AL2336-Blueberry Amnesia Residual Solvents Pass · PDF fileResidual Solvents 218 GCMS1...

Certi cate of Analysis Powered by Con dent Cannabis1 of 17

Accu LabsIndependence, OR [email protected](503) 559-8139Lic. #010-10045154B27

Sample: 1711CH0311.1662Strain: None

Batch#: ; Batch Size: - gramsSample Received: 11/29/2017; Report Created: 12/11/2017; Expires: 12/11/2018

Sampling: Random; Environment: Room Temp

AL2336-Blueberry AmnesiaConcentrates & Extracts, Hash - OilHarvest Process Lot: ; METRC Batch: ; METRC Sample: 1A40130000B2E9000000286

Residual Solvents218 GCMS1 20171204-112/04/2017

Pass

LOQ = Limit of Quanti cation; PPM = Parts Per Million; NR = Not Reported; ND = Not Detected. Method: EPA 8260C, Agilent 6890A GCMS with 7679A Headspace Autosampler; ORELAP ID 4057

Analyte LOQ Limit Mass StatusPPM PPM PPM

1,4-Dioxane 10 380 <LOQ Pass2-Butanol 10 5000 <LOQ Pass2-Ethoxy-Ethanol 10 160 <LOQ Pass2-Propanol IPA 10 5000 111 PassAcetone 10 5000 71 PassAcetonitrile 40 410 <LOQ PassBenzene 2 2 <LOQ PassButanes 10 5000 309 PassCumene 10 70 <LOQ PassCyclohexane 10 3880 <LOQ PassDichloromethane 10 600 <LOQ PassEthyl-Acetate 10 5000 <LOQ PassEthyl-Ether 10 5000 <LOQ PassEthylene Glycol 620 620 <LOQ PassEthylene Oxide 10 50 <LOQ PassHeptane 10 5000 <LOQ PassHexanes 10 290 <LOQ PassIsopropyl-Acetate 10 5000 <LOQ PassMethanol 40 3000 <LOQ PassPentanes 10 5000 <LOQ PassPropane 10 5000 <LOQ PassTetrahydrofuran 10 720 <LOQ PassToluene 10 890 <LOQ PassXylenes 10 2170 <LOQ Pass

5691 SE International Way C-2Portland, OR(503) 305-5252http://chemhistory.comLic# 010-1002015CA5E

Values reported relate only to the product tested. ChemHistory makes no claims as to the consumer safety or other risks associated with any detected or non-detected levels of any pesticides or residual solvents. This Certi cate shall not be reproduced except in full, without the written approval of ChemHistory. ORELAP accredited ID#4057 and OLCC Licensed Cannabis Testing Laboratory #010-1002015CA5E.

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support@con dentcannabis.com(866) 506-5866

www.con dentcannabis.comAnnabeth Rose

Laboratory Director







Pesticides382 LCQQQ1 20171208-112/08/2017

Pass

Method: Modi ed AOAC 2007.01, Triple Quad analysis; LOQ = Limit of Quanti cation; PPB = Parts Per Billion; ND = Not Detected; NR = Not Reported; ORELAP ID 4057

Analyte LOQ Limit Mass StatusPPB PPB PPB

Abamectin 300 500 <LOQ PassAcephate 200 400 <LOQ PassAcequinocyl 900 2000 <LOQ PassAcetamiprid 200 200 <LOQ PassAldicarb 300 400 <LOQ PassAzoxystrobin 200 200 <LOQ PassBifenazate 200 200 <LOQ PassBifenthrin 200 200 <LOQ PassBoscalid 400 400 <LOQ PassCarbaryl 200 200 <LOQ PassCarbofuran 200 200 <LOQ PassChlorantraniliprole 200 200 <LOQ PassChlorfenapyr 500 1000 <LOQ PassChlorpyrifos 200 200 <LOQ PassClofentezine 200 200 <LOQ PassCy uthrin 1000 1000 <LOQ PassCypermethrin 1000 1000 <LOQ PassDaminozide 200 1000 <LOQ PassDiazinon 200 200 <LOQ PassDichlorvos 800 1000 <LOQ PassDimethoate 200 200 <LOQ PassEthoprophos 100 200 <LOQ PassEtofenprox 200 400 <LOQ PassEtoxazole 100 200 <LOQ PassFenoxycarb 200 200 <LOQ PassFenpyroximate 200 400 <LOQ PassFipronil 100 400 <LOQ PassFlonicamid 200 1000 <LOQ PassFludioxonil 400 400 <LOQ PassHexythiazox 500 1000 <LOQ Pass

Analyte LOQ Limit Mass StatusPPB PPB PPB

Imazalil 200 200 <LOQ PassImidacloprid 100 400 <LOQ PassKresoxim Methyl 100 400 <LOQ PassMalathion 200 200 <LOQ PassMetalaxyl 100 200 <LOQ PassMethiocarb 200 200 <LOQ PassMethomyl 200 400 <LOQ PassMethyl Parathion 200 200 <LOQ PassMGK-264 100 200 <LOQ PassMyclobutanil 200 200 <LOQ PassNaled 500 500 <LOQ PassOxamyl 200 1000 <LOQ PassPaclobutrazol 100 400 <LOQ PassPermethrins 200 200 <LOQ PassPhosmet 200 200 <LOQ PassPiperonyl Butoxide 200 2000 1277 PassPrallethrin 200 200 <LOQ PassPropiconazole 400 400 <LOQ PassPropoxur 200 200 <LOQ PassPyrethrins 1000 1000 <LOQ PassPyridaben 100 200 <LOQ PassSpinosad 100 200 <LOQ PassSpiromesifen 100 200 <LOQ PassSpirotetramat 200 200 <LOQ PassSpiroxamine 100 400 <LOQ PassTebuconazole 200 400 <LOQ PassThiacloprid 200 200 <LOQ PassThiamethoxam 200 200 <LOQ PassTri oxystrobin 200 200 <LOQ Pass





www.con dentcannabis.comAnnabeth Rose

Laboratory Director







Quality Control DataAnalytical Batch ID QC Sample ID Assay Name QC Category Name217 GCQQQ1 20171204-4 MRMB11291701 Required Pesticides BlankQC NotesNone

Compounds LOQ (PPB) Blank Result PPB NotesChlorfenapyr 500 <LOQ -Cy uthrin 1000 <LOQ -Cypermethrin 1000 <LOQ -Fipronil 40 <LOQ -Fludioxonil 40 <LOQ -MGK-264 200 <LOQ -Methyl Parathion 200 <LOQ -





www.con dentcannabis.com







Quality Control DataAnalytical Batch ID QC Sample ID Assay Name QC Category Name382 LCQQQ1 20171208-1 MRMB11291704 Required Pesticides BlankQC NotesNone

Compounds LOQ (PPB) Blank Result PPBAcephate 200 <LOQAcequinocyl 900 <LOQAcetamiprid 200 <LOQAldicarb 300 <LOQAbamectin 300 <LOQAzoxystrobin 200 <LOQBifenazate 200 <LOQBifenthrin 200 <LOQBoscalid 400 <LOQCarbaryl 200 <LOQCarbofuran 200 <LOQChlorantraniliprole 200 <LOQChlorpyrifos 200 <LOQClofentezine 200 <LOQDaminozide 200 <LOQDiazinon 200 <LOQDichlorvos 800 <LOQDimethoate 200 <LOQEthoprophos 100 <LOQEtofenprox 200 <LOQEtoxazole 100 <LOQFenoxycarb 200 <LOQFenpyroximate 200 <LOQFlonicamid 100 <LOQHexythiazox 500 <LOQImazalil 300 <LOQImidacloprid 100 <LOQKresoxim Methyl 100 <LOQMalathion 200 <LOQMetalaxyl 100 <LOQ












Quality Control DataAnalytical Batch ID QC Sample ID Assay Name QC Category Name382 LCQQQ1 20171208-1 MRMB11291704 Required Pesticides BlankQC NotesNone

Compounds LOQ (PPB) Blank Result PPBMethiocarb 200 <LOQMethomyl 200 <LOQMyclobutanil 200 <LOQNaled 500 <LOQOxamyl 200 <LOQPaclobutrazol 100 <LOQPermethrin 200 <LOQPhosmet 300 <LOQPiperonyl Butoxide 200 <LOQPrallethrin 200 <LOQPropiconazole 400 <LOQPropoxur 200 <LOQPyrethrins 1000 <LOQPyridaben 100 <LOQSpinosad 100 <LOQSpiromesifen 100 <LOQSpirotetramat 200 <LOQSpiroxamine 100 <LOQTebuconazole 200 <LOQThiacloprid 200 <LOQThiamethoxam 200 <LOQTri oxystrobin 200 <LOQ












Quality Control DataAnalytical Batch ID QC Sample ID Assay Name QC Category Name217 GCQQQ1 20171204-4 MRLCS11291701 Required Pesticides Lab Control SampleQC NotesNone

Compounds LCS % Rec % Limits NotesChlorfenapyr 111.000 69 - 132 -Cy uthrin 104 68 - 136 -Cypermethrin 101 67 - 134 -Fipronil 96 67 - 136 -Fludioxonil 100 69 - 139 -MGK-264 95 65 - 145 -Parathion Methyl 102 66 - 131 -












Quality Control DataAnalytical Batch ID QC Sample ID Assay Name QC Category Name382 LCQQQ1 20171208-1 MRLCS11291704 Required Pesticides Lab Control SampleQC NotesNone

Compounds LCS % Rec LCS % Limits NotesAcephate 95.1 56 - 149 -Acequinocyl 98.7 30 - 142 -Acetamiprid 99.5 56 - 149 -Aldicarb 98.6 53 - 150 -Abamectin 114.3 30 - 140 -Azoxystrobin 98.9 55 - 138 -Bifenazate 101.4 53 - 137 -Bifenthrin 136.3 30 - 150 -Boscalid 106.4 55 - 142 -Carbaryl 100.2 56 - 150 -Carbofuran 100.6 57 - 142 -Chlorantraniliprole 99.9 54 - 141 -Chlorpyrifos 116.5 34 - 150 -Clofentezine 110.1 44 - 150 -Daminozide 102.7 30 - 150 -Diazinon 93.8 55 - 134 -Dichlorvos 94.5 49 - 149 -Dimethoate 98 56 - 149 -Ethoprophos 91.6 52 - 143 -Etofenprox 136.5 46 - 140 -Etoxazole 86.9 50 - 134 -Fenoxycarb 104.1 53 - 139 -Fenpyroximate 89.6 45 - 127 -Flonicamid 90.8 55 - 145 -Hexythiazox 106.6 39 - 141 -Imazalil 77.2 40 - 149 -Imidacloprid 97.3 54 - 150 -Kresoxim Methyl 101.8 57 - 139 -Malathion 108.7 51 - 147 -Metalaxyl 95.7 58 - 142 -












Quality Control DataAnalytical Batch ID QC Sample ID Assay Name QC Category Name382 LCQQQ1 20171208-1 MRLCS11291704 Required Pesticides Lab Control SampleQC NotesNone

Compounds LCS % Rec LCS % Limits NotesMethiocarb 103.8 50 - 150 -Methomyl 99.9 55 - 150 -Myclobutanil 101.1 54 - 145 -Naled 102.1 49 - 146 -Oxamyl 98.2 56 - 147 -Paclobutrazol 96.2 56 - 139 -Permethrin 132.5 30 - 138 -Phosmet 103.7 57 - 146 -Piperonyl Butoxide 95.6 48 - 146 -Prallethrin 112.8 53 - 146 -Propiconazole 87.7 49 - 129 -Propoxur 101.7 56 - 150 -Pyrethrins 118.81 30 - 150 -Pyridaben 100.9 50 - 132 -Spinosad 64.3 30 - 150 -Spiromesifen 102.1 52 - 136 -Spirotetramat 95.7 46 - 150 -Spiroxamine 60.7 30 - 150 -Tebuconazole 91.3 48 - 136 -Thiacloprid 98.3 47 - 150 -Thiamethoxam 99.9 57 - 147 -Tri oxystrobin 104.5 46 - 147 -












Quality Control DataAnalytical Batch ID QC Sample ID Assay Name QC Category Name217 GCQQQ1 20171204-4 MRMS11291701 Required Pesticides SpikeQC NotesNone

Compounds Matrix Spike Duplicate % RPD RPD Max % % RPD Result Matrix Spike % Rec % Limits NotesChlorfenapyr 5.01 20 <20 116.8 62 - 130Cy uthrin 0.78 20 <20 103.6 63 - 128Cypermethrin 1.92 20 <20 105.2 58 - 126Fipronil 1.89 20 <20 106.8 62 - 134Fludioxonil 3.27 20 <20 99.6 62 - 139MGK-264 3.55 20 <20 103.2 56 - 150Methyl Parathion 6.24 20 <20 112.4 63 - 135












Quality Control DataAnalytical Batch ID QC Sample ID Assay Name QC Category Name382 LCQQQ1 20171208-1 MR11291704 Required Pesticides SpikeQC NotesNone

Compounds Matrix Spike Duplicate % RPD RPD Max % % RPD Result Matrix Spike % Rec % Limits NotesAcephate 2.54 30 <30 105.1 52 - 150 -Acequinocyl 9.97 30 <30 79.1 30 - 147 -Acetamiprid 1.34 30 <30 96.3 47 - 148 -Aldicarb 1.71 30 <30 98.7 48 - 145 -Abamectin 2.08 30 <30 119 41 - 150 -Azoxystrobin 2.14 30 <30 94.6 50 - 150 -Bifenazate 4.24 30 <30 124.7 50 - 150 -Bifenthrin 10 30 <30 176.7 46 - 150 Above Limit RangeBoscalid 0.49 30 <30 121.6 50 - 150 -Carbaryl 4.14 30 <30 97.1 57 - 150 -Carbofuran 4.46 30 <30 92 51 - 150 -Chlorantraniliprole 1.03 30 <30 96.2 52 - 150 -Chlorpyrifos 0.5 30 <30 140.5 30 - 150 -Clofentezine 4.18 30 <30 119.5 53 - 146 -Daminozide 4.64 30 <30 96.9 30 - 150 -Diazinon 1.93 30 <30 102.7 41 - 145 -Dichlorvos 1.27 30 <30 94.2 54 - 141 -Dimethoate 2.79 30 <30 95.3 49 - 149 -Ethoprophos 3.6 30 <30 109 47 - 146 -Etofenprox 12.66 30 <30 167.2 38 - 150 Above Limit RangeEtoxazole 1.54 30 <30 83.7 34 - 150 -Fenoxycarb 5.3 30 <30 123 54 - 150 -Fenpyroximate 4.54 30 <30 92.6 34 - 150 -Flonicamid 2.55 30 <30 92.8 45 - 143 -Hexythiazox 6.16 30 <30 108.5 30 - 150 -Imazalil 5.56 30 <30 77 30 - 147 -Imidacloprid 2.98 30 <30 82.6 43 - 148 -Kresoxim Methyl 8.75 30 <30 77.6 56 - 144 -Malathion 3.33 30 <30 133 55 - 150 -Metalaxyl 3.05 30 <30 87.2 50 - 150 -












Quality Control DataAnalytical Batch ID QC Sample ID Assay Name QC Category Name382 LCQQQ1 20171208-1 MR11291704 Required Pesticides SpikeQC NotesNone

Compounds Matrix Spike Duplicate % RPD RPD Max % % RPD Result Matrix Spike % Rec % Limits NotesMethiocarb 0.68 30 <30 88.1 50 - 150 -Methomyl 3.09 30 <30 92.5 42 - 150 -Myclobutanil 4.360 30 <30 114.5 43 - 150 -Naled 6.27 30 <30 105 46 - 150 -Oxamyl 2.52 30 <30 93.9 41 - 150 -Paclobutrazol 2.45 30 <30 104.9 47 - 150 -Permethrin 0.13 30 <30 150.6 37 - 150 Above Limit RangePhosmet 2.82 30 <30 118.7 35 - 150 -Piperonyl Butoxide 4.21 30 <30 86 30 - 149 -Prallethrin 1.27 30 <30 125.5 46 - 150 -Propiconazole 5.22 30 <30 97.1 40 - 150 -Propoxur 4.89 30 <30 93.7 53 - 150 -Pyrethrins 3.93 30 <30 160.15 30 - 150 Above Limit RangePyridaben 3.33 30 <30 97.5 41 - 150 -Spinosad 5.46 30 <30 67.7 30 - 150 -Spiromesifen 2.05 30 <30 96.6 43 - 150 -Spirotetramat 0.98 30 <30 91.5 48 - 150 -Spiroxamine 2.7 30 <30 62.2 30 - 143 -Tebuconazole 3.12 30 <30 123.2 45 - 150 -Thiacloprid 2.66 30 <30 96.3 50 - 147 -Thiamethoxam 1.08 30 <30 92.4 40 - 147 -Tri oxystrobin 2.44 30 <30 109.5 50 - 150 -












Quality Control DataAnalytical Batch ID QC Sample ID Assay Name QC Category Name218 GCMS1 20171204-1 RSMB11291701 Required Solvents BlankQC NotesNone

Compounds Method LOQ (PPM) Blank Result PPM NotesXylenes 30 <LOQ -1,4-Dioxane 10 <LOQ -2-Butanol 10 <LOQ -2-Ethoxy-Ethanol 10 <LOQ -2-Methyl-Butane 10 <LOQ -2-Methyl-Pentane 10 <LOQ -2,2-Dimethyl-Butane 10 <LOQ -2,3-Dimethyl-Butane 10 <LOQ -3-Methyl-Pentane 10 <LOQ -Acetone 10 <LOQ -Acetonitrile 40 <LOQ -Benzene 0.5 <LOQ -Butane 10 <LOQ -Cumene 10 <LOQ -Cyclohexane 10 <LOQ -Dichloro-Methane 10 <LOQ -Ethyl-Acetate 10 <LOQ -Ethyl-Benzene 10 <LOQ -Ethyl-Ether 10 <LOQ -Ethylene Glycol 10 <LOQ -Ethylene Oxide 10 <LOQ -Heptane 10 <LOQ -Isobutane 10 <LOQ -Isopropyl-Acetate 10 <LOQ -Isopropyl Alcohol 10 <LOQ -Methanol 40 <LOQ -Neopentane 10 <LOQ -n-Hexane 10 <LOQ -Pentane 10 <LOQ -Propane 10 <LOQ -












Quality Control DataAnalytical Batch ID QC Sample ID Assay Name QC Category Name218 GCMS1 20171204-1 RSMB11291701 Required Solvents BlankQC NotesNone

Compounds Method LOQ (PPM) Blank Result PPM NotesTetrahydrofuran 10 <LOQ -Toluene 10 <LOQ -












Quality Control DataAnalytical Batch ID QC Sample ID Assay Name QC Category Name218 GCMS1 20171204-1 RSLCS11291701 Required Solvents Lab Control SampleQC NotesNone

Compounds LCS % Rec % Limits NotesXylenes 70.73 67 - 133 -1,4-Dioxane 68.4 67 - 133 -2-Butanol 69.2 70 - 130 Below Limit Range2-Ethoxy-Ethanol 68.6 70 - 130 Below Limit Range2-Methyl-Butane 73.6 52 - 148 -2-Methyl-Pentane 102.6 54 - 146 -2,2-Dimethyl-Butane 59.6 54 - 146 -2,3-Dimethyl-Butane 102.6 53 - 147 -3-Methyl-Pentane 64.6 55 - 145 -Acetone 66.4 56 - 144 -Acetonitrile 64.4 60 - 140 -Benzene 72.2 70 - 130 -Butane 63.6 42 - 150 -Cumene 72.4 68 - 132 -Cyclohexane 66.4 56 - 144 -Dichloro-Methane 67 58 - 142 -Ethyl-Acetate 70.8 61 - 139 -Ethyl-Benzene 70.8 61 - 139 -Ethyl-Ether 69.4 55 - 145 -Ethylene Glycol 73 33 - 150 -Ethylene Oxide 73.2 65 - 135 -Heptane 65.8 51 - 149 -Isobutane 64 37 - 150 -Isopropyl-Acetate 65.8 61 - 139 -Isopropyl Alcohol 82.6 70 - 130 -Methanol 64.4 56 - 144 -Neopentane 67.8 42 - 150 -n-Hexane 67 53 - 147 -Pentane 65.8 51 - 149 -Propane 55.6 30 - 150 -












Quality Control DataAnalytical Batch ID QC Sample ID Assay Name QC Category Name218 GCMS1 20171204-1 RSLCS11291701 Required Solvents Lab Control SampleQC NotesNone

Compounds LCS % Rec % Limits NotesTetrahydrofuran 65.6 60 - 140 -Toluene 72 62 - 138 -












Quality Control DataAnalytical Batch ID QC Sample ID Assay Name QC Category Name218 GCMS1 20171204-1 RSMS11291701 Required Solvents SpikeQC NotesNone

Compounds LOQ Matrix Duplicate % RPD Duplicate RPD Notes Matrix Spike % Rec % Limits NotesXylenes 30 <LOQ <LOQ 83 30 - 142 -1,4-Dioxane 10 <LOQ <LOQ 84 53 - 147 -2-Butanol 10 <LOQ <LOQ 89 70 - 130 -2-Ethoxy-Ethanol 10 <LOQ <LOQ 88 53 - 147 -2-Methyl-Butane 10 <LOQ <LOQ 88 34 - 150 -2-Methyl-Pentane 10 <LOQ <LOQ 115 45 - 150 -2,2-Dimethyl-Butane 10 <LOQ <LOQ 74 44 - 150 -2,3-Dimethyl-Butane 10 <LOQ <LOQ 115 45 - 150 -3-Methyl-Pentane 10 <LOQ <LOQ 81 45 - 150 -Acetone 10 27.85 <30 87 30 - 150 -Acetonitrile 40 <LOQ <LOQ 80 50 - 150 -Benzene 2 <LOQ <LOQ 93 56 - 144 -Butane 10 24 <30 71 30 - 150 -Cumene 10 <LOQ <LOQ 101 30 - 150 -Cyclohexane 10 <LOQ <LOQ 83 47 - 150 -Dichloro-Methane 10 <LOQ <LOQ 87 49 - 150 -Ethyl-Acetate 10 <LOQ <LOQ 95 30 - 150 -Ethyl-Benzene 10 <LOQ <LOQ 84 48 - 150 -Ethyl-Ether 10 <LOQ <LOQ 88 45 - 150 -Ethylene Glycol 620 <LOQ <LOQ 107 30 - 150 -Ethylene Oxide 10 <LOQ <LOQ 92 53 - 147 -Heptane 10 <LOQ <LOQ 93 44 - 150 -Isobutane 10 <LOQ <LOQ 74 30 - 150 -Isopropyl-Acetate 10 <LOQ <LOQ 82 49 - 150 -Isopropyl Alcohol 10 21.92 <30 80 70 - 130 -Methanol 40 <LOQ <LOQ 80 30 - 150 -Neopentane 10 <LOQ <LOQ 79 31 - 150 -n-Hexane 10 <LOQ <LOQ 84 43 - 150 -Pentane 10 <LOQ <LOQ 80 40 - 150 -Propane 10 <LOQ <LOQ 67 30 - 150 -












Quality Control DataAnalytical Batch ID QC Sample ID Assay Name QC Category Name218 GCMS1 20171204-1 RSMS11291701 Required Solvents SpikeQC NotesNone

Compounds LOQ Matrix Duplicate % RPD Duplicate RPD Notes Matrix Spike % Rec % Limits NotesTetrahydrofuran 10 <LOQ <LOQ 83 49 - 150 -Toluene 10 <LOQ <LOQ 90 49 - 150 -






AL2336-Blueberry Amnesia Residual Solvents Pass · PDF fileResidual Solvents 218 GCMS1...

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