· 2007. 7. 31. · UST Closure Report UST NO. AS-146 GWNST-12 UNDERGROUND STORAGE TANK CLOSURE...

GW-UST 12 REPORT Delivery Order No. 044

UST Removal At AS146

Marine Corps Air Station - New River Camp Lejeune, North Carolina

Prepared for

The Atlantic Division, Naval Facilities Engineering Command

July, 2000

Prepared by

J.A. Jones Environmental Services Company

61 35 Park South Drive, Suite 250

Charlotte, North Carolina 2821 0

J.A. Jones No. 005.044

UST Closure Report UST NO. AS-146

GWNST-12 UNDERGROUND STORAGE TANK CLOSURE REPORT

UST NO. AS-146

Location: MCAS, New River, NC

The closure report should contain, at a minimum, the following information. Any other information that is pertinent to the site should be included.

I I. General Information I

A. Ownership of UST(s) 1. Name of UST owner:

Commanding General Marine Corps Base, Camp Lejeune, North Carolina

2. Owner address and telephone number: Commanding General ACIS, Environmental Management Department PSC 20004 MCB, Camp Lejeune, NC 28542 910-451-5837

B. Facility Information 1. Facility name:

Building AS- 146

2. Facility ID #: N/A

3. Facility address, telephone number, and county: Conlmanding General AC/S, Environmental Management Department PSC 20004 MCB, Camp Lejeune, NC 28542 910-451-5837 Onslow County

C. Contacts 1. Name, address, telephone number and job title of primary contact person:

Brian Marshburn - Environmental Engineer AC/S, EMD PSC 20004 MCB, Camp Lejeune, NC 28542 9 10-45 1-5 837

2. Name, address, and telephone number of closure contractor: J.A. Jones Environmental Services Company 6135 Park South Drive, Suite 250 Charlotte, North Carolina 282 10 704-553-3595

J.A. Jones Environmental Services Company Contract No. N62470-93-D-3033, DO-44

UST Clos~~re Report UST NO. AS-1 46

3. Name, address, and telephone number of primary consultant: J.A. Jones Environmental Services Company 6135 Park South Drive, Suite 250 Charlotte, North Carolina 282 I0 704-553-3595

4. Name, address, telephone number, and State certification number of laboratory: Prism Laboratories, Inc. 449 Springbrook Road Charlotte, NC 282 17 704-529-6364 North Carolina certification #: 402

D. UST Information

E. Site Characteristics 1. Describe any past release at this site:

No past release has been reported.

Tank No. AS-146

2. Is the facility active or inactive at this time? If the facility is inactive note the last time the USTs were in operation:

The facility is active but the UST was inactive.

3. Describe surrounding property use (for example, residential, commercial, farming, etc.): The site is on a military base. The UST was located in a fuel farm which is surrounded on all directions by roads, open field. Therefore this site may fall into the commercial/industriaI category.

Installation Date Unknown

4. Describe site geology/hydrogeology: The area is located in the Outer Coastal Plain of North Carolina. Regionally, the predominant soil type is sandy silt to clayey silt with unknown thickness. The depth to the underlain bedrock of Tertiary aged Belgrade Formation is unknown, but is estimated to be more than 50 feet. The average depth-to-water is estimated to be 8 feet from ground surface. The nearest surface water body is New River, which is approximately 6,000 feet from the site. The flow direction of groundwater in the surficial aquifer is unknown, but is assumed to flow towards the river. All buildings in this area are supplied by a public water supply system. There are two drlnking water wells located within 1500 ft radius. However, these wells are currently under contract for demolition. The demolition contract is scheduled for completion January 2001.

I 11. Closure Procedures

Size in Gallon 5,000

A. Describe preparations for closure including the steps taken to notify authorities, permits obtained, and the steps taken to clean and purge the tanks:

A GWIUST-3 form was submitted to the Environmental Management Department of the Base on 7/12/1999. A copy of the GWJUST-3 form is included in Appendix B. The UST was a cubic concrete tank (Photo 1 and 2) and was completely empty with the exception of small amounts of dry sludge on the floor and 2 - 3 gallons of liquid in a pump sink of the floor. Prior to removal, the UST was cleaned through sweeping the solid and scooping the liquid out of the pump sink. Both the solids and liquids were stored in a 55-gallon drum, which was transported off-base on 611 512000 and treated at a certified wastewater treatment facility in High Point, North Carolina. The transportation manifest of the waste is included in Appendix D, and the lab analytical results for both solid and liquid are included in Appendix F.

J.A. Jones Environmental Services Company Contract No. N62470-9343-3033, DO-44

Tank Dimension 17'4" x 1 1 '6" x 6'

Last Content JP-5

UST Closure Report UST No. AS-146

B. Note the amount o f residual material pumped from the tank(s): See Section 11. A.

C. Describe the storage, sampling, and disposal o f the residual material: See Section 11. A.

D. Excavation 1.- Describe excavation procedures noting the condition of the soils and the dimensions of

the excavation in relation to the tanks, piping and/or pumps: The concrete UST was demolished on-site during 5/23/2000 and 5/25/2000. Excavation was kept to a minimum to avoid jeopardizing the supporting poles of a 6.5 inch diameter fuel pipe that is 4 feet from the east edge of the tank. A landslide occurred when excavating to expose the south wall of the tank (Photo 8). After the 4 walls of the tank were demolished, it was found that the size of the bottom slab was larger than the horizontal dimensions of the tank, at least 2 feet beyond the wall on all directions. Therefore, it was decided not to remove the bottom slab of the UST.

Slight petroleum odor was observed in soil on the north sidewall of the UST.

The final dimensions of the excavation were 23.5' (L) x 14.5' (W) x 7' (D).

2. Note the depth of tank burial(s) (from land surface to top of tank): The top of the tank was flush with the ground surface.

3. Quantity of soil removed: Approximately 10 tons of soil was excavated to expose the sidewalls of the tank.

4. Describe soil type(s): Based on field observation, soil above the underside of the UST was brown silty sand that might be the backfill material when the tank was constructed. Below the bottom slab was limestone gravel with unknown thickness, which is believed to be the UST construction base.

5. Type and source of backfill used: Common fill (sand) obtained from a borrow pit on the Base.

E. Contaminated Soil The excavated soil was stockpiled on-site and a composite soil sample was taken from the stockpile. Upon receiving analytical results of the sample that indicate diesel range total petroleum hydrocarbon (TPH) concentration of 28 ppm and gasoline range TPH concentration of 110 ppm, this material was transported off-base on 6/19/2000 and disposed of by ES&J Enterprises, Inc. at its facility located in Autryville, North Carolina. A copy of the contaminated soil transportation manifest is included in Appendix E and a copy of the lab analytical report is included in Appendix G.

1 111. Site Investigation

A. Provide information on field screening and physical observations, including methods used to calibrate field screening instrument(s):

A FOXBORO TVA PIDIFID was used for field screening during the soil sample collection activities prior to the UST demolition. The instrument was calibrated per the user's menu provided by the manufacture. Table 1 is a summary of the screening results.

J.A. Jones Environmental Services Company Contract No. N62370-93-D-3033, D O 4


No apparent soil discoloration was observed during either soil collection activities or UST demolition. However, slight petroleum odor was observed during excavation on the north sidewall of the tank.

B. Describe soil sampling points and sampling procedures used: Prior to UST demolition, 4 soil borings (AS 146- 1 through AS 146-4) were advanced to 10' below land surface, one at each comer of the UST as illustrated on the site drawing. One soil sample was collected at approximately 10 feet below the land surface from each soil boring. After the UST was demolished on 5/25, one additional soil sample (AS146-MID) was collected at the bottom center of the tank by drilling a hole through the concrete slab into the soil beneath it. The samples were tested using EPA Methods 3550 for TPH-DRO, 5030 for TPH-GRO, 305 1 for total Cr and Pb, 8080 for PCBs and pesticides.

C. Describe groundwater or surface water sampling procedures used: One groundwater sample was collected at the bottom center of the tank when a hole was drilled through the bottom slab for both soil and water sampling purpose. The water samples was tested using EPA Methods 6230 for volatiles, 625 for semi-volatiles, 3030C for total Cr and Pb, MADEP VPH and EPH for alkanes/aromatics.

D. Quality control measures; Lab-provided containers and dedicated disposable gloves were used for sampling. Upon collection, the samples were stored in a cooler, chilled by ice, and sent to the laboratory through an over-night carrier.

E. Investigation results Except for slight petroleum odor observed in soil at the north sidewall, no soil discoloration or petroleum odor were observed in the soil borings and the excavation. No free product was observed on groundwater surface that was visible at the sampling hole drilled through the floor slab.

As shown in Table 2, TPH-GRO concentration in soil sample AS146-4, and both TPH-GRO and TPH- DRO concentrations in soil samples AS146-2 and AS146-MID are above the State Reportable Limit of 10 ppm. Trace concentration of certain pesticides were detected in samples AS146-1 and AS146-MID. Possibly attributed to a regional background, total Pb and/or total Cr are at detectable levels in all soil samples. In some samples, total Pb and/or total Cr levels are above the 5 ppm regulatory level set forth for Toxicity Characteristic Leakage Procedure.

In groundwater, as shown in Table 3, a number of compounds are detected at a level above the laboratory's Method Detection Limit. Among organic compounds, benzene, naphthalene, and C9-C 10 aromatics are at concentration above North Carolina Groundwater Standards or Interim Groundwater Standards. However, all of them are significantly below the corresponding Groundwater Gross Contamination Level (GCL). It is noted that both total Pb and total Cr concentrations are above Groundwater GCL.

I IV. Conclusions and Recommendations

Petroleum hydrocarbon contamination is indicated in soil at concentrations above the state reportable levels. Groundwater contamination is also indicated. However, this contamination is likely a portion of a contamination plume that was derived from sources in the he1 farm other than this concrete used-oil UST.

The petroleum hydrocarbon contamination levels in both groundwater and soil at this location are relatively low in view of the industrial land use category. Therefore, natural attenuation is considered to be the optimum remediation choice.



/ V. Signature and Seal of Professional Engineer or Licensed Geologist 7

A. Figures 1. Site Location Map 2. Site Drawing

B. Tables 1. Field Soil OVA Screening Results 2. Analytical Results of Soil Samples 3. Analytical Results of Groundwater Sample

C. Appendices Appendix A: Appendix B: Appendix C: Appendix D: Appendix E: Appendix F: Appendix G: Appendix H:

GW-UST-2 Form Copy of GW-UST-3 Form Certificate of UST Disposal Waste Transportation Manifest Contaminated Soil Transportation Manifest Laboratory Analytical Report for Tank Contents Laboratory Analytical Report for Soil and Groundwater Photographs of UST Closure Activities



FIGURES

1. Site Location Map

2. Site Drawing


SCALE 1:24 000

H H H

New River, North Carolina

Remove UST AS-146

- So11 Bonng AS-146-1 , 10' from land surlace

TPH-DRO BDL "d TPH-GRO BDL Total Cr 5 6 pprn

Soil Sample AS-146-MID Total Pb 2 8 pprn

10' fmm land surface 8' from land surface TPH-DRO BDL TPH-DRO 170 pprn ' except 4.4'-DDD 0 00466 pprn

4,4'-DDE 0 00233 ppm

Pest~udes BDL

- So11 Bor~ng AS-146-3 10' from land surface TPH-DRO BDL TPH-GRO 30 ppm TPH-GRO BDL Total Cr 24 pprn Total Cr 5 3 pprn

Pest~udes BDL

5000 gal. Concrete Used Oil UST 17'4'~ 11'2'xW(D)

Concrete Drive-Way

- . - - - -- -. - - - - - - -- - -- -


TABLES

Table 1. Field Soil OVA Screening Results

Date: 511 812000 Instrument: Foxboro TVA- 1 000

Note: No soil sample was recoverable from Soil Boring AS-146-2, only a small amount of soil collected at 10' below land surface for lab test.

Sample ID Matrix Location Depth FID Reading (ppm) PID Reading (ppm)

1-9 Gravel Soil Boring AS- 146-1 9' 3

1-10 Gravel Soil Boring AS-146-1 10' 285

3-7 Sand Soil Boring AS-146-3 7' 890

3-9 Gravel Soil Boring AS-146-3

Table 2. Analytical Results of Soil Samples

3-10

4-7

4-9

4-10

Note: Concentration in ppm * ---- Except 4,4'-DDD (0.00466 ppm) and 4,4'-DDE (0.00233 ppm) ** ---- Except 4,4'-DDT (0.0057 ppm)

Gravel

Sand

Gravel

Gravel

Sample ID

AS-146-1

AS-146-2

AS-I 46-3

AS- 146-4

AS- 146-MID

J.A. Jones Environmental Services Company Contract No. N62470-93-D3033, DO-44

Soil Boring AS-146-3




Date

511 8/00

511 8/00

511 8/00

511 8/00

5/25/00

10' ppppp

7'

9'

10'

Pesticides

BDL*

BDL

BDL

BDL

BDL**

101

1600

1380

485

TPH-DRO

BDL

36

BDL

BDL

170

Depth

10'

10'

10'

1 0'

8'

19

14

18

19

Cr Total

5.6

24

5.3

9.5

2.6

TPH-GRO

BDL

3 0

BDL

15

200

Pb Total

2.8

16

1.2

BDL

3.4

PCBs

BDL

BDL

BDL

BDL

BDL


Table 3. Analytical Result of Groundwater Sample

Sample ID: AS-146-Water Sample Date: 5/25/00 Concentration in ppb

Note: N/E ---- Not established * ---- set for petroleum aliphatic carbon fraction class C9-C18 ** ---- set for petroleum aromatics carbon fraction class C9-C32

n-butylbenzene naphthalene

0 2,4-dimethylphenol Phenol C5-C8 aliphatics C9-C 12 aliphatics C9-C 10 aromatics


6230D 6230D

625 625

VPH VPH VPH

46 56

7 17 2 1 420 330 560

70 2 1

6,900 15,500

140 3 00 420

4,200* 210**

UST Closure Report

APPENDIX A

GW-UST-2 Form


UST NO. AS-146

Contract No. N62470-93-D-3033. DO-44

Return Completed Form To: State Use Only TANKS The appropriate DWQ Regional Office according to the county of the facility's

IN Location. [SEE REVERSE SIDE OF OWNER'S COPY (PINK) FOR REGIONAL I.D. Number

NC OFFICE ADDRESS]. Date Received

I Complete and return within (30) days following completion of site investigation. I

Owner Name: Commanding General, MCB Capos Wwhl, Wlr *Inr*. - m a r haw)

Street Address: AC/S, EMD, MCB, PSC20004 County: OnsIow City: Camp Lejeune State: NC Zip Code: 28542 Tele. No. (Area Code): (910) 451-5837

Facility Name or Company: Building AS-146, MCAS

Facility ID #: Street Address or State Road: Camp Lejeune County: Onslow City:Camp Lejeune Zip Code: 28542 Tele. No. (Area Code): (910) 451-5837

Name: Mr. Brian Marshburn Job Title: Environmental Engineer Tel. No.: (910) 451-5837

Closure Contractor: LA. Jones Environmental Serv. Address: 6135 Park South Dr. Charlotte,NC Tel. No.: (704) 553-3595

Primary Consultant: Same Address: Same Tel. No.: Same

Lab: Prism Laboratories Address: 449 Springbrook Rd. Charlotte,NC Tel. No.: (704) 529-6364

See reverse side of pink copy (owner's copy) for additional

information required by N.C. - DWQ in the written

report and sketch.

Tank No.

NOTE: If a release from the tank(s) has occurred, the site

assessment portion of the tank closure must be conducted under the supervision of a P.E. or L.G., with all closure site assessment

reports bearing the signature and seal of the P.E. or L.G.

PERMANENT CLOSURE (For Removing or Abandoning-in-place)

Contact local fire marshal Notify DWQ Regional Office before abandonment. Drain & Flush piping into tank.

ULI Remove all product and residuals tiom tank. ULI Excavate down to tank. ULI Clean and inspect tank. a Remove drop tube, fill pipe, gauge pipe, vapor recovery tank connections,

submersible pumps and other tank fixtures. 'LEI Cap or plug all lines except the vent and fill lines.

Purge tank of all product & flammable vapors. O Cut one or more large holes in the tanks.

Backtill the area. Date Tank@) Permanently Closed: 5/23/2000 Date of Change-in-Service:

AS-146 5000 17.3 'x 11.5 56' Used Oil X x x

Size in Gallons

ABANDONMENT IN PLACE

Fill tank until material overflows tank opening. Plug or cap all openings. Disconnect and cap or remove vent line. Solid inert material used - specify:

REMOVAL

Create vent hole. O Label tank. U Dispose of tank in approved manner.

Final tank destination: Base Landfill Marine Corps Base, Camp Leieune, NC

Tank Dimensions

I certify under penalty of law that I have personally examined and am familiar with the information submitted in this and all attached uments, and that based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that the

brnitted information is true, accurate, and complete. name and official tide of owner or owner's authorized representative Signature Date Signed

JamesX Tan Project Geologist 1 6/1/2000 I I

GWNST-2 (Rev. 10196) While Copy - Regional Office Yellow Copy - Cenvsl Office Pink Copy - Owner

Last Contents

Water in Excavation

Yes

Free Roduct

No Yes

Notable Odor or Visible Soil Contamination

No Yes No

UST Closure Report

APPENDIX B

Copy of GW-UST-3 Form


UST NO. AS-146

Contract No. N62470-93-D-3033, DO-44

The appropriate DWQ Regional Office according to the county of the facility's Location. [SEE REVERSE SIDE OF OWNER'S COPY (PINK) FOR REGIONAL OFFICE ADDRESS].

INSTRUCTIONS Complete and return at least five (5) working days prior to closure or change-in-service if a Professional Engineer (P.E.) or a

Licensed Geologist (L.G.) provides supervision for closure or change-in-service site assessment activities and signs and Seals all closure reports. Otherwise, thirty (30) days notice is required.

Tank Owner Name: Commanding General, MCB - - W l i r A " w , ~ a " ~ )

Street Address: ACIS, EMD. PSC20004 County: Onslow City: Camp Leieune State: NC Zip Code: 28542 Tele. No. (Area Code): (910) 451-5837

Facility Name or Company: AS146. MCAS

Facility ID # (if available):N/A Street Address or State Road: MCAS New River County: Onslow City:Camp Leieune Zip Code: 28542 Tele. No. (Area Code): (9 10) 451-5837

I Name: Mr. Brian Marshbum Job Title: Environmental Engineer Telephone Number: /9 10) 451-5837 1

1. Contact Local Fire Marshall. 5. Provide a sketch locating piping, 2. Plan the entire closure event. tanks and soil sampling locations. 3. Conduct Site Soil Assessments. 6. Submit a closure report in the format of 4. If Removing Tanks or Closing in Place GWNST-12 and include the form

refer to API Publication 2015 "Cleaning GWNST-2 within 30 days following the Petroleum Storage Tanks" & 1604 site investigation. "Removal & Disposal of Used Under- 7. If a release fk0m the tank(s) has occurred, ground Petroleum Storage Tanks". the site assessment portion of the tank

Closure must be conducted under the Supervision of a P.E. or L.G., with all Closure site assessment reports bearing Signature and seal of the P.E. or L.G. If a release has not occurred, the Supervision, signature, or seal of a P.E Or L.G. is not required.

8. Keep closure records for 3 years.

- I (Contractor) Name: J.A. Jones Environmental Services. Company

Address: 6 135 Park South Drive Suite 250 Charlotte State: North Carolina Zip Code: 282 10

Contact: Bryan Steiner Phone: (704) 553-36 18

Primary Consultant: Jim Tan L.G. (J.A.J.E.S.) Phone: 1704) 553-3379

I - - - ~ - - - - - - - -- - -. . - - -

I Removal I Abandonment I New Contents Stored I

AS 146 5.000 Gallons Used Oil

• * Scheduled Removal Date: 8/3/99 ate Submitted: 711 2/99

GWNSK~ (Rev. 6/96) White copy - kegibnal Ofice Yellow Copy - Central Ofice Pink Copy - Owner

UST Closure Report

APPENDIX C

Certificate of UST Disposal


UST NO. AS- 146

Contract No. N62470-93-D-3033, DO-44

6135 Park South Drive, Suite 250, Charlotte, NC 28210 (704) 553-3595 / (704) 553-3599

TANK DISPOSAL MANIFEST 1. Tank Owner:

Commanding General, Marine Corps Base, Camp Lejeune, North Carolina ACE, Environmental Management Division, MCB, Camp Lejeune, NC 28542

- -

2. Tank Owner / Authorized Representative: Contact: Mr. Gene Jones Phone# (910)451-1482

3. Description of Tanks:

Tank ID No. Capacity Previous Content Comtnents

AS-146 9,000 Gallons Used Oil

-

4. Tank Owner / Authorized Representative Certification: The undgrsigned certifies that the above listed storage tank(s) have been removed from the premises of the tank owner.

5) Transporter: The undersigned certifies that the above listed storage tank(s) have been demolished into debris and transported to the landfill, Marine Corps Base, Camp Lepune, North Carolina.

6) Disposal Certification: The undersigned certifies that the above named storage tank(s) have been demolished into debris and accepted by the landfill facility.

Receving Facility: Landfill, MCB, Camp Lejeune, NC (9 10) 45 1-2946 /, - 3 - - /'.'.-'<

'"w C / . N / ~ / . / /se e :/-ft A , . . I.%-< 5-=:3 5 - 2 ~ .d .;

Printed / Typed N a d -

Signaturq' 'i. MontWDq/Year \ 1 'w

UST Closure Report

APPENCIX D

Waste Transportation Manifest


UST NO. AS-I46

Contract No. N62470-93-D-3033. DO-44

Nan-Hazardous Waste Shipping Document c. ..

Document #: 6 3 7 7 i

1 i Page 1 of

I

*.- . .

ContaiuerlTag Number:

. ,: ,. . .

: . ,

Lab: P pi m La. b ,449 $&*ybrVo& ~ d . , ' ($03(0(f~, AIc. 2 1224 . .

Additional 1nfonnatio.n and ~ i ; c G ~ ~ c ~ Indication: . ii, . . .. , m. . . *

.- . . .

GENERATOR'S STATEMENT: The materials described ahve on th for proper disposal of hazardous,.,wqste. Pi$eter$nqion of non-h8)adous . . . . .,? .> . . . analysis provided by: . .

?. ~ri i~te .d~T)pd Name . .

/ ,. . .FUS~&. p. '5i' ./

~rans~orter's+ame , . .

. . 1 Avc &a.,.- ,w- 6 . / j - ~ d ., C#. /c=5 ':

Profile #: , ' .

accepting Facility

. ,

6-/L- uq a ~

V ~ ---

Destination Facility's chpy *.

I signa&\e; Date:

UST Closure Report

APPENCIX E

Contaminated Soil Transportation Manifest

UST NO. AS-146

J.A. Jones Environmental Services Company Contract No. N62470-93-D-3033, D O 4

. . . ,

Marine Corps Base, Camp L e j k ~ e . . ' .

--- e & Mailblg Address: Corn~llandi~lg Ge~ieral

AUS EMDllXD

PSC Box 20004 Camp Lejeune, NC 28542-0004

Nullher Type

--

h o m e #:

ion and ~ i s c r e ~ m c ~ Indication:

UST Closure Report

APPENDIX F

Laboratory Analytical Reports for Tank Contents

UST NO. AS-146


L LABORATORIES, INC.

Full Service Analytical & Environmental Solutions

811 9/99

James Tan

J.A. Jones Management Service

61 35 Park South Dr, Ste 250

Charlotte, NC 2821 0

Paae 1 of 4

Customer Project ID: 005-044-AS146 Customer Sample ID: AS146-SEDIMEN

Prism S a r n ~ l e ID: A638021 Loain Grouo: 9394E2

Sample Collection Datemime: 8/5/99 08:30 Lab Submittal Datemime: 8/6/99 10:30

The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:

TEST TEST METHOD DATEfr l ME PARAMETER RESULT UNITS MDL - REFERENCE STARTED ANALYST

TCLP EXTRACTION (VOLATILES ONL

TCLP EXTRACTION

PREP. METHOD 3510

PREP. METHOD 3510 WlTH EXCHAN

PREP. METHOD 3510 WlTH EXCHAN

ARSENIC, LEACHABLE

SELENIUM, LEACHABLE

CADMIUM, LEACHABLE

Completed

Completed

Completed

Completed

Completed

Less than

Less than

Less than

CHROMIUM, LEACHABLE Less than rnolL 0.50 6010

LEAD. LEACHABLE

SILVER, LEACHABLE

BARIUM, LEACHABLE

MERCURY, LEACHABLE

MERCURY DIGESTION

METALS DIGESTION

CHLORDANE

ENDRIN

HEPTACHLOR

LINDANE

METHOXYCHLOR

TOXAPHENE

HEPTACHLOR EPOXIDE

. . . .>. - Less than mg/L 0.50 601 3

Less than mg/L 0.50 6010

Less than

Less than

Completed

Completed

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

6010

7471

7471

EPA 3010

SW-846 8081

SW-846 8081

SW-846 8081

SW-846 8081

SW-846 808 1

SW-846 8081

SW-846 8081

LAC

LAC

LAC

S A

S A

MSP

MSP

MSP

8/12/99 14:OO MSP

8/12/99 14:OO MSP

8/12/99 14:OO MSP

MSP

GRR

GRR

GRR

S A

S A

S A

S A

S A

S A

S A

Not detected mg/L I .O SW-846 8150 811 3/99 10:29 S A

Not detected mg/L 0.10 SW-846 81 50 811 3/99 10:29 S A

---------- BENZENE Not detected mg/L 0.01 SW846-8260 811 1199 12:42 MP

CARBON TETRACHLORIDE Not detected mg/L 0.01 SW846-8260 811 1199 12:42 MP

CHLOROBENZENE Not detected mg/L 0.01 SW846-8260 811 1199 12:42 M P

CHLOROFORM Not detected mg/L 0.01 SW846-8260 811 1199 12:42 MP

14-DICHLOROBENZENE Not detected mg/L 0.014 SW846-8260 811 1199 12:42 MP

1,2-DICHLOROETHANE Not detected mg/L 0.01 SW846-8260 811 1/99 12:42 MP

1,l-DICHLOROETHENE Not detected mg/L 0.01 SW846-8260 811 1199 12:42 MP

NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification N. E87519

449 Springbrook Road - P.O. Box 240543 Charlotte, NC 282244543

Phone: 704/529-6364 -Toll Free Number: 1-800l529-6364 A Fw: 704/525-0409

PRISM LABORATORIES, INC.

Full Service Analytical 8 Environmental Solutions

811 9/99 Paae 2 of 4

James Tan Customer Project ID: 005-044-AS146

J.A. Jones Management Service Customer Sample ID: ASI46-SEDIMEN

61 35 Park South Dr, Ste 250 Prism Samole ID: A638021

Charlotte, NC 28210 L o ~ i n Group: 9394E2

Sample Collection Date/Time: 8/5/99 08:30 Lab Submittal DatefTime: 8/6/99 10:30


TEST TEST METHOD DATEKIME PARAMETER RESULT UNITS MDL REFERENCE STARTED ANALYST

METHYL ETHYL KETONE Not detected mg/L 0.04 SW846-8260 811 1/99 12:42 MP

TETRACHLOROETHENE Not detected mg/L 0.012 SW846-8260 811 1 I99 12:42 MP

TRICHLOROETHENE Not detected mg/L 0.01 S W 846-8260 811 1 I99 12:42 MP

VINYL CHLORIDE Not detected mg/L 0.02 S W 846-8260 811 1/99 12:42 MP

CRESOLS

1,4-DICHLOROBENZENE

2,4-DINITROTOLUENE

HEXACHLOROBENZENE

HEXACHLOROBUTADIENE

HEXACHLOROETHANE

NITROBENZENE

PENTACHLOROPHENOL

PYRlDlNE

2,4,5-TRICHLOROPHENOL


Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

Sample Comments:

TCLP pesticides and herbicides subcontracted to NC certified lab # 387.

is sample was raised due to sample matirx.

Angela D. Overcash, V.P. Laboratory Services

NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification N. E87519

449 Springbrook Road A P.O. Box 240543 -Charlotte, NC 28224-0543

Phone: 7041529-6364 A Toll Free Number: 1-8001529-6364 A Fax: 7041525-0409 --


Paae 3 of 4

James Tan Customer Project ID: 005-044-AS1 46

J.A. Jones Manaaement Service Customer Sample ID: AS146-LIQUID - 6135 Park South Dr, Ste 250


Prism S a m ~ l e ID: A838022 Lonin Grou~: 9394E2

Sample Collection DateKime: 8/5/99 09:45 Lab Submittal DateKime: 8 /6 /99 10:30

The following analytical results have been obtained for the Indicated sample which was submitted to this laboratory:

TEST TEST METHOD DATErrlME PARAMETER RESULT UNITS MDL STARTED ANALYST - REFERENCE

TCLP EXTRACTION (VOLATILES ONL

TCLP EXTRACTION

PREP. METHOD 3510

PREP. METHOD 3510 WITH EXCHAN

PREP. METHOD 3510 WITH EXCHAN

ARSENIC, LEACHABLE

SELENIUM, LEACHABLE

CADMIUM, LEACHABLE

CHROMIUM. LEACHABLE

a LEAD, LEACHABLE

SILVER. LEACHABLE

BARIUM, LEACHABLE

MERCURY, LEACHABLE

MERCURY DIGESTION

METALS DIGESTION

CHLORDANE

ENDRIN

HEPTACHLOR

LINDANE

METHOXYCHLOR

TOXAPHENE

HEPTACHLOR EPOXIDE

Completed

Completed

Completed

Completed

Completed

Less than

Less than

Less than

Less than

Less than

Less than

Less than

Less than

Completed

Completed

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

I311

1311

3510

3510

3510

6010

6010

6010

6010

6010

6010

6010

7471

7471

EPA 3010

SW-846 8081

SW-846 8081

SW-846 8081

SW-846 8081

S W-846 8081

SW-846 8081

SW-846 8081

LAC

LAC

HWC

S A

S A

MSP

MSP

MSP

MSP

MSP

MSP

MSP

GRR

GRR

GRR

S A

S A

S A

S A

S A

S A

S A

Not detected mg1L 1 .O S W-846 8 1 50 811 3199 10:29 S A

Not detected mq/L 0.10 SW-846 8150 811 3199 10:29 S A

BENZENE Not detected mq/L 5.0 SW846-8260 811 1/99 14:27 MP

CARBON TETRACHLORIDE Not detected mg/L 5.0 SW846-8260 811 1199 14:27 M P

CHLOROBENZENE Not detected mg/L 5.0 SW846-8260 811 1199 14:27 MP

CHLOROFORM Not detected mg/L 5.0 S W 846-8260 811 1199 14:27 MP

1,4-DICHLOROBENZENE Not detected mg/L 7.00 SW846-8260 811 1/99 14:27 MP

1,2-DICHLOROETHANE Not detected mg/L 5.0 SW846-8260 811 1199 14:27 MP

@ 1.1-DICHLOROETHENE Not detected mg/L 5.0 SW846-8260 811 1199 14:27 M P

NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - F L Certification N. E87519

449 Springbrook Road A P.O. Box 240543 r- Charlotte, NC 28224-0543

Phone: 7091529-6364 -Toll Free Number: 1-8001529-6364 A Fax: 7041525-0409

,. Lao neport

James Tan




Full Sewice Analytical 8 Environmental Solutions

Paae 4 of 4

Customer Project ID: 005-044-AS146 Customer Sample ID: AS146-LIQUIQ

Prism S a m ~ l e ID: A838022 Lonin G rou~ : 9394E2

Sample Collection DateKime: 8/5/99 09:45 Lab Submittal DateKime: 8/6/99 10:30


TEST PARAMETER

METHYL ETHYL KETONE

TETRACHLOROETHENE

TRICHLOROETHENE

VINYL CHLORIDE

--------- CRESOLS

1 4-DICHLOROBENZENE

24-DINITROTOLUENE

HEXACHLOROBENZENE

HEXACHLOROBUTADIENE

HEXACHLOROETHANE

NITROBENZENE

PENTACHLOROPHENOL

PYRlDlNE

TEST RESULT

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

METHOD . UNITS MDL REFERENCE

DATEn-l ME STARTED ANALYST -

811 1199 14:27 MP

811 1/99 14:27 M P

811 1199 14:27 M P

811 1199 14:27 MP

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

Sam~le Comments:

TCLP pesticides and herbicides subcontracted to NC certified lab # 387.

ample was raised due to sample matrix. The sample was analyzed as a waste dilution.


NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification N. €87519

449 Springbrook Road A P.O. Box 240543 A Charlotte, NC 28224-0543 Phone: 704,529-6364 -Toil Free Number: 1-8001529-6364 A Fax: 7w525-0409

.. . . . . . .

S PECIALI ZED AS SAYS ENVIRONMENTAL 2960 Foster Creighton Drive Nashville, Tennessee 37204

ANALYTICAL REPORT

Original report and a copy of the chain of custody will follow by mail.

PRISM LABORATORIES 5625 ANGELA OVERCASH P.O. BOX 240543 CHARLOTTE, NC 28224

Lab Number: 99-A119749

Sample ID: AB38021 Date Collected: 8/ 5/99

Project : 9394E Time Collected: 8:30

Pro j ec t Name : Date Received: 8/10/99

Sampler: Time Received: 9:00

State Certification: 387 Sample Type: Solid waste

P?? hesults

Iqatrlx Spike

aal:;te Re sul t Units Beg l imi t fieicver:~ !'%) Dace Time anal:rst Methrd - - - - - - - - - - - m a - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - --------.

shlcrdane c L.l.23 mg.:'l 0.030 63 8,:13..;03 10: 27 H. k.>fers SO&

2.4-D < 1 .#:' my$.'l lc.;: 15 T a!,ij~~oo lo: r? ll.Rosers 31%)

Endrin < 3. ,:,:c.2,: mi-il 2. 32 1s; 8..;13,;33 112: 27 H.Bogerr SC6'.

Heptachlor ~0.0:nX mq/l C . CC& 13: d..,13/99 lo:?! M.Rogers 5O8O

Li ndane cO.tXjliO m.g/l 0.; l r r O dil3:99 10::' N.R;gers 5080

Hegtachlor epo.nde c L ~:;1':8 mgil 82. ,224 135 8.(13/9? LO: 27 M.Rogers 8C83

T'?! Extra; tion Init iated 2:10;,44 16:s:G E. Mabr: 1511

EIC~ - tlot detected at the repJrt l imi t .

surrogate

p s t w r - T ~ G s u r -Pibu~:lshlorMdate

mrr - DCPU

la. 33. - 122. 4 D . 15. - 120.

a?. 20. - 133.

Report Approved By: Report Date: 8/13/99

Theodore J. Duello. Ph-D., Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell. Dir. Technical Services Eric Smith, Assistant Technical Director Gail A Lage, Technical Services

Laboratory Certification Number: 387

SPECIALIZED ASSAYS ENVIRONMENTAL 2960 Fos t e r Creighton Drive Nashvi l le , Tennessee 37204

ANALYTICAL REPORT

Or ig ina l r e p o r t and a copy of t h e c h a i n of custody w i l l fo l low by mi l .

PRISM LABORATORIES 5625 ANGELA OVERCASH P.O. BOX 240543 CHARLOTIE, NC 28224

Lab Number: 99 - A 1 19750

Sample ID: AB38022 Date Collected: 81 5/99

P r o j e c t : 9394E Time Co l l ec t ed : 9:45

P r o j e c t Name: Date Received: 8/10/99

Sampler : Time Received: 9 : 00

S t a t e C e r t i f i c a t i o n : 387 Sample Type: Liquid was te

'hlnrdane

2,4-C.

Endrin

Heptachlcr

Lindane

Mehr,.chlor

T a xaphene

Si lvex Hepcacklcr e p z i d e

Matrix Spike

Xesd t Units P.eg Limi t Rezr;'er:r ( 5 , Gate Time u-I*::~ Meth3 - - - - - - - - - - - - - - - - - - - - - - - _ - - - - - - - - :- _ - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -

hn, - Mot detected a t the r e p r t l i m i t .

H.Xn~ei-s

M.R~gers

M.Rcfers

M.'noqers

r.l.Rogars

M.Rogers

H.Rogers

N. Rogers

Pf .Rogers

Surrogate d i lu ted out due tc smple matrix

Report Approved By: Report Date: 8/13/99

Theodore J. Duel lo . Ph.D. , Lab Di rec to r Michael H . Durn, M.S., Technica l D i r e c t o r Johnny A. M i t c h e l l , Dir. Technical S e r v i c e s E r i c Smith, A s s i s t a n t Technical D i r e c t o r Ga i l A Lage, Technica l Se rv ices

Laboratory C e r t i f i c a t i o n Number: 387

CHAIN OF CU PAGE r' OF ' QU

. . Samples INTACT upon arrival? 1 449 Springbroolr Road A Charlotte, NC 282 17 Received ON WETICE? Tenlp h ...%- +. - . . .

P.0. BOX 240543 A Charlotte, NC 28224-0543 PROPER PRESERVATIVES indicated? . .~--. .. - . .. . - -

Phone: 704/529-6364 A Fax: 704/525-0409. Received WITHIN HOLDING TIMES?

CUSTODY SEALS INTACT?

Full Service Analytical & Environmental Solutions ... .. . .") , ! . . , , . . , - ; ! ; - . , , , , , j ! . . . . l < < , \ : l t + c ,. . Client '...-.I,-

(', . . .. , / , . - "

. , ' , .; ,, # .:. TF ,r; f, , , - 1 ;- .. , '. .. . : . . I ' Physical A?dress - , . - % . - - . --

, ,;,.,',~~,) :. .- , . . . < ' ,. $ ,. - :: . , 2 ! .." . i'' ,'., ,i ; . .,,, : ,, , " * < .,.i > - .? -:; .:; ':; .,, '.' ,[. \ ' < . ,; : .l 7

Phone A- ._.- Fax ' , .: , ::, ..

P.O.#IBilling Reference ;. ' - " . . , .

.... , ..':a. ;.., ! . ,! Project Name

I ,_.d .

.. : ;;? REPORT TO: Name

,>) :.. . >. . > c, Address : ,!; ,

-- BILL TO: Name ,,-' . . --,i. :F : ,. ;"" % - a .:F. . < ; I --

Address , I J., !':

:. . . . . Requested Due Date---.? ' :' 1 - '

(SEE REVERSE SIDE FOR RUSH TURNAROUND FEES)

VOLATILES rec'd WlOUT HEADSPACE? .

--

State Certification /' . .

Requested NC % SC 0ther:NA p~

Water Chlorinated Yes No NA - Sample Iced Upon Collection Yes No -

*CON,~AINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon-Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

PRISM I-AB

ID NO.

: , ,

.: ,

. . . . . . . . . ,

- .-

--

-

--

ANALYSES REPIJESTED I

,." . /; / ' ,' /', . . /, ,/" REMARKS ?

/ .', ,*',!.!./ ,,

/ L,

7

CLIENT SAMPLE DFSCRIPTION

-. ., -..

SC'B ' LAB CERT. ID NO.

DATE COLLECTED

TIME COLLECTED

MILITARY HOURS

- , ; .\I

.-.-- " ' - - . .., ..+ . . . 8 ?,,

Sampler's Signat~~re . ' Sampled By (Print Name) '.' .'" ' -- Atfiliation

Additional Comrnents

- - -- - .. ----- -- . - -- Relinquished By: (Signature) Dale

.,. ,

Relinq~~ished By: (Signal~~re)

Method of Sldprnenl ; ,/ A

NPDES NC UST NC GROUNDWATER: NC DRINKING 'NATER: NC - SOLID WASTE: NC - OTHER: NC SC SC -- SC SC

' SC - SC OTHER OTHER- OTHER - OTHER - OTHER- OTHER -

. . 'i,.i,/,:!t,.. . ~ : ~ ~ ~ / 8 , ! i ~ . , ! ~ J

. . . ! !,! ! ; . ,; , , ; : . e ; ; ,.

,

MATRIX (SOIL,

WATER OR SLUDGE)

, ! ' .s . . ; ' 3

::;:':\ /'?!/'

2j /'j- r:',-: , . .il 'i

[;$*/.' , .

.> ,$, f .. -

I . . . . .,. . j ! . i-: , '. , I , .

, i

-

--

~ - -

/ I"

... I 1 1 - , .

? , :; ! . , ! j <.:

PRESERVA- TIVES

SAMPLE CONTAINER

-. ---

*TYPE SEEBELOW

.- ..

--

-.

SIZE

-

. ' i ,,': t

- --

. . i .; . ),., -, .

;: 1

-

-.

1.;" . .

. - -- .-

.- .. - --

-.

.

-

--

-

[, 1 ,;.i.. ..

~

i .c ,? ' - . ,; ,:

James Tan J.A. Jones Management Service 6135 Park South Dr., Ste 250 Charlotte, NC 28210

Main Office: 449 Springbrook Road

P.O. Box 240543 Charlotte, NC 28224-0543

Phone: 7041529-6364 118001529-6364 REVISED LABORATORY REPORTFax: 704,525-0409

Client Project ID: 005-044-AS146 Client Sample ID: AS 146-Liquid Prism Sample ID: AB38022

Prism Login Group: 9394E2

The attached laboratory report is a revision and supersedes our original laboratory report dated August 5, 1999 .

If you have questions, please call us.

Angela D. Overcash. V.P. Laboratory Services

Prepared by: Peggy Kendall

F:\common\revlab.xls Created 3/16/00 Revised 3/30/00


Page 3 of 5

James Tan


6135 Park South Dr, Ste 250


Customer Project ID: 005-044-AS146 Customer Sample ID: AS146-LIQUID

Prism S a m ~ l e ID: AB38022 Lonin G r o u ~ : 9394E2

Sample Collection DatelTime: 8/5/99 09:45 Lab Submittal DatelTime: 8/6/99 10:30


TEST PARAMETER

TCLP EXTRACTION (VOLATILES ONLY)

TCLP EXTRACTION

PREP. METHOD 3510

PREP. METHOD 3510 WITH EXCHANGE

ARSENIC, LEACHABLE

SELENIUM, LEACHABLE

CADMIUM. LEACHABLE

CHROMIUM, LEACHABLE

LEAD, LEACHABLE

SILVER, LEACHABLE

BARIUM, LEACHABLE

MERCURY, LEACHABLE

MERCURY DIGESTION

CHLORDANE

ENDRIN

HEPTACHLOR

LlNDANE

METHOXYCHLOR

TOXAPHENE

HEPTACHLOR EPOXIDE

TEST RESULT

Completed

Completed

Completed

Completed

Less than

Less than

Less than

Less than

Less than

Less than

Less than

Less than

Completed

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

UNITS REPORTING LIMIT

METHOD DATEnlME REFERENCE STARTED ANALYST

1311 8/9/99 16:15 LAC

1311 8/9/99 16:OO LAC

3510 811 2199 14:30 HWC

3510 811 0199 1 6:OO S A

6010 811 2199 14:OO MSP

601 0 811 2199 14:OO MSP

6010 811 2/99 14:OO MSP

6010 811 2/99 14:OO MSP

601 0 811 2199 14:OO MSP

6010 811 2199 14:OO MSP

6010 811 2/99 14:OO MSP

7471 811 2199 14:OO G RR

Not detected mg/L 1 .O 815011311 811 3199 10:29 S A

Not detected mg/L 0.10 815011311 811 3199 10:29 S A

--------- PREP. METHOD 3510 WITH EXCHANGE Completed 8151 811 0199 16:OO S A

METALS DIGESTION Completed EPA 3010 811 1199 17:OO GRR

BENZENE Not detected mg/L 5.0 SW846-8260 811 1/99 14:27 MP

CARBON TETRACHLORIDE Not detected mg/L 5.0 SW846-8260 811 1/99 14:27 MP

CHLOROBENZENE Not detected mg/L 5.0 SW846-8260 811 1199 14:27 MP

CHLOROFORM Not detected mg/L 5.0 SW846-8264 811 1199 14:27 M P

NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certif~ation IVo. E87519

449 Springbrook Road A P.O. Box 240533 -Charlotte, N C 28224-0543 Phone: 7031529-6364 A Toll Free Number: 1-8001529-6369 A Fax: 7041525-0409

e


5/3/00 Page 4 of 5

James Tan





Prism S a m ~ l e ID: AB38022 Loain Grou~ : 9394E2

Sample Collection Datenime: 8/5/99 09:45 Lab Submittal Datenime: 8/6/99 10:30


TEST PARAMETER

1,4-DICHLOROBENZENE

1,2-DICHLOROETHANE

1,l-DICHLOROETHENE

METHYL ETHYL KETONE

TETRACHLOROETHENE

TRICHLOROETHENE

VINYL CHLORIDE

TEST RESULT

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

UNITS

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

REPORTING LIMIT

7.00

5.0

5.0

20

6.00

5.0

10

METHOD REFERENCE

SW846-8260

SW846-8260

SW846-8260

SW846-8260

SW846-8260

SW846-8260

S W846-8260

DATElTlME STARTED

811 1199 14:27

811 1199 14:27

811 1199 14:27

811 1199 14:27

811 1199 14:27

811 1199 14:27

811 1199 1427

ANALYST

M P

M P

M P

M P

MP

MP

MP

CRESOLS

1.4-DICHLOROBENZENE

2,4-DINITROTOLUENE

HEXACHLOROBENZENE

HEXACHLOROBUTADIENE

HEXACHLOROETHANE

NITROBENZENE

PENTACHLOROPHENOL

PYRlDlNE


2.4,6-TRICHLOROPHENOL

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

811 2199 1532 HWC

811 2199 1532 HWC

811 2199 15:32 HWC

811 2199 1532 HWC

811 2/99 1532 HWC

811 2/99 1532 HWC

811 2199 1532 HWC

811 2/99 1532 HWC

811 2199 1532 HWC

811 2199 1532 HWC

811 2/99 1532 HWC

NC Certification No. 402 - SC Certification No. 9901 2 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519

449 Springbrook Road A P.O. Box 240543 A Charlotte, NC 28224-0543 Phone: 7041529-6364 A Toil Free Number: 1-8001529-6364 A Fax: 7041525-0409

eau m e p u r l -

5/3/00

James Tan

J.A. Jones Management Service -



V A

INC.

Full Sewice Analytical 8 Env~ronmental Solutions

Page 5 of 5


Prism Sam~le ID: A838022 Login Group: 9394E2

Sample Collection Datemime: 8/5/99 09:45 Lab Submittal Datemime: 8/6/99 10:30


TEST TEST REPORTING METHOD DATEKIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST

Sample Comments:

TCLP pesticides and herbicides subcontracted to NC certified lab # 387

Analysis note for 8270: The MDLs for this sample were raised due to sample matrix. The sample was analyzed as a waste dilution.

Analysis note for 8260 : The MDLs for this sample were raised due to the sample matrix, This sample required a 1 : I 000 dilution due to the presence of non-target compounds. This 1 : I 000 dilution gives detection limits of 5.0 mg/L.


NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519

449 Springbrook Road A P.O. Box 240543 A Charlotte, NC 28224-0543 Phone: 7041529-6364 A Toll Free Number: 1-8001529-6364 A Fax: 7041525-0409

UST Closure Report

APPENDIX G

Laboratory Analytical Report for Soil and Groundwater

UST NO. AS-146

J.A. Jones Environmental Services Company Contract NO. N624M-93-D-3033, DO-44

Lab Report

Full Service Analytical B Environmental Solutions

5/23/00 Page 1 of 8

JA Jones Management Services

Mr. James Tan 61 35 Park South Dr, Ste 250


Customer Project ID: POLRAC-D044-AS146 Customer Sample ID: AS-146-1

Prism S a m ~ l e ID: A668912 Lonin Group: A0522F4

Sample Collection Datemime: 511 8/00 08:43 Lab Submittal Datemime: 511 9/00 10:20


TEST TEST REPORTING METHOD DATErrlME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST

METALS DIGESTION METHOD 3050 Completed

PREP. METHOD 3550 Completed


3050 511 9/00 13:OO PRF

3550 511 9/00 20:30 JMK

3550 5120100 S A

CHROMIUM, TOTAL 5.6 mg/kg 1 .O 6010 5120100 19:42 MSP

LEAD, TOTAL

TPH - DIESEL RANGE

TPH-GASOLINE RANGE

CALCULATIONS BASED ON DRY WT.

PREP. METHOD 3550

ALDRlN

A-BHC

B-BHC

D-BHC

G-BHC, LINDANE

CHLORDANE

4,4'-DDD

4,C-DDE

4,C-DDT

DIELDRIN

ENDOSULFAN l

ENDOSULFAN ll

ENDOSULFAN SULFATE

ENDRIN

ENDRIN ALDEHYDE

HEPTACHLOR

HEPTACHLOR EPOXIDE

4,C-METHOXYCHLOR

TOXAPHENE

2.8 mg/kg 1 .O 6010 5120100 19:42 MSP

Less than mg/kg 10 8015MOD13550 5/22/00 09:03 ESR

Less than mg/kg 1 .O 8015MOD15030 5/20/00 14:23 KV

85

Completed

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

0.00466

0.00233

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

% DRY WT. JDP

S A

S A

S A

S A

S A

S A

S A

S A

S A

S A

S A

S A

S A

S A

S A

S A

S A

S A

S A

S A


449 Springbrook Road A P.O. Box 240543 A Charlotte, NC 28224-0543 Phone: 7041529-6364 A Toll Free Number: 1-800/529-6364 A Fax: 7041525-0409

Lab Report

Full Service Analytical 8 Env~ronmental Solut~ons

5/23/00


Mr. James Tan



Page 2 of 8


Prism S a m ~ l e ID: AB68912 Lonin Group: A0522F4

Sample Collection DateKime: 5/18/00 08:43 Lab Submittal DateKime: 5/19/00 10:20


TEST PARAMETER

TEST RESULT

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

REPORTING UNITS LIMIT

METHOD REFERENCE

DATEnIME STARTED ANALYST

Sample Comments:

ted to NC certified lab # 387.



449 Springbrook Road A P.O. Box 240543 A Charlotte, NC 28224-0543 Phone: 7041529-6364 A Toll Free Number: 1-8001529-6364 A Fax: 7041525-0409

Lab Report i

kk LABORATORIES. I N C


5/23/00


Mr. James Tan



Page 3 of 8


Prism Sam~le ID: A668913 Loain Group: A0522F4

Sample Collection DatelTime: 511 8/00 09:30 Lab Submittal DatelTime: 5/19/00 10:20


TEST TEST REPORTING METHOD DATEKIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST



3050 511 9/00 13:OO PRF

3550 511 9/00 20:30 JMK

PREP. METHOD 3550 Completed 3550 5/20/00 S A

CHROMIUM, TOTAL 24 mglkg 1 .O 6010 5/20/00 19:51 MSP

LEAD, TOTAL 16 mglkg 1 .O 6010 5/20/00 19:51 MSP

TPH - DIESEL RANGE 36 mglkg 10 801 5MODI3550 5/22/00 09:51 ESR

TPH-GASOLINE RANGE 30 mglkg 10 8015MOD/5030 5/22/00 10:21 KV

CALCULATIONS BASED ON DRY WT. 61 % DRY WT. 0.01 SM 2540 G 5/19/00 13:OO JDP

PREP. METHOD 3550 Completed SW846-3550 5/20/00 S A

ALDRIN

A-BHC

B-BHC

D-BHC

G-BHC, LINDANE

CHLORDANE

4,4'-DDD

4,4'-DDE

4,4'-DDT

DIELDRIN

ENDOSULFAN l

ENDOSULFAN ll

ENDOSULFAN SULFATE

ENDRIN

ENDRIN ALDEHYDE

HEPTACHLOR

HEPTACHLOR EPOXIDE

4,4'-METHOXYCHLOR

TOXAPHENE

Not detected mg/kg 0.001 66 SW846-8081 5/21/00 07:30 S A

Not detected rnglkg 0.00166 SW846-8081 5/21/00 07:30 S A

Not detected rnglkg 0.001 66 SW846-8081 5/21/00 07:30 S A

Not detected mglkg 0.001 66 SW846-8081 5/21/00 07:30 S A

Not detected rnglkg 0.00166 SW846-8081 5/21/0007:30 S A


Not detected mg/kg 0.00333 SW846-8081 5/21/00 07:30 S A













---------- PCB-1016 Not detected rnglkg 0.02 SW846-8082 5/22/00 17:33 S A


149 Springbrook Road A P.O. Box 240543 A Charlotte, NC 28224-0543 Phone: 7041529-6364 A Toll Free Number: 1-800/529-6364 A Fax: 704/525-0409

-- -

Lab Report

Full Service Analytical 8 Environmental Solulions

Page 4 of 8


Mr. James Tan

6135 Park South Dr, Ste 250 Charlotte, NC 2821 0


Prism S a m ~ l e ID: AB68913 Lonin Grou~: A0522F4

Sample Collection Datemime: 511 8/00 09:30 Lab Submittal Datemime: 511 9/00 10:20


TEST TEST REPORTING METHOD DATErTlME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST




Not detected mglkg 0.02 SW846-8082 5/22/00 17:33 S A



Sample Comments:

Methods 8081 and 8082 subcontracted to NC certified lab # 387.


449 Springbrook Road A P.O. Box 240543 A Charlotte, NC 28224-0543

Phone: 70415294364 A Toll Free Number: 1-800/529-6364 A Fax: 7041525-0409 . - - - - -- -- - --- -

Lab Report

JA Jones Management Services Mr. James Tan 6135 Park South Dr, Ste 250 Charlotte, NC 28210


Page 5 of 8


Prism S a m ~ l e ID: AB68914 Loain Group: A0522F4

Sample Collection DateKime: 5118100 10:02 Lab Submittal DateKime: 511 9100 10:20



METALS DIGESTION METHOD 3050 Completed 3050 511 9/00 13:OO PRF

PREP. METHOD 3550 Completed 3550 511 9/00 20:30 JMK

PREP. METHOD 3550

CHROMIUM. TOTAL

LEAD, TOTAL

TPH - DIESEL RANGE

TPH-GASOLINE RANGE

Completed 3550 5/20/00 S A

5.3 mg/kg 1 .O 6010 5/20/00 19:27 MSP

1.2 mg/kg 1 .O 6010 5/20/00 1927 MSP

Less than mg/kg 10 801 5MODl3550 5/21/00 04:46 ESR

Less than mg/kg 1 .O 8015MOD/5030 5/20/00 15:35 KV

CALCULATIONS BASED ON DRY WT. 88 % DRY WT. 0.01 SM 2540 G 511 9/00 13:OO JDP

0 PREP. METHOD 3550

ALDRIN

A-BHC

B-BHC

D-BHC

G-BHC. LINDANE

CHLORDANE

4,4'-DDD

4,4'-DDE

4,4'-DDT

DIELDRIN

ENDOSULFAN I

ENDOSULFAN ll

ENDOSULFAN SULFATE

ENDRIN

ENDRIN ALDEHYDE

HEPTACHLOR

HEPTACHLOR EPOXIDE

4,4'-METHOXYCHLOR

TOXAPHENE

Completed

Not detected mglkg

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected


449 Springbrook Road A P.O. Box 240543 A Charlotte, NC 28224-0543 Phone: 7041529-6364 -Toll Free Number: 1-8001529-6364 A Fax: 704f525-0409

Lab Report

Full Serv~ce Analytical 8 Environmental Solutions


Mr. James Tan



Page 6 of 8

Customer Project ID: P O L R A C - D O ~ ~ - A S I ~ ~ Customer Sample ID: AS-146-3

Prism Sample ID: AB68914 Login Group: A0522F4

Sample Collection DateRime: 511 8/00 10:02 Lab Submittal DateRime: 511 9/00 10:20


TEST TEST REPORTING METHOD DATEnlME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST




Not detected mg/kg 0.02 SW846-8082 5/22/00 17:55 SA




NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. EB7519

149 Springbrook Road A P.O. Box 240543 A Charlotte, NC 28224-0543 Phone: 7041529-6364 A Toll Free Number: 1-800/529-6364 A Fax: 7041525-0409

- -

Lab Report


5/23/00


Mr. James Tan

61 35 Park South Dr, Ste 250 Charlotte. NC 2821 0

Page 7 of 8



Sample Collection Datemime: 5/18/00 10:40 Lab Submittal Datemime: 511 9/00 10:20





3050 511 9/00 13:OO PRF

3550 5/19/00 20:30 JMK

PREP. METHOD 3550 Completed 3550 5/20/00 J MV

CHROMIUM, TOTAL

LEAD, TOTAL

TPH - DIESEL RANGE

TPH-GASOLINE RANGE

PREP. METHOD 3550 - ALDRIN

A-BHC

8-BHC

D-BHC

G-BHC. LINDANE

CHLORDANE

4,4'-DDD

4,4'-DDE

4,4'-DDT

DIELDRIN

ENDOSULFAN l

ENDOSULFAN ll

ENDOSULFAN SULFATE

ENDRIN

ENDRIN ALDEHYDE

HEPTACHLOR

HEPTACHLOR EPOXIDE

4,C-METHOXYCHLOR

TOXAPHENE

9.5 W/kg 1 .O 6010 5/20/00 19:46 MSP

Less than mg/kg 1 .O 6010 5/20/00 19:46 MSP

Less than

15

89

Completed

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

mg/kg

mg/kg % DRY WT.

ESR

KV

JDP

S A

S A

S A

S A

S A

S A

S A

S A

S A

S A

S A

S A

S A

S A

S A

S A

S A

S A

S A

S A


449 Springbrook Road A P.O. Box 240543 A Charlotte, NC 28224-0543 Phone: 704/529-6364 A Toll Free Number: 1-8001529-6364 A Fax: 7041525-0409

Lab Report LABORATORIES, INC.

Full Service Analyllcal 8 Environmental Solutions

5/23/00


Mr. James Tan


Charlotte, NC 28210

Page 8 of 8


Prism S a m ~ l e ID: A66891 5 Login Group: A0522F4

Sample Collection Datenime: 511 8/00 10:40 Lab Submittal Datenime: 511 9/00 10:20


TEST TEST REPORTING METHOD DATE/TlME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST







Sample Comments:

Methods 8081 and 8082 subcontracted to NC certified lab # 387.


NC Certificati~n No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519

449 Springbrook Road A P.O. Box 240543 A Charlotte, NC 28224-0543 Phone: 7041529-6364 -Toll Free Number: 1-8001529-6364 A Fax: 7041525-0409

-

SPECIALIZED ASSAYS, INC.

2980 Faeter Creightm Dr. P.O. Box 40566

A N A L V T I C A L REPORT Nashville. M 372044586

Phone 1-81 57260177

PRISM LABURATl3RIES 5623 W E # 0 v E R c m P. 0. BOX 24Q343 GHARLOTTEt Nf a8224

Project: AD322F4 P r o j e c t Name; A 0 32ZF4 ssmp 1 er:

Lab Numb er : 00 -A69776 S a m p l ~ ID: AB be912 Sample Type: . JaL1 Site 10:

D a t e Co l l ec ted: 31 18/00 T i m e Collected: 8: 43 Date Aecclved: 3120/00 Tlme Received: 7: W

COW 1


2960 Foster Crelghton Dr. P.O. Box 40566

Nashville, TN 37204-0566 Phone 1-81 5-726-0177

Labormtory Number: 00-A69776 S a m p l e 1D; AB MHIZ

-I__----- -- - --- Snpk Lirtrutla Data

Iltm1 P a ~ w e t Extrwtel Extrxt W Bate Ilaalpt lktW

----- - C I I_.# ---- 7-

ss. 9b. 94. M-

These results r e l a t e only to the items t e s t e d . this report shall not be reproduced mxcept i n Pull and mith poraission oP the loboratory.

Report Approved Bq: Report Date: 3/22/00

Theodore J. Duel lo, Ph. 0. , Technica l Serv. Paul E. Jr. Lab Director nirhael H. Durn, n. S. , Technical Director Glenn L. Nortonl Technical Serv. Johnay A. l l l t t h e l l l D i p . Technical Serv. Kelly S. Ruppe3~ Technica l Serv. E r i c S. Salth, i ) s s i s t a n t Technica l Director Pcaslo h. Ldagfordl Technica l Serv. G a i l 6 Lager Techaical Serv.

Labaratorq Cer t i f i c a t i a n WabQr : 387

all o f Sanple Report.


2960 Fostw Crsighton Dr. P.O. Box 40588

Nashville, TN 372044566 Phtme 14157264177

PRISM LABDRATORIES 5633 ANGELA OVERCASH P. D. BOX 240343 CHARLOTTE, NC -24

Project: P r o j e c t Name; Ai3 32ZF4 Sarnp ler :

ANALYT X C A L m E P O R T

Lab Number; 00-A69777 Sample ID: AB 68913 Sample Type: 3 ~ 1 1 3 1 t e ID:

Date Co l l ec ted: 3118t00 Tirae Collected: 9: 30 Ddte Received: 3/20IOQ Tlme Recelved: ?:00

7:3l 11. ClotLcr W 7:s K c l t r t ra 7: R ll. SrrtIrr WM 7:#)/A Cnttkr dBs[UI 7:% n. c&r 7:#1 II. C & k r lwla 1:s A. Cmhr 8wln 7: 36 L C#tb8 UWU 7:s s. CmIthR 7: n n. rroerr ?:a n. Crvtkr 7:s A. CPrR lm W 7:30 n. cwwo ?:38 R. Crrtkr 8WM 7 : n. Cautkfi ami 7:30 It. Clotbr 9WU 7:s n. c w c r a arru 7:a IL C W ~ ~ U t:38 ?I. E&hr Wtlll t : ~ n. C U ~ P mm I:R n. CaaUea mu

17: 33 R. lbrt 8Pa iT:n R. I k8 t aar 1T:f 8 . W sogz I?: 33 O. Rmt W a 1?33 -Elk* mu 1T:n rrrrurt m 17: 33 R. Hurt

COPY 1


2960 Foster Cre-*ion Of. P.0. Box 40568

Nashville. TN 37204.4568 A N A L Y T I C A L REPORT Phone 16157280177

~ a b o r a t i v Numb or: 00-4369777 Gample ID: AB 6891 3

Page 2

---- --------I-------- -- -I__

Surpb Cxtrxtiaa Data

Bt kst 3abg SO.OIrl -3nWOO !.Ro)rr 3SN R a . 5 30.1p 1B.Bl i l Y21V(R B Y 33s

These results re la te o a l y t o the item5 tsrted. This report s h a l l not be reproduced except i n foil and ~ i t h permir%to~ of the Idbordtory.

Report hpproved By: Report Date; 5/22/00

Theodore J. Duel101 FII.D. , Technical seiv. fdul E. Lane, Jr. ~ a b Director n i c h d e i H. DURII R. S. T e ~ h ~ i c d l OirectOr Glenn L. Norton, fechnteal Srru. Johnny R. nttchell, D i r . Technical Strv. Kelly Fi. Ruppel~ Technical Serv. Eric S. Saitha Assistant Technical Oirector Pameld 8. L a n g f a r d ~ Technicdl Sew. 6 n i l CI Laqe, Technical Serv.

Laboratoty CertiPication Humbar: 387


2980 Foster Creighton Or. P.O. Box 40566

Nashvllle. TN 372040566 Phone 1-615726-0177

PRISM LABORATORIES 3623 W E L A WERCASH P. O. BOX 240343 CHARLUTTE, NC 18,234

Project: Pro jec t Name: AD 322F4 Samp l e r :

A N A L Y T I C A L REPORT

Lab Number: 00-A69798 Samp.1.e ID: AB 68914 ~ s m p l e Type: t io i l B i t e ID:

~ a i e Col l ~ c t e d : 3/18/00 Time Collected: 10: 02 Date Received: 3/ZO/OO T ime Received: ?:OO


2960 Fobter Creighlon Dr. P.O. Box 40568

Nashville, TN 372060566 Phone 1-81 5-7SO177

Labor. t o r y Numbar: O O - A C I V I ~ Sample ID: AB -914

------- ---- ---c-.----- -- Satjle Extr3ctlon Data

These results r e l e t e only t o the itms tested. This raport s h a l l not be reproduced except i n W l l md rith pernission af the labbratcry.

Report Approved By: Rspar t Date : W22f 00

Theodore J. Duello, Ph. D. I Technical Serv. Peul E. Lane, Jr. r Lab DlrectOr nicheel H. DIIBR, H. S. Technical ~ i r e c t o r Olenlr L. Wortonl Technics3 Serv. J&hn~y A. ni tcho l l , DIP. Technical Sorv. Kelly 6. Ruppel, t e c h n i c a l Serv. E r i c 6. Smithr A5sistant Technical Director Pamela R. L a n g f o r d ~ T ochnlcal Serv. G a i l b lager Technical Serv.

Labaratory tertitlcatlon W e r : 387

COPY 1


2900 Foster CraLghton Dr. P.O. Box 40566

Nashville. TN 372040568 Phone 1-61 5-726.0177

PRISM LABORATDRIES 3623 ANGELA OVERCASH P. 0. BOX 240343 CMRLOTTE, NC 28.224

ANALYT ICAL REPORT

Lab Number: 00-A67779 Sample ID: A 8 68913 sample s y p e : so31 S i t e ID:

Date . Corrected: 3/16/00 Project: T 1ne Collected: 10: 40 Project Name: ClD 322F4 'Date Racaived: 3/ZO/OQ S a m p l e r : Time Rece ived : ?: 00

-

aprt RM Dl1 AIa.I$? Wt Ilmlts Llalt LRlt Factor Date T lsr 8 ~ 9 g s t k t k 4 sttoll -----..-- .. .------ -- -C_ _U -- -- ----- __LI -

~2ilff) 0:s n. S&LI mu SRUOB 8:n (I. CrrUsr WJld SLWW 8:Zt R. CuUoc a O l M ynm rr:n n. c#tm cwrr M1/00 8:29 It Cwth~ JMme 8:n CwtMt ytlmr) 8 : s . t-r Bens P ~/lypg en n, cwnm r o a ~ ~mma o:n n. c u t m mu ytyge a : a n. c a m r a m YZVBO 6129 R. tiertler a@8U -m s:n n. CXWI ma 3121100 a:n n. cwm mm -am a:n n. C M ~ B mm j n ~ ~ 8:n (I, curttea a m m m R29 s Ratbe3 m a YZVOO a n R. cwh ma 3/21(09 t29 If. Cwtlrr 8fNU a m an a Cautkn S t 2 u W 8:29 I. C a t b e lillU smm u:n n. t&lp~ m a Smm U:LO R . W am 'JmtW !El8 j l5. M,rt Jmna zs.l$J R. llrrt a82

R . I k D t 'a100 18rU J. mat lUH2 smm UI:21) t.mt ow2 K22/DO 18:16 P. (bra so81

COPY 1


2980 Foster Creighton Dr. P.O. Box 40586

Nashville, TN 372040566 A N A L Y T X C A L REPOCIT Phone 1-615-726.0177

Cab or at or y Number : 00-M9?79 Sample ID: A 0 68913

P a g e 2

. - - -- Smjle Entrattlor Data

(IC: hrt 30.6 pl u.e n~ ~20m0 b . v c r j ~ )SCD

m'r 2 F . 8 ~ Ib.Ud J/dDrrm B.Veye , 355U

plLt ~ 1 C m t p b u n r T r n (mi : ,*?PS~

Fb - These results relate only t o t h e items t e s t e d . This report she13 not be reprvavccd r ~ c u p t In full and with permission o f the l aboratorg.

Repart &p~?oved Bq : Report Date: S/22/00

Theodore J. duel lo^ Ph. D. , Technical ~ i r v . Paul E. Lane, Jr., Lab Director Michael H. b a n , H. S. r Technical Direr-tor Glens L. Hortonr Technical Serv. M a n y A. nitchell , D l r . Technical Serv. Kelly s. R u p p ~ l , Tecnr lca l Sew. Eric 6. Smith, Assistant Technical OirmcZor Pa#la A. LangMrd, Technica l Serv. G a i l 6 Lager Technical Serv.

Laboratory Cert i f icrtfon W b a r : 387

! I SPECIALIZED

ASSAYS, INC. 2960 Fodor Creighton Dr.

P.O. Box 40586 Nashville. TN 372044568

Phone 1815-M6-0177

PR03ECT Q U A L I T Y CONTROL DATA

Irrlpx ------- a)rjo EmR WPK tQM:

gJRt, Llrtaw 4,Y -DOD 4,V-m 4 , m r V l d 8 1 L EnlbMfma 1 Etlasulfrr 11 C&?iulfan sulfate t 1 6 1 4

trUlr rl&w E u t l r K f i e p o

HoptlaLla Rqtrllw mi k *tbaycUar aq l r tuaww

Twpt Ruy Q. C. Batch Smpt Silkel --- -- 33. - I s . m ~ 7 7 7 6 33. - 136. m at= B. - 1PI. . 497 a M m 7 6 a. - le. 4n -9776 35. -W. 49; -7776 0. - 1%. at W-Mms If. - 1Q. -9776

Tafjet Ra~p ---- 33 - l23 3 - M 66 - 123 53 - ll? a - m 56 - 131 w - m $5-ZtJ # - m zi - In 38 - 13l 69 - rn & - 144 45 - 1211 53-m P - W 49 - 193 39-Ub 51- ItP a! - 1-

2960 Foster Greighton Dr. , .

P.O. Box 40566 Nashville. TN 37204-6566

Phone 1-61 5726.01 77

PROJECT O U A L X T Y CONTROL DATA

CHAIN OF C U ~ D Y RECORD PAGELOF I QUO= t Samples INTACT upon arrival?

;f - 449 Springbrook Road A Charlotte. NC 282 17 Received ON WET ICE? Temp --- ,./

P.O. Box 240543 A Charlotte, NC 28224-0543 Phone: 7041529-6364 A Fax: 7041525-0409

F~JII Service Analytical R Environmental Solutions

. . ' I ,,

,i ! -; :' , . . ,.. <v.'>

' I / * V ? ~ . . . ;:.. 3 , ,;3!.I+r:.,:~:/..! f Client

PROPER PRESERVATIVES indicated? - A ,-' I.' _ Received WITHIN HOLDING TIMES?

C --- 4

CUSTODY SEALS INTACT? J' --- .-, VOLATILES rec'd WIOUT HEADSPACE? - 2''

PROPER CONTAlNERSused? lp- ' / .-; ,.;. ,..

REPORT TO: Naine ...! . a .., . '.. .~i +.I; i ,"> ,? /$, State Certification

Address '"

- ...* \: 1 ,4 , , i,:..cr; ? f : i ' , < ~ s t , '; , ..- 7 . . ' ,," ,;. , r . ' BILL TO: Name ':., ; - . '" ' ' ~ e ~ u e s t e d NC - SC - O t h e r NA -

! . j :, <; ;; ":;? .;,> Fax > , . !, ,; .; ' : ,:. (?' Phone <'.,,$ > >, :,a Address ,,,,': w ! Water Chlorinated Yes - No NA -

P.O.IIBilling Reference , ,., (f. &, .;: :,;;< <:., ( ,,,,.~#>! Requested Due Date -, . - I Sample Iced Upon Collection Y e s NO -

; , . ! . - : : . ; . ,,'< .;; I . ! 4 . Project Name (SEE REVERSE SIDE FOR RUSH TURNAROUND FEES)

r

CLIENT SAMPLE DESCRIPTION

C'. .,; ( . : . , ; d ' . ,- , 'CL

,'; < . ;. :.g , .;- , . ,

' i I,' ..> . ' . . ( ! . ~ , ..

I ; ;, . . , j . :.: ; ', ' ' ,

DATE COLLECTED

? i

!> ; :,$,/';!, (: I' r

- ,

- - ., ,. ,., *..:,..:, ,.."*. L ..... . . ,,. .. , ;.,,:. -. ., 8 7 , . .-?,:,,,,:

, . Sampler's Signature 7_. Sampled By (Print Name) "'.J 'f '" E ' . Affiliation L. ... ...

TIME COLLECTED

MILITARY HOURS

(.: g ;,<. 2 '.. : ... . . < * '"1

i , { .i(:,

$ : ' i. ;),

; ' c <. , ,. . . i <

--

.. .,--, ' -- a'

Additional Comments

MATRIX' (SOIL,

WATER OR SLUDGE)

.-.>

.I*

I

L .

Relinquished By: (Signature) - -;<d,''';7 a ,,,.::" ,.*. ; ,;:z:- . . .;,,, ", " ' ' .,."

Relinquished By: (Signature)-'

Relinquished By: (Signature)

PRISM LAB

ID NO.

, . c.",. . .;.

7 , . :

# , ..I , . )

! , : ; J , l . : .

, , . . . . . . . ,:

-

Method or Shipment

Date

Date

Date c; . j . , 3,. .- ,

Received By: (Signature)

Received By: (Signature)

R.ecei ed For Prism Labo!atoQes By: , ! Y , , .,. i ,.A : ,,<~i. &: n .... .....",~..,{ &.-.

SAMPLE CONTAINER

Log-In Group No. ;!:: ?,; :,-.. , j , r,:. l.1 i p.t : : A

M i f i t a v / ~ z

i ;:ij;.$

t

q y p ~ SEE BELOW

NPDES NC - - UST: NC GROUNDWATER: NC DRINKING WATER: NC SOLlD WASTE: NC OTHER: NC SC SC SC SC SC - SC

OTHER - OTHER- OTHER -- OTHER OTHER- OTHER -

'CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon-Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

CERT ID NO.

PRESERVA- TIVES

'+*; ,,,:;., :

-

"..1 < -...

* ~ -

. .

'IZE

.:I . ,. . : ~2:

, ? I r

. .

~

, ,,, ... .." ) ,. . REMARKS

; 5 , ' , : . , . , .. , . ....:, ,.r,, .!:, $,.!.. ,':

,,A

$,.,'

! -

j

-

\

i ...<" : /

Lab Report


6/6/00


Mr. James Tan 6135 Park South Dr, Ste 250


Page 1 of 10

Customer Project ID: AS1 46 Customer Sample ID: AS146 STOCKPIL

Prism S a m ~ l e ID: AB69730 Loain Grou~ : A062F3

Sample Collection DateKime: 5/25/00 15:lO Lab Submittal DateKime: 5/26/00 10:OO


TEST TEST REPORTING METHOD DATEfTIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST

METALS DIGESTION METHOD 3050 Completed 3050 5/31 100 09:45 PRF

PREP. METHOD 3550

PREP. METHOD 3550

LEAD, TOTAL

CHROMIUM, TOTAL

TPH - DIESEL RANGE

Completed 3550 5/30/00 08:OO JDP

Completed 3550 5/31/00 10:30 J MV

3.3 mg/kg 1 .O 6010 513 1 I00 2 1 :02 MSP

3.3 mg/kg 1 .O 6010 513 1 I00 2 1 :02 MSP

28 ' mg/kg 10 8015MOD13550 5/31/00 18:38 ESR

TPH-GASOLINE RANGE 110 mg/kg 100 8015MOD15030 5130100 18:02 KV

CALCULATIONS BASED ON DRY WT

PREP. METHOD 3550

ALDRIN

A-BHC

B-BHC

D-BHC

G-BHC. LINDANE

CHLORDANE

4,4'-DDD

4,4'-DDE

4,4'-DDT

DIELDRIN

ENDOSULFAN l

ENDOSULFAN ll

ENDOSULFAN SULFATE

ENDRIN

ENDRIN ALDEHYDE

HEPTACHLOR

HEPTACHLOR EPOXIDE

4,4'-METHOXYCHLOR

TOXAPHENE

86

Completed

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

0.0068

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

% DRY WT. 0.01 J MV

J MV

CWA

CWA

CWA

CWA

CWA

CWA

CWA

CWA

CWA

CWA

CWA

CWA

CWA

CWA

CWA

CWA

CWA

CWA

CWA

Not detected mg/kg 0.05 SW846-8082 6/1/00 09:38 CWA



Phone: 7041529-6364 A Toll Free Number: 1-8001529-6364 A Fax: 7041525-0409 - - - -- -- -

Lab Report

6/6/00


Mr. James Tan



f \ &,ISM = LABORATORIES, INC.

1 **I- Full Service Analytical 8 Environmental Solutions

Page 2 of 10

Customer Project ID: AS146 Customer Sample ID: AS146 STOCKPIL

Prism Sample ID: AB69730 Login Group: A062F3

Sample Collection DatelTime: 5/25/00 15:lO Lab Submittal DatelTime: 5/26/00 10:OO


TEST TEST REPORTING METHOD DATEfllME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

CWA

CWA

CWA

CWA

CWA

CWA

CWA

CWA

----------

Sam~le Comments: -

Angel


419 Springbrook Road r P.O. Box 240543 -Charlotte, NC 28224-0543 Phone: 704/529-6364 A Toll Free Number: 1-800/529-6364 A Fax: 7041525-0409

Lab Report A , LABORATORIES. INC.


6/6/00


Mr. James Tan


Charlotte, NC 28210

Page 3 of 10

Customer Project ID: AS146 Customer Sample ID: AS146 MID

Prism S a m ~ l e ID: AB69731 Login Group: A062F3

Sample Collection Datenime: 5/25/00 15:20 Lab Submittal Datenime: 5/26/00 10:OO



METALS DIGESTION METHOD 3050 Completed 3050 5/31/00 09:45 PRF

PREP. METHOD 3550 Completed 3550 5/30/00 08:OO JDP

PREP. METHOD 3550

LEAD. TOTAL

CHROMIUM, TOTAL

TPH - DIESEL RANGE

TPH-GASOLINE RANGE

CALCULATIONS BASED ON DRY WT.

PREP. METHOD 3550

ALDRIN

A-BHC

B-BHC

D-BHC

G-BHC, LINDANE

CHLORDANE

4,4'-DDD

4.4'-DDE

4.4'-DDT

DIELDRIN

ENDOSULFAN l

ENDOSULFAN ll

ENDOSULFAN SULFATE

ENDRIN

ENDRIN ALDEHYDE

HEPTACHLOR

HEPTACHLOR EPOXIDE

4,4'-METHOXYCHLOR

TOXAPHENE

Completed 3550 5/31/00 10:30 JMV

3.4 mg/kg 1 .O 6010 5/31/00 21:07 MSP

2.6 mg/kg 1 .O 6010 513 1 100 2 1 :07 MSP

170 mg/kg 10 8015MODl3550 5/31/00 19:14 ESR

200 rng/kg 100 801 5MODl5030 5/30/00 18:37 KV

85

Completed

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

0.0057

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

O h DRY WT JMV

JMV

CWA

CWA

CWA

CWA

CWA

CWA

CWA

CWA

CWA

CWA

CWA

CWA

CWA

CWA

CWA

CWA

CWA

CWA

CWA

Not detected mg/kg 0.05 SW846-8082 6/1/00 10:22 CWA

N C Certification No. 402 - S C Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. €87519


Phone: 7041529-6364 A Toll Free Number: 1-8001529-6364 A Fax: 7041525-0409 - . . -

Lab Report

6/6/00


Mr. James Tan



PRISM-; LABORATORIES, INC.

*,'


Page 4 of 10

Customer Project ID: AS146 Customer Sample ID: AS146 MID

Prism S a m ~ l e ID: A669731 Lonin Group: A062F3

Sample Collection Datenirne: 5/25/00 1520 Lab Submittal Datenirne: 5/26/00 10:OO



Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

611 100 10:22 CWA

611 100 1 0:22 CWA

6/1/00 10:22 CWA

6/1/00 10:22 CWA

6/1/00 10:22 CWA

6/1/00 10:22 CWA

6/1/00 10:22 CWA

6/1/00 10:22 CWA

Sample Comments:




Phone: 7041529-6364 A Toll Free Number: 1-8001529-6364 A Fax: 704/525-0409

Lab Report PRISM -- LABORATORIES, INC.

6/6/00


Mr. James Tan


Charlotte, NC 28210


Page 5 of 10

Customer Project ID: AS146 Customer Sample ID: AS146 WATER

Prism S a m ~ l e ID: AB69732 L o ~ i n Group: A062F3

Sample Collection Datenime: 5/25/00 1530 Lab Submittal Datenime: 5/26/00 10:OO


TEST TEST REPORTING METHOD DATERIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST

METALS DIGESTION13030C

LEAD, TOTAL IN GROUNDWATER

CHROMIUM. TOTAL IN GROUNDWATER

DICHLORODIFLUOROMETHANE

CHLOROMETHANE

VINYL CHLORIDE

BROMOMETHANE

CHLOROETHANE

TRICHLOROFLUOROMETHANE

1,l-DICHLOROETHENE

METHYLENE CHLORIDE

trans-l,2-DICHLOROETHENE

1,l-DICHLOROETHANE

2,2-DICHLOROPROPANE

cis-l,2-DICHLOROETHENE

CHLOROFORM

BROMOCHLOROMETHANE

1,1,1-TRICHLOROETHANE

1,l-DICHLOROPROPENE

CARBON TETRACHLORIDE

BENZENE

1,2-DICHLOROETHANE

TRICHLOROETHENE

1,2-DICHLOROPROPANE

BROMODICHLOROMETHANE

DIBROMOMETHANE

TOLUENE

1,1,2-TRICHLOROETHANE

TETRACHLOROETHENE

1.3-DICHLOROPROPANE

Completed

0.018

0.34

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

1.5

Not detected

Not detected

Not detected

Not detected

Not detected

8.0

Not detected

Not detected

Not detected

PRF

MSP

MSP

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

C MB

NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certif~ation No. E87519

449 Springbrook Road A P.O. Box 240543 -Charlotte, NC 28224-0543 Phone: 7041529-6364 A Toll Free Number: 1-800/529-6364 A Fax: 7041525-0409

Lab Report PRISM. I

LABORATORIES, INC.


Mr. James Tan


Charlotte, NC 28210

Full Serv~ce Analytical 8 Environmental Solut~ons

Page 6 of 10


Prism S a m ~ l e ID: AB69732 Loain Group: A062F3

Sample Collection DatelTime: 5/25/00 15:30 Lab Submittal DatelTime: 5/26/00 10:OO



DIBROMOCHLOROMETHANE

1,2-DIBROMOETHANE (EDB)

CHLOROBENZENE

ETHYLBENZENE

1,1,1.2-TETRACHLOROETHANE

TOTAL XYLENES

STYRENE

ISOPROPYLBENZENE

BROMOFORM

1 , l ,2,2-TETRACHLOROETHANE

BROMOBENZENE

1,3,5-TRIMETHYLBENZENE

2-CHLOROTOLUENE

4-CHLOROTOLUENE

tert-BUTYLBENZENE

1,2,4-TRIMETHYLBENZENE

sec-BUTYLBENZENE

p-ISOPROPYLTOLUENE

1 ,3-DICHLOROBENZENE

1,4-DICHLOROBENZENE

n-BUTYLBENZENE

1.2-DICHLOROBENZENE

1.2-DIBROMO-3-CHLOROPROPANE

1,2,4-TRICHLOROBENZENE

HEXACHLOROBUTADIENE

NAPHTHALENE

Not detected ug/L

Not detected ug/L

Not detected ug/L

7.8 ug/L

Not detected ug/L

29 ug/L

Not detected ug/L

3.4 ug/L

Not detected ug/L

Not detected ug/L

Not detected ug/L

8.7 ug/L

Not detected

14

Not detected

Not detected

Not detected

47

8.2

5.8

Not detected

Not detected

46

Not detected

Not detected

Not detected

Not detected

56

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

CMB

1,2,3-TRICHLOROBENZENE Not detected ug/L 0.5 6230D 5/30/00 18:03 CMB

CIS-1 ,3-DICHLOROPROPENE Not detected ug/L 0.5 6230D 5/30/00 18:03 CMB

NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - F L Certification No. E87519


Phone: 7041529-6364 A Toll Free Number: 1-8001529-6364 A Fax: 7041525-0409

Lab Report

Full Service Analytical B Environmental Solutions

Page 7 of 10


Mr. James Tan


Charlotte, NC 28210


Prism S a m ~ l e ID: A869732 Loain Group: A062F3

Sample Collection Datemime: 5/25/00 15:30 Lab Submittal Datemime: 5/26/00 10:OO



TRANS-1,3-DICHLOROPROPENE Not detected ug/L 0.5 6230D 5/30/00 18:03 CMB

MTBE Not detected ug/L 0.5 6230D 5/30/00 18:03 CMB

IPE Not detected ug/L 0.5 6230D 5/30/00 18:03 CMB

---------- PREP. METHOD 625

ACENAPHTHENE

ACENAPHTHY LENE

ANTHRACENE

BENZO(K)FLUORANTHENE

BENZO(A)PYRENE

BENZO(GH1)PERYLENE

BlS(2-CHLOROETH0XY)METHANE

BlS(2-CHLOROETHY L)ETHER

BlS(2-CHLOROlSOPR0PYL)ETHER

BIS(2-ETHY LHEXYL)PHTHALATE

4-BROMOPHENYL PHENYL ETHER

BUTYL BENZY L PHTHALATE

4-CHLORO-3-METHY LPHENOL

2-CHLORONAPHTHALENE

2-CHLOROPHENOL

4-CHLOROPHENYL PHENYL ETHER

CHRYSENE

DlBENZO(A,H)ANTHRACENE

Dl-N-BUTYLPHTHALATE

1,2-DICHLOROBENZENE

1 ,3-DICHLOROBENZENE

1 -4-DICHLOROBENZENE

Completed

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

Not detected

625 5/30/00 13:OO GRR

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC


449 Springbrook Road A P.O. Box 240543 A Charlotte, NC 28224-0543 Phone: 7041529-6364 toll Free Number: 1-8001529-6364 A Fax: M4/525-0409

Lab Report



Mr. James Tan



Page 8 of 10


Prism Sarnf.de ID: A869732 L o ~ i n Group: A062F3

Sample Collection DatelTime: 5/25/00 15:30 Lab Submittal DatelTime: 5/26/00 10:OO


TEST TEST REPORTING METHOD DATEfflME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST

DIETHYL PHTHALATE

2,4-DIMETHYLPHENOL

DIMETHYL PHTHALATE

2,4-DINITROPHENOL

2,4-DINITROTOLUENE

2.6-DINITROTOLUENE

Dl-N-OCTYLPHTHALATE

FLUORANTHENE

FLUORENE

HEXACHLOROBENZENE

HEXACHLOROBUTADIENE

HEXACHLOROCYCLOPENTADIENE

HEXACHLOROETHANE

INDENO(1,2,3-CD)PYRENE

ISOPHORONE

2-METHYL-4,6-DINITROPHENOL

NAPHTHALENE

NITROBENZENE

2-NITROPHENOL

4-NITROPHENOL

N-NITROSODIPHENYLAMINE

N-NITROSODI-N-PROPYLAMINE

PENTACHLOROPHENOL

PHENANTHRENE

PHENOL

PYRENE

1,2,4-TRICHLOROBENZENE


Not detected ug/L

17 u ~ / L

Not detected ug/L

Not detected ug/L

Not detected ug/L

Not detected ug/L

Not detected ug/L

Not detected uglL

Not detected ug/L

Not detected ug/L

Not detected uglL

Not detected ug/L

Not detected ug/L

Not detected ug/L

Not detected ug/L

Not detected ug/L

30 u ~ / L

Not detected ug/L

Not detected ug/L

Not detected ug/L

Not detected ug/L

Not detected ug/L

Not detected ug/L

Not detected ug/L

2 1 ug/L

Not detected ug/L

Not detected ug/L

Not detected ug/L

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

HWC

BENZlDlNE Not detected ug/L 100 625 5/31/00 21:19 HWC

1,2-DIPHENYLHYDRAZINE Not detected ug/L 100 625 5/31/00 21:19 HWC

NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - F L Certification No. E87519


Phone: 7041529-6364 A Toll Free Number: 1-8001529-6364 A Fax: 704/525-0409

Lab Report



Mr. James Tan


Charlotte, NC 28210

Page 9 of 10


Prism S a m ~ l e ID: A669732 Loain Group: A062F3

Sample Collection Datemime: 5/25/00 15:30 Lab Submittal Datemime: 5/26/00 10:OO



---------- TICS BY SEMIVOLATILE GCIMS 62518270 5/31/00 21:19 HWC

625/8270 Tentatively Identified compounds (10-largest TICS) :

<Identification Class> ................................. ................................. Unknown aliphatic hydrocarbon Unknown aliphatic hydrocarbon Unknown aliphatic hydrocarbon Unknown aliphatic hydrocarbon Unknown aliphatic hydrocarbon Unknown aromatic hydrocarbon Unknown aromatic hydrocarbon Unknown aromatic hydrocarbon Unknown Unknown

<Closest Spectral Fit> ~ E s t . Cone.> ...................... ------------ ...................... ------------ (Unknown ) 57 ug/L (Dodecane ) 44 ug/L (Unknown) 37 ug/L (Unknown ) 67 ug/L (Pentadecane ) 35 u g / ~ (Methylnaphthalene) 62 ug/L (Methylnaphthalene) 51 ug/L (Dimethylnaphthalene) 40 ug/L (Unknown ) 350 ug/L (Unknown) 60 ug/L

C5-C8 Aliphatics 420 ug/L 300 MADEP VPH 5/31/00 0853 KV

C9-C12 Aliphatics 330 ug/L 200 MADEP VPH 5/31/00 0853 KV

C9-C10 Aromatics 560 ug/L 100 MADEP VPH 5/31/00 0853 KV

Surrogate % Recovery - PID 89 YO (70-130) MADEP VPH 5/31/00 0853 KV

Surrogate % Recovery - FID 92 YO (70-1 30) MADEP VPH 5/31/00 0853 KV

Dilution Factor 2 ug/L MADEP VPH 5/31/00 0853 KV

EXTRACTION FOR EPH

C9-C18 ALIPHATICS

C19-C36 ALIPHATICS

C11-C22 AROMATICS

SURROGATE RECOVERY - ALIPHATIC

SURROGATE RECOVERY - AROMATIC

SURR:2-BROMONAPHTHALENE

SURR:2-FLUOROBIPHENYL

DILUTION FACTOR

Completed

Not detected

Not detected

Not detected

106

117

116

111

1

MADEP-EPH

500 MADEP-EPH

400 MADEP-EPH

aoo MADEP-EPH

(40-140) MADEP-EPH

(40-1 40) MADEP-EPH

(40-1 40) MADEP-EPH

(40-140) MADEP-EPH

MADEP-EPH

GRR

ESR

ESR

ESR

ESR

ESR

ESR

ESR

ESR


449 Springbrook Road A P.O. Box 240543 A Charlotte, N C 28224-0543

Phone: 7041529-6364 A Toll Free Number: 1-8001529-6364 A Fax: 7041525-0409

Lab Report



Mr. James Tan



Page 10 of 10



Sample Collection Datemime: 5/25/00 15:30 Lab Submittal Datemime: 5/26/00 1O:OO


TEST TEST REPORTING METHOD DATEfrlME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST

Sample Comments:



449 Springbrook Road A P.O. Box 240543 A Charlotte, NC 28224-0543 Phone: 704/524-6364 A Toll Free Number: 1-800/529-6364 A Fax: 704/525-0409

PRISM LABORATORIES, INC.


Main Office: 449 Springbrook Road

P.O. Box 240543 Charlotte, NC 28224-0543

Phone: 7041529-6364 1 I8001529-6364

Fax: 7041525-0409

Date: k,/4/@

/ To: ]A /hW. Lab Group ID: A O/,

The State of North Carolina requires the enclosed VPH and EPH forms be submitted with our laboratory report. Before submitting these forms to the state, please insert the project name and/or site location.

Cc: Lab File

VPH (AliphaticslAromatics) Laboratory eporting Form

Client Name J.A. Jones Management Service

a Laboratory Name Prism Laboratories, Inc.

Project Name AS146 NC Certification # (Lab) 402

Site Location INCLUDE APPROPRIATE UNITS

* Option 1 = Established fill line on vial Option 2 = Sampling Device (indicate brand, e.g. Encore) Option 3 = Field weight of soil *' Unadjusted value. Should exclude the concentration of any surrogate(s), internal standards, andlor concentrations of other ranges that elute within the sp e.

Page 1 No trip blank was requested.

Percent Recovery - Fortified Blank (Spike) - PID Relative Percent Difference - PID Duplicate Percent Recovery - Fortified Blank (Spike) - FID Relative Percent Difference - FID Duplicate

Revision 516198

NA N A

117% 2.0%

NA NA

124% 5.0%

123% 2.0% N A N A

J.A. Jones Management Services Proj: AS146

Attachment 2

Initial Calibratior~ Date 411 7/00 Calibration Ranges and Limits

Method of Quantitation (circle one): Curve e Response Factor Calibration Concentration Levels

C5 -C8 Aliphatics C9 - C12 Aliphatics C9 -C10 Aromatics

- Aliphatics 375 ua/L 15%

Aliphatics 275 ug/L 5.3%

NOTE: Please include units as appropriate

47 ug/L 28 ug/L 10 ug/L

C9 - C10 Aromatics 17%

100 ug/L 150 ug/L

NOTE: Please indicate units as appropriate.

150 ug/L 89 ug/L 32 ug/L

Calibration Check Date 5/30/00 Calibration Check

150 ug/L 100 ug/L 50 ug/L

MDL = Method Detection Limit

C9 - C12 Aliphatics C9 -ClO Aromatics

ML = Mimimum Limit

RL = Reportable Limit

275 ug/L 50 ua/L

%RSD = Percent Relative Standard Deviation

CCC = Correlation Coefficient of Curve

2.0% 5.0%

AB69732 Revision 5/6/98

EPH (AliphaticslAromatics) Lab d ) atory Reporting Form Client Name J.A. Jones Management Service Laboratory Name Prism Laboratories. Inc.

Project AS146 NC Certification # (Lab) 402

Site Location

Unadjusted value. Should exclude the concentration of any surrogate(s), internal standards, and/or concentrations of other ranges that elute within the specified range. ** The surrogate recovery was above the control limits. Matrix interference is suspected.

Fractionation Surrogate % Recovery Fractionation Surrogate O h Recovery

116°h 1 1 1 O/O

Page 1

Percent Recovery-Fortified Blank (Spike)

Relative Percent Difference - Sample Duplicates

Revision 5/6/98

90%

3.0%

77%

7.0%

47%

37%

J.A. Jones Management Service Proj: AS146

0 EPH Laboratory Reporting Form

Initial Calibration Date 5/20/00-5/31 100 Calibration Ranaes and Limits

IC9 4 1 8 Aliphatics 130 ug/L 413 ug/L 500 ug/L

NOTE: Please include units as appropriate

Method of Quantitation (circle one): Curve or AGrage Response Factor Calibration Concentration Levels

C19 - C36 Aliphatics C11 -C22 Aromatics

C9 -C18 Aliphatics 9.0%

I Aliphatics "

400 mg/L 1

120 ug/L 240 ug/L

~

170 mg/L C l I - c22 425 ma/L

I -

Aroniatics 850 mg/L

382 ug/L 763 ug/L

I 1700 mg/L I NOTE: Please indicate units as appropriate.

400 ug/L 800 ug/L

Calibration Check Date 611 100 Calibration Check

IC9 4 1 8 Aliphatics 300 mg/L 4.0% I

MDL = Method Detection Limit

ML = Minimum Limit

RL = Reportable Limit

C19 - C36 Aliphatics C11 4 2 2 Aromatics

RPD = Relative Percent Difference

%RSD = Percent Relative Standard Deviation

CCC = Correlation Coefficient of Curve

Revision 5/6/98

400 mg/L 850 ma/L

3.0% 13%

CHAIN OF C U ~ D Y RECORD PAGE O P Q U O 8

Samples INTACT upon arrival7 449 Springbrook Road r Charlotte, NC 2821 7 Rece~ved ON WET ICE? Temp ; 1 --- ,, I

P.0. BOX 240543 r Charlotte, NC 28224-0543 PROPER PRESERVATIVES indicated7 A

Phone: 7041529-6364 r Fax: 7041525-0409 Recelved WITHIN HOLDING TIMES? --- Fclll Serwce Analytical & Environmental Solutions

CUSTODY SEALS INTACT7 --- ,' VOLATILES rec'd WlOUT HEADSPACE? - - -

PROPER CONTAINERS used? --- 1 "

Client - I j ' i ,. , 1 , . , -- .

' $ ' TPORT TO: Name Physical Address ;,I' ' : L --,: 4' .d.-i k

Address ' ' * State Certification

, J $. 2 # # , 7 , I BILL TO: Name . r e iT/c', Requested // NC - SC - O t h e r NA -

. > -, 7 5- ,* Phone Fax * -

Address ,$*<, L Water Chlorinated Yes - No - NA - - I P.O.lf/Billing Referen e '' 4 .I' f >'

Requested Due Date Sample Iced Upon Collect~on Y e s NO - fc , * , , . Project Name .- ' (SEE REVERSE SIDE FOR RUSH TURNAROUND FEES) t t

I '

?{ NPDES NC

.t< UST: NC GROUNDWATER: NC '- DRINKING WATER: NC SOLlD WASTE: NC OTHER: NC

SC SC SC - SC SC - SC OTHER - OTHER-- OTHER - OTHER OTHER OTHER -

Rel~nqutshed By. (Stgnature)

*CONTAINER TYPE CODES: A = Amber C = Clear G =Glass P = Plastic; TL = Teflon-Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

FINAL REPORT COPY

PRISM LAB

ID NO.

L . - I

CLIENT SAMPLE DESCRIPTION

( I , , ' ,

' 1 , , lPi

i Rece~ved For Prtsm Laboratones By

, . I 1

DATE COLLECTED

/ I I " ?

I

,; ,,? 1 . - , { I , L < ' .,* $ 1 , - Sampler's Signature , i ' i - Sampled By (Print Name) Affillatlon

Date

I .

Method of Shtpment Log-In Group No

TIME COLLECTED

MILITARY HOURS

i ,

,I

I

< I -

Additional Comments Relinqutshed By (Stgnature) I - . I :

fleltnqut;hed ~~'(~Gnature)

MATRIX (SOIL,

WATER OR SLUDGE)

-.

Rece~ved By (S~gnature)

Recelved By. (Signature)

Date

Date

SUB

CERT' ID NO.

~ t l l l a r ~ / ~ o u r s

SAMPLE CONTAINER PRESERVA-

TIVES

$i( i., I

* ' 1

li (,, L~

3 2

w p ~ SEE BELOW

2

,

, > >

. ,

(-

\

i -*

. *

\ .'

- ,.' ,' ,

, \

'. ,- *-*. ,

"4

A,

1

i I

\

I

UST Closure Report

APPENDIX H

Photographs of UST Closure Activities

UST NO. AS-146



Photo 1 Pre-construction site view

Photo 2 Set-up for UST cleaning ---- Confined space entry

Contract Number N62460-93-D-3033 Task Order No. 044

UST Closure Report UST NO. AS-1 46

Photo 3 Set-up for UST cleaning and demolition

Photo 4 UST cleaning ---- Confined space entry

Conbact Number N62460-93-D-3033 Task Order No. 044


Photo 5 Concrete UST demolition





Photo 8 Concrete UST demolition ---- Note landslides occur around supports of a fuel pipe


UST Closure Report UST NO. AS-1 46

Photo 9 Partially backfill and cutting concrete re-bar prior to sampling at UST bottom

Photo 10 After construction site view

Contrsct Number N62460-93-D-3033 Task Order No. 044

· 2007. 7. 31. · UST Closure Report UST NO. AS-146 GWNST-12 UNDERGROUND STORAGE TANK CLOSURE...

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Transcript of · 2007. 7. 31. · UST Closure Report UST NO. AS-146 GWNST-12 UNDERGROUND STORAGE TANK CLOSURE...