=====================================================================Acq. Operator : ROLANDO Seq. Line : 5Acq. Instrument : Instrument 1 Location : Vial 105Injection Date : 11/17/2015 5:33:45 PM Inj : 1 Inj Volume : 0.5 µlSequence File : C:\Chem32\1\DATA\151117\140423 2015-11-17 11-38-16\140423.SMethod : C:\CHEM32\1\DATA\151117\140423 2015-11-17 11-38-16\SIMDIS-BLANK.M (Sequence Method)Last changed : 11/12/2015 9:53:45 AM by ROLANDO Method Info : Method splitless para inyeccion de BLANK AIR para destilacion simulada. Vol 0.5 ul- gas saver from 3.5 min CON enjuague de AIRE ===================================================================== Column(s)===================================================================== Column Description : Simdis CP7592Inventory# : autoID-1Model# : CP7592 Manufacturer: Diameter : 530.00 µm Length : 10.0 mFilm thickness : 0.53 µm Void time : 0.069 min# Injections : 0Maximum Temperature: 450.0 °CComment :

min0 0.5 1 1.5 2 2.5

15 µV

0

1000

2000

3000

4000

5000

AIB2 D, AIB2D, 4th Signal (DIESEL NAOH 10 %.D) FID1 A, FID1A, Front Signal (DIESEL NAOH 10 %.D)

0.2

18 0

.274

0.4

20

0.6

28

0.7

38

1.1

45

1.3

17

1.8

25

2.1

13

2.3

54

2.6

09

2.9

80

===================================================================== Area Percent Report with Performance ===================================================================== Multiplier: : 1.0000Dilution: : 1.0000Do not use Multiplier & Dilution Factor with ISTDs

Data File C:\CHEM32\1\DATA\151117\140423 2015-11-17 11-38-16\DIESEL NAOH 10 %.DSample Name: DIESEL NAOH 10 %

Instrument 1 11/17/2015 6:39:58 PM ROLANDO Page 1 of 2

Signal 1: AIB2 D, AIB2D, 4th Signal Signal 2: FID1 A, FID1A, Front Signal RetTime k' Area Height Symm. Width Plates Resol Select [min] [pA*s] [pA] [min] ution ivity -------|------|----------|----------|-----|-------|-------|-----|------ 0.218 2.17 7055.18652 3785.73926 2.07 0.0256 400 - - 0.274 2.98 2.17657e4 6049.62891 0.79 0.0576 125 0.79 1.38 0.420 5.10 4.39736e4 5468.38770 0.82 0.1550 41 0.81 1.71 0.628 8.12 1.20140e4 2474.45410 1.95 - - - 1.59 0.738 9.72 3.70607e4 3837.20825 0.67 0.1464 141 - 1.20 1.145 15.62 1.53515e4 1397.31567 3.28 - - - 1.61 1.317 18.12 3.28562e4 2662.04224 0.82 0.1767 308 - 1.16 1.825 25.50 1.07805e4 770.39935 1.79 - - - 1.41 2.113 29.68 2.75850e4 2275.90747 1.34 0.1883 698 - 1.16 2.354 33.17 4412.72217 468.59644 0.68 - - - 1.12 2.609 36.88 8279.14648 586.30444 0.97 0.2808 478 - 1.11 2.980 42.26 2.19117e4 1868.17126 1.54 0.1842 1451 0.94 1.15 3.501 49.83 7870.18945 476.81699 1.88 0.1992 1712 1.60 1.18 3.856 54.97 1.93621e4 1725.08032 1.40 0.1758 2664 1.11 1.10 4.705 67.31 2.50460e4 1832.30115 1.96 0.1650 4506 2.93 1.22 5.143 73.66 5322.18652 333.47131 1.13 0.2938 1698 1.12 1.09 5.519 79.13 1.86731e4 1796.98645 1.30 0.1575 6804 0.98 1.07 5.935 85.16 7124.11182 474.82065 1.07 0.2508 3101 1.20 1.08 6.290 90.31 1.60527e4 1737.92908 1.30 0.1442 10545 1.06 1.06 6.678 95.94 5805.70264 503.72736 0.84 0.1975 6333 1.33 1.06 7.024 100.96 1.46506e4 1627.42407 1.22 0.1392 14111 1.21 1.05 7.388 106.25 5329.85010 481.87405 0.83 0.1942 8020 1.28 1.05 7.724 111.13 1.29406e4 1472.62366 1.13 0.1342 18361 1.20 1.05 8.078 116.27 4691.21289 384.42743 1.64 0.1817 10955 1.32 1.05 8.387 120.75 1.13089e4 1280.74744 1.21 0.1350 21381 1.14 1.04 9.014 129.86 1.33153e4 1088.23865 1.85 0.1375 23809 2.70 1.08 9.620 138.65 1.07407e4 865.97906 2.12 0.1375 27118 2.59 1.07 10.205 147.14 8766.83203 636.33044 2.63 0.1417 28745 2.46 1.06 12.984 187.48 3.99858e4 601.29175 8.51 0.2717 12654 7.90 1.27 13.418 193.79 4324.12891 335.16364 0.37 0.1525 42887 1.20 1.03 13.834 199.83 4861.02197 365.91125 0.60 0.1992 26728 1.39 1.03 30.033 434.99 863.40948 264.08203 2.21 0.0483 2139018 76.90 2.18 ===================================================================== *** End of Report ***

Data File C:\CHEM32\1\DATA\151117\140423 2015-11-17 11-38-16\DIESEL NAOH 10 %.DSample Name: DIESEL NAOH 10 %

Instrument 1 11/17/2015 6:39:58 PM ROLANDO Page 2 of 2