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BRITISH STANDARD BS EN12697-34:2004Incorporating amendment no. 1
Bituminous mixtures — Test methods for hot mix asphalt —Part 34: Marshall test
The European Standard EN 12697-34:2004, incorporating amendment A1:2007, has the status of a British Standard
ICS 93.080.20
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BS EN 12697-34:2004
This British Standard was published under the authority of the Standards Policy and Strategy Committee on 7 July 2004
© BSI 2007
ISBN 978 0 580 59824 1
National foreword
This British Standard is the UK implementation of EN 12697-34:2004, incorporating amendment A1:2007.The UK participation in its preparation was entrusted by Technical Committee B/510, Road materials, to Subcommittee B/510/1, Coated macadam and hot asphalt.A list of organizations represented on this subcommittee can be obtained on request to its secretary.This publication does not purport to include all the necessary provisions of a contract. Users are responsible for its correct application. Compliance with a British Standard cannot confer immunity from legal obligations.
Amendments issued since publication
Amd. No. Date Comments
17288 31 August 2007 Implementation of CEN amendment A1:2007.
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EUROPEAN STANDARD
NORME EUROPÉENNE
EUROPÄISCHE NORM
EN 12697-34:2004+A1
July 2007
ICS 93.080.20 Supersedes EN 12697-34:2004
English Version
Bituminous mixtures - Test methods for hot mix asphalt - Part34: Marshall test
Mélanges bitumineux - Méthodes d'essai pour mélange hydrocarboné à chaud - Partie 34: Essai Marshall
Asphalt - Prüfverfahren für Heißasphalt - Teil 34: Marshall-Prüfung
This European Standard was approved by CEN on 1 April 2004 and includes Amendment 1 approved by CEN on 16 May 2007.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION C O M IT É E U R O P É E N DE N O R M AL IS A T I ONEUROPÄISCHES KOMITE E FÜR NORMUNG
Management Centre: rue de Stassart, 36 B-1050 Brussels
© 2007 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members.
Ref. No. EN 12697-34:2004+A1:2007: E
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EN 12697-34:2004+A1:2007 (E)
2
Contents
page
Foreword..............................................................................................................................................................3
1 Scope ......................................................................................................................................................6
2 Normative references ............................................................................................................................6
3 Terms and definitions ...........................................................................................................................6
4 Principle..................................................................................................................................................7
5 Apparatus ...............................................................................................................................................7
6 Procedure ...............................................................................................................................................7
7 Expression of results ............................................................................................................................8
8 Test report ..............................................................................................................................................9
9 Precision.................................................................................................................................................9
Annex A (normative) Marshall quotient .........................................................................................................10
Annex B (normative) Testing head.................................................................................................................11
Bibliography ......................................................................................................................................................13
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EN 12697-34:2004+A1:2007 (E)
3
Foreword
This document (EN 12697-34:2004+A1:2007) has been prepared by Technical Committee CEN/TC 227 “Road materials”, the secretariat of which is held by DIN.
This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by January 2008 and conflicting national standards shall be withdrawn atthe latest by January 2008.
This document includes Amendment 1, approved by CEN on 2007-05-16.
This document supersedes EN 12697-34:2004.
The start and finish of text introduced or altered by amendment is indicated in the text by tags!".
This European Standard is one of a series of standards as listed below:
EN 12697-1, Bituminous mixtures — Test methods for hot mix asphalt — Part 1: Soluble binder content
EN 12697-2, Bituminous mixtures — Test method for hot mix asphalt — Part 2: Determination of particle size distribution
EN 12697-3, Bituminous mixtures — Test methods for hot mix asphalt — Part 3: Bitumen recovery: Rotaryevaporator
EN 12697-4, Bituminous mixtures — Test methods for hot mix asphalt — Part 4: Bitumen recovery:Fractionating column
EN 12697-5, Bituminous mixtures — Test methods for hot mix asphalt — Part 5: Determination of the maximum density
EN 12697-6, Bituminous mixtures — Test methods for hot mix asphalt — Part 6: Determination of bulk density of bituminous specimens
EN 12697-7, Bituminous mixtures — Test methods for hot mix asphalt — Part 7: Determination of bulk densityof bituminous specimens by gamma rays
EN 12697-8, Bituminous mixtures — Test methods for hot mix asphalt — Part 8: Determination of void characteristics of bituminous specimens
EN 12697-9, Bituminous mixtures — Test methods for hot mix asphalt — Part 9: Determination of the reference density
EN 12697-10, Bituminous mixtures — Test methods for hot mix asphalt — Part 10: Compactibility
EN 12697-11, Bituminous mixtures — Test methods for hot mix asphalt — Part 11: Determination of the affinity between aggregate and bitumen
EN 12697-12, Bituminous mixtures — Test methods for hot mix asphalt — Part 12: Determination of the watersensitivity of bituminous specimens
EN 12697-13, Bituminous mixtures — Test methods for hot mix asphalt — Part 13: Temperaturemeasurement
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EN 12697-34:2004+A1:2007 (E)
4
EN 12697-14, Bituminous mixtures — Test methods for hot mix asphalt — Part 14: Water content
EN 12697-15, Bituminous mixtures — Test methods for hot mix asphalt — Part 15: Determination of the segregation sensitivity
EN 12697-16, Bituminous mixtures — Test methods for hot mix asphalt — Part 16: Abrasion by studded tyres
EN 12697-17, Bituminous mixtures — Test methods for hot mix asphalt — Part 17: Partial loss of porousasphalt specimen
prEN 12697-18, Bituminous mixtures — Test methods for hot mix asphalt — Part 18: Binder drainage
EN 12697-19, Bituminous mixtures — Test methods for hot mix asphalt — Part 19: Permeability of specimen
EN 12697-20, Bituminous mixtures — Test methods for hot mix asphalt — Part 20: Indentation using cube orMarshall specimens
EN 12697-21, Bituminous mixtures — Test methods for hot mix asphalt — Part 21: Indentation using plate specimens
EN 12697-22, Bituminous mixtures — Test methods for hot mix asphalt — Part 22: Wheel tracking
EN 12697-23, Bituminous mixtures — Test methods for hot mix asphalt — Part 23: Determination of the indirect tensile strength of bituminous specimens
EN 12697-24, Bituminous mixtures — Test methods for hot mix asphalt — Part 24: Resistance to fatigue
EN 12697-25, Bituminous mixtures — Test methods for hot mix asphalt — Part 25: Cyclic compression test
EN 12697-26, Bituminous mixtures — Test methods for hot mix asphalt — Part 26: Stiffness
EN 12697-27, Bituminous mixtures — Test methods for hot mix asphalt — Part 27: Sampling
EN 12697-28, Bituminous mixtures — Test methods for hot mix asphalt — Part 28: Preparation of samples fordetermining binder content, water content and grading
EN 12697-29, Bituminous mixtures — Test methods for hot mix asphalt — Part 29: Determination of the dimensions of a bituminous specimen
EN 12697-30, Bituminous mixtures — Test methods for hot mix asphalt — Part 30: Specimen preparation by impact compactor
EN 12697-31, Bituminous mixtures — Test methods for hot mix asphalt — Part 31: Specimen preparation by gyratory compactor
EN 12697-32, Bituminous mixtures — Test methods for hot mix asphalt — Part 32: Laboratory compaction ofbituminous mixtures by vibratory compactor
EN 12697-33, Bituminous mixtures — Test methods for hot mix asphalt — Part 33: Specimen prepared byroller compactor
EN 12697-34, Bituminous mixtures — Test methods for hot mix asphalt — Part 34: Marshall test
EN 12697-35, Bituminous mixtures — Test methods for hot mix asphalt — Part 35: Laboratory mixing
EN 12697-36, Bituminous mixtures — Test methods for hot mix asphalt — Part 36: Determination of the thickness of a bituminous pavement
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EN 12697-34:2004+A1:2007 (E)
5
EN 12697-37, Bituminous mixtures — Test methods for hot mix asphalt — Part 37: Hot sand test for theadhesivity of binder on pre-coated chippings for HRA
EN 12697-38, Bituminous mixtures — Test methods for hot mix asphalt — Part 38: Common equipment andcalibration
EN 12697-39, Bituminous mixtures — Test methods for hot mix asphalt — Part 39: Binder content by ignition
EN 12697-40, Bituminous mixtures — Test methods for hot mix asphalt — Part 40: In situ drainability
EN 12697-41, Bituminous mixtures — Test methods for hot mix asphalt — Part 41: Resistance to deicing fluids
EN 12697-42, Bituminous mixtures — Test methods for hot mix asphalt — Part 42: Amount of coarse foreignmatters in reclaimed asphalt
EN 12697-43, Bituminous mixtures — Test methods for hot mix asphalt — Part 43: Resistance to fuel
The annexes A and B are normative.
According to the CEN/CENELEC Internal Regulations, the national standards organizations of the followingcountries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain,Sweden, Switzerland and United Kingdom.
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EN 12697-34:2004+A1:2007 (E)
6
1 Scope
This European Standard specifies a test method for determining the stability, flow and the Marshall Quotientvalues of specimens of bituminous mixtures mixed according to!EN 12697-35:2004+A1" and prepared using the impact compactor method of test!EN 12697-30:2004+A1". It is limited to dense graded asphaltconcrete and hot rolled asphalt.
2 Normative references
This European Standard incorporates by dated or undated reference, provisions from other publications.These normative references are cited at the appropriate places in the text, and the publications are listed hereafter. For dated references, subsequent amendments to or revisions of any of these publications apply tothis European Standard only when incorporated in it by amendment or revision. For undated references the latest edition of the publication referred to applies (including amendments).
EN 12697-6, Bituminous mixtures — Test methods for hot mix asphalt — Part 6: Determination of bulk densityof bituminous specimens
EN 12697-29, Bituminous mixtures — Test methods for hot mix asphalt — Part 29: Determination of the dimensions of a bituminous specimen
!EN 12697-30:2004+A1", Bituminous mixtures — Test methods for hot mix asphalt — Part 30: Specimenpreparation by impact compactor
EN ISO 7500-1, Metallic materials — Verification of static uniaxial testing machines — Part 1:Tension/compression testing machines (ISO 7500-1:1999)
3 Terms and definitions
For the purposes of this European Standard, the following terms and definitions apply.
3.1stability Smaximum resistance to deformation, in kilonewtons (kN), of a moulded asphalt specimen
3.2flowFdeformation of the moulded specimen in millimetres (mm) at maximum load less the nominal deformationobtained by extrapolation the tangent of the graph of load against deformation back to zero load (A to M’ inannex A)
3.3tangential flowFtnominal deformation of the moulded specimen, in millimetres (mm) obtained by extrapolation the tangent of the graph of load against deformation forward to the stability load less the nominal deformation obtained byextrapolation the tangent back to zero load (A to B’ in annex A)
3.4Marshall quotient ratio of the stability, S, to the flow, F, S/F, see annex A
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EN 12697-34:2004+A1:2007 (E)
7
4 Principle
Marshall specimens are compacted in accordance with!EN 12697-30:2004+A1". The Marshall stability,flow and quotient are subsequently determined on these specimens using defined procedures and reportedalong with the bulk density of the specimen.
5 Apparatus
5.1 Compression testing machine of Grade 2 or better according to EN ISO 7500-.1 having arecommended minimum capacity of 28 kN and capable of applying loads to test specimens at a constant rateof deformation of (50 ± 2) mm/min after a transitory period less than 20 % of the loading time. The rate ofdeformation is to be maintained.
5.2 A flow!measuring" device capable of determining deformation to an accuracy of ± 0,1 mm.
5.3 Graphical plotter: device for evaluating the curve of force versus flow, e.g. graphical plotter, striprecorder or software program.
5.4 Testing head: upper and lower breaking heads with the dimensions given in annex B.
5.5 Water bath, at least 150 mm deep and capable of thermostatically maintaining the water at atemperature of (60 ± 1) °C. This bath shall have a perforated false bottom or shelf that can suspend the testspecimens at least 25 mm above the bottom of the bath, and allow at least 25 mm depth of water above thespecimens. The size of the bath shall allow specimens to be placed face down and not in contact with one another. A device to ensure continuous circulation of water shall also be fitted.
5.6 Thermometer, capable of measuring a temperature of 60 °C accurate to 0,5 °C.
5.7 Oven, capable of maintaining temperature of (110 ± 5) °C.
6 Procedure
6.1 Specimen preparation
6.1.1 Specimens shall be compacted in accordance with !EN 12697-30:2004+A1" ensuring that 50 blows are applied to each side within the acceptable temperature range given.
6.1.2 The compacted specimens shall be demoulded ensuring that they are cooled in air to avoid any dangerof deformation and tested in accordance with section 6.5 to 6.7. After demoulding wait at least 4 h before further testing begins. All tests shall be complete within 32 h of demoulding.
The bulk density of each specimen shall be determined in accordance with EN 12697-6.
6.1.3 The height of each specimen shall be measured in accordance with EN 12697-29, or the volume shall be calculated from the bulk density measurement.
6.1.4 Immerse the cylindrical specimens, on their flat surface, in the water bath for at least 40 min and not longer than 60 min. Maintain the temperature of the water in the bath at (60 ± 1) °C.
6.2 Test procedure
6.2.1 Thoroughly clean the guide rods and the inside surfaces of the test heads. Lubricate the guide rods toensure that the upper test head slides freely over them.
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EN 12697-34:2004+A1:2007 (E)
8
6.2.2 Prepare the test head by preheating for at least 30 min at (60 ± 1) °C in the water bath or for 1 h in theoven.
This action shall be undertaken at the start of testing of a batch of specimens not greater than twelve innumber. In the event of a delay of more than 3 min between the testing of each specimen the test head shall be heated in a suitable oven or water-bath maintained at the specified test temperature. The minimumreheating period shall be the lesser of the delay encountered and 30 minutes when heated in a water bath, ordouble that when heated in an oven.
6.2.3 Remove the test specimen from the water bath and place it centrally on its side in the test headensuring good surface contact between the specimen and the test head. Place the complete assemblycentrally on the testing machine.
Prior to testing each specimen the test head shall be cleaned as required. An environmentally suitable solventmay be used for cleaning and a silicone spray applied to prevent specimens adhering to the test head.
6.2.4 Apply the load to the test specimen to achieve a constant rate of deformation of (50 ± 2) mm/minallowing for the transitory period. Continue the application of this load until the maximum reading is obtained on the load measuring device. Record the load indicated. This section of the test shall be carried out within40 s of removal of the test specimen from the water bath.
Also measure the distance to ±0,5 mm, from the intersection of the tangent and the base line, A, to the pointwhere the maximum load is achieved, M.
6.2.5 Carry out the stability and flow tests on a set of four specimens.
7 Expression of results
7.1 The maximum load attained represents the stability of the mix only if the specimen height equals the required 63,5 mm. A corrected stability shall be reported by multiplying the maximum load with the correction factor calculated from the following equations using the volume of the specimen as determined in accordancewith 6.2:
!
vh eec6102,30258,0 24,524,5
−×−− ==
where
c is the correction factor;
h is the height of the specimen (in millimetres);
v is the volume of the specimen determined in 6.2 (in millilitres)."
The stability, S, is reported to the nearest 0,1 kN.
NOTE Corrections outside the range of specimen heights from 60,5 mm to 66,5 mm can lead to inaccurate results.
7.2 Record the flow values, F and Ft, obtained to the nearest 0,1 mm.
7.3 !Test results shall be considered reliable if both the variation in stability between specimens, VS, is less than 15 % and the variation in flow between specimens, Vf, is less than 20 %. Reject the test specimen with thelargest variation and obtain the average value of the other specimens if either:
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EN 12697-34:2004+A1:2007 (E)
9
the stability value from one or more specimens differ from the average stability by more than 15 %, or
the flow value from one or more specimens differ from the average flow by more than 20 %.
Furthermore, if any value differs from the new average by more than 15 % for stability or 20 % for flow, repeatthe test."
7.4 The Marshall quotient shall be obtained by calculation S/F and reporting the value obtained to 0,1 kN/mm.
8 Test report
The test report shall include the following information:
a) the average results F, Ft, S and Marshall quotient for each set of specimens;
b) the average bulk density of the specimen set;
!deleted text"
c) the number and date of this European Standard.
9 Precision
Table 1 — Asphalt concrete
Repeatability ReproducibilityMarshall Standard deviation,
σrRepeatability, r
Standard deviation,σR
Reproducibility, R
Stability (kN) 0,61 1,7 0,78 2,2
Flow (mm) 0,25 0,7 0,29 0,8
The precision data are estimated from DIN 1996/11 and NL-Standard for asphalt concrete- 2000 Standard RAWBepalingen.
Table 2 — Hot rolled asphalt
Repeatability ReproducibilityMarshall Standard deviation,
σrRepeatability, r
Standard deviation,σR
Reproducibility, R
Stability (kN) 0,36 1,0 0,78 2,2
Flow (mm) 0,21 0,6 0,46 1,3
The precision data are estimated from TRRL Research report 281.
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EN 12697-34:2004+A1:2007 (E)
10
Annex A(normative)
Marshall quotient
Figure A.1 is a graphical representation of the definitions for stability, S, flow, F, and tangential flow, Ft, contained in clause 3.
Key
1 Stability S2 Tangent3 Flow F
Figure A.1 — Marshall quotient
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EN 12697-34:2004+A1:2007 (E)
11
Annex B(normative)
Testing head
Figure B.1 illustrates the essential dimensions of a suitable breaking head for use in this test. This testinghead is used in conjunction with the compression testing machine to determine the stability and flow of the moulded specimens.
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EN 12697-34:2004+A1:2007 (E)
12
Dimensions in millimetres
The radius shall be the same for both upper and lower segments.
Key
1 Upper testing head 2 Lower testing head
Figure B.1 — Testing head
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EN 12697-34:2004+A1:2007 (E)
13
Bibliography
!EN 12697-35:2004+A1", Bituminous mixtures — Test methods for hot mix asphalt — Part 35: Laboratory mixing
DIN 1996/11, Testing of bituminous materials for road building and related purposes: Determination ofMarshall stability and of Marshall flow value
NL Standard for Asphalt concrete — 2000 Standard RAW Bepalingen
TRRL Research Report 281: Precision of tests used in the design of rolled asphalt
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BS EN 12697-34:2004
BSI389 Chiswick High RoadLondonW4 4AL
BSI — British Standards InstitutionBSI is the independent national body responsible for preparingBritish Standards. It presents the UK view on standards in Europe and at the international level. It is incorporated by Royal Charter.
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