Agilent 5977B MSD Technologies, Inc.‌ ‚¬ „...

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  • Agilent Technologies

    Agilent 5977B MSD

  • Agilent Technologies, Inc. 2015

    Agilent Technologies, Inc. ( ) .

    G7077-99003

    , 2015 8

    Agilent Technologies, Inc.5301 Stevens Creek BoulevardSanta Clara, CA 95051

    " " . , Agilent ( ) . Agilent , . Agilent .

    . , . .

    . , . .

  • Agilent 5977 3

    Agilent 5977B (MSD) .

    1

    1 , 5977B MSD .

    2 GC

    2 MSD , GC , GC/MSD MSD .

    3 EI(Electron Ionization)

    3 , , , . CI .

    4 CI(Chemical Ionization)

    4 CI .

    5

    5 EI CI .

    6 CI

    6 CI MSD .

  • 4 5977B MSD

    , , . . Agilent GC GC/MS DVD

    (G4600-64006)

    Agilent GC/MS (G1701-60175)

    USB DVD MassHunter Agilent 5977B MSD(G7077-99105) .

  • 5977B MSD 5

    1

    5977B HES MSD 12

    13

    5977B HES MSD 15

    MSD 17

    19

    21

    GC 21 24

    26

    / 29

    29

    MSD 29

    30

    2 GC

    34

    / 37

    40

    GC/MS 41

    GC/MS 46

  • 6 5977B MSD

    3 EI(Electron Ionization)

    MSD 50

    GC MSD 51

    (WUI) MSD 55

    MSD 55

    eModule 58

    LED 58

    GC/MSD 59

    MSD 61

    62

    62

    62

    MSD 63

    MSD 64

    MSD 66

    69

    MassHunter GC/MSD 71

    72

    75

    EI MSD 78

    80

    81

    83

    85

  • 5977B MSD 7

    86

    (5977B MSD) 87

    MSD 90

    MSD 91

    MSD 94

    MSD 97

    4 CI(Chemical Ionization)

    100

    CI GC/MSD 101

    CI 103

    CI MSD 105

    CI MSD 106

    CI 107

    109

    112

    115

    PCI ( ) 118

    NCI ( ) 120

    PCI 122

    NCI 123

    CI 124

    5

    128

    133

  • 8 5977B MSD

    134

    136

    EI 139

    EI 141

    EI 143

    EI 145

    EI 149

    EI 152

    HES 157

    HES 159

    EI 160

    162

    166

    169

    EI CI 170

    CI EI 172

    6 CI

    176

    CI MSD 176

    CI/ 177

    CI 179

    CI 183

    CI 185

    CI 186

    CI 189

  • 5977B MSD 9

    CI 192

    CI 195

    CI 197

    CI 199

  • 10 5977B MSD

  • 11

    Agilent 5977B MSD

    Agilent Technologies

    1

    5977B MSD 12

    13

    5977B MSD 15

    MSD 17

    19

    21

    26

    / 29

    29

    MSD 29

    30

    , MSD .

  • 12 5977B MSD

    1

    5977B MSD

    5977B MSD ( ) (TMP) Pfeiffer DUO 2.5 . EI EI Inert Plus MSD EI , . CI , CI . MSD ( 1) .

    1

    /

    5977B MSD G7080B EI(Electron ionization)/

    5977B MSD G7081B EI(Electron ionization)/

    5977B Inert+ MSDEI

    G7077B MSD EI(Electron ionization)/

    5977B EI/CI MSD G7078B MSD Electron ionization, (Electron ionization)/ CI(Chemical Ionization) /PCI, NCI

  • 1

    5977B MSD 13

    1 . .

    2

    AC Alternating current,

    ALS Automatic liquid sampler,

    BFB Bromofluorobenzene ( ),

    CI Chemical ionization,

    DC Direct current,

    DFTPP Decafluorotriphenylphosphine ( ),

    DIP Direct insertion probe,

    DS Data System,

    EI Electron ionization,

    EM Electron multiplier ( ),

    EMV Electron multiplier voltage,

    EPC Electronic pneumatic control,

    eV Electron volt,

    GC Gas chromatograph,

    HED High-energy dynode, ( )

    Inert EI

    Inert+ EI

    id Inside diameter,

    LAN Local Area Network,

    m/z Mass to charge ratio,

  • 14 5977B MSD

    1

    MFC

    MSD Mass selective detector,

    NCI Negative CI, CI

    OFN Octafluoronaphthalene ( ),

    PCI Positive CI, CI

    PFDTD Perfluoro-5,8-dimethyl-3,6,9-trioxydodecane( )

    PFHT 2,4,6-tris(perfluoroheptyl)-1,3,5-triazine( )

    PFTBA Perfluorotributylamine( ),

    Quad Quadrupole mass filter, 4

    RF Radio frequency,

    RFPA Radio frequency power amplifier,

    Torr , 1mm Hg

    ( )

    2 ( )

  • 1

    5977B MSD 15

    5977B MSD

    5977B MSD Agilent 7890B Agilent 7820 GC ( 3). MSD :

    MSD WEB (WUI)

    Pfeiffer DUO 2.5

    MSD EI(Electron-Ionization) : .

    (CI) , , CI (PCI/NCI)

    MSD 4

    (HED)

    GC GC/MSD

    5977B MSD 41cm, 30cm, 54cm . 39kg, EI 44kg, EI/CI 46kg . ( ) 11kg( ) MSD .

    / , , GC , .

  • 16 5977B MSD

    1

    MSD ( ) . MassHunter GCMS ( ) . . (CI) .

    3 5977B MSD

    mL/min

    1 1~2

    mL/min*

    * MSD : ( ). . .

    1.5 4

    , mL/min

    2 6.5

    ID 0.25 mm(30m) 0.53mm(30m)

    CI

    CI .

    GC 7890 7890

    Pfeiffer Duo 2.5 Pfeiffer Duo 2.5, MVP-070-3, MVP-070-3C, IDP3 24V

    DIP** ( )

    ** .

  • 1

    5977B MSD 17

    MSD

    1 5977B GC/MSD , Agilent 7890B GC

    ALS

    7890B GC

    5977B MSD

    MSD

    GC

    LED

  • 18 5977B MSD

    1

    CI MSD CI G7078B G7077B MSD . , .

    CI MSD CI . . 4, CI(Chemical Ionization) .

    5977B CI 5977B MSD .

    EI/CI GC/MSD

    EI CI

    PCI NCI HED

    / . , , .

    (G3397B) . CI MSD EI .

    MSD CI CI CI 4 . .

    CI . GC/MSD .

    (bake out) 1~2 , CI EI 1 . PCI NCI 2 .

  • 1

    5977B MSD 19

    MSD .

    MSD .

    MSD , .

    MSD AC , AC AC

    .

    ( , , )

    , MSD , MSD . .

    MSD .

    MSD . . .

    . , . , , .

    . Agilent .

    MSD .

  • 20 5977B MSD

    1

    .

    GC/MSD . , .

    GC GC , GC/MS GC

    GC GC GC

    MSD , 4

    . . . . , .

    .

    , MSD .

    . GC .

    GC , , . , , , , , .

    ( ) , ( / ) . , .

  • 1

    5977B MSD 21

    GC . .

    . 4%~74.2% .

    .

    .

    .

    .

    GC

    GC MSD . .

    GC .

    (H2) GC . , , .

    . . , . .

  • 22 5977B MSD

    1

    GC/MSD

    . , GC GC/MSD . , .

    GC (GC GC )

    MSD

    MSD

    ( 3 - 22 ) . MSD .

    MSD / . , .

    4

    . , . MSD . , .

    . . . .

  • 1

    5977B MSD 23

    . . . .

    GC GC . , . GC . EPC (Electronic Pressure Control) 7890 GC EPC . GC EPC . , . .

    GC . , . , GC . .

    4 ( )

    . .

    , . .

  • 24 5977B MSD

    1

    GC/MSD .

    . . .

    5977B MSD . .

    . .

    ( , , ) .

    ( ).

    .

    GC MSD .

    MSD ( ).

    MSD ( ).

    .

    MSD .

  • 1

    5977B MSD 25

    GC/MSD , .

    1 .

    2 GC .

    3 MSD 1 .

    4 .

    5 MSD .

    6 10 .

    7 GC MSD .

    (EHS) . . GC .

  • 26 5977B MSD

    1

    5977B MSD .

    (CSA): CAN/CSA-C222 No. 61010-1-04

    CSA/ (NRTL): UL 610101

    (IEC): 610101

    EuroNorm(EN): 610101

    5977B MSD (EMC