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A General Approach for the Asymmetric Synthesis of Densely ... › suppdata › ra › c3 ›...
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A General Approach for the Asymmetric Synthesis of Densely Substituted Piperidines and Fully Substituted Piperidinones Employing the Asymmetric Mannich Reaction as Key Step Ainara Iza a , Uxue Uria a , Efraím Reyes a , Luisa Carrillo* a and Jose L. Vicario* a a Departamento de Química Orgánica II, Facultad de Ciencia y Tecnología, Universidad del País Vasco/Euskal Herriko Unibertsitatea (UPV/EHU), P.O. Box 644, E-48080 Bilbao, Spain. Corresponding author. Tel.: +34-94-601-5434; fax: +34-94-601-2748; e-mail: [email protected] Corresponding author. Tel.: +34-94-601-5454; fax: +34-94-601-2748; e-mail: [email protected] Electronic Supplementary Material (ESI) for RSC Advances This journal is © The Royal Society of Chemistry 2013
Transcript of A General Approach for the Asymmetric Synthesis of Densely ... › suppdata › ra › c3 ›...
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A General Approach for the Asymmetric Synthesis of Densely
Substituted Piperidines and Fully Substituted Piperidinones
Employing the Asymmetric Mannich Reaction as Key Step
Ainara Izaa, Uxue Uria
a, Efraím Reyes
a, Luisa Carrillo*
a and Jose L. Vicario*
a
aDepartamento de Química Orgánica II, Facultad de Ciencia y Tecnología,
Universidad del País Vasco/Euskal Herriko Unibertsitatea (UPV/EHU), P.O. Box 644,
E-48080 Bilbao, Spain.
Corresponding author. Tel.: +34-94-601-5434; fax: +34-94-601-2748; e-mail: [email protected]
Corresponding author. Tel.: +34-94-601-5454; fax: +34-94-601-2748; e-mail: [email protected]
Electronic Supplementary Material (ESI) for RSC AdvancesThis journal is © The Royal Society of Chemistry 2013
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Figure 1. NMR spectra of compound 4
Electronic Supplementary Material (ESI) for RSC AdvancesThis journal is © The Royal Society of Chemistry 2013
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Figure 2. NMR spectra of compound 5
Electronic Supplementary Material (ESI) for RSC AdvancesThis journal is © The Royal Society of Chemistry 2013
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Figure 3. NMR spectra of compound 6
Electronic Supplementary Material (ESI) for RSC AdvancesThis journal is © The Royal Society of Chemistry 2013
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Figure 4. NMR spectra of compound 7
Electronic Supplementary Material (ESI) for RSC AdvancesThis journal is © The Royal Society of Chemistry 2013
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Figure 5. NMR spectra of compound 8
Electronic Supplementary Material (ESI) for RSC AdvancesThis journal is © The Royal Society of Chemistry 2013
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Figure 6. NMR spectra of compound 9
Electronic Supplementary Material (ESI) for RSC AdvancesThis journal is © The Royal Society of Chemistry 2013
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Figure 7. NMR spectra of compound 10
Electronic Supplementary Material (ESI) for RSC AdvancesThis journal is © The Royal Society of Chemistry 2013
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Figure 8. NMR spectra of compound 11
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Figure 9. NMR spectra of compound 12
Electronic Supplementary Material (ESI) for RSC AdvancesThis journal is © The Royal Society of Chemistry 2013
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Figure 10. NMR spectra of compound 13
Electronic Supplementary Material (ESI) for RSC AdvancesThis journal is © The Royal Society of Chemistry 2013
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Figure 11. NMR spectra of compound 14
Electronic Supplementary Material (ESI) for RSC AdvancesThis journal is © The Royal Society of Chemistry 2013
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Figure 12. NMR spectra of compound 15
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Figure 13. NMR spectra of compound 16
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Figure 14. NMR spectra of compound 17b
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Figure 15. NMR spectra of compound 18a
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Figure 16. NMR spectra of compound 18b
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Figure 17. NMR spectra of compound 19/19´
Electronic Supplementary Material (ESI) for RSC AdvancesThis journal is © The Royal Society of Chemistry 2013
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Figure 18. NMR spectra of compound 20
Electronic Supplementary Material (ESI) for RSC AdvancesThis journal is © The Royal Society of Chemistry 2013
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Figure 19. NMR spectra of compound 21
Electronic Supplementary Material (ESI) for RSC AdvancesThis journal is © The Royal Society of Chemistry 2013
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Figure 20. NMR spectra of compound 22
Electronic Supplementary Material (ESI) for RSC AdvancesThis journal is © The Royal Society of Chemistry 2013
![CATALYTIC ASYMMETRIC SYNTHESIS€¦ · Catalytic asymmetric synthesis / [edited by] Iwao Ojima. – 3rd ed. p. cm. Includes index. ISBN 978-0-470-17577-4 (cloth) 1. Asymmetric synthesis.](https://static.fdocuments.net/doc/165x107/5f0448457e708231d40d352e/catalytic-asymmetric-synthesis-catalytic-asymmetric-synthesis-edited-by-iwao.jpg)