American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~...

71
American Environmental Testing . . Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com Ordered By Number of Pages 13 - Suite 370 Date Received 08/01/2006 Date Reported 08/04/2006 Telephone: (714) 985-3434 Job Number Order Date Client Attention: Tom Tatnall 38375 1 08/01/2006 1 H &A Project ID: 32486-007 Project Name: Delphi System Corp. Site : 1201 N. Magnolia Avenue Anaheim, CA 92801 Enclosed please find results of analyses of 1 water and 11 solid waste samples which were analyzed as specified on the attached chain of custody. If there are any questions, please do not hesitate to call. Checked By: . .- Approved By: Cyrus Razmara, Ph. D. Laboratory Director

Transcript of American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~...

Page 1: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American Environmental ~~ Testing .. . Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com

Ordered By

Number of Pages 13 - Suite 370 Date Received 08/01/2006

Date Reported 08/04/2006

Telephone: (714) 985-3434 Job Number Order Date Client

Attention: Tom Tatnall 38375 1 08/01/2006 1 H &A

Project ID: 32486-007 Project Name: Delphi System Corp.

Site : 1201 N. Magnolia Avenue Anaheim, CA 92801

Enclosed please find results of analyses of 1 water and 11 solid waste samples which were analyzed as specified on the attached chain of custody. If there are any questions, please do not hesitate to call.

Checked By: PA . .-

Approved By:

Cyrus Razmara, Ph. D. Laboratory Director

Page 2: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American Environmental Testing Laboratory Inc. 2834 & 2908 North Naomi Street, Burbank, CA 9 1504 DOHS NO: 1541, LACSD NO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aet1ab.com

CHAIN OF CUSTODY RECORD NO 427'09

Page 3: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:
Page 4: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

TABLE Summary of Aqueous Analytical Results for Polychlorinated Biphenyls (PCBs) by GC

1201 N. Magnolia Avenue Anaheim, CA 92801

Polychlorinated Biphenyls (PCBs) by GC. Method: 8082

Sample Date

Laboratory Job Number

Aroclor-1016 (PCB-1016) ug/L

Aroclor-1221 (PCB-1 221 ) ug/L

Aroclor-1232 (PCB-1 232) uglL

Aroclor-1242 (PCB-1 242) ug/L

Aroclor-I 248 (PCB-1 248) ug1L

Aroclor-I254 (PCB-1254) uglL

Aroclor-1260 (PCB-1260) uglL

Aroclor-I 262 (PCB-1262) uglL

Aroclor-1268 (PCB-1 268) ug/L

1) "ND<Xn INDICATES CONSTITUENT(S) NOT DETECTED AT OR ABOVE METHOD DETECTION LIMIT.

2) "J" INDICATES ANALYTE WAS DETECTED. HOWEVER, ANALYTE CONCENTRATION IS AN ESTIMATED VALUE WHICH IS BETWEEN

THE METHOD DETECTION LIMIT (MDL) AND THE PRACTICAL QUANTITATION LIMIT(PQL).

3) "D" INDICATES THE SAMPLE WAS DILUTED TO BRING THE ANALYTE CONCENTRATION WITHIN CALIBRATION RANGE.

File: AQ-8082.~1~

Page 5: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:
Page 6: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:
Page 7: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

TABLE Summary of Solid Waste Analytical Results for Polychlorinated Biphenyls (PCBs) by GC

1201 N. Magnolia Avenue Anaheim, CA 92801

Polychlorinated Biphenyls (PCBs) by GC. Method: (8082)

Sample Date

Laboratory Job Number

Aroclor-1016 (PCB-1 01 6) udKg

Aroclor-1221 (PCB-1 221) uglKg

Aroclor-1232 (PCB-1 232) uglKg

Aroclor-1242 (PCB-1 242) %\Kg

Aroclor-I 248 (PCB-1 248) uglKg

Aroclor-1254 (PCB-1254) udKg

Aroclor-I 260 (PCB-1260) udKg

Aroclor-I 262 (PCB-1 262) usn<S

Aroclor-I 268 (PCB-1268) udKg

1) "ND<X" INDICATES CONSTITUENT(S) NOT DETECTED AT OR ABOVE METHOD DETECTION LIMIT.

2) "J" INDICATES ANALYTE WAS DETECTED. HOWEVER, ANALYTE CONCENTRATION IS AN ESTIMATED VALUE WHICH IS BETWEEN

THE METHOD DETECTION LIMIT (MDL) AND THE PRACTICAL QUANTITATION LIMIT(PQL).

3) "D" INDICATES THE SAMPLE WAS DILUTED TO BRING THE ANALYTE CONCENTRATION WITHIN CALIBRATION RANGE.

File: SW-8082.~1~

Page 8: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American Environmental Testing Laboratory Inc. 2834 & 2908 North Naomi Street, Burbank, CA 9 1504 DOHS NO: 1541, LACSD NO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (81 8 ) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

Ordered By --

/ Haley & Aldrich 7 ; 500 South Kraemer Blvd. i

1 g:, z 1 9 2 8 2 1-6723

Site

Anaheim, CA 92801

Telephone: (714)985-3434 Attn: Tom Tatnall

Pane: 2

Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 080206

"

Clienq -- H&A , -- L

Project ID: 32486-007 Project Name: Delphi System Corp .

/ Our Lab I.D. Client Sample I.D.

Date Sampled

1 Matrix 1 1 Solid Waste / Solid Waste Solid Waste Solid Waste I Solid Waste 1

AETL Job Number 38375

MethodBlank

08/01/2006 08/01/2006 ~08/01/2006 /08/01/2006

Submitted 0 8 / 0 1 / 2 0 0 6

Date Pre~ared 08/02/2006 108/02/2006 08/02/2006 08/02/2006 /08/02/2006

3 5 5 0 ~ 1 3 5 5 0 ~ Preparation Method

38375.0% CSO257-CC-0

oo-ol

3 5 5 0 ~

Date Analvzed

Units Dilution Factor Analy te s MDL

Aroclor-1232 (PCB-1232) Aroclor-1242 (PCB-1242) Aroclor- 1248 (PCB- 1248) Aroclor- 1254 (PCB- 1254) Aroclor-1260 (PCB-1260) Aroclor- 1262 (PCB-1262)

Aroclor- 1268 (PCB- 1268)

38375.02 CSO258-CC-0

00-01

08/02/2006 /08/02/2006 08/02/2006 08/02/2006 08/02/2006

PQL

50.0

50.0

Aroclor- 10 16 (PCB- 10 16)

Our Lab I.D. Surrogate s I%~ec.~imit

38375.03 / 38375.04 CSO259-CC-01 CSO260-CC-0

oo-ol I o ~ - ~ l i

3 5 5 0 ~

25.0

25.0

25.0

25.0

25.0

25.0

25.0

25.0

3 5 5 0 ~

1 R e s u l t s

ND

ND Aroclor- 122 1 (PCB- 122 1) 1 25.0

% R e c .

50.0

50.0

50.0

50.0

50.0

50.0

50.0

1 R e s u l t s

ND

ND

38375.01 % R e c .

ND

ND

ND

ND

ND

ND

ND

% K g 1

R e s u l t s ND

ND

38375.02 1 38375.03 % R e c . 1 % R e c .

ND

ND

12 9

ND

ND

ND

ND

38375.04 1 % R e c . 1

ugKg 1

R e s u l t s ND

ND

@Kg 1

Results

ND

ND

ND

ND

ND

ND

ND

ND

ND

I N D ND I ND

288

ND

ND

ND

ND

, 64.0

ND

ND

m i ND i

Page 9: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American Environmental Testing Laboratory Inc. 2834 & 2908 North Naomi Street, Burbank, CA 91504 -DOHS NO: 1541, LACSDNO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (8 18) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

O r d e r e d By Haiey & Aldrich 500 South Kraemer Blvd. Suite 370

i Brea, CA 9282 1-6723

S i t e

Anaheim, CA 9280 1

Telephone: (714)985-3434 Attn : Tom Tatnall

Paae: 3

Method : (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 080206

L,

Project ID: 32486-007 Project Name: Delphi System Corp .

Our Lab I.D. Client Sample I.D.

Date Sampled Date Pre~ared

1 Matrix 1 I Solid Waste Solid Waste / I 1 1

- Client 1

- - H&A 1

AETL Job Number 38375

38375.05 CSO261-CC-0

00-01

1 ~ r e ~ a r a t i b n Method 3 5 5 0 ~ 3 5 5 0 ~

Submitted 0 8 / 0 1 / 2 0 0 6

08/02/2006

I Date Analyzed

38375.06 CSO262-CC-0

00-01 08/01/200608/01/2006

08/02/2006

108/02/2006 08/02/2006

Dilution Factor Analytes MDL

Aroclor- 10 16 (PCB- 10 16) 1 25.0

Aroclor-122 1 (PCB-122 1) 1 25.0

1

I I

Aroclor-1232 (PCB-1232)

Aroclor- 1242 (PCB- 1242)

Aroclor-1248 (PCB-1248)

1 Aroclor-1268 (PCB- 1268) I -- ~

PQL

50.0

50.0

Aroclor- 1254 (PCB- 1254)

Aroclor- 1260 (PCB- 1260)

Aroclor-1262 (PCB-1262)

25.0

25.0

25.0

1 Results

ND

ND

25.0

25.0

25.0

/Our Lab I.D. /Surrogates ]%~ec.~imib

1 Results

ND

ND

50.0

50.0

50.0

50.0

50.0

50.0

38375.05 % Rec.

ND

ND

28.3J

38375.06 % Rec.

ND

ND

ND

ND

ND

ND

ND

ND

ND

Page 10: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

O r d e r e d By [%ley& Aldrich 500 South Kraemer Blvd. Suite 370 Brea. CA 9282 1-6723

American Environmental Testing Laboratory Inc. -- - -- - - - - - . ppp

2834 & 2908 North Naomi Street, Burbank, CA 91504 DOHS NO: 1541, LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

S i t e --

120 1 N. Magnolia Avenue Anaheim, CA 9280 1

Telephone: (7 14)985-3434 Attn: Tom Tatnall

Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 080306

Page: 4

/ Method ~lankl 38375.07 / 1 / o u r Lab I.D. I

1 Client Sample I.D.

Client H &A

Project ID: 32486-007 Project Name: Delphi S y s t e m Corp.

AETZ Job Number 38375

- Submitted 08/01/2006

Anal ytes MDL

1 Aroclor- 1242 (PCB- 1242)

/ Aroclor-1248 (PCB-1248)

Aroclor-1254 (PCB-1254)

PQL

50.0

50.0

50.0

Aroclor- 10 16 (PCB- 10 16) Aroclor- 1221 (PCB-1221)

Aroclor- 1232 (PCB-1232)

25.0

25.0

25.0

25.0

25.0

25.0

---

1

Results

ND

ND

ND

-- Our Lab I.D.

50.0

50.0

50.0

% Rec.

94

Surrogates

Results

ND

ND

ND

%Rec.Limit

I

I

ND

ND

ND

38375.07 % Rec.

98 Tetrachloro-m-xylene 1 30-150 /

--

ND

286

ND 1

Page 11: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American Environmental Testing Laboratory Inc. --- - - - -- .- - --

2834 & 2908 North Naomi Street, Burbank, CA 9 1504 DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (8 18) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

Ordered By Ull.7 & Aldrith 500 South Kraemer Blvd. Suite 370 Brea, CA 9282 1-6723

Telephone: (714)985-3434 Attn: Tom Tatnall

Page: 5 Project ID: 32486-007 Project Name: Delphi Sys tem Corp .

Site

1201 N. Magnolia Avenue Anaheim, CA 9280 1

/ AETL Job Number / Submitted I ~1Kt-1

Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 080206

--

Our Lab I.D. Client Sample I.D.

I

Date Sampled Date Prepared Pre~aration Method

Matrix 1 1 Solid Waste / Solid Waste I Solid Waste Solid Waste / I

38375.11 CSO267-CC-0

I I 1 I

1 Units 1 I ugKg / u d K g / ugKg ugfKg 1 1

I

I

38375.08 CSO264-CC-0

08/02/2006

3550B

Date Analyzed

I Dilution Factor 1 / 1 1 1 1 1 / 1 / ~ n a l ~ t e s MDL PQL ( Results I Results I Results 1 Results / I

I

I 00-0 1

108/02/2006 /08/02/2006 j08/02/2006 /08/02/2006 1

38375.09 CSO26.5-CC-0

08 /0 l /200608/0 l /2006

08/02/2006

3550B

- 38375.10

CSO266-CC-0

00-01

/ rocl lor- 10 16 (PCB- 10 16)

00-01 1 00-01 08/01/2006

08/02/2006

3550B

/ Aroclor-1232 (PCB-1232)

Aroclor- 1242 (PCB- 1242)

Aroclor-1248 (PCB-1248)

1 Aroclor- 1268 (PCB-1268) / 25.0 50.0 I ND ND ND 1 ND 1 1

25.0

/ Aroclor-1254 (PCB-1254)

1 Aroclor- 1260 (PCB- 1260) 25.0 50.0 ND ND ND ND

08/01/2006

08/02/2006

3550B

ND

25.0

25.0

25.0

Aroclor- 1262 (PCB-1262)

I I I

I

50.0

ND

Our Lab I.D. Surrogates I%~ec.~imib

1 Aroclor- 122 1 (PCB-1 22 1) 1 25.0 1 50.0 ND ND

50.0

50.0

50.0

25.0

ND

1 38375.08 1 %Rec.

ND

ND

36.95

50.0

ND

38375.09 1 38375.10 %Rec. / % R e c .

ND

ND

32.05

ND

38375.11 1 %Rec. 1

ND

ND

ND

44 .6J

ND

ND

ND

ND

475

I

ND ND

Page 12: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American .. -. . . Environmental - - Testing Laboratory Inc. .......--pp..-p--.- ~p

2834 8~2908 North Naomi Street, Burbank. CA 91 504 *DOHS NO: 1541, LACSD NO: 10181 T e l : (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com

- ANALYTICAL RESULTS

Ordered By

500 South Kraemer Blvd. Suite 370

Telephone: (714) 985-3434 Attn : Tom Tatnall

Page 6 Project ID: 32486-007 Project Name: Delphi System Corp.

S i t e

120 1 N. Magnolia Avenue Anaheim, CA 9280 1

AETL Job Number 1 Submitted / Client

38375 1 08/01/2006 / H&A

- - , " "

Analytes Arsenic ' , I 1"" " ' . . I

tr.

Methods of Analvses 1 1601 OBSCAN)

Date Prepared Date Analyzed

\ - - - - - - z

08/02/2006

08/02/2006 Matrix QC Batch Number

- - Lab ID I Sample ID Sampled

- - Results

Method Detection Limit Practical Quantitation Limit

, Dilution Factor

Units i mg/Kg

Solid Waste

080206-1

- - 0.5

5.0

1

--

I

38375.11 1~~0267-CC-000-01

N/AI Method Blank .--,

08/01/2006

l I -.

3.905

ND .. -

Page 13: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American Environmental - Testing Laboratory -- -- Inc. 2834 & 2908 North Naomi Street, Burbank, CA 9 1504 DOHS NO. 1541, LACSD NO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (81 8) 845-8840 www.aetlab.com

ANALYTICAL RESULTS O r d e r e d By

Haley & Aldrich 500 South Kraemer Blvd. Suite 370

Telephone: (714)985-3434 Attn: Tom Tatnall

Page: 7

Project ID: 32486-007 Project Name: Delphi System Corp

S i t e

Anaheim, CA 92801

AETL Job Number 1 Submitted 1 Client 38375 1 0 8 / 0 1 / 2 0 0 6 1 H&A

Method: 8082, Polychlorinated Biphenyls (PCBs) by GC - - -

QC Batch No: 080206

Our Lab I.D. Method Blank 38375.12 Client Sample I.D. EB-080106

Date Sampled 08/01/2006

Date Prepared 08/02/2006 08/02/2006

Preparation Method 3510~ 3 5 1 0 ~

Date Analyzed 08/04/2006 08/04/2006

Matrix Units Dilution Factor

Aroclor-1232 (PCB-1232) 1 1.0

Aroclor- 1242 (PCB- 12421 1.0

PQL 5.0

10.0

Analytes

Aroclor- 10 16 (PCB- 10 16)

Aroclor-122 1 (PCB-1221)

MDL 1.0

2.0

5.0

5.0

Aroclor- 1248 (PCB- 1248) 1 1.0

I Aroclor- 1262 (PCB- 1262)

Aroclor- 1268 (PCB- 1268) - -- -. -- ---

Aqueous

ug/L 1

Results

ND

ND

5.0

5.0

5.0

Aroclor-1254 (PCB-1254)

Aqueous

ug/L 1

Results

ND

ND

ND

ND

1.0

1.0

1.0

ND

ND

ND

ND

ND Aroclor- 1260 (PCB- 1260) 1 1.0

ND

ND

ND

5.0

5.0

Our Lab I.D. Method Blank % Rec.

108

Surrogates

I Tetrachloro-m-xylene --

ND

ND

38375.12 % Rec,

9 1

% R e c .Limit

30-150

ND

ND - -

Page 14: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American Environmental Testing Laboratory Inc. -- - - -- - - --

2834 & 2908 North N a o m ~ Street, Burbank, CA 9 1504 DOHS NO. 1541, LACSD NO. 10181 Tel. (888) 288-AETL (818) 845-8200 Fax (818) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

S i t e

120 1 N. Magnolia Avenue Anaheim, CA 92 80 1

--

T e l e p h o n e : (714) 985-3434 A t t n : Tom T a t n a l l

P a g e 8 C l i e n t

H &A P r o j e c t I D : 32486-007

P r o j e c t Name: Delphi S y s t e m Corp.

AETL Job Number 3 8 3 7 5

S u b m i t t e d - 0 8 / 0 1 / 2 0 0 6

Page 15: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American -- Environmental -- - Testing -- Laboratory Inc. 2834 &2908 North N a o m ~ Street, Burbank, CA 91504 DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

Ordered By k a F & Aldrich / 500 South Kraemer Blvd. ! Suite 370 I Brea, CA 9282 1-6723

S i t e

Magnolia Avenue Anaheim, CA 9280 1

Telephone: (714)985-3434 Attn: Tom Tatnall

QUALITY CONTROL REPORT

Page: 9

QC Batch No: 080106 Sample Spiked: 38354.08 QC Prepared: 08/01/2006 QC Analyzed: 08/01/2006 Units: mglL

- --- -- .- -

/ Sample I MS I MS 1 MS 1 MS DUP MS DUP / MS DUP RPD 1 M S I M ~ ~

Client -.

H &A Project ID: 32486-007 ProjectName: Delphi S y s t e m Corp.

Method: 60 1 OBSCAN, Total Arsenic

QC Batch No: 080106 Sample Spiked: 38354.08 QC Prepared: 08/01/2006 QC Analyzed: 08/01/2006 Units: mglL

aETL Job Number 38375

-

Analytes

I Arsenic

Submitted 08/01/2006

Result

0.007

Concen

1.00

-- --

LCSILCSD

% Limit Analytes

I

Recov

0 .91

I

LCS

Concen

80-120 -

Arsenic - - - - - -

% REC

90

LCS

Recov

1.00

LCS

% REC

Concen

1.00

0.85

Recov

0.92

85

% REC

91

%

1.1

% Limit

80-120

% Limit

(15 /

Page 16: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American Environmental Testing Laboratory Inc. - -. .. .-

2834 &2908 North Naomi Street, Burbank, CA 91 504 DOHS NO: 1541, LACSD NO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

Ordered B y -.

Haley & Aldrich 500 South Kraemer Blvd. Suite 370 Brea. CA 92821-6723

Site

120 1 N. Mkgnolia Avenue Anaheim, CA 92801

Telephone: (714)985-3434 Attn: Tom Tatnall

Method: 8082, Polychlorinated Biphenyls (PCBs) by GC QUALITY CONTROL REPORT

Page: 10

QC Batch No: 080206 Sample Spiked: 080206 QC Prepared: 08/02/2006 QC Analyzed: 08/04/2006 Units: uglL

Project ID: 32486-007 Project Name: Delphi S y s t e m Corp.

I 1 Sample MS 1 MS MS 1 MS DUP 1 MS DUP MS DUP RPD MSIMSD MS RPD 1

QC Batch No: 080206 Sample Spiked: 080206 QC Prepared: 08/02/2006 QC Analyzed: 08/04/2006 Units: uglL

C l i e n t ; H&A i

AETL Job Number 38375

Analytes

Aroclor- 1260 (PCB- 1260) -- -

Submitted 08 /01 /2006

Analytes / Concen Recov % REC 1 % Limit I 1 1 I I 1 !

Result

0 . 0

1

Concen

2.50

LCSILCSD T L C S 1 LCS I

! I I I I I I i I I 1

LCS

I Aroclor-1260 (PCB- 1260) --

Recov

2 .53

2.50 --

% REC

101

2.03

Concen

2.50

81

Recov

2 .70

75-125

% REC

108

%

6 . 7

% Limit

75-125

% Limit

<20

Page 17: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American Environmental Testing Laboratory Inc. -- - - - p~

2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (818) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

O r d e r e d By paley & Aldrich 500 South Kraemer Blvd. Suite 370 Brea. CA 9282 1-6723

S i t e -

1201 N. Magnolia Avenue Anaheim, CA 9280 1

Telephone: (7 14)985-3434 Attn: Tom Tatnall

QC Batch No: 080206-1 Sample Spiked: 38375.01 QC Prepared: 08/02/2006 QC Analyzed: 08/02/2006 Units: mglKg

Page: 11

QC Batch No: 080206-1 Sample Spiked: 38375.01 QC Prepared: 08/02/2006 QC Analyzed: 08/02/2006 Units: mglKg

client-- H &A

--

Project ID: 32486-007 Project Name: Delphi System Corp.

Analytes

Arsenic

Method: (60 1 OBSCAN), Arsenic by ICP QUALITY CONTROL REPORT

AETL Job ~ilmber 38375

Sample

Result

0.062

7 Analytes

Arsenic

-submitted 08/01/2006

MS

Concen

1.00

LCS

Concen

1.00

MS

Recov

1.07

LCS

Recov

1.01

MS

% REC

101

LCS

% REC

101

LCSILCSD

% Limit

80-120

MS DUP

Concen

1.00

MS DUP

Recov

1.06

MSDUP

% REC

100

RPD

%

<1

MSIMSD

% Limit

80-120

MS RPD

% Limit

<15

Page 18: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (8 18) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

O r d e r e d B y

500 South Kraemer Blvd.

Brea. CA 9282 1-6723

S i t e

Anaheim, CA 9280 1

Telephone: (714)985-3434 Attn: Tom Tatnall

Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QUALITY CONTROL REPORT

Page: 12

QC Batch No: 080206 Sample Spiked: 080206 QC Prepared: 08/02/2006 QC Analyzed: 08/02/2006 Units: uglKg

I I Sample MS / MS MS MS DUP 1 MS DUP MS DUP 1 RPD MSlMSD 1 MS RPD 1

Submitted 1 Client

08/01/2006 L-_ H&A , Project ID: 32486-007 Project Name: Delphi S y s t e m Corp.

- AETL J O ~ Number

38375

QC Batch No: 080206 Sample Spiked: 080206 QC Prepared: 08/02/2006 QC Analyzed: 08/02/2006 Units: ug/Kg

Analytes / Result Concen

500.00 Aroclor-1260 (PCB-1260) - -.

0.0

--

1

Recov

440.00

I

LCSILCSD

% Limit

50-150

Analytes

Aroclor- 1260 (PCB-1260)

% REC

88

LCS

Concen

500.00

Concen

500.00

LCS

Recov

495.00

Recov

500.00

LCS

% REC

99

% REC

100

%

12.8

% Limit

50-150

% Limit

<50

Page 19: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

Ordered Bv

American Environmental --- - Testing -- Laboratory Inc. 2834 8~2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (8 18) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

I Haley & Aldrich 1 500 South Kraemer Blvd. Suite 370

Telephone: (714)985-3434 Attn: Tom Tatnall

S i t e

120 1 N. Magnolia Avenue Anaheim, CA 9280 1 1

Method: (8082), Polychlorinated Biphenyls (PCBs) by GC

Page: 13

QUALITY CONTROL REPORT

QC Batch No: 080306 Sample Spiked: 080306 QC Prepared: 08/03/2006 QC Analyzed: 08/03/2006 Units: uglKg

Client - 1 H&A 1 '

Submitted 08/01/2006

Project ID: 32486-007 Project Name: Delphi System Corp.

QC Batch No: 080306 Sample Spiked: 080306 QC Prepared: 08/03/2006 QC Analyzed: 08/03/2006 Units: uglKg

AETL Job Number 38375

Analytes

Aroclor- 1260 (PCB- 1260) - --

I

I 1 Analytes

LCS LCS LCS LCSILCSD

Concen Recov % REC % Limit

Sample

Result

0.0

MS

Concen

500.00

MS

Recov

450.00

MS

% REC

90

MS DUP

Concen

500.00

MS DUP

Recov

520.00

MSDUP

% REC

104

RPD

%

14.4

MSIMSD

% Limit

50-150

MS RPD

% Limit

<50 , _--A

Page 20: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American - Environmental Testing - Laboratory Inc. 2834 & 2908 North Naomi Street, Burbank, CA 9 1504 -DOHS NO: 1541, LACSD NO. 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com

Data Qualifiers and Descriptors

Data Qualifier:

*. In the QC section, sample results have been taken directly from the ICP reading. No preparation factor has been applied.

Analyte was present in the Method Blank.

Result is from a diluted analysis.

Result is beyond calibration limits and is estimated.

Analysis was performed over the allowed holding time due to circumstances which were beyond laboratory control.

Analyte was detected . However, the analyte concentration is an estimated value, which is between the Method Detection Limit (MDL) and the Practical Quantitation Limit (PQL).

Matrix spike recovery is outside control limits due to matrix interference. Laboratory Control Sample recovery was acceptable.

Surrogate recovery is outside control limits due to matrix interference.

The analysis of the sample required a dilution such that the surrogate concentration was diluted below the method acceptance criteria.

Results represent LCS and LCSD data.

Definition :

%Limi: Percent acceptable limits.

%REC : Percent recovery.

C0n.L: Acceptable Control Limits

Conce: Added concentration to the sample.

LCS: Laboratory Control Sample

MDL: Method Detection Limit is a statistically derived number which is specific for each instrument, each method, and each compound. It indicates a distinctively detectable quantity with 99% probability.

MS: Matrix Spike

MS DU: Matrix Spike Duplicate

Page 21: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American Environmental Testing Laboratory Inc. -- ~ -~ -- ~ -- ~ - ~ - - -.

2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO. 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com

Data Qualifiers and Descriptors

ND : Analyte was not detected in the sample at or above MDL.

PQL: Practical Quantitation Limit or ML (Minimum Level as per RWQCB) is the minimum concentration that can be quantified with more than 99% confidence. Taking into account all aspects of the entire analytical instrumentation and practice.

Recov: Recovered concentration in the sample.

RPD : Relative Percent Difference

Page 22: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American Environmental Testing -- - Laboratory -. Inc. pp -p -

2834 & 2908 North N a o m ~ Street, Burbank, CA 91504 -DOHS NO. 1541, LACSD NO. 10181 Tel. (888) 288-AETL (818) 845-8200 Fax. (818) 845-8840 www.aetlab.

Telephone: (714) 985-3434 Attention: Tom Tatnall

Ordered By H-

Job Number Order Date Client

38386 1 08/02/2006 1 H &A

Haley & Aldrich 500 South Kraemer Blvd. Suite 370

Brea, CA 92821-6723

Project ID: 32486-007 Project Name: Delphi System Corp.

Site : 1201 N. Magnolia Avenue Anaheim, CA 92801

Number of Pages 12 ch, Iflc. Date Received 08/02/2006

Date Reported 08/07/2006

Enclosed please find results of analyses of 1 water and 11 solid waste samples which were analyzed as specified on the attached chain of custody. If there are any questions, please do not hesitate to call.

Checked By: Approved By:

Cyrus Razmara, Ph. D. Laboratory Director

Page 23: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

CHAIN OF CUSTODY RECORD N? 43951

Page 24: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:
Page 25: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

TABLE Summary of Aqueous Analytical Results for Polychlorinated Biphenyls (PCBs) by GC

1201 N. Magnolia Avenue Anaheim, CA 92801

Polychlorinated Biphenyls (PCBs) by GC. Method: 8082

1) "ND<X" INDICATES CONSTITUENT(S) NOT DETECTED AT OR ABOVE METHOD DETECTION LIMIT.

2) "J" INDICATES ANALYTE WAS DETECTED. HOWEVER, ANALYTE CONCENTRATION IS AN ESTIMATED VALUE WHICH IS BETWEEN

THE METHOD DETECTION LIMIT (MDL) AND THE PRACTICAL QUANTITATION LIMIT(PQL).

3) "D" INDICATES THE SAMPLE WAS DILUTED TO BRING THE ANALYTE CONCENTRATION WITHIN CALIBRATION RANGE.

File: AQ-8082.~1~

Page 26: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

TABLE Summary of Solid Waste Analytical Results for Arsenic by ICP

1201 N. Magnolia Avenue Anaheim, CA 92801

Arsenic by ICP. Method: (6010BSCAN)

1) "ND<X" INDICATES CONSTITUENT(S) NOT DETECTED AT OR ABOVE METHOD DETECTION LIMIT.

2) "J" INDICATES ANALYTE WAS DETECTED. HOWEVER. ANALYTE CONCENTRATION IS AN ESTIMATED VALUE WHICH IS BETWEEN

THE METHOD DETECTION LIMIT (MDL) AND THE PRACTICAL QUANTITATION LIMIT(PQL).

3) "D" INDICATES THE SAMPLE WAS DILUTED TO BRING THE ANALYTE CONCENTRATION WITHIN CALIBRATION RANGE.

Sample Date

Laboratory Job Number

Arsenic

File: SW-6010BSCAN.xls

5.0 5.0 500 mg/Kg

8/2/2006

38386

2.305

- 8/2/2006

38386

3.655

8/2/2006

38386

16.4

8/2/2006

38386

4.60J

8/2/2006

38386

4.20J

8/2/2006

38386

14.9

8/2/2006

38386

4.60J

8/2/2006

38386

24.5

8/2/2606

38386

4.305

Page 27: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:
Page 28: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

TABLE Summary of Solid Waste Analytical Results for Polychlorinated Biphenyls (PCBs) by GC

1201 N. Magnolia Avenue Anaheim, CA 92801

Polychlorinated Biphenyls (PCBs) by GC. Method: (8082)

Sample Date

Laboratory Job Number

Aroclor-1016 (PCB-1016) udKg

Aroclor-1221 (PCB-? 221 ) -

udKg

Aroclor-1232 (PCB-1232) udKg

Aroclor-1242 (PCB-1242) ug/Kg

Aroclor-1248 (PCB-1 248) ug/Kg

Aroclor-1254 (PCB-1 254) ug/Kg

Aroclor-1260 (PCB-1260) ug/Kg

Aroclor-1262 (PCB-1 262) ug/Kg

Aroclor-1268 (PCB-1 268) udKg

1) "NDcX" INDICATES CONSTITUENT(S) NOT DETECTED AT OR ABOVE METHOD DETECTION LIMIT.

2) "J" INDICATES ANALYTE WAS DETECTED. HOWEVER, ANALYTE CONCENTRATION IS AN ESTIMATED VALUE WHICH IS BETWEEN

THE METHOD DETECTION LIMIT (MDL) AND THE PRACTICAL QUANTITATION LIMIT(PQL).

3) "D" INDICATES THE SAMPLE WAS DILUTED TO BRING THE ANALYTE CONCENTRATION WITHIN CALIBRATION RANGE.

File: SW-8082.~1~

Page 29: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

. . . .- - .- .- -

American Environmental .- - Testing -- - Laboratory -. Inc. 2834 &2908 North N a o m ~ Street, Burbank, CA 91504 =DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (81 8) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

Ordered By

Anaheim, CA 9280 1 Suite 370

Telephone: (714)985-3434 Attn : Tom Tatnall

Page: 2 Client

H&A I Project ID: 32486-007 Project Name: Delphi System Corp .

Our Lab I.D.

Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 080306

i

% Rec.

94

Surrogates

1 Tetrachloro-m-xylene 4-

AETL Job Number 38386

% R e c . Limit 30-150

Submitted

08/02/2006

38386.01 % Rec.

7 9

38386.02 % Rec.

8 4

38386.03 % Rec.

8 7

38386.04 % Rec.

9 6

Page 30: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American - Environmental . - -. -- - --- Testing Laboratory - -- Inc. 2834 8 ~ 2 9 0 8 North Naom~ Street, Burbank, CA 91504*DOHS NO. 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (8 18) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

Ordered By

500 South Kraemer Blvd. Suite 370

Telephone: (714)985-3434 Attn: Tom Tatnall

S i t e

Anaheim, CA 9280 1

Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 080306

Page: 3

H &A Project ID: 32486-007 Project Name: Delphi System C o r p .

38386.09 CSO276-CC-0

Aroclor- 1248 (PCB- 1248)

Aroclor-1254 (PCB-1254)

Aroclor-1260 (PCB-1260)

AETL Job Number 38386

Aroclor- 1262 (PCB- 1262)

Aroclor-1268 (PCB-1268)

- Submitted 08/02/2006

38386.07 CSO274-CC-0

38386.06 CSO273-CC-0

- - - Our Lab I.D. Client Sample I.D.

25.0

25.0

25.0

/ Our Lab I.D. Surrogates / % ~ e c . ~ i r n i b

- 38386.08

CSO275-CC-0 38386.05

CSO272-CC-0

25.0

25.0

50.0

50.0

50.0

38386.05 % Rec.

50.0

50.0

107

ND

ND

38386.06 % Rec.

ND

ND

ND

ND

ND

38386.07 % Rec.

ND

ND

ND

ND

ND

38386.08 % Rec.

ND

ND

38386.09 ' % Rec.

ND

ND

ND

42.05

ND

ND

ND

ND

ND

ND

Page 31: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American Environmental - - --. . - - Testing Laboratory Inc. - -- -- -- -- - -- . . --

2834 & 2908 North Naomi Street, Burbank, CA 91 504 *DOHS NO: 1541, LACSD NO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

O r d e r e d By 1 Haley & Aldrich 500 South Kraemer Blvd. Suite 370 Brea, CA 9282 1-6723

Telephone: (714)985-3434 Attn: Tom Tatnall

Page: 4 Project ID: 32486-007 Project Name: Delphi Sys tem Corp.

S i t e

1201 N. Magnolia Avenue Anaheim, CA 92801

Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 080306

AETL Job Number ( Submitted 38386 1 08/02/2006

Client H &A

Our Lab LD. i Client Sample I.D.

38386.10 CSO277-CC-0

Date Sampled Date Prepared Pre~aration Method

08/02/2006

08/03/2006

3 5 5 0 ~

Date Analyzed Matrix

08/04/2006

Solid Waste

Analytes MDL

Aroclor- 1232 (PCB- 1232)

Aroclor-1242 (PCB-1242)

, Aroclor-1248 (PCB-1248)

1 Aroclor- 1268 (PCB-1268) 1 500 / 1000 1 ND 1 1 I 1 1

i

PQL

1000

1000

Aroclor- 10 16 (PCB- 10 16)

Results

ND

ND

500

500

500

500

I Aroclor-1254 (PCB-1254)

Aroclor-1260 (PCB-1260)

Aroclor- 1262 (PCB- 1262)

Aroclor- 122 1 (PCB- 122 1) 1 500

1000

1000

1000

500

500

500

1000

1000 ----

1000

ND

ND

ND

38386.10 % Rec.

Our Lab I.D. , Surrogates

ND

ND

% R e c . L i m i t i

I

I

23,400

Page 32: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

Ordered BY

American Environmental - -- - Testing Laboratory - - Inc. 2834 &2908 North N a o m ~ Street, Burbank, CA 91504 DOHS NO. 1541,LACSDNO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (81 8) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

S i t e

1500 South Kraemer Blvd. I Suite 370 ~ r e a . CA 92821-6723

1201 N, Magnolia Avenue Anaheim, CA 9280 1

Telephone: (714)985-3434 Attn: Tom Tatnall

Pane: 5

Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 080306

- a -

Client -

H &A Project ID: 32486-007 Project Name: Delphi System Corp.

- - Our Lab I.D. Client Sample I.D.

38386.11 CSO278-CC-0

00-01

Date Sampled Date Prepared Preparation Method Date Analyzed Matrix Units

- AETL Job Number

38386

I Dilution Factor / ~ n a l ~ t e s MDL PQL

/ rocl lor- 10 16 (PCB- 10 16) 1 25.0 50.0

Submitted

08/02/2006

08/02/2006

08/03/2006

3550B

08/04/2006

Solid Waste

udKn 1

Results

ND

Aroclor- 122 1 (PCB- 122 1) 25.0 50.0

Aroclor-1232 (PCB-1232) 25.0 50.0

Aroclor- 1242 (PCB-1242) 25.0 50.0

Aroclor- 1248 (PCB-1248) 25.0 50.0

Aroclor- 1254 (PCB- 1254) 25.0 50.0

Aroclor- 1260 (PCB-1260) 25.0 50.0

ND

ND

ND

167

ND

ND

Aroclor-1262 (PCB-1262) 25.0 50.0

Aroclor- 1268 (PCB- 1268) 25.0 50.0

I

ND

ND

Our Lab I.D. Surrogates % R e c . Limib Tetrachloro-m-xvlene 1 30-150

I

38386.11 % Rec.

98

Page 33: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American Environmental Testing Laboratory Inc. - - pppp -- - - - - - - -

2834 &2908 North Naom~ Street, Burbank, CA 91504 DOHS NO 1541,LACSDNO 10181 Tel (888) 288-AETL (8 18) 845-8200 Fax. (8 18) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

Ordered By

Haley & Aldrich 500 South Kraemer Blvd.

/ Suite 370 I Brea, CA 92821-6723

Attn :

I Telephone: (714) 985-3434

Tom Tatnall

Page 6 Project ID: 32486-007 Project Name: Delphi System Corp.

Site

Anaheim, CA 9280 1

AETL Job Number Submitted Client 38386 08/02/2006 H&A

- .

Analytes Arsenic 62-32 *;n ""'q-' ' <y " "" ' <I%

i i ,> -i-

Methods of Analyses (601 OBSCAN) I

1 Date Prewared I I I !

08/02/2006 ! Date Analyzed 08/02/2006

Matrix Solid Waste

OC Batch Number 080206-2 ! -

/Units mg/Kg

Method Detection Limit 0.5 Practical Quantitation Limit 5.0

1 Dilution Factor I I

1

N / A ~ z h o d Blank 1 / I ND / I !

Page 34: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American Environmental - - - - Testing - - Laboratory Inc. 2834 &2908 North Naom~ Street, Burbank, CA 91504 DOHS NO. 1541,LACSDNO. 10181 Tel. (888) 288-AETL (818) 845-8200 Fax. (818) 845-8840 www.aetlab.com

ANALYTICAL RESULTS Ordered B y

500 South Kraemer Blvd. Suite 370 Brea, CA 9282 1-6723

Telephone: (7 14)985-3434 Attn: Tom Tatnall

S i t e 120 1 N. Magnolia Avenue Anaheim, CA 92801

Page: 7

Project ID: 32486-007 AETL Job Number Submitted Client Project Name: D e l p h i S y s t e m C o r p . 3 8 3 8 6 0 8 / 0 2 / 2 0 0 6 H &A

Method: 8082, Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 080206

Our Lab I.D. Method Blank 38386.12 Client Sample I.D. EB-080206

Date Sampled 08/02/2006

Date Pre~ared 08/02/2006 08/02/2006

1 Preparation Method 3510~ 3510~

1 Date Analyzed 08/04/2006 08/04/2006

i Matrix Aqueous Aqueous

I Units I I ug/L I ug/L I I I i I

- - 1 Dilution Factor 1 1 Analytes MDL PQL Results Results

I

Aroclor- 122 1 (PCB- 122 1) 2.0 10.0 ND ND 1 i

Aroclor- 1232 (PCB- 1232) 1.0 5.0 ND ND i

Aroclor- 1242 (PCB- 1242) 1.0 5.0 ND ND

Aroclor- 1248 (PCB- 1248) 1.0 5.0 ND ND I

Aroclor-1260 (PCB-] 260) 1.0 5.0 ND ND

Aroclor- 1262 (PCB- 1262) 1.0 5.0 ND ND

Aroclor- 1268 (PCB- 1268) 1.0 5.0 ND ND

Our Lab I.D. Method Blank 38386.12 / Surrogates %Rec.Limib % Rec. % Rec. 1 Tetrachloro-m-xvlene 1 30-150 108 77 1

Page 35: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American Environmental Testing Laboratory Inc. - --- -- - pp - -- - pppp - -

2834 &2908 North Naom~ Street, Burbdnk, CA 91504 -DOHS NO. 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 F a x (818) 845-8840 www.aet lab.com

ANALYTICAL RESULTS

Ordered By . - .-

Haley & Aldrich South Kraemer BLvd.

/ Suite 370 / Brea, CA 92821-6723 Telephone: (714) 985-3434

Attn : Tom Tatnall

Page 8 Project ID: 32486-007 Project Name: Delphi System Corp.

Site

120 1 N. Magnolia Avenue Anaheim, CA 92801

AETL Job Number Submitted I Client 38386 / 08/02/2006 / H&A

ilution Factor

Units Method Detection Limit Practical Quantitation Limit

mglL i 0.05

0.10 i , I

Page 36: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American Environmental Testing Laboratory Inc. -- - - - - - -- - - --- -- -- -- pp - -

2834 &2908 North Naom~ Street, Burbank, CA 91504-DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL ( 8 18) 845-8200 Fax: (8 18) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

O r d e r e d By

500 South Kraemer Blvd. Suite 370

Telephone: (714)985-3434 Attn: Tom Tatnall

S i t e

120 1 N. Magnolia Avenue Anaheim, CA 9280 1

Pane: 9

Method: 60 1 OBSCAN, Total Arsenic

"

QUALITY CONTROL REPORT

QC Batch No: 080306 Sample Spiked: 38392.01 QC Prepared: 08/03/2006 QC Analyzed: 08/03/2006 Units: mglL

Submitted

08/02/2006 Project ID: 32486-007 Project Name: Delphi SYS t em Corp .

Sample MS MS 1 MS 1 MS DUP MS DUP I MS DUP RPD 1 MSlMSD I MS RT

- AETL Job Number

38386

/ Analytes / Result I Concen Recov / % REC I Concen Recov / % REC % % Limit / % Limit 1

QC Batch No: 080306 Sample Spiked: 38392.01 QC Prepared: 08/03/2006 QC Analyzed: 08/03/2006 Units: mglL

- .

LCSILCSD

% Lim~t

80-120

Analytes

Arsenic --

LCS

Concen

1.00

LCS

Recov

0.98

LCS

% REC

98

Page 37: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

O r d e r e d Bv

American Environmental Testing --- Laboratory -- Inc. 2834 & 2908 North Naom~ Street, Burbank, CA 91504 *DOHS NO 1541, LACSDNO. 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax. (8 18) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

1 Haley & Aldrich 1 500 South Kraemer Blvd. Suite 370 Brea. CA 9282 1-6723

S i t e

1201 N. Magnolia Avenue Anaheim, CA 9280 1

Telephone: (714)985-3434 Attn: Tom Tatnall

Page: 10

Method: 8082, Polychlorinated Biphenyls (PCBs) by GC QUALITY CONTROL REPORT

-

QC Batch No: 080206 Sample Spiked: 080206 QC Prepared: 08/02/2006 QC Analyzed: 08/04/2006 Units: uglL

Client H &A

--A

Project ID: 32486-007 Project Name: Delphi System Corp .

QC Batch No: 080206 Sample Spiked: 080206 QC Prepared: 08/02/2006 QC Analyzed: 08/04/2006 Units: uglL

Analytes

Aroclor- 1260 (PCB- 1260) - - - - - .. - -. -

LCS LCS LCS LCSILCSD

Analytes Concen Recov % REC % Limit

2.50 2.03 81 75-125

AETL Job Number 38386

Submitted 08/02/2006

Sample

Result

0.0

MS

Concen

2.50

MS

Recov

2.53

MS

% REC

101

MSDUP

Concen

2.50

MS DUP

Recov

2.70

MSDUP

% REC

108

RPD

%

6.7

MSIMSD

% Limit

75-125

MSRPD

% Limit

<20

Page 38: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American Environmental - Testing Laboratory Inc. - -- -- - - -. --- -- .. -

2834 8 ~ 2 9 0 8 North N a o m ~ Street, Burbank, CA 91504-DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (81 8) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

Ordered By

500 South Kraemer Blvd. Suite 370 1 Brea, CA 92821-6723

Telephone: (714)985-3434 Attn: Tom Tatnall

Page: 11 Project ID: 32486-007 Prni~rt Name. D e l ~ h i Svs tem Corr,.

S i t e --

1201 N. Magnolia Avenue Anaheim, CA 92801

AETL Job umber / Submitted 1 Client 38386 1 08/02/2006 1 H &A

Method: (6010BSCAN), Arsenic by ICP QUALITY CONTROL REPORT

QC Batch No: 080206-2 Sample Spiked: 38386.04 QC Prepared: 08/02/2006 QC Analyzed: 08/02/2006 Units: mglKg

QC Batch No: 080206-2 Sample Spiked: 38386.04 QC Prepared: 08/02/2006 QC Analyzed: 08/02/2006 Units: mglKg

I I Analytes

Arsenic

Sample

Result

0.092

1

MS

Concen

1.00

LCSILCSD

% Limit

80-120

--

Analytes

Arsenic

MS

Recov

1.06

LCS

Concen

1.00

MS

% REC

97

LCS

Recov

1.06

LCS

% REC

106

MS DUP

Concen

1.00

MS DUP

Recov

1.08

MSDUP

% REC

9 9

RPD

%

2.0

MSIMSD

% Limit

80-120

MSRPD

% Limit

4 5 _1

Page 39: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American Environmental Testing Laboratory Inc. - - - . .-A - - -- . . - - - -

2834 8 ~ 2 9 0 8 North N a o m ~ Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (81 8) 845-8200 Fax: ( 8 18) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

Ordered By

Anaheim, CA 92801

Telephone: (714)985-3434 Attn: Tom Tatnall

Page: 1 2 Client

H&A - -. 1 Project ID: 32486-007 ProjectName: Delphi System Corp.

AETL Job Number 38386

Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QUALITY CONTROL REPORT

QC Batch No: 080306 Sample Spiked: 080306 QC Prepared: 08/03/2006 QC Analyzed: 08/03/2006 Units: uglKg

Submitted 08/02/2006

MSIMSD

% Lim~t

75-125

Analytes

Aroclor-1260 (PCB-1260)

M S ~ % Limit

<20

MSDUP

% REC

104

QC Batch No: 080306 Sample Spiked: 080306 QC Prepared: 08/03/2006 QC Analyzed: 08/03/2006 Units: uglKg

RPD

%

14.4

Sample

Result

0 .0

Analytes

Aroclor- 1260 (PCB- 1260) - -

MS

Concen

500 .00

LCS

Concen

500.00

MS

Recov

450 . O O

LCS

Recov

545.00

MS

% REC

90

LCS

% REC

109

LCSILCSD

% Limit

75-125

MSDUP

Concen

500.00

MS DUP

Recov

520.00

Page 40: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American Environmental ~ .--- - - Testing ~ p p ~ Laboratory Inc. 2834 8 ~ 2 9 0 8 North Naomi Street, Burbank, CA 91 504*DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (81 8) 845-8200 Fax: (8 18) 845-8840 www.aetlab.com

Data Qualifiers and Descriptors

Data Qualifier:

*. In the QC section, sample results have been taken directly from the ICP reading. No preparation factor has been applied.

Analyte was present in the Method Blank.

Result is from a diluted analysis.

Result is beyond calibration limits and is estimated.

Analysis was performed over the allowed holding time due to circumstances which were beyond laboratory control.

Analyte was detected . However, the analyte concentration is an estimated value, which is between the Method Detection Limit (MDL) and the Practical Quantitation Limit (PQL).

Matrix spike recovery is outside control limits due to matrix interference. Laboratory Control Sample recovery was acceptable.

Surrogate recovery is outside control limits due to matrix interference.

The analysis of the sample required a dilution such that the surrogate concentration was diluted below the method acceptance criteria.

Results represent LCS and LCSD data.

%Limi: Percent acceptable limits.

%REC: Percent recovery.

C0n.L: Acceptable Control Limits

Conce: Added concentration to the sample.

LCS: Laboratory Control Sample

MDL: Method Detection Limit is a statistically derived number which is specific for each instrument, each method, and each compound. It indicates a distinctively detectable quantity with 99% probability.

MS: Matrix Spike

MS DU: Matrix Spike Duplicate

Page 41: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American -- Environmental - Testing - Laboratory Inc. 2834 & 2908 North Naom~ Street, Burbank, CA 9 1504 DOHS NO: 1541, LACSD NO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (81 8) 845-8840 www.aetlab.com

Data Qualifiers and Descriptors

ND: Analyte was not detected in the sample at or above MDL.

PQL: Practical Quantitation Limit or ML (Minimum Level as per RWQCB) is the minimum concentration that can be quantified with more than 99% confidence. Taking into account all aspects of the entire analytical instrumentation and practice.

Recov: Recovered concentration in the sample.

RPD: Relative Percent Difference

Page 42: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

Enclosed please find results of analyses of 1 water and 13 solid waste samples which were analyzed as specified on the attached chain of custody. If there are any questions, please do not hesitate to call.

Page 43: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:
Page 44: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:
Page 45: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

TABLE Summary of Aqueous Analytical Results for Polychlorinated Biphenyls (PCBs) by GC

1201 N. Magnolia Ave. Anaheim, CA 92801

Polychlorinated Biphenyls (PCBs) by GC. Method: 8082

Sample Date 912612006

Laboratory Job Number 39098

Aroclor-1016 (PCB-1016) ug/L ND<l 0

~ r o c l o ~ 2 2 1 (PCB-1221 ) uglL ND<2 0 -- - -

Aroclor-1232 (PCB-1232) uglL NDc1 0

rocl lor-1 242 (PCB-1242) uglL ND<1 0

Aroclor-1248 (PCB-7248) u g l ~ ~ D c i 0

Aroclor-1254 (PCB-1254) ug/L ND<l 0

~roclor-~260<P~~-1260) ug1L ND<1 0

~rockr-1262 (PCB-1262) -

uglL NDc1 0 - --- -- -

Aroclor-1268 (PCB-1268) uglL ND<1 0 - -

1) "ND<X INDICATES CONSTITUENT(S) NOT DETECTED AT OR ABOVE METHOD DETECTION LIMIT.

2) "J" INDICATES ANALYTE WAS DETECTED. HOWEVER, ANALYTE CONCENTRATION IS AN ESTIMATED VALUE WHICH IS BETWEEN

THE METHOD DETECTION LIMIT (MDL) AND THE PRACTICAL QUANTITATION LIMIT(PQL).

3) "D" INDICATES THE SAMPLE WAS DILUTED TO BRING THE ANALYTE CONCENTRATION WITHIN CALIBRATION RANGE.

File: AQ-8082.~1~

Page 46: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

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Page 47: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

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Page 48: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

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Page 49: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:
Page 50: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American Environmental Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank. CA 91504*DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (81 8) 845-8200 Fax: (818) 845-8840 www.aetlab.com

-

ANALYTICAL RESULTS

O r d e r e d By S i t e

Haley & Aldrich 500 South Kraemer Blvd. Suite 370 Brea, CA 9282 1-6723 I Telephone: (714) 985-3434 Attn: Tom Tatnall

Page 2 Project ID: 32486-007 Project Name: Delphi System Corp.

39098.09 39098.1 0 39098.1 1 39098.12 39098.13

NIA

CSO287-CC-000-01 CSO288-CC-000-01 CSO289-CC-000-01 CSO290-CC-000-01

CS0291 -CC-000-01 Method Blank

09/26/2006 09/26/2006 09/26/2006 0912612006

09/26/2006 I I

3.905

20.3

17.4

3.105

5.05

ND

Page 51: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

Ordered By

American Environmental Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (81 8 ) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

Haley & Aldrich 500 South Kraemer Blvd. Suite 370 Brea, CA 9282 1-6723 1

S i t e

Telephone: (714)985-3434 Attn: Tom Tatnall

Page: 3

Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 092706

Project ID: 32486-007 Project Name: Delphi System Corp .

, ,&ETZ1' Sob; ,Nq#bW 39098

211 r~abx*hb- I 1""" , - 'lt\lj ,,,,,, ,,L,, ,, I

Client Sample I.D.

' " 8 9 i t t e d ' " 0 9 / 2 6 / 2 0 0 6

;\:- ' 1 Mq*?a B~X&

" Cliant '

H &A ,

1 1 1 ; , , , ~ ~ ~ ~ ~ ~ ~ ~ ~ ~ , l , I I , , , ~ ~ ~ ~ . ~ 2 ~ ~ ~ ! i ~ ~ ~~0279-CC-01 ~ ~ 0 2 8 0 - C C - 0

,' ; 320p~03~ 1'

CS028 1-CC-0 ir,&s*o4 i : CSO282-CC-0

Page 52: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American Environmental Testing Laboratory Inc. 2834 8 ~ 2 9 0 8 North Naomi Street, Burbank. CA 91504 DOHS NO: 1541,LACSDNO. 10181 Tel: (888) 288-AETL (81 8) 845-8200 Fax: (81 8 ) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

Telephone: (7 14)985-3434 Attn: Tom Tatnall

S i t e

Page: 4

Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 092706

&ur L S ~ -' i'i I I

Client Sample I.D. CSO283-CC-0 CSO285-CC-0 CSO284-CC-0 CSO286-CC-0 A$M$r CSO287-CC-0

Page 53: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American Environmental Testing Laboratory Inc. 2834 8 ~ 2 9 0 8 North Naomi Street, Burbank, CA 91504*DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

Ordered Bv Site

Telephone: (7 14)985-3434 Attn: Tom Tatnall

Page: 5 Project ID: 32486-007 Proiect Name: Delphi S y s t e m Corp.

''8bb ' N*? 1' ~ S U i t t e ? , - 1 "Client 39098 1 09 /26 /2006 1 H &A

Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 092706

0"IH ' "XD. .~ 1 ' 1 1 ' $ Client Sample I.D. CSO290-CC-0 CSO291-CC-0 CSO288-CC-0 CSO289-CC-0

Page 54: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American Environmental Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (8 18) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

Telephone: (714)985-3434 Attn: Tom Tatnall

Page: 6 Project ID: 32486-007 Proiect Name: Delphi System Corp .

S i t e

Method: 8082, Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 092706

Page 55: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

Ordered Bv

American Environmental Testing Laboratory Inc. 2834 8~2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

Telephone: (7 14)985-3434 Attn: Tom Tatnall

Page: 7 Project ID: 32486-007 Project Name: Delphi S y s t e m Corp.

S i t e

Method: 601 OBSCAN, Total Arsenic QUALITY CONTROL REPORT

QC Batch No: 092906 Sample Spiked: 39098.14 QC Prepared: 09/29/2006 QC Analyzed: 09/29/2006 Units: mglL

QC Batch No: 092906 Sample Spiked: 39098.14 QC Prepared: 09/29/2006 QC Analyzed: 09/29/2006 Units: mglL

Page 56: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

O r d e r e d By

American Environmental Testing Laboratory Inc. 2834 8~2908 North Naorni Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

Telephone: (714)985-3434 Attn: Tom Tatnall

- Project ID: 32486-007 Proiect Name: Delphi Sys tem Corp.

S i t e

Method: 8082, Polychlorinated Biphenyls (PCBs) by GC QUALITY CONTROL REPORT

QC Batch No: 092706 Sample Spiked: 092706 QC Prepared: 09/27/2006 QC Analyzed: 09/28/2006 Units: uglL

QC Batch No: 092706 Sample Spiked: 092706 QC Prepared: 09/27/2006 QC Analyzed: 09/28/2006 Units: uglL

Page 57: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American Environmental Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 -DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (81 8) 845-8200 Fax: (81 8) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

Attn: Tom Tatnall

QC Batch No: 100206 Sample Spiked: 39098.01 QC Prepared: 10102/2006 QC Analyzed: 10/02/2006 Units: mglKg

Page: 9

QC Batch No: 100206 Sample Spiked: 39098.01 QC Prepared: 1010U2006 QC Analyzed: 10lOU2006 Units: mglKg

Project ID: 32486-007 Project Name: Delphi System Corp .

Method: (6010BSCAN), Arsenic by ICP QUALITY CONTROL REPORT

AETL 39098 J P - ~

0 9 / 2 6 / 2 0 0 6 1 H &A

Page 58: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American Environmental Testing Laboratory Inc. 2834 & 2908 North Naomi Street, Burbank, CA 91504 DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (8 18) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

O r d e r e d By S i t e

Telephone: (7 14)985-3434 Attn: Tom Tatnall

Page: 10 - Project ID: 32486-007 Project Name: Delphi Sys tem Corp.

Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QUALITY CONTROL REPORT

QC Batch No: 092706 Sample Spiked: 092706 QC Prepared: 09/27/2006 QC Analyzed: 09/28/2006 Units: uglKg

QC Batch No: 092706 Sample Spiked: 092706 QC Prepared: 09/27/2006 QC Analyzed: 09/28/2006 Units: uglKg

Page 59: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American Environmental Testing Laboratory Inc. 2834 & 2908 North Naomi Street, Burbank, CA 9 1504 DOHS NO: 1541, LACSDNO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (8 18) 845-8840 www.aetlab.com

Data Qualifiers and Descriptors

Data Qualifier:

Definition:

%Limi:

%REC :

C0n.L:

Conce:

LCS:

MDL:

MS:

MS DU:

In the QC section, sample results have been taken directly from the ICP reading. No preparation factor has been applied.

Analyte was present in the Method Blank.

Result is from a diluted analysis.

Result is beyond calibration limits and is estimated.

Analysis was performed over the allowed holding time due to circumstances which were beyond laboratory control.

Analyte was detected . However, the analyte concentration is an estimated value, which is between the Method Detection Limit (MDL) and the Practical Quantitation Limit (PQL).

Matrix spike recovery is outside control limits due to matrix interference. Laboratory Control Sample recovery was acceptable.

Surrogate recovery is outside control limits due to matrix interference.

The analysis of the sample required a dilution such that the surrogate concentration was diluted below the method acceptance criteria.

Results represent LCS and LCSD data.

Percent acceptable limits.

Percent recovery.

Acceptable Control Limits

Added concentration to the sample.

Laboratory Control Sample

Method Detection Limit is a statistically derived number which is specific for each instrument, each method, and each compound. It indicates a distinctively detectable quantity with 99% probability.

Matrix Spike

Matrix Spike Duplicate

Page 60: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:
Page 61: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American Environmental Testing - Laboratory Inc. 2834 & 2908 North Naomi Street, Burbank, CA 9 1504 DOHS NO: 1541, LACSD NO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (81 8) 845-8840 www.aetlab.com

RECrT"-- ' ~ 3

Ordered B y O C T 1 9 2006

Telephone: (714) 985-3434

Attention: Tom Tatnall

Jag Number Order Date Client 39287 1 10/09/2006 1 H&A

Project ID: 32486-007 Project Name: Delphi System Corp.

Site : 1201 N. Magnolia Ave.

Anaheim, CA 92801

Enclosed please find results of analyses of 13 concrete samples which were analyzed as specified on the attached chain of custody. If there are any questions, please do not hesitate to call.

Checked By: Approved By: v-

Cyrus Razmara, Ph. D.

Laboratory Director

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Cyrus Razmara

From: Hoggan, Kelly [[email protected]]

Sent: Monday, October 09,2006 11 :51 AM

To: Cyrus Razmara; Jim Lin

Subject: Additional Analysis for Job # 39098

Jim and Cyrus,

Please run lead 6010B on all thirteen concrete matrix samples from Job # 39098 with 3 day TOT. CS0279-SS-000-01 through CS0291~SS~000~01 .

Thanks,

Kelly Hoggan Geologist Haley A. Aldrich, Inc. 500 S. Kraemer Blvd., Suite 370 Brea, CA 92821-6723 Direct Line: 714.984.21 04 Cell: 714.709.3072 Office: 714.985.3434 Fax: 714.985.3433 [email protected] www.HaleyAldrich.com

NOTICE

The information contained in this communication is confidential and privileged proprietary information intended only for the individual or entity to whom it is addressed. Any unauthorized use, distribution, copying or disclosure of this communication is prohibited. If you have received this communication in error, please contact the sender immediately.

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American Environmental Testing Laboratory Inc. 2834 & 2908 North Naomi Street, Burbank, CA 9 1504 *DOHS NO: 1541, LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

Ordered Bv S i t e

500 South Kraemer Blvd. Suite 370

Telephone: (714)985-3434 Attn: Tom Tatnall

- - Q - --

Project ID: 3 2 4 8 6 - 0 0 7 Project Name: Delphi Sys tem Corp.

Method: (601 OB.LEAD), Lead, ICP QC Batch No: 101106

Page 67: American Environmental Testing Laboratory Inc. · 2019. 2. 19. · American Environmental ~~ Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO:

American Environmental Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 -DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

Ordered Bv S i t e

500 South Kraemer Blvd. Suite 370

Telephone: (7 14)985-3434 Attn: Tom Tatnall

Pane: 3 " Project ID: 32486-007 Project Name: Delphi Sys tem Corp.

Method: (60 1 OB.LEAD), Lead, ICP QC Batch No: 101106

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American Environmental Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504-DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

O r d e r e d Bv Site - - -- - - - -

500 South Kraemer Blvd. Suite 370

Telephone: (714)985-3434 Attn: Tom Tatnall

Page: 4 - Project ID: Proiect Name: Delphi System Corp.

Method: (601 OB.LEAD), Lead, ICP QC Batch No: 101106

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American Environmental Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504.DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com

ANALYTICAL RESULTS Ordered By Site

500 South Kraemer Blvd. Suite 370

Telephone: (7 14)985-3434 Attn: Tom Tatnall

Page: 5

Project ID: 32486-007 Project Name: Delphi Sys tem Corp.

Method: (60 1 OB.LEAD), Lead, ICP QUALITY CONTROL REPORT

QC Batch No: 101106 Sample Spiked: 39287.01 QC Prepared: 10/1112006 QC Analyzed: 10/11/2006

QC Batch No: 101106 Sample Spiked: 39287.01 QC Prepared: 10/11/2006 QC Analyzed: 10/11/2006

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American Environmental Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, C A 91504 DOHS NO: 1541,LACSDNO: 10181 Tel : (888) 288-AETL (81 8 ) 845-8200 Fax: (81 8) 845-8840 www.aetlab.com

Data Qualifiers and Descriptors

Data Qualifier:

* : In the QC section, sample results have been taken directly from the ICP reading. No preparation factor has been applied.

Analyte was present in the Method Blank.

Result is from a diluted analysis.

Result is beyond calibration limits and is estimated.

Analysis was performed over the allowed holding time due to circumstances which were beyond laboratory control.

Analyte was detected . However, the analyte concentration is an estimated value, which is between the Method Detection Limit (MDL) and the Practical Quantitation Limit (PQL).

Matrix spike recovery is outside control limits due to matrix interference. Laboratory Control Sample recovery was acceptable.

Surrogate recovery is outside control limits due to matrix interference.

The analysis of the sample required a dilution such that the surrogate concentration was diluted below the method acceptance criteria.

Results represent LCS and LCSD data.

Definition:

%Limi: Percent acceptable limits.

%REC : Percent recovery.

C0n.L: Acceptable Control Limits

Conce: Added concentration to the sample.

LCS: Laboratory Control Sample

MDL: Method Detection Limit is a statistically derived number which is specific for each instrument, each method, and each compound. It indicates a distinctively detectable quantity with 99% probability.

MS: Matrix Spike

MS DU: Matrix Spike Duplicate

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American Environmental -- Testing Laboratory Inc. 2834 8~2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com

Data Qualifiers and Descriptors

ND: Analyte was not detected in the sample at or above MDL.

PQL: Practical Quantitation Limit or ML (Minimum Level as per RWQCB) is the minimum concentration that can be quantified with more than 99% confidence. Taking into account all aspects of the entire analytical instrumentation and practice.

Recov: Recovered concentration in the sample.

RPD: Relative Percent Difference