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    Flowsheeting

    2000 AEA Technology plc - All Rights Reserved.Chem 3_4.pdf

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    WorkshopIn evaporation, a solution consisting of a non-volatile solute and a

    volatile solvent is concentrated by the addition of heat. In multiple

    effect evaporation, the volatile solvent recovered from the first

    evaporator is condensed and used as a heat source for the next

    evaporator. This means that the second evaporator must operate at a

    lower temperature and pressure than the first evaporator.

    In this module you will simulate a series of three evaporators to

    concentrate a solution of sucrose/water. Each evaporator is modelled

    using a flash tank. You will convert the completed simulation to a

    template, making it available to connect to other simulations.

    On the next page, a Process Overview is shown. This represents the

    actual process. On the third page a Simulation PFD is shown. This

    represents the simulation as you will build it in this module. Building

    the simulation in this way allows more flexibility in the design.

    Learning Objectives

    Once you have completed this section, you will be able to:

    Add and connect operations to build a Flowsheet

    Add and use logical operations, Sets and Adjusts

    Use the graphical interface to manipulate flowsheets in HYSYS

    Understand information propagation in HYSYS

    Convert HYSYS flowsheet to templates

    PrerequisitesBefore beginning this section you need to know how to:

    Define a Fluid Package

    Define Streams

    Navigate the Workbook interface

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    Process Overview

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    Simulation PFD

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    Building the SimulationThe first step to building any simulation is defining a Fluid Package. A

    brief recap on how to define a Fluid Package and install streams is

    described below. For a complete description see: Defining the

    Simulation Basis, Module 1.

    Defining the Simulation Basis

    1. Start a New Case and add a Fluid Package.

    2. UseWilson/Ideal as the Property Package with the components

    Sucrose and H2O.

    3. Move to the Binary Coefficients page. Notice that the interactionparameters for Aij and Bij are empty.

    The program warns you that the binary coefficients have not been

    determined and the model will assume values of zero. Answer OKto

    this message. Enter the Simulation Environment.

    The Wilson equation cannotbe used for problems involving

    liquid-liquid equilibrium.

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    4. Add a stream with the following values.

    5. Add a second stream with the following properties:

    In this cell Enter

    Name Feed

    Vapour Fraction 0

    Pressure 101.3 kPa (14.7 psia)

    Flowrate 50 kg/h (110 lb/hr)

    Mass Fraction Surcose 0.3

    Mass Fraction H2O 0.7

    Note that the compositionvalues for this stream are inMassfractions. Double-clickon the Mass Flow cell to enterthese values.

    In this cell Enter

    Name Steam

    Vapour Fraction 1.0

    Pressure 275 kPa (40 psia)

    Mass fraction H2O 1.0

    What is the temperature of stream Feed? __________

    What is the temperature of stream Steam? __________

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    Adding Unit Operations to a FlowsheetAs with streams, there are a variety of ways to add Unit Operations in

    HYSYS:

    The Triple Effect Evaporator consists of six operations:

    A series of three evaporators modelled as flash tanks (2 Phaseseparators)

    Three coolers

    In this exercise, you will add each operation using a different method of

    installation.

    To use the Do this

    Menu Bar SelectAdd Operation from the

    Flowsheet menu.

    Or

    Press the hot key.

    The UnitOps window displays.

    Workbook Open the Workbook and go to the

    UnitOps page, then click theAdd

    UnitOpbutton.

    The UnitOps window displays.

    Object Palette Select Object Palette from the

    Flowsheet menu or press to

    open the Object Palette and double

    click the icon of the Unit Operation

    you want to add.

    PFD/Object Palette Using the right mouse button,

    dragndrop the icon from the Object

    Palette to the PFD.

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    Adding a Separator

    The Evaporator is modelled using a Separator in HYSYS.

    The Separator will be added using the hot key.

    1. Press the hot key. The UnitOps window displays:

    2. Select Separator from theAvailable Unit Operations list.

    3. Press theAddbutton. The Separator property view displays.

    4. On the Connections page enter the data as shown here:

    Note: Drop down boxes, such as for Feed and Product streams, containlists of available streams which can be connected to the operation.

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    Adding a CoolerAdd the first Cooler using the same method.

    1. Press the hot key

    2. The UnitOps window displays. Click the CategoryHeat TransferEquipment and select Cooler.

    3. Press theAdd button. The Cooler property view displays.

    4. On the Connections page enter the information as shown below:

    5. Go to the Parameters page.

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    6. Enter a value of 0 kPa(0 psi) for the Pressure Drop.

    7. Go to theWorksheet tab.

    8. Specify aVapour Fraction of0 for the stream Condensate.

    To completely define the separation we need to provide an energy flow.

    9. On the Worksheet tab, enter a value of2.42e4 kJ/h(2.29e4 Btu/hr) for the Energy stream q1.

    What is the flowrate of Water in the stream L1? __________

    What is the temperature of the stream V1? __________What is the mass flow of steam through the Cooler?__________

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    Add the Second CoolerThis procedure describes how to add Unit Operations using the

    UnitOps page of the Workbook.

    1. Open the Workbook and click the UnitOps tab.

    2. Click theAdd UnitOpbutton. The UnitOps window displays:

    3. Select Heat Transfer Equipment from the Categories group.

    4. Select Cooler from theAvailable Unit Operations list.

    5. Press theAddbutton. The Cooler property view displays.

    6. On the Connections page enter the information as shown below:

    7. On the Parameters page specify a Pressure Drop of0 kPa (0 psi).8. Go to theWorksheet tab and specify theVapour Fraction of the

    stream C2 as 0. Close this view.

    What is the Heat Flow for stream q2? __________

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    Add Another SeparatorThis procedure describes how to add a Separator using the Object

    Palette. The Object Palette contains icons for all the Streams and Unit

    Operations in HYSYS.

    1. Press the hot key. The Object Palette displays:

    2. Double click the Separatorbutton on the Object Palette. TheSeparator property view displays.

    Separator button

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    3. On the Connections page enter the stream information as shownhere:

    4. On the Parameters page, delete the pressure drop specification.The Separator should become unsolved; Unknown Delta P.

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    Add a Set OperationThe Set Operation is a steady-state logical operation used to set the

    value of a specific Process Variable (PV) in relation to another PV. The

    relationship is between the same PV in two like objects -- for instance,

    the temperature of two streams, or the UA of two exchangers.

    In order for the energy to flow from Cooler 2 to Effect 2, the Separator

    outlet temperature must be cooler then the condensate from the

    Cooler. A Set operation will be used to maintain this relationship.

    1. Add a Set operation by double-clicking on the Set icon in theobject palette.

    2. Complete the Connections page as shown here:

    3. Go to the Parameters tab. Complete the view as shown below, ifusing field units the value for the offset will be -5 oF:

    What is the Delta P of Effect 2? __________

    Set operation button

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    Add the Third CoolerWorking with a graphical representation, you can build your flowsheet

    in the PFD using the mouse to install and connect objects. This

    procedure describes how to install and connect the Cooler using the

    Object Palette Dragndrop technique.

    To DragnDrop in the PFD:

    1. Press the Coolerbutton on the Object Palette.

    2. Move the cursor to the PFD. The cursor will change to a specialcursor, with a box and a plus (+) symbol attached to it. The boxindicates the size and location of the cooler icon.

    3. Click the left mouse button to drop the Cooler onto the PFD.

    There are two ways to connect the operation to a stream on the PFD:

    To connect using the Do this

    Attach Modetoggle button

    Insert Icon

    Press theAttach Modetoggle button.

    Place the cursor over the operation.

    The Feed stream connection point is

    highlighted in dark blue.

    Move the cursor over the stream you

    want to connect.

    Press and hold the left mouse

    button.

    Move the cursor to the operation

    icon and release the mouse button.

    key Press and hold the key and

    pass the cursor over the operation.

    Place the cursor over the stream you

    want to connect.

    Press and hold the left mouse

    button.

    Move the cursor to the operation

    icon and release the mouse button

    and the key.

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    4. Double click on the Cooler icon on the PFD. The Cooler propertyview displays. Enter the data shown below:

    5. On the Parameters page specify a Pressure Drop of0 kPa (0 psi).

    6. Go to theWorksheet tab and specify theVapour Fraction of thestream C3 as 0. Close this view.

    Add the Third Separator

    1. Drag n drop the Separator onto the PFD. Connect the stream L2as the Feed to the Separator.

    2. Double click on the Separator. Make the following connections:

    3. On the Parameters page delete the pressure drop specification.

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    Set Operation1. Add a Set operation and complete the Connections page as

    shown here:

    2. On the Parameters tab enter a value of3 C (-5F) as the Offset,and 1.0 for the Multiplier.

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    Add an AdjustThe Adjust operation is a Logical Operation - a mathematical operation

    rather than a physical operation. It will vary the value of one stream

    variable (the independent variable) to meet a required value or

    specification (the dependant variable) in another stream or operation.

    It is desired to reach 15 weight% water in stream L3. The only

    parameter we have to manipulate this variable is the energy supplied tothe first Effect. To meet a target concentration in L3 we can use an

    Adjust operation.

    1. Add theAdjust operation. The Adjust property view displays.

    2. Press the Select Var button in theAdjusted Variable group toopen theVariable Navigator.

    3. From the Object list select q1. From theVariable list which is nowvisible, select Heat Flow.

    4. Press the OKcell to accept the variable and return to theAdjustproperty view.

    5. Press the Select Var button in the Target Variable group.

    What is the weight percent of Water in stream L3?__________

    Adjust button

    The adjusted variable mustalways be a user specifiedvalue.

    Always work left to right in theVariable Navigator. Dontforget you can use the ObjectFilter when the Object list islarge.

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    6. Select L3 and Comp Mass Frac (H2O) as the target variable.

    7. On the Connections page, enter a value of0.15 in the SpecifiedTarget Value box.

    The completed Connections page is shown below.

    8. Switch to the Parameters tab, and enter 2000 kJ/h (1900 Btu/hr)as the Step Size.

    9. Press the Startbutton to begin calculations.Note: once the case issolved (OK status), this button will disappear from the propertyview.

    10. To view the progress of the Adjust, go to the Monitor tab.

    When adjusting certainvariables, it is often a goodidea to provide a minimum ormaximum which correspondsto a physical boundary, such

    as zero for pressure or flow.

    Note theToleranceandStepSizevalues. When consideringstep sizes, use larger ratherthan smaller sizes. TheSecantmethod works best once thesolution has been bracketedand by using a larger step size,you are more likely to bracketthe solution quickly.

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    If you enter a step size too large for the energy HYSYS will not calculate

    because all the liquid has been flashed. You need to decrease the step

    size, enter a new value for q1 and restart the simulation.

    Note that HYSYS does not predict the formation of solids; this will have

    to be verified separately.

    Manipulating the PFDThe PFD is designed around using the mouse and/or keyboard. There

    are a number of instances in which either the mouse or the keyboard

    can be used to perform the same function. One very important PFD

    function for which the keyboard cannot be used is Object Inspection.

    You can perform many of the tasks and manipulations on the icons in

    the PFD by using Object Inspection. Place the mouse pointer over the

    icon you wish to inspect and press the secondary mouse button. An

    appropriate menu is produced depending upon the icon selected

    (Stream, Operation, Column, or Text Annotation).

    A list of the objects which you can Object Inspect are shown below with

    What is the energy required to achieve a concentration of85 wt% of sucrose in the product stream? __________

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    the corresponding menus.

    Object... Object Inspection Menu...

    PFD

    Unit Operations

    Streams

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    Customize the PFD by performing the following:

    1. Add a Title, Triple Effect Evaporator.

    2. Add aWorkbook Table for the Material Streams in the simulation.

    3. Add a Table for stream L3.

    Adding Unit Operation Information tothe Workbook

    Each WorkBook has a UnitOps page by default that displays all the Unit

    Operations and their connections in the simulation. You can add

    additional pages for specific Unit Operations to the WorkBook. For

    example, you can add a page to the WorkBook to contain only Coolers

    in the simulation.

    To add a Unit Operation tab to theWorkBook:

    1. Open theWorkbook.

    2. In the Menu Bar, selectWorkbook, and then Setup.

    3. In the Setup view, press theAddbutton in the UnitOps group.

    4. From the New Object Type view, select Heat TransferEquipment, then Cooler.

    5. Click OK. A new page, Cooler, containing only Cooler informationis added to the WorkBook.

    Double clicking on a title witha "+" sign will open anexpanded menu.

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    Adding Unit Operation Information tothe PFD

    For each Unit Operation, you can display a Property Table on the PFD.

    The Property Table contains certain default information about the Unit

    Operation.

    Add Unit Operation information to the PFD:

    1. Open the PFD.

    2. Select the Separator Effect 1.

    3. Object Inspect the Unit Operation.

    4. Select Show Table from the menu.

    5. TheVessel Temperature, Pressure, Liquid Molar Flow, and Dutyare shown as defaults in the table. Object Inspect the table andinsert theVapour Mass Flow.

    6. Create two tables for the streams Feed and L3 showing theComponent Mass Fraction of Sucrose and the Mass Flow.

    Remember you can ObjectInspect an object by selecting itand then clicking on it withthe right mouse button.

    Save your case!

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    Exploring with the SimulationExercise 1

    Try running the case for different final sucrose concentrations. Can you

    find any cases in which the program does not solve?

    Watch for cases when the Adjust block takes too large of a step in energy,

    causing all of the liquid to be flashed.

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    Saving the Simulation as a TemplateA template is a complete Flowsheet that has been stored to disk with

    some additional information included that pertains to attaching the

    Flowsheet as a Sub-Flowsheet operation. Typically, a template is

    representative of a plant process module or portion of a process

    module. The stored template can subsequently be read from disk and

    efficiently installed as a complete Sub-Flowsheet operation any

    number of times into any number of different simulations.

    Some of the advantages of using templates are:

    Provide the mechanism by which two or more cases can belinked together

    Can employ a different property package than the main case towhich it is attached

    Provide a convenient method for breaking large simulationsinto smaller, easily managed components

    Can be created once and then installed in multiple cases

    Before you convert a case to a template, it needs to be made generic so

    it can be used with gas plants of various flowrates.

    1. Delete the Flowand Composition of stream Feed.

    2. Choose Main Properties from the Simulation menu.

    3. Press the Convert to Templatebutton.

    4. Press Yesto convert the simulation case to a template.

    5. Answer No to the question Do you want to save the simulationcase.

    6. Save the template as 3-Effect-Evap.tpl.

    Note that once a case has beensaved as a template, it can notbe re-converted back into a

    normal simulation case.

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