\ --

Testi»gIECitSQ 170;!'S Cttrtifi,'.etio(l JOQ9.01

Slate of Tennessee (lD #O2034)jl.l,~barmf Dept of E'nvironmenfal M<magem&llt (ID U(}780j

ANALYTICAL INnUSl'RIAL RESEARCH LAHORA'I'OIUES, INC.1550 37TH STREET, NE

CLEVELAND. TENNESSEE 37312(423) 476 . 7766 Fax: (423) 476-7714

5WlfJt! Of A<YN,lila/ion:

II'4fli'Wai.." Surfa.t' Wate" C;rmmd WIlt«.DtinAing H'tfI..,. SluMs. Ha;ar,j<Jl/s Wllfl.., Sajl~.S",lim'~IIII. 'IlItl Slitrig.,s,

Dille Re(~ei..,!tl

Diltt~SmuplellDate Reque.\'u!tfRush .Vla/IISPlumeE.\:/en.siotl

! Pi/X~! eMail:

PO#

t /31/201tNone GiVL'112 /8 /201tRush

Lab Report 243631

7682Hem\Uellt!on: B.J. Kumar05 Riddhi Siddhi Apt:;..Mithagar "X" RQad

Murnbai, India 400 08t

Sample InformationPn:clUus Chandan[(KltIBC'Sth;f:S

jIIi.

Bflnzene

cttlylbenzeneTo!uern:

Method1S0 16017ISO10017

SDL Dllfe 11me .4l1u{rMLab Ree.°rl 243631

ISO1t>017

0.005 2/11/2011 23-26 GVVl

0005 1111/2011 2326 OWL0005 2/11/2011 2326 OWL

I QAQ( hOut0Un,: rcquired b'lh~ Merno~(,) "ere nI~lowudtinJ~"dhltrwi,c Ildl.d, Pult'fIlmllcc and ac\:'cj!\:u"'emmJard!i 10tH!<;mrd,Q/\.!QC pl;:,ecdull'Swetep> ,"'!h~'d I'm"" )\!,crWiW"ni~'\,) 'ii, ,rf!,mh;a,j\ moGih.'Ih"", 1\;1\-';b<;""JtJi\<k10the M.;>!h\x!(F! aUe,) that h'lwd lip'M1Hl}mQua) (it IHi"" mU1\.Ju;;h mun.:d'''kIJre'IX*,.hk I,,, r,'vk',' ,wi:rk m1h!IDJIwn.Ih~m1!h'n;d oomn..ocdi" !hI, fl:l"m K m lhe !x"l Qfmy kfh'wkdgc ~nd khd- i!<'4:Unlll,'~nd tOf,mr,kk

! IhC\Q lQ,uhsld,*, - tilt' .l~11" l"ICd. lh" fCpWI.,hQiJ no! I>c rcpn>;h,ccd ""1'\ III lull4JHJ '..<ilh l1<m\'''''I\>I\ ,d Ihl' 1abGlahwy. Ihc iab(,riitory rdar", ,okI ,~w!V'0hm01 ,hi" lid ,"unoorsf:m"nl h!h />''''0 111M.:.

-* ",' _.~",,' ,t

Report iJpprm'l?ilby:

~

#Ii

Mcmda)l, February 14, 2GH [>af.:" f iil I

I a - - = - <---- -- .. Iii -~

Result LCL<:0.005 mglCuM 000<0.006 m9iCuM 000<0.005 mglCuM 0.00

Ii"omary 14. ZO! I

Attention: MI. B. J. Kumar, Hem Corporation$ubJcct I'r~ci[)u, Chandan

lab Code: 243631ISO: 16017

Dear Mr. Kuma!,

fncense stickwas allowed to burn ioa lifter vacuum flask at a control rate, an air sample wastaken at a rate of ZOOcc,tmin. for 10 Olin for a total sample volume of 2 liter.The vapors were collected on a Tenax r Acartridge then thermaUydesorped under the followingconditions:

~i Desorption Temperature:Desorptioo Time:

3000c10min.

Instrument tiP S972 GqMS

Column: 30meter06~l,Lo-umFilmThicko&

':If

Temperature Prog.ram: Initial 35° chold4mIn,8° c per min. to 1500c15° c per min..to 3000 c

Detector Temperature (MS): 2809 C

Results: Benzene: CAS71~43.2 <0.OQ5m9/Cu~1Toluene: CAS108~88.3 <0.005 mg/CuMEthylBenzeoe:.CAS100-41-4 <D.OOSmg/CuM

No other analytes requested.

If you ha~any questions, plea$e call Roy Patterson at: 423-476-7765

Thank you,

Roy R. Patterson, Technical DirectorAIRt.

1m

~Ii

,..,., _...-. , ., m....._....

--.. _..

-..,..,= ::-~~- :::=:_~~L;;::~-'=';..~5..~"'-

-esting

IEC/1S0 17025 Certification 3009.01State of rel1n~ssee (ID#02(34)AI~~rna Difpt of Environmental Management (ID#40780)

Lab Report 243621

ANALYTICAL INDUSTRIAL RESEARCH LABORATORIES, INC.155037TIISTREET, NE,

CLEVELAND,TENNESSEE37312(423)416.7766 Fax: (423)476-7714

SctJPtf -if Al:crlfditatim/:

WUJtItHiater, Sur/flce Wtl(er, GrilttrUl Wtuer,DritlAinf: If'uter, Slllitk, Hazarduu$ WU-tfe. SlJil$,Sediltll!lU$. omit .filudges.

7682HemCorporattonAttention: BJ, Kumar

Riddhi Siddhi Aptg" Mithagar "X" RoadMulund (East), Mumbai, India 400 081

Date ReceivedDtlleS'i"#mplctfDate Rei{lll!!itl!dHllsl, StatllsPlumeE."dem';oHFirx

IV'IeMai/:PO#

1/31!2() 11None Given2 /8 /20 IIRush

S;'mpl~]nformatioo

"-t(,!USIncense Sticks

Lah Re2!!rt 243621 Result LCL lYetllodISO16017ISO1aOt7ISO

SDL I)utt! Time AnalystBenzene <0.005 mg/CuM 0.00

€:lhylb$!l2;1'Ine < 0,005 mgtCuM 0.00To!uene 0:O,OOS' mgfCtiM tuX)

Lmvnt Cllhbrntioo 1,<,,;d [LCLj. reponing limit; Sample EklecliQIlLe...d ($DLI.' Sampl.:"Sp"i!ic,

Q.>iii)(' l'rOi.x;;jm\)~ Nitulr",! by lht Mdhodtsj were jotl(),,~-d un1e:;c~\)jherwise OOttd, Per!brm.mcc<llldtlcc<ptam:c st~uldaf(ts for required QNQC p(ocedur~) "crt'ilclU1.t\'wlunl;:;;>()thcrw,se rH'K'd m\Xhlk;;;tlous haveb;."'11madeII) Ill..:Mclhod(s) I aUolt!llllat, rntwd upoo myinquil)' .Iflho:sc ttllthidUill$ ullfflcdialcl}'lesp9n",hk th~ mllien:al corttai!1~'d in this fCpilf!lS,IO tbch\Jst iJfmy"n()wh~dM, J\O'dbdid;;,u:clII4kam!"'()!I!plcte,

0,005 211112011 1704 aWL

t!.OOS :U11i2011 17'04 aWL

tlO05 2/t1l20n 17:04 ,aWL

This rcp'''11"hilll nOt be 1Cpr;ld\I;;~HjCX,,~plill full tII'Idwith IMmisiiul1 ofdl1slab,nlOry, 11,,, i"bural0ry rd"ins sokhM h<xnmade,

Report llPprtwed b)':..,-,-'-""-

ruesda}t, February 15, 2011 Page I <ifI

""-""'~'--'"'-''''''' , ,,,,,, ""-"""~~'

.~~v'~1..~~~~~s.:::-.,,~~.~ -=~ "i'f-- --------' ~

~~-=<::'~. "'.- --,o;.".~~ aw=

I ,"""

~", ,-"r'~

~.. -,-" ~

..z\",- ~ '''~ ..,.....

,.1!~~:riCi~~~Wi&Wil¥~~i,MS!"':P"ry/Pi'~,.;~~...!87.+,,1f;.",._!':!.i~7~,~,!t1,'W~~'&~~~~%i;

February 15 . 2(i J I

Attentioo: ,.1r.B. ). Kumar, Hem Corporation

Subject: Lotlts

Lab Code: 243621ISO: 16011

Dear Mr. Kumar,

~Im:ense $tick was allowedtobum Ina 1 liter vacuumflask.at a controlrate, an air sample wastakeoat a fate of 200cc:lmio. for 10 min for a rotaI sample volume of 2 liter.The vapors were coIle<ied on a Tenax TA.cartr~ then tt!ermally desorped un<ier the followingconditloos:

Desorption Temperature;Desorption Time:

3009 c10m!n.

Instrument: HP 5972 GC/MS

COlumn: 30 meter DB-l,1.0-umFHm Thickness

:ttTemperature Program: Initlal3So c hold 4 min.

69C per min. ro 1500c15° c per min. to 3000 c

Detector Temperature ("\5): 2809c

ResUlts: Benzene: CAS71-43-2 <0.005 mgJCuMToluene: CAS108-S8-3 <0.005 mg/CuMEthyl Benzene: CAS10()..41-4 <0.005 mgfCUM

No otoer analytes. requested.

If you Mve any questions, please call ROY Patterson at: 423-476-7766-

Thankyou,

Roy R. Patterson, Technlcal.DJreaorAIR!.

1m

'F-!

o_-~~~ - ---= =~.:::::::..~:-:=.:::--=-::,~ ~ ~~,

w ~-_.- ~ ~

IiIii - - - - :- -- -=-.. 1i""-':- '5' ----- ~ -= ~ c-~

-ANALYTICAL INDUSTRIAL RESEARCH LABORATORIES, INC.

1550 37TH STREET, NECLEVELAND, TENNESSEE 37312(423) 476 -7766 Fax: (423) 476-7714

Scope ujAe<:redi,afilJlI:

W",uewater. Surface .'Vilter. Ground Wtllel',Dril,kll'f/ WaleI'. Solids. HI1Z.III'dJJu$WlUte. SlJifs.Sediments, and Studg(!$.

TestingJfiC!1SDH025 C1JrtificIitioo 300$.01

srOiW of TiffllU'I$$$$ (lD#C2Q34)A'!)~maDept. of Eil'lvironme:ntal Mifnagernftltt (ID #40780)

{,ab Report 243612

7682HI,.¥tnCorporation

BJ. KumarCISRiddhi Siddhi Apts., Mithagar "X" Road!\.1uJund(East), Mumbai, India 400 081

Dille ReceivedDate SampledDate Rt'qae.wed-Has!tStatusPlumeExtensiQnFaxeMail:PO#

1 /31/2011None Given2 is/2011Rush

Sample Information

~Citwl11tllaIncenseStick,;

TOHxen1J

Rqj'ult LC'L.(OJXJ5 rogiCuM 0,00<:0.005 fl'lglCuM 0.000;;0.005 mg/CuM 0.00

MetllOdISO16017ISO16017

SlJL Vale Time AnalystL£lbReport 243612

ISO 161H?

0.005 2i121'20t1 3;53 GWl0.005 211212011 3;53 GWl

0.005 211212011 3:53 GWl

Beru.ene

Ethy!!>eru.ene

Qtv"A' ,,, ""'TI' fiNed f'e11hnnarn.'\tandaccep!IifH.:e$!andard$ f(>rr'qui",'" Ql\.lQC pmccdun.'S W"'"mad\: 10II.\:1>1CII1,III($I.1)£1(118\that bas;;d up~'n I1lY1II'l!IH),11'Itlnse !mh¥id\''Ih irnrnCIJIdldy

tlll$Kp<1ftis, iiI tli<best vI'my krmwkdg<::IIml~Ikf, !Kcu,lIlc 1\ndcomple!e,FnpN\i;.bk

Thc>;; !i.'Sall' {cJ,uc ,,"I) W.m1\Cf>tHf' M dala <lm,1 hill

b<;"jfHx!lIccli '''ccpt 111full Jal:x;>rdh'r) 1<\11111' .",1.;be""I1l~

Report appravt!:£( by:

~ ""-.

------- .----.-.-----------..------.-

,..

I

f

Monday. FebnJary 14.2011 I'age J Ilf I

-...-.---...--. ._.~ ~.-

...~"" ~.~ '~..,~. "~~"'i'i!'" ,..., ~ 'Oii!"""102 ClIo 'Ii! II!'.

.",,,",,.~,."~"'" "~-"=..,,.-' .,uT":£:!!II'!It... u~~.,~.....

Attention: Mr. 6. J.

CiIrQl1dla

1m

(fi\

~ -~ .. ~ 5--~ >-, ~",-",,~ ... C '!'~-

~...g~._....- ~"""'s. "":":',;~' - ~ ~ ....~- ~:J

Cl:rtfficatio(/3(WfUf1SllIll: af TeftHlMIS" (iD#Q20$4)Aial1ama Dept. of Envttonmental Management (10 #407(0)

ANALYTICAL INDUSTRIAL RESEARCH LABORATORIES, INC.155037TII STREET, NE

CLEVELAl\I'D,TENNESSEE37312(423)476 - 7766 Fax: (423)476-7714

.">('Opt' {If Arx:rctfi1utimt:

W4fI.-I>'m'U.Suifilce If'illU. Gl'tlkmJ "'0lil0.Drinldng Walf£r,Solhb, H;rzJIrdum.J#'4fle. Selh,S¥di1ftffJttf. atl.IS/uilger,

HemCorporatio!1Attention: BJ. Kumar05 Riddhi Siddhi Apts" Mithagar "X" Road

081

Date Receh'ed

Date Sample(JDate Reque.\'tetlRit.~'11Sut/usPhoneExtensionFa.'(dlai/:PO#

II3112011None Given2 1812011Rush

Lab Report 243646

Sample Information'r' Vanilla

Im;ense Sticks

8om:eru!Ethy~eneToluene

Result<0,005 mgtCuM<0 005 mgtCuM<0.005 mglCuM

Lg0.00

Metho(1180 t6017ISO100170,00

0'.00 ISO 16017

(l005 2/14120n

(toos 2/141201 I

(1;005 2/1412011

17I1leAnul)'S1

14;19 OWL

W19 OWl

1419 OWl

l"hcse "",liB td~ W 1119IIcl!\\ IL"S1edThi5H;PWI sblll! nN 00 ti:prtldu~C1J \:"'\:.1'1 in fuHandwith pl.7mISS!l,n \)f Ihb fabnnllp[~. Ihe lah<uu\f'l)' Ict"ins >'1khll>!x:'(cl1tila""

Rt'pftrJ uppnwed bJ: ')J... .{._..,,--, ~-'"

rrI

("

rtl~<:sa)'. February 1~, 2011 PftgeJof I

I

,..; , ". ~' ~"E"""'", -'~ [!"1i"""

~

I.

"(

If' "''''I :ii""~ ""~"::.. ~ fi ." " ,~tli" III' ~ ,~,';'c;'",~~=,""'"

243646

1m

an air sample w~s

under the fu4lowing

,~ '~''''OC' ~_.,