80-227-1959-5 (Po)

[30] Khunová, V.: Polymérne nanokompozity. Polymer Nanocomposites. International conference NANO/SME/IST, 17-18 marec 2003, pp. 11-12, Smolenice, SK

[31] Kršiak, M.*, Alexy, P., Hudec, I., Janypka ,P., Bakoš, D., Kramárová, Z.: Nové typy vysokomodulových PVAL vlákien. New types of high modulus PVAL fibres. 15. ročník medzinárodnej konferencie SRC 2003, 21.-22.máj 2003, Púchov, Zorník prednášok, s. 28, na CD -SRC 03-PA-0240, s.1-4 ISBN 80-968099-8-9 (Pr)

[32] Krump, H.*, Hudec, I., Dayss E., Janypka, P., Černák, M.: Surface modification of PES reinforcing materials by atmospheric plasma treatment. 15. ročník medzinárodnej konferencie SRC 2003, 21.-22.máj 2003, Púchov, Proceedings, s. 30, na CD - SRC03-PA-0250, s.1-7, ISBN 80-968099-8-9 (Pr)

[33] Černáková, Ľ*., Kováčik, D., Černák, M., Hudec, I., Kozánková, J.: Surface Grafting of Acrylic Acid onto Polypropylene Foil. In: Proc. Int. conf. Polymer materials, Bratislava, October 29-30, 2003, Ed.: Alexy P., STU Bratislava, 2003. p. 45. ISBN 80-227-1959-5

[34] Černáková, Ľ*., Kováčik, D., Zahoranová, A., Kozánková, J., Hudec, I.: Modification of Polypropylene Surface by Grafting with Acrylic Acid. Proc. 18th Bratislava International Conference on Modified Polymers, Stará Lesná, October 5-8, (2003). pp.52. ISBN 80-968433-2-X. (Po)

[35] Hoffmann, J.*, Julinová, M., Alexy, P., Bakoš, D.: Employing Wastes for Producing Biodegradable Plastics Based on Polyvinyl Alcohol Ninth International Waste Management and Landfill Symposium, 6-10, oct., Sardinia, Abstracts, p. 578 (Po)

[36] Kolláriková, G.*, Lathová, E., Lath, D., Chorvát, D., Gemeiner, P., Vikartovská, A., Bučko, M., Štrbák, V., Benický, J., Bačová, Z., Alexy, P., Lacík, I.: Encapsulation of the bioactive substances in microcapsules based on polyelectrolyte complexation. 18th Bratislava International Conference on Modified Polymers ModPol2003, Oct.5-8 2003, Stara Lesna, High Tatras, proceedings p.71 ISBN 80-968433-2-X(Po)

[37] Šustek, J., Kyselá, G., Kosár, K.: Vlastnosti vulkanizátov modifikovaného polyizoprénu. Properties of modified polyisoprene vulcanizates. International Conference Polymer materials, Bratislava, October 29-30, (2003), ISBN 80-227-1959-5 (Po)

[38] Volfová, P*., Chrástová, V., Černáková, Ľ.: Properties of Crosslinked Polystyrene/Poly(Butylacrylate) Films Functionalized with N-Methylol Acrylamide. Proc. International Conference Polymer materials, Bratislava, October 29-30, (2003). pp. 44, ISBN 80-227-1959-5. (Po)

[39] Gregorová, A.*, Košíková, B., Alexy, P., Ďuračka, M.: nfluence of Lignin on Properties of Model Rubber Blends. "4th International Symposium ""Materials from Renewable Resources"", 11.-12. september 2003,Erfurt, Proceeding p. 96 (Pr)"

[40] Kelnar, I., Kotek, J., Kaprálková, L., Khunová, V.: Melt Intercalated Polyamide Nanocomposites with Improved Balance of properties. International Conference NANO '03, October 21-23, 2003, Brno, Czech Republic, ISBN 80-214-2486-9, p. 35

[41] Khunová, V., Kelnar, I., Jesenák K.: Polypropylene/clay Nanocomposites: Influence of Reactive Modifiers on Structure and Interphase Development. International Conference NANO '03, October 21-23, 2003, Brno, Czech Republic, ISBN 80-214-2486-9, p. 32

[42] Bakoš, D.: Biomaterials based on natural polymers for tissue engineering University Darmstadt, Darmstadt, May 4, (2003) [43] Bakoš, D., Báleš, V.: University education of technology - from tradition to sustainable development. Int.Conf. WPP 2003,

Bratislava, September 17-19, (2003), Plen.predn. [44] Hudec, I*., Špirk, E.: An Overwiew of Research Projects on the Department of Plastics and Rubber. International Conference

Polymer Materials, october 29-30, 2003, Bratislava (Pr), [45] Janypka, P.*, Mlčúch, M., Gažo P., Šuriová, V., Ďuriš, Š., Hudec, I., Szostak, M.: Adhesion properties of steel reinforcement

materials. The 3rd European Conference for Tire Design and Manufacturing Technology Tire Technology 2003, (Pr) [46] Khunová, V.: Reactive Melt Processing of Nano-structured Polyolefin Matrix Composites. Nanoved 2003, International

Conference, January 28-29, 2003, Bratislava , prednáška, bez zborníka C. Patents

[1] Alexy, P., Kolomazník, K., Sedlák, M., Sedláková, E., Bakoš, D.: Polymeric water-soluble biodegradable material and method of its preparation. GB 2 351 497 (10.9.2003).

D. Books and Textbooks [1] Marcinčin, A., Hudec, I., Majling, J.:Technológia materiálov, Materiály z plastov a elastomérov. Technology of materials.

Vysokoškolské skriptum, STU Bratislava, 2002, 183 strán. ISBN 80-227-1798-3 [2] Špirk, E.: Reológia polymérov. Interné skriptá Katedry plastov a kaučuku pre pracovníkov Vipotestu, s.r.o. a Matador, a.s.

CENTRAL LABORATORIES

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Head of Department: Telephone: ++421-7-59 325 433 Assoc.Prof. Ján Lokaj, PhD. Fax: ++421-7-52 92 60 18


I. STAFF

Associate Professors: Ján Lokaj, PhD; Tibor Liptaj, PhD; Research Fellows: Tibor Jakubík, PhD; Technical staff: Vladimír Dobiš; Svatava Kašparová; Mária Mravcová; Eva Pappová; Naďa Prónayová; Walter Weis


B. Research laboratories: Laboratory of NMR Spectroscopy (NMR) Laboratory of Mass Spectrometry (MS) Laboratory of X-Ray Microanalysis

III. TEACHING


A. Development of NMR techniques for the structure determination of modular molecules (Tibor Liptaj) The main goals of the project are: Development of the NMR techniques which provide long-range structural information on the studied molecules. These methods relay on measurement and interpretation of residual dipolar coupling constants which appear in high resolution spectra because of partial orientation of moleculesT the main results are: a/ development of the methods for the precise determination of the value of coupling constants b/ determination of the dipolar 1H-1H and 1H-13C coupling constants in the model oligosaccharide. c/ structural and dynamic interpretation of the experimental dipolar couplings Project duration: from 2002 to 2004

B. High Resolution Solution Structures of Carbohydrates by NMR Spectroscopy. (NATO COLLABORATIVE LINKAGE GRANT PST.CLG.979696)

Uhrín Dušan, Dr., The University of Edinburgh, School of Chemistry, West Mains Road, King's Buildings, Edinburgh EH9 3JJ, U.K. NMR spectroscopy, high-resolution solution structure, dipolar couplings, liquid crystalline media, carbohydrates, monosaccharide, oligosaccharide, conformation, ab initio calculations Determination of high-resolution solution structures of monosaccharides. The aim is achieved by the analysis of small residual dipolar coupling constants measured in dilute liquid crystalline media. Different types of dipolar coupling constants, such as nDH,H,, 1DCH,, 2DCH,, and 1DCC, are measured using new NMR techniques recently developed in our laboratories. The accuracy and very high precision of these techniques will allow us to use NMR approaches developed previously for the analysis of molecular structures in nematic liquid crystals. For flexible monosaccharides, conformation of the glycosidic linkage will be investigated. Experimental solution structures will be compared with their solid state equivalents known from diffraction studies. The developed methodology for high-resolution structure determination of small molecules by NMR spectroscopy in dilute liquid crystalline media will be applicable to a variety of small molecules, not only carbohydrates. Project duration: from 2003 to 2005

C. State program of reseach and science development, Project: Establishment of the "top-class" laboratory for Nuclear Magnetic Resonance (Tibor Liptajˇ)

Establishment of national NMR laboratory consistoing of the group of 5 specialized NMR labs with the aim to initiate the exploitation and development of NMR methods in the broad area of natural science research and education.



184

VI. COOPERATION



Duration

Jessenius Faculty of Medicine Martin grant, publications Prof. MUDr.Dušan Dobrota,

PhD. 2003 - 2005

Institute of Preventive and Clinical Medicine, Bratislava

publications Doc. MUDr. J. Horecký, PhD. continuous

Pharmacobiochem.Lab., Medical Faculty, Commenius University Bratislava

publications MUDr. A. Gvozdjáková, PhD RNDr. Z. Sumbalová continuous

Slovak Academy Sciences, Chemical Institute Bratislava

state program 339/2003 Ing. Miloš Hricovíni, PhD 2003 - 2006

Comenius University, Faculty of Natural Sciences, Bratislava

state program 339/2003 RNDr.E.Solčániová 2003 - 2006

Derer Hospital, Bratislava state program 339/2003 Ing. V.Mlynárik, DrSc. 2003 - 2006

Faculty of Natural Sciences UPJŠ, Košice

state program 339/2003 Doc. RNDr. J.Imrich, PhD 2003 - 2006

Comenius University, Faculty of Pharmacy, Bratislava

publications Ing. J.Světlík, PhD. continuous

Research Institute of Animal Production, Nitra

ZoD, publications Ing. R.Lahučký, PhD. continuous

Slovnaft Bratislava ZoD Ing.A.Malíková continuous Slovakofarma (Zentiva) Hlohovec ZoD Ing. B. Proksa, DrSc. continuous

Duslo Šaľa ZoD Ing. J.Uhlár, PhD Ing. J.Balko, PhD continuous

Institute of Polymers, Slovak Academy Sciences

publications Ing. Š. Chmela, PhD. continuous

Soil Sciensce and Conservation Research Institute, Prešov

ZoD RNDr. G.Barančíková, PhD continuous

University of Pardubice publications Prof. V. Macháček, DrSc., continuous

Comenius University,Faculty of Pharmacy, Bratislava

publications Ing. V. Kettmann, DrSc continuous



Duration

University of Edinburg, Chemistry Dep., UK

grant Prof. D. Uhrín, PhD. 2003 - 2005

Université Blaise Pascal, Clermont-Ferrand, France

publications Prof. J.F. Pilichowski 2000 - 2003

Univesita di Bari, Institutodi Clinica Chirurgica, Italy

publications Prof. V. Lombardi 2003


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Valid date

T.Liptaj Slovak Spectroscopic Society member T.Liptaj Slovak Chemical Society member



[1] Blanáriková-Hlobilová, I., Fišera, L., Prónayová, N., Koman M.: 1,3-dipolar cycloadditions of D-erythrose- and D-threose-derived alkenes with nitrones. Collect. Czech. Chem. Commun. 68, 951-964, (2003)

[2] Blanáriková-Hlobilová, I., Kubánová, Z., Fišera, L., Cyranski, M.K., Salanski, P., Jurczak, J., Prónayová, N.: Stereoselectivity of 1,3-dipolar cycloadditions of L-valine-derived nitrones with methyl acrylate. Tetrahedron 59, 3333-3339, (2003)

[3] Fiala, R., Sulová, Z., El-Saggan, A.H., Uhrík, B., Liptaj, T., Dovinová I., Hanušovská, E., Drobná, Z., Barančík, M., Breier, A.: P-glycoprotein-mediated multidrug resistance phenotype of L1210/VCR cells is associated with decreases of oligo- and/or polysaccharide contents. Biochim. Biophys. Acta -Molecular Basis of Disease 1639 (3), 213-224, (2003)

[4] Lahučký, R., Baulain, U., Henning, M., Demo, P., Krška, P., Liptaj, T.: In vitro P-31 NMR studies on biopsy skeletal muscle samples compared with meat quality of normal and heterozygous malignant hyperthermia pigs Meat Science 61 (3), 233-241, (2002)

[5] Milata, V., Kada, R., Lokaj, J.: Carbazol-9-yl-methanol. Molecules 2003 [6] Pilichowski, J.F., Liptaj, T., Morel, M., Terriac, E., Baba, M.: Cross-linking of polybutadiene: correlation between solid-state H-

1 NMR spectroscopy, thermoporosimetry, densimetry and crystallinity measurements. Polymer Internat. 52 (12), 1913-1918, (2003)

[7] Saloň, J., Milata, V., Chudík, M., Prónayová, N., Leško, J., Seman, M., Belicová, A.: Synthesis, properties, and reactions of 5-substituted derivatives of 2,3-diphenylquinoxaline [1]. Monatshefte Chemie/Chemical Monthly 2003, Springer-Verlag Wien, ISSN: 0026-9247

[8] Sedláček, J., Jamnický, M., Lokaj, J.: Microstructural analysis and properties of fused cast zirconia refractories corroded in lead. Solid State Phenomena 90-91, 253-258, (2003)

[9] Szemes, F.,Jr., Marchalín, Š., Prónayová, N., Szemes, F., Daich, A.: A facile access to 2-ethynyl-1,4-dihydropyridines via Hantzsch three-component reaction. Heterocycles 52 (2), 779-783, (2003)

[10] Čertík, M., Dercová, K., Finďová M., Jakubík M., Sejáková Z.: Effect of polyaromatic hydrocarnons (PAHs) on the membrane lipids of bacterial cell. Biológia 58(6): 1111-1117 (2003)

[11] Rebroš, M., Jamnický, M., Piják, M., Lokaj, J., Kadlečíková, M.: Vplyv rôznych fyzikálno-chemických faktorov na zvetrávanie kryštálového skla. Influence of various physico chemical factors on crystal glass weathering. Chemical Papers 9, 863-873, (2003)

B. Conferences [1] Nociar, A., Hudec, P., Smiešková, A., Jakubík, T., Židek Z.: Alkylation of benzene by linear 1-olefins C16 over dealuminated

Y-zeolites and mordenites. 41st International Petroleum Conference, Bratislava, October 6-8, 2003, 7 pages, CD-ROM ISSN 1335-888X, ISBN 80-968981-6-7

[2] Nociar, A., Hudec, P., Smiešková, A., Jakubík, T., Židek Z.: Alkylation of benzene by linear a-olefin C16 over zeolite catalysts in flow pressure reactor. XXXV Symposium on catalysis, November 3 - 4, 2003, Praha, ČR, p 26-27

[3] Štetinová, J.,* Milata, V., Prónayová N., Leško J., Petrov O.: Syntéza a vlastnosti niektorých 1,2,4-trisubstituovaných pyrolov Synthesis and properties of some 1,2,4-trisubstituted pyrroles. In: 55. zjazd chemických spoločností, Košice, 8.9.-12.9.2003, Chem. Listy 97, 770, (2003). (Po)

[4] Lokaj, J.*, Kettmann, V., Dobiš, V.: Structure of 1-(5-Nitrobenzo[c]-1,2-thiazol-3-yl)-3-butyl-3-phenyltriazene Structure of 1-(5-Nitrobenzo[c]-1,2-thiazol-3-yl)-3-butyl-3-phenyltriazene. In: Conference on Thermal Analysis, Tatranská Lesná 2003

[5] Nociar, A., Hudec, P., Smiešková, A., Jakubík, T.: Alkylation of benzene by linear alpha-olefins C16 over dealuminated Y-zeolites and mordenites. X Zeolitic forum „Zeolites – synthesis, adsorption and catalysis“, September 21 – 26, 2003, Tuczno, Poland, p.107-112

[6] Rebroš, M.*, Jamnický, M., Piják, M., Lokaj, J., Kadlečíková, M.: Influence of the atmosphere's composition on weathering of crystal glass by cyclic changes of temperature . "Konferencia ""Príprava keramických materiálov, Herľany 2003"

[7] Dobrota, D., Likavčanová, K., Kašparová, S.*, Liptaj, T., Prónayová, N., Mlynárik, V., Belan, V.: The study of the creatine kinase in rat brain during ischemia by magnetization transfer and biochemical analysis. Journal of Neurochemistry 85, 22-22 Suppl. 2, June 2003, Warsaw, Poland (Po)

[8] Kašparová, S., Horecký, J., Bystrický, P., Liptaj, T., Mlynárik, V., Sumbalová, Z., Kucharská, J., Gvozdjáková, A.: New MRS biomarker for monitoring neurodegenerative disseases: Animal models. In: Book of Abstracts ESMRMB 2003, 20th Annual Scientific Meeting, Rotterdam, Sept. 18-21, 2003, p. 20, Nietherland, MAGMA 16, suppl. 1, (2003)

[9] Kašparová, S., Horecký, J., Bystrický, P., Liptaj, T., Mlynárik, V., Sumbalová, Z., Kucharská, J., Gvozdjáková, A.: New MRS biomarker for monitoring neurodegenerative disseases: Animal models. "In: 11th International Symposium ""New Frontiers of Neurochemistry and Neurophysics on Diagnosis and Treatment of neurological Diseases!, Martin 2003, Slovak Republic, p.38-39"

[10] Likavčanová, K.*, Dobrota, D., Liptaj, T., Prónayová, N., Galanda, M., Belan, V.: In vitro H-1 magnetic resonance spectroscopy differences between meningeoma and astrocytoma. Journal of Neurochemistry 85, 22-22 Suppl. 2, (2003)


186

[11] Milata, V.,* Kada R., Lokaj J., Goljer I., Štetinová, J., Hammetner Ch., Belicová A.: Preparation, spectral and biological properties of Sulfones of 2-hetarylcinnamonitriles. In: 10th Blue Danube Symposium on Heterocyclic Chemistry, Vienna 2003, Austria (Po)

[12] Sumbalová, Z., Gvozdjáková, A., Kucharská, J., Mlynárik, V., Bystrický, P., Kašparová, S., Uličná, O., Vančová, O., Singh, R.B.: Brain energy metabolism in streptozotocin diabetes - effect of coenzyme Q10 and n-3 fatty acids. "In: 11th International Symposium ""New Frontiers of Neurochemistry and Neurophysics on Diagnosis and Treatment of neurological Diseases!, Martin 2003, Slovak Republic, p.80"

[13] Sumbalová, Z., Gvozdjáková, A., Kucharská, J., Mlynárik, V., Bystrický, P., Kašparová, S., Uličná, O., Vančová, O., Singh, R.B.: Coenzyme Q10 and w-3 fatty acids improve brain energy metabolism in experimental diabetes. In: 3rd International Conference VITAMINS 2003, Pardubice, Czech republic, p. 211-213

[14] Štetinová, J.,* Milata, V., Prónayová N., Leško J., Petrov O.: Synthesis and properties of some 1,2,4-trisubstituted pyrroles. In: 10th Blue Danube Symposium on Heterocyclic Chemistry, September 3-6, 2003, Vienna, Austria (Po)

[15] Sumbalová, Z.*, Kašparová, S., Bystrický, P., Kucharská, J., Liptaj, T., Mlynárik, V., Gvozdjáková, A.: Účinok koenzýmu Q10 a vitamínu E na energetický metabolizmus mozgu v experimentálnom modeli Huntingtonovej choroby. The effect of coenzyme Q10 and E vitamine on energy brain metabolism in the Huntington disease experimental model Slov.spol.pre biochémiu a molekulárnu biológiu, seminár, LF UK Bratislava, 2003 Pr

FACULTY ADMINISTRATION SERVICES

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FACULTY ADMINISTRATION SERVICES

1. DEAN`S OFFICE Registrar of Faculty Žúbor Vladimír, PhD Secretary Ledecká Anna Economic Department Rečlová Aurélia, Kluvancová Soňa, Gézeová Agnesa, Uhláriková Libuša, Levická Gabriela, Tanczerová Mária, Košťanová Alžbeta, Čaplová Alena, Martinkovičová Oľga Pedagogical Department Kusý Pavol, PhD, Borovská Anna, Danášová Eva, Hrušková Veronika, Zítková Mária Office of PhD Study Šupejová Iveta Office of Scientific Research Kutešová Mária Department of Employees` Affairs Kršáková Viera, Pustaiová Lýdia, Steinerová ZitaHaláthová Ľudmila, Kajanová Kamila, Nagyová Jana Office of Foreign Cooperation Burešová Valéria Department of Safety Labour Protection and Fire Safety Hodálová Jolana

2. MAINTENANCE DEPARTMENT Performance Manager: Sabol Vladimír

3. INFORMATION CENTRE Supervisor: Dzivák Jozef

4. CAFETERIA Supervisor: Kuchariková Agáta

Annual Report 2003-work-6 · 5. semester (Bc) Analytical Chemistry II 2/2/0/0 Bustin, Čakrt...

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