0233' - United States Environmental Protection Agency · 2018-06-19 · bamplb ipd77q (iuant1tatei)...
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Transcript of 0233' - United States Environmental Protection Agency · 2018-06-19 · bamplb ipd77q (iuant1tatei)...
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>AT/v 1FD77QV. TJ>9/lO/Q4 788:00IAMPLC: iro VOA OAPIPLE BAIK QO-770, BUD* C7491, CASE* £640ADMITTED ov: EPA ANALYBT; RJMMWNT-ARBA • REP, AMNT/IREP. AREA)* RBBP.PACT)
P. PAC. PROM LIDRARY ENTRY
NO NAMEI DROMQCHLOROIIKTHANBIVO L10RARY ID)8 B-DROnO-1-CHLOROPROPANE (UY INTERNAL STANDARD)3 1.4-DlCHLQRODUTANB IU2 INTERNAL STANDARD)4 DO-l.R-DlCHLOROBTHANB (BURROOATE)9 PQ-TOLUENE (BURROOATE)6 P-DRDHOPLUORODENZBNE (KB CHECK)7 DlCHLQROflETHANfi
NO M/B SCAN T1HB RBP HRT (1ETH AREAIHOHT) AMOUNT HOT1 188 88t 7; SB 1 .000 ADD 940QO, 890. 000 t* 16. 388 77 400 16:00 8 .000 ADD 118797, 890.000** 16.30'3 99 601 80:08 3 .000 ADD 09361, 890. 000 »« 16.38t 69 877 ?: 04 1 . 386 A DO 99090. 898, 094 «« 16, 919 100 633 81:06 3 .093 ADD 180908, 849,306** 16,066 99 784 26; OB 3 .304 ADD 118446, 847, 3<70 «« 16,34<r 04 199 9:10 1 0.678 ADD 81610. 87 . 7B7 •« 1.70
NO RET(L) RATIO RRT(L) RATIO AUNT AMNT(L) R FAC R.PAC(L) RATJO7: IB ,08 ,000 1,00 890.00 890,00 ,000 1.000 1,0016:00 ,00 .000 1,00 890.00 890,00 ,000 1.000 1.0080:00 .00 .000 1.00 890.00 890.00 ,000 1,000 1,007:46 .01 330 0.77 898,09 890,00 ,007 1.000 1,01
81: OB .00 .097 1.00 849.81 890,00 ,909 1,934 0.7886:06 ,00 .309 1.00 847,37 890.00 .317 1.380 1,004,96 09 0.676 1,08 87.77 890,00 0376 3.384 0.18
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UlOUNT»AREA • REP. AMNT/tREF, AREA)* RE8P.PACT), FAC, FROM L1DRARY ENTRY
NO NAMEI PROnOCHLOROnCTHANElVO L1DRARY IB)8 3-OROtlO-l-CHLOROPROPANE (UY INTERNAL STANDARD)3 1,4-DICHLORODUTANE (UZ INTERNAL BTANDAflD) ,4 CYCLOTRIBILOXANE.HEXAMETHYL- C ««**- o'*<S.
MO n/E SCAN TIME HEP RRT HETM AREA(HOHT) AMOUNT XTOT1 RIC 884 7:88 1 1,000 ADS 877777, 890,000 *» 18,18S RIC 4BO 16:00 8 1000 ADD 303B73. 890,000** 18,183 RIC 601 20:08 3 1,000 ADO 146474, 8190,000** 18,184 RIC 706 26.18 3 130B ADD 777879. HfltBr-W- 63.69
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DATA 1PD77Q, TI05/ii/B4 17:87:00SAMPLE; EPA/IPD CASPrMO «C9««! DUA (SAI KB9-77Q)SUBMITTED DY 1PD ANALYST EPP
AMQUNT»AREA • REP AMNT/MREF AREA)" REBP.FACT)RE8P PAC. PROM LIORARY ENTRY
NO NAME1 D4-1.4-DICHLORODENZENE (I, B 1-1 /30/04 VERSION)8 OB-NAPHTHALENE (C8 I.B, -1/80/84 VERSION)3 DIO-ACENAPMTHBNE (C3 1,3. -1/80/04 VERB10N)4 D18-CHRYBBNE (C4 1 B -1/30/04 VERSION)9 D10-PHENANTHRENE (C6 I B -1/20/84 VERBION)6 D9-PHENOL (ACID BURROOATE)7 8-FLUOROPMENOL (ACID BURROOATE)0 D9-N1TRODBNZENE (D/N BURROOATE) " . •7 8-PLUOROD1PHBNYL (D/N 6URROOATB)10 D14-P-TBR PMRNYL (66. )11 D10-PYRBNE (B. B. )18 8. 4.6-TRIDROMOPHENOL (B B. I13 8-CHLOROPHENOL14 PHENOL19 DIB(S-ETHYLHEXYL)PHTHALATE04 DI-N-DUTYL PHTHALATE
NO M/B SCAN TIME REP RRT MBTH AREA(HOHT) AMOUNT '/.TOTI 198 947 7:07 I8 136 737 13.07 33 163 1008 16:48 34 340 1604 80:049 108 1834 80:34
000 A DD 76613 40.000 »« 7.98000 A OD 806697 40 000 ** 7. 98000 A DD 138367 40.000 <• 7. 93
. 000 A7DD 6B309. 40 000 • « 7. 93000 A OD 341978 10 000 »« 7 9!
6 77 900 0:80 1 0714 ADD 77706 3 0 < 1 l S * < i 7.887 118 387 6:87 1 0.711 ADD 10799B r t 3 3 1 9 « « 8.148 83 688 10:80 8 0.061 ADD 131367 DO 830 •« 7,44<? 178 B76 14 96 < 3 1 387 A DD 137770 31 696 • « 9 7910 ,T*4 1487 34:47 4 0 (184 ADD 130330 33681 *« 6.1311 SIS 1463 84 83 4 0 067 A DD 198780 'JO 449 «« ft 6618 3310 1187 10:47 9 0913 ADD 19906 47 676 m 87713 1J1Q 983 0:43 1 0,794 ADD 180170 A'J 743 «* 0.8314 74 908 0:88 1 0 "10 ADD 1R8BO 3.811 •« 0.6019 147 1678 20:18 4 1 009u A DD 9047, 1. 169 »» 0,8816 147 1333 23:13 9 1 0001 A DD 34810, 4309** 003
NO RBTIL) RATIO RRT(L) RATIO AMNT AMNTIL) R PAC R.PAC(L) RATIO1 7,07 1,00 1 0008 1813 1,00 1.0003 1649 1,00 1,0004 30; 07 1,00 1,0009 BO 37 1 00 1,000
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00 40,00 40,00 1 00000 40,00 40,00 1 00000 40,00 40 00 1 00000 40,00 40.00 1 00000 40,00 40.00 1 00000 30,48 90.00 1 08000 43.31 90,00 I 144
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00 9083 90,00 0,366 0369 1,0000 3l,6b 90,00 0 370 0 616 0,6300 38,68 90,00 1,907 8
NO RET(L) RATIO HRT(L) RATIO AMNT AMNT(L) R FAC R.FAC(L) RATIO*\ 84:34
.' 18:4713 B 4414 8:8419 88.1016 88 16
00 0067 1 00 39,49 9000 1 771 3.987 0.71,00 0.713 1.00 47 70 90.00 0.098 0.094 0.79.00 0794 1.00 43,74 9000 1 399 1 439 087.00 0.718 1.00 3.21 90.00 0.188 I. 770 0.06.00 1009 1.00 l . l b 9000 0.067 S 741 0. OS.00 1. ODD 1 00 4 30 90 00 0 113 1.873 0 07
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QUANTITAT10N REPORT FILE UNKO
A: IPD770, TI09/31/84 17:37:00SAMPLE: EPA/1FD CABE3640 HC7491 DNA (BAI H09-77Q)8UDM1TTBO DY; 1FB ANALYST: EFP
AMOUNT-AREA • REF. AMNT/IREF. AREA)" HEBP.FACT)REBP. FAC. FROM LIBRARY ENTRY
NO NAME1 D4-I.4-D1CHLORODBNZENG (1 B 1-1/30/84 VERSION)8_O.YCUOHBXENE- - J»(u<ruT3 NAPHTHALENE.1-(CHLOROMETHYL)-4 CYCLOPENTANOL,3-METHYL-9 DO-NAPHTHALENE (C8 I, B, -1/80/84 VERB ION)6 D10-ACENAPHTHBNE (C3 I. B -1/80/84 VERSION)7 D13-CHRYBENE (C4 1. B. -1/80/84 VERSION)B D10-PHENANTHRENE (C6 1 & -1/80/04 VERSION)
NO M/E SCAN TIME REF RRT METH AREAtHOHT) AMOUNT '/JOT1 RIC 947 7:07 11 000 A DD 437476. 40.000 ** 1.078 RIC 1"2 3:18 1 0,391 ADD 10948900. 1734.770 88,113 RIC Bill 3:91 I 0488 ADD 107318, 10.830 0.404 RIC 4j>3 6:43 1 0.737 A DV 1778710. 167.760 7.749 RIC 7127 18:07 9 1000 ADD 617330. 40,000** 1.876 RIC 1008 16:48 6 '.000 ADD 603778. 40.000** 1.07
RIC 1604 88:04 7 I 000 A DV 967808 40,000 *« 1.87RSC 1834 30:34 0 1.000 ADD 617676, 40,000*' 1,87
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NO NAME1 DROMOCHLOROMBTHANEIVO L10RARY IB)8 8-DRQMQ-l-CHLQROPROPANB (UY INTERNAL UTANDARD)3 I,4»DICHLORQDUTANB (UZ INTERNAL STANDARD)4 D4-I,8-DICHLORQRTHANE (BURR09ATE)9 OB-TOLUENE (BURRQQATE)6 P-DROMOPLUORODiNZBNE (MO CHECK)7 D1CHLOROMETHANB
NO n/B BCAN TIME REP RRT METH AREA(HOHT) AMOUNT XTOTI 188 380 7:808 77 477 19'OB3 D9 600 80:004 6B 879 7:009 100 638 81:04 3
. 000 A DO 90703, 300, 000 «« 16,87000 ADD 117301. 800,000** 16, 87000 A DD B7B4B. 890.000 »« 16.89341 ADO 96837, 891.808** 16.36093 A DD 133677. 848, 404 »* 19,77
6 79 708 86:04 3 1,303 ADO 183778, 860, 706 «« 17,00H 04 100 9:00 1 0.603 A 00 88740, 30,977** 1,77
NO RET(L) RATIO RRT(L) RATIO AMNT AMNT(L) R.PAC R, PAC(L) RATIO1 7: IB8 16:003 80:004 7'469 81: OB6 86:067 4:96
00 1,000 1,00 890,00 890.00 1.00000 1,000 1.00 800,00 800,00 1,00000 1,000 1,00 800,00 890.00 1.00001 1,333 1.00 891.80 890.00 1,00900 1.007 1.00 848,40 890,00 1,4BB00 1,309 1,00 860.71 890,00 1.370
000 1,00000 1,00000 1.00000 1,00934 0,77380 1,04
,01 0,676 101 30,98 890,00 0,407 9384 0,18
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^OMITTED DY; EPA ANALYST: RJM
nMQUNTBAREA « REP, AMNT/IRBP, AREA)* REBP.PACT)HE8P, PAC, PROM LIDRARY ENTRY
NO NAME1 DROMOCHLOROMETMANEIVO LIORARY 16)2 8-DROMO-l-CHLORQPROPANE <UY INTERNAL STANDARD)3 1,4-DICHLORODUTANE (UZ INTERNAL STANDARD)
MO M/B 8CAN TIMS REP RRT METH AREA(HOHT) AMOUNT XTOT1 RIC 880 7:80 1 1.000 ADD 314806, 890,000** 33.338 RIC 477 19: 9B 8 1.000 ADD 307618. 890,000** 33,333 RIC 600 80:00 3 1000 ADD 196796. 290,000** 33,33
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DATA: 1F07BQ. Tl06/01/84 18:30:00BAMPLIi: iCA/'iru Cn5E!640 SC943S- SKA !OAI 8SS-728!BUDM1TTED DY: 1PD ANALYST: EPP
AMDUNT"AREA * REP AMNT/IREP AREA)* REBP.PACT)MEBP, PAC. PROM LIDRARY ENTRY
NO NAMEI D4-1,4-DICHLORODGNZENC (1. Q 1-1/30/04 VERSION)8 DO-NAPHTHALENE ICS I. D -1/80/04 VERSION)3 D10-4CENAPHTHBNE (C3 1.8 -1/80/B4 VERSION)'4 Dli'-CHRYBENE <C4 I, B, -1/80/04 VBRBIDN)9 DIO-PHENANTMRENE (C6 1 B -1/80/B4 VERB10N)6 D9-PHENOL (ACID BURROOA1E)7 8-FLUOROPHENOL (ACID 8URROQATE)B D9-NITRODENZENE (D/N BURROOATE)7 S-FLUORQDIPHENYL (0/N BURROOATE)10 D14-P-TBR PHENYL (B B, )11 D10-PYRBNE (B. 6, )18 8, 4.6-TR1DROMOPHENOL (C. B. )13 8-CHLOROPHENOL14 PHBNOL19 NAPHTHALENE
Mfe B-METHYLNAPHTHALENEW7 DIB(8-ETHYLHE)(YL)PHTHALATEIB DI-N-DUTYL PHTHALATE
NO M/E SCAN TIME REP RRT MBTH AREA(HOKT) AMOUNT HOT1 198 044 7:04 1 1000 ADD 78967 40.000** B, B7S 136 789 1809 S 1.000 ADD 268779 10000** 0, B73 168 770 16:3B 3 I O'JO A?DD 147494 40 000 •• 0. B74 840 1601 2001 4 1000 A?DD 09833, 40.000** 0,679 1BB 1831 80.31 9 1020 ADD 274084 40000** B, 096 77 477 B: 17 1 0,714 A DD 30170 11,890 *« 8.907 118 3D6 6:86 i 0710 ADO 00917. 81747** 4. BBB B2 684 10 34 S 0 061 A DO 7B473 38.1)48 *« 7 177 178 078 14,98 S 1 830 A DD <| 148667 87660** 6,0710 844 1487 84:47 4 0.800 ADD 843803. 36,067** 0.0811 818 1407 84:17 4 0 068 ADD 8360BB. 33,787** 7.0118 330 1183 10:43 0 0,718 ADD 87840 47.007** ID, B713 18B 017 0:37 1 0704 ADD 84189. 30.166** 6,7014 74 477 0:17 1 0717 ADD 4131. 1,080** 0.8319 188 787 18:07 8 1.006 ADD 4018. 0 U3S ** 0.18Id 148 033 13:93 8 1 147 A?DD 8419.. 0,666** 0.1917 147 1670 88:10 4 1,009 ADD 19109, 1.973** 0,3PIB 147 1330 88:10 9 1,000 ADD I7B78, 1.718** 0,43
NO RBTtL) RATIO RRT(L) RATIO AMNT AMNTtLI R, PAC R, PAC(L) RATIO1 7:07 0,77 1.000 1,00 40,00 40.00 1,000 1.000 1.00
IS: 11 0,117 1,000 1.00 4000 40.00 1,000 1,000 1,0016:44 0,/''7 1.000 1,00 40.00 40.00 1.000 1,000 1,00
4 8B:Q7 100 1,000 1,00 40.00 40i 00 1,000 1.000 1,000 SO: 38 0, V7 1,000 1,00 40.00 40(00 1.000 1.000 1.006 0:88 0,77 0,714 1,00 11.80 40,00 0,086 1,071
t 31
NO RCT(L) RATIO HRT(L) RATIO AMNT AMNT(L) P, PAC R PAC(L) RATIO/* 6 31 0 77 0 718r ' 10:87 0.77 0. B607 14:90 0,77 1,82010 84:93 1.00 0. 8B411 84:86 1.00 0,06018 18 90 077 071313 8:44 0. 77 0 79414 0 84 0 77 0 71B19 18 14 0, 77 1. 00416 13' 98 0 77 1. 14617 SB 10 1 00 I 009IB 28 16 1.00 1.077
00 81 79 90,00 0 618 1.374 0.44. 00 38, 39 90. 00 0. 300 0, 463 0,69. 00 87 67 90. 00 0 434 0. 738 0, 97.00 36.07 00.00 8, 8B7 3.173 0,78,00 3377 90,00 8,221 3 8B6 0.6800 47,01 90.00 0.077 0, OBI 0,7000 30,17 100.00 0.464 1.937 0,3000 1.03 90.00 0.046 8814 0.08CO 0.93 90.00 0012 1. 148 0.01
. 00 0. 67 90. 00 0. 007 0, 992 0.0100 1 97 90.00 0,148 4983 0.0300 1.72 90.00 0,098 1 396 0.04
OUANTITATION REPORT F1LK UNKO
A'A IFD7QO. Tl06/01/04 18:39:003AWLE: EPA/IFD CABE8640 MC7492 DNA (BA1 HB9-7BQ)SUIIMITTED DY: IFD ANALYST: EFP
AMOUNT-AREA • REP AMNT/IREP AREA)* REBP.PACT)RB8P PAC, PROM L1DRARY ENTRY
NO NAMEI D4-l,4-DICHLORODENZENE (IS 1-I/30/Q4 VERSION)8 METHANE. D1CHLORO- } y,tM jr3 CYCLOHEXENC ' ' '4 DB-NAPHTHALENG (C2 1 B. -1/20/04 VERSION)9 D10-ACBNAPHTHENE (C3 I B -I/80/B1 VERSION)6 D18-CHRYBENE (C4 1 S -1/80/04 VERSION)7 D10-PHENANTHRENE (06 1 S.-1/80/04 VERSION)
NO M/E SCAN TIME REP RRT METH AREA(HOHT) AMOUNT HOT1 RIC 944 7:04 1 1 000 ADD 483318. 40000 ** 1. 878 RIC IB1 301 I 0333 A DV 8847780:———81fc-9fl» 7.783 RIC 170 3:10 1 0347 A VD 18081100;"•• nTHrSTO BO. 704 RIC 789 18:09 4 1.000 ADD 681704, 40, 000 «» I. B79 RIC 77B 16:30 9 1 000 A DD 697034, 40 000 *« 1. 876 RIC 1601 SB: 01 6 1000 A DV 660803, 40,000** 1,077 RIC 1831 80:31 7 1.000 ADD 637038. 40,000 «« 1. 87
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|AMOI;NT«AREA • REF. AUNT/(REF, AREA)• REBP.FACTIIIIBBP, CAC. FROM LIBRARY ENTRYNO NAME1 DROnOCHLOROMBTHANBIVO LIBRARY IB)8 3-BRQMQ-l-CHLORQPROPANE (UY INTERNAL STANDARD)3 1,4-DICHLOROOUTANE (UZ INTERNAL STANDARD)4 D4-1,8-DICHLORO?THANE (SURR09ATB)0 OS-TOLUENE (SURROGATE)6 P-OROMOPLUORQBBNZENE (MB CHECK)7 CHLORQETHANEB DICHLQROMETMANE9 1.1-DICMUORQETHANE
NO M/B SCAN TINE REP RRT METH ARBA(HOHT) AMOUNT XTOT1 1SQ 834 7:88 1 1,000 ADD 6030B, 800.000** 3,378 77 4BO 16:00 8 1.000 A 00 13D17S, 800.000 «* 9,973 99 601 80:02 3 1,000 ADD 104140, 890,000 «« 9,374 60 897 9:94 i 1.386 A 00 60794, 801. 784 »» 9.41PI 00 634 81:08 3 1,090 ABO 14BB11,' 838, BIO «* 9,00
79 703 86:06 3 1,303 ADD 138900. 898,971** 9.487 64 11B 3:96 1 0.987 ADD 38088, OB, 098 ** 1,86B B4 103 0:06 1 0,683 A7BB 8696010, 3104,810 «« 66,699 63 847 8:14 I 1.103 ADD 4909, 0,870** 0. Ii
NO RKTtU RATIO RRT(L) RATIO AUNT AMNT(L) R FAC R,PAC(LI RATIO1a34967(19
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[ 1ATA: IPB79QV Tl19/10/84 10 46:00
|3Af"\E: IFD VOA SAMPLE BAIN 09-79Q, BMON C9493. CABEN 8640tUUrllTTED DY: BPA ANALYST: RJM
«MOUNT«AREA « REF, AMNT/( REF, AREA)* REBP. FACT)FAC. FROM LIBRARY ENTRY
NO NAME1 OROnOCMLOKOMETHANEIVO LIBRARY IB)8 8-OROnO-l-CHLOROPROPANE (UY INTERNAL STANDARD)3 li4-DlCHLOROOUTMIE <UZ INTERNAL STANDARD)4 CYCLOTRIBILOXANEiHEXAnETHYL- G
NO H/E BCAN TIME REK RRT PIETH AREA(HOHT) AMOUNT XTOTI RIC 884 7:88 1 1,000 ADD 3739B4, 890,000** 11.768 RIC 4B1 16:08 S 1,000 ABB 36B044, 890.000** 11,763 RIC 601 80:08 3 1,000 ADO 189018, 890,000** 11,764 RIC 7B9 86:10 3 1,306 ABB 101B190, «i*-W-- 64,78
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PA,A: IFD790. TI06/09/B4 10:47:00SAMPLE: 1FO D/N/A SAMPLE BA1H 09-79Q, BMON C9493, CASED B640'SUBMITTED BY: EPA/IFD ANALYDT. RJM
AMQUNT«AREA » REF AMNT/(REF AREA)» REBP.FACT)RG9P PAC FROM LIBRARY ENTRY
NO NAME1 D«-li4-DlCMLOROBENZGNE (I B. 1-I/30/B4 VERQ10N)8 DO-NAPHTHALENE (C8 I S -1/20/04 VERSION)3 D10-ACENAPHTHENE (C3 1 3 -1/80/B4 VERSION)4 D12-CMRY9ENE lC4 I.Q -I/SO/01 VERSION)9 DIO-PHENANTHRENE <Cb 1 B -1/20/04 VERSION)6 D9-PMENQL (ACID BURROOATE)7 2-FLUOROPMENOL (ACID BURROOATE)B D9-N1TROUENZENE (D/N BURROOATE)9 2-FLUOROOIPMENYL (B/N SURROGATE)10 D14-P-TER PHENYL (SB I11 D10-PYRENG (B, B )12 2,4,6-TRIDROMOPMENQL IB S )13 B1S(S-CHLOROETHYL)ETMER14 8-CHLOROPHENOL15 PHENOL16 Dl-N-DUTYL PHTHALATE
NU M/E SCAN TIME REF RRT METM ARHA(HUHT) AMOUNT '/.TOT1 192 940 9; OB I 000 ADD 93700, 40.000** 7,692 136 731 12:11 8 000 ADD S80W 40 000 •« 7,693 lt>2 1003 16:43 3 000 ADD 109439 40 000 *« 7.600 240 160B 80: OB 4 .000 A?DD 63918 40.000** 7.609 I OB 1236 80,36 9 000 ADO 806199 40 000 •» 7,60o 99 903 B 23 I 0 910 A BO 7B89S. 3" 537 ** 7,06' 112 39!l 6:33 1 0717 ABO 70921 49. 090 •» B, 68Q £12 63" 10:29 2 0 060 A 00 97933, SO 0.10 • » 9 78<9 172 B"7 14:97 2 1 287 A BD 95493 2(> Q75 »• 9,7110 244 1492 84:92 4 0 064 ABO 101020, ?3 072 «• 4,97II 212 I4o9 8429 4 0 060 ABO I039Q9 R/l W •• 4.60U 330 1120 1Q 4S 9 0.913 ABO 1B44B, 37 362 »« 10,9713 '93 91B B:3B I 0 H>49 ADO 6636, 8701 •» 0,0814 120 984 0:44 I 0996 ADD 00403, >|4 83B «« 8,4619 «4 909 8:89 I 098. ADO 63B9, 2.399** 0,4016 149 1334 88:14 0 1079 ABO 17499, 8.904** 0,48
NO HETILI RATIO RRT(L) RATIO AMNT MINT(L) R FAC R, FAC(L) RATIO9 09
2 il2'OQ3 16.484 SO OB9 80:39' QiI9V 6:260 10:879 14:9710 84:91
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000 1,00000 1, 00OOQ 1,00000 1,00000 1,00467 0.99160
00 90,04 90,00 0393 034700 89,08 90,00 0,346 0,978 0.6000 83.07 90.00 1,893 8.700 0.40
M) RET(L) RATIO RRT(L) RATIO AMNT AMNT(L) R.PAC R. FAC(L) RATIO^1 24:89 1,00 0.069 1,00 84.90 90,00 1 391 8. 79B 0,4912 18:46 1,00 0.913 100 97.36 90.00 0072 0062 1,1913 8:39 1,01 0,949 1.00 2.70 9000 0.090 1080 0,0914 8:12 1.00 0. 990 1.00 44,24 9000 1.191 1.347 0, BB19 022 1.01 0921 1 00 236 9000 0099 2007 0.0916 22.13 1 00 1.079 1 00 8.90 90.00 0,060 1.393 0,09
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1FDV9Q, Tl06/09/04 10 47:00SAMPLE 1FB 0/N/A SAMPLE 8A1H 03-/90, SMON C9493i CABGM 2640SUBMITTED DY: EPA/IFB ANALYST' RJM
AMOUNT-AREA • REF AMNT/tREF AREA)* KEEP,FACT)REBP FAC. FROM I.10RARY ENTRY
NO NAME1 1)4-1,4-D1CHLORUDENZUNG (1 6 1-1/30/04 VERSION)2 METHANE,D1CHLORO-\ fifl/., K7r-3 GTHENE.TRICHLORO-v' '*A(vn4 1-PENTYN-3-OL,4-METHYL-9 DB-NAPHTHALENE (C3 1-6 -1/20/04 VGRB10N)6 8H-AZEPlN-2-ONE,MIUAHYDRO-7 PHENOL, 4-1 h I-D1MGTHYLETHYD-B PHOBPHOIUCTR1 AMIDEi HEXAMET.HYL-9 DIO-ACBNAI'HTHENE (C3 I B -1/80/04 VERSION) " • '10 D12-CHRVBQNE <C4 l.S -1/20/64 VERSION)11 D10-PHBNANTHRBNE <C6 1 B,-1/80/B4 VERSION)
MO M/E BCAN TIME REF RR1 METH AREA(HOHT) AMOUNT 7.TOT1 RIC 519 9 00 II 000 A OD 362304, 40.000 ** 9,702 RIC 203 3 25 I 0 374 A DV 1667380 104 040v . j86,883 RIC 212 332 I 0.307 AW I71HOO, 160, 672 ™" 36,91
RIC 3?9 6 19 1 J 69! A DD ' 135224 14.986 2,13000 A DV 409986. 40, 000 ** 9. 70OB9 A DD 070864 ' 71 696 10,88180 A OD 191460 15, 773 8,89|A| A OD 388470. 26 967 3,7?000 A OD 938640 40. 000 *« 9,70000 A UD 469794. 40 000 »« 9,70000 A DD 490460. 40 000 ** 0, 70
« RIC 731 12.11 96 RIC 793 13.13 57 RIC 019 13 M 9B RIC 034 1394 99 RIC 1003 1643 910 RIC 16QO 80 00 1011 RIC 1836 20 36 II
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AMOUNT«AREA « REF, AMNT/IREF. AREA)" RB8P, FACT)REBP FAC. PHQll L1DRARY ENTRY
NO NAME1 DRDMOCHLOROMCTHANE(VO LIORARY IB)S B-QROnO-1-CHLDRQPROPANE (UY INTERNAL OTANDARD)3 1.4-D1CHLOROOUTANB <UZ INTERNAL STANDARD)4 D4-1,8-D1CHLOROSTHANR (OURROOATB)9 DB-TOLUENE (BURROOATE)6 P-OROI10PLUOROORNZENB (118 CHECK)7 DICHLOROMBTHANE
NO M/B 8CAN TIME REF RRT METH AREAIH8HT) AMOUNT XTOT1 130 S88 7:84 1S 77 479 19:98 i!3 99 600 30:00 34 60 ST9 9:00 19 100 633 81:04 36 99 703 8606 3
. 000 A DO 64638. 890, 000 «« Id, 47.000 A 00 134961, 890,000 «» Id, 47000 A 00 109303. 890.000 «» U. 47389 A 00 6930V. 393. 469 «* Id, 63093 ADD 146033, 330, 966 «* 14. W309 ADD 133Q87. 840, 700 «» IB.
7 04 198 9:04 . 1 0.609 ADD 48017. 40, 894 »» 3,88
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NO NAMC1 DR(]l10CHLOROnETHANS(VQ LIDRARY IB)8 3-DRQMO-l-CMLOROPROPANE (UY INTERNAL STANDARD)3 li4-01CHLOROBUTANE (UZ INTERNAL STANDARD) Q4 CYCLOTRIB1LOXANB. HEXAMETHYL- C Jt--, W**0
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AMOUNT-AREA • REF, AMNT/IR6F. AREA)* REBP,FACT)REBP, FAC. FROM LIDRARY KNTRY
NO NAME1 D4-1.4-DICHLORODSNZENE 11 B, 1-1/30/04 VERSION)8 DO-NAPHTHALENB <C8 l.B -1/30/04 VERSION)3 D10-ACENAPHTHENE (C3 IB -1/30/04 VERSION)4 D18-CHRY8BNE <C4 l.B. -1/30/B4 VERSION)9 D10-PHENANTHRENB (C6 l.B,-1/80/84 VERSION)6 D9-PHENOL (ACID 6URROOATE)7 D9-NITRODENZENE (D/N BURROOATE)6 8-PLUOR001PHENYL (D/N BURROOATE)9 D14-P-TBR PHENYL (B. B, )10 D10-PYRBNE (B. B, )11 8-CHLOROPHENOL18 DI-N-DUTYL PHTHALATB
NO M/B BCAN TIME RBF RRT METH AREA(HOMT) AMOUNT XTOT198 944 >>:04136 787 18:07
,3 168 1001 16:41 34 840 1604 SO:04 49 IBS 1834 80 34 9
000 A 110 93613. 40.000** 10,94000 A?OD 806136, 40, 000 «* 10. 94000 ADD OB94B, 40,000** 10,94000 ADD 40947, 40,000** 10,94000 ADD 160661. 40,000** 10.94
6 99 497 8:17 1 0914 ADO 6707. 3.886** 1,067 88 689 10:89 8 0.060 ADO 604B1, 33. 184 «« 8.00B 178 099 14:99 3 1,831 ADD 103987. 38,788 «« 8,999 844 1409 84:49 4 0084 ADD 100005, 48,999** 11,7610 818 1468 34:88 4 0.060 ADD 117187, 49.733 «« 18,0011 130 019 0:39 1 0.994 ADD 0960, 4.941 «« 1,8418 149 1338 88:18 9 1.079 ADD 19168, 3,698** 1,01
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00 40.00 4000 1 000 1,000 1,0000 40.00 40.00 1 000 1,000 1,0000 40,00 40.00 1,000 1,000 1,0000 40,00 40.00 1.000 1,000 1,0000 40,00 40.00 1 000 1,000 1,0000 3.09 00,00 0,103 1,380 0.0000 ,38,18 00,00 0,830 0,369 0.6400 38.73 90.00 0,403 0616 0,6900 43,00 90,00 1,909 8,313 0,0600 40,73 00,00 3,311 8,087 0,9100 4,04 90.00 0,130 1,430 0,0900 3,69 90,00 0,099 1,898 0,07
023480
QUANT 1 TAT ION REPORT PILE UNKO
1FDOOO, Tl09/31/04 9:94:00BAMPLE: 1PD 0/N/A BAMPLE BAlll Q9-QOO. OMOK C9494. CA3BH 8640BUDMITTED OY: IFD ANALYST: RJM
AMOUNT-AREA • REP. AMNT/IREF, AREA)* RESP.FACT)REBP. FAC. PROM LIDRARY ENTRY
NO NAME1 D4-I,4-D1CHLORODENZSNE (1 B 1-1/30/84 VERSION)8 METHANE, 01 CHLORO- \^ttltt^r3 CYCLODUTANE. BTHBNYL-4 DB-NAPHTHALBNE (C8 1,B -1/80/04 VERSION)9 D10-ACBNAPHTHENE <C3 1. S -1/80/84 VERB I ON)6 D13-CHRYBENE <C4 1,8-1/80/04 VERSION)7 DIO-PHENANTHRENE (C6 1 B -1/80/84 VERSION)
NO M/B SCAN TIME REP RRT METH ARBA(HOHT) AMOUNT HOTI RIC 944 9:04 1 1.000 A OD 3794BB. 40.000** 1,468 RIC 101 8:31 1 0878 ADD 10037800. "14367380' 98.493 RIC 104 3:04 1 0.330 ADD 7700990. -4*06-1-90— 40.844 RIC 787 18:07 4 1.000 ADO 410348. 40000** 1.469 RIC 1001 16.41 9 1 000 ADD 439393, 40 000 «« 1,466 RIC 1604 38:04 6 1 000 ADD 301970, 40,000 *• 1.467 RIC 1834 80:34 7 1,000 ADD 376638. 40.000** 1.46
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023474
| aUANTITATlON RBPORT PILE VOUNKO
DATA: 1FD010V Tl09/10/64 12:06:00tttMPLE: IFD VOA BAMPLE BAIN 09-010, BMQIt C'M9D. CAOK» 3640B MITTBD DY; EPA ANALYST: RJT
AMOUNT-AREA * REF,AMNT/IREF. AREA)* RESP.FACT)REBP, FAC, FROM LIDRARY ENTRY
NO NAME1 OROnQCHLOROMETHANEIVO LIDRARY IB)8 8-DROMO-l-CHLOROPHOPANE (UY INTERNAL BTANDARD)3 1,4-DICHLORODUTANE (UZ INTERNAL BTANDARD)
HO M/6 SCAN TIME REF RRT METH AREA(HOHT) AMOUNT XTQT1 RIC 884 7 SB 1 1,000 ADD 370111, 890,000** 33,338 RIC 401 1608 8 1.000 ADD 3988B7. 890,000** 33,333 RIC 601 8008 3 1.000 A D O . 169479. 890,000** 33,33
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AMOUNT»AREA « RGF AMNT/IREF AREA)* RE6P FACT)REBP. FAC FROM LIDRARY ENTRY
NO NAMEI D4-1,4-DICMLORODCNZENII I I 0, 1-1/30/U4 VBRB10N)8 DB-NAPHTHALENE IC8 I Q -1/80/04 VERSION)3 D10-ACENAPMTHBNE <C3 1 S -1/80/64 VERSION)4 D18-CHRYOBNE (C4 1,B -1/80/04 VERSION)9 D10-PHENANTHRENE <C6 1 0 -1/80/04 VERSION)6 D9-PHENOL (ACID SURROQATEI7 8-FLUOROPHENOL (ACID SURROOATEI6 D9-NITRODBNZBNB (D/N SURROGATE) •• , •7 8-FLUORODIPHBNYL (D/N BURROOATE)10 D14-P-TER PMENYL (B. 6. I11 D10-PYRENE (89)18 8, 4,6-TRlDROMOPHENOL IB S )13 8-CHLOROPHBNOL14 PHENOL
NO M/B SCAN TIME REF RRT MBTH AREA(HOHT) AMOUNT '/.TOT*1 198 947 707 II 000 ADD 97388. 40,000** 7,64W8 136 731 12:11 8 1000 ADD 889803, 40000** 7,64
3 168 1009 16:49 3 1000 ADD 110733. 40, 000 «« 7,644 840 1607 86:07 '! 1 000 A?DD 60010 40,000 ** 7,649 166 1837 80:37 9 1 000 ADD 883300, 40,000** 7,646 77 908 688 1 0914 ADD 78837. 31780** 6,107 118 370 6.30 1 0710 ADD 71614. 40. 694 »« 7. BO0 68 687 10:87 8 0660 ADD 74773. 411 171 «* 7,807 178 070 14:96 8 1.886 ADD 107770, 38,131 "» 6,1410 844 1473 84 93 4 0 009 ADD 164068, 37841 •« 7,47II 818 1466 84:86 4 0 067 ADD 167179. 40 303 »» 7,7118 330 1187 16:47 9 0713 ADD 17636. 90.401 ** 7,6313 186 984 6 44 10 794 A DD 70697, 36 631 ** 7 4114 74 903 6:83 1 0716 ADD 9803, 1, 717 ** 0,33
NO RET(L) RATIO RRT(L) RATIO AMNT AMNT(L) R. FAC R.FAC(L) RATIO1 7.098 18:073 16:434 86079 80:366 6:817 6:306 10:8B7 14:9610 84:91.11 84:841,8 10:4813 6:4114 0:80
,01,00,0000,00
,000 1,00 40,00 40,00. 000 1, 00 40, 00 40, 00, 000 I 00 40. 00 40, 00000 1 00 40,00 40.00
,000 1.00 40,00 40,00.00 0,716 1.00 31,78 40,00
000 1,000 1,00000000
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00 0.713 i 00 40,69 90.00 0.766
000 1,00000 1,00000 1,00000 1, 00986 0,001P8 0.08
, 00 0.061 1 00 4P 17 90, 00 0. 337 0, 390 0,76,00 1,887 1,00 38,13 90.00 0.370 0,607 0,64,00 0,091 100 37,84 90,00 1.707 8,430 0, 7B,00 0,660 1.00 40,38 90,00 1767 8,439 0,61,00 0,713 1,00 90,49 90,00 0,063 0,063 1,01, OH 0,796 1,00 30,03 90,00 1.061 1,366 0,7(301 0,717 100 1,78 90,00 0070 8,043 0,03
023488
OUANTITATION REPORT FILE UNKO
1FDB1Q. TI06/04/Q4 746:00SAMPLE: IFD fl/N/A BAMPLE BAIN 69-010, BMON C7499, CAGEH 8640BUOMITTED DY: IFD ANALYST RJM
AMQUNT»AREA • REF. AMNT/IRCF AKCAIt REBP FACT)RE8P. FAC. FROM LIDRARY ENTRY
NO NAMEI D4-I,4-DICHLORODENZENE (I B 1-1/30/04 VERSION)S CYCLOPENTANOL.S-METHYL-3 DB-NAPHTHALENE ics i B -1/20/54 VERSION)4 DlO-ACBNAPHTHBNE (C3 1 S -I/20/B4 VERSION)9 D18-CHRY8ENE IC4 I Q -1/80/64 VERSION)6 D10-PHBNANTHRENE IC6 1 6 -1/20/84 VERSION)
NO M.'E SCAN TIME RBF HRT METH ARBA(HOHT) AMOUNT '/JOT1 RIC 947 7:07 11 000 A 00 390064 , 40,000 •« 13 618 RIC 403 6:43 1 0734 A DV 881313 73847 31 743 RIC 731 IK: 11 3 I. 000 ADD 9397B4 40,000** 13614 RIC 1009 16:49 4 1000 ADO 604410. 40.000** 13.619 RIC 1696 86:06 9 1000 ADD 966676, 40,000** 13,616 RIC 1837 80 37 6 1 000 A DD 964776 40.000 «« 13.61
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OUANTITAT10N /WORT PILtt, TOPIC
TI05/10/Bt IS:91:00BAWLE: IP'0 VOA BAMPLE BAIN BO-020, BMOH C7496, CABEd 2640SUBMITTED DY: EPA ANALYST: RJT
AMOUNT-AREA • REP. AttNT/(REP. AREA)* REBP. PACT)RBBP. PAC. PROM LIDRARY ENTRY
NO NAMEI DROnOCHLOROrtSTHANIIIVO LIBRARY IB)8 8-DROMO-l-CHLOROPROPANE (UY INTERNAL STANDARD)3 1,4-DlCHLORODUTANE (UZ INTERNAL BTANDARD)4 D4-l,2-DlCMLOROBTHAN(t (BURROOATE)9 DB-TQUUENE (BURROOATE)6 P-DRQMOPLUORODBNZENE (MB CHECK)7 CHUORO&THANE0 DICHLOROMBTHANE9 I,1-DICHLOROETHANE10 TRANB-I,S-D1CMLORD6TH6NB11 BBNZBNB18 MVP-X"LENEB (HBL)13 , 0-XYLKNE (HBL)
NO n/E BCAN TIME REP RRT METH AREA(HOHT) AMOUNT »TOTI 18B 889 7:30 I*77 4Q1 16:08 S
90 601 80:08 34 69 870 9: 96 19 100 634 81:08 3
000 A 00 68406. 890,000 *« 13. ft000 ADO 130699. 890,000 »« 13,77000 A OB 101903, 890.000** 13,77384 A 00 63347. 893,376 ** M, II099 A 00 13B717, 388,700** 18,41
6 70 7B4 86:00 3 1,304 A OB 131199, 844603** 13,677 64 183 4:06 1 0.947 A 00 D0864, 76,090** 9,370 04 190 916 1 0,708 ADO 89091, 31,119** 1,719 63 84D Q: 16 I 1.108 ADO 14310 16,070** 0,7010 76 870 7:00 I 1,800 ADD 1163, 8,171 «« 0,18II 76 446 14:98 8 0.787 A 00 47477, 31,304** 1,7918 106 683 87 86 3 1.367 A7DV 83017, 67,643 «* 3,00H 10* B44 80.08 3 1,404 A OB 33407, 71.609** 4,01
NO RgT(L) RATIO RRT(L) RATIO AMNT AflNT(L) R, PAC R.PACIL) RATIOI 7: IB£ 16:003 80:00>1 7:469 81:OB6 36:067 3:3BB 4.967 0:0610 0:4011 14:4018 87:861.1 80:04
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LOUANTITATION IMPORT FILE VOUNKO
DATA: IfOBSOV, Tl09/10/04 13:91:008W1PLB; IFD VOA SAMPLE SAIM 09-080, BtlOH C7496( CA8EK 8640
DY: SPA ANALVOT: RJT
AHOUNT«AREA • REF. AMNT/< REF. AREA)* RE6P, FACT)REBP. FAC. FROM LIDRARY ENTRY
NO NAME1 DROnOCMLOROtlETHANElVO LIBRARY IQ83 ETHANE, 1, l'-OXYDID-4 8-DROI10-I-CHLOROPROPANE (UY INTBRMAL STANDARD)9 1,4-DlCHLORODUTANB (UZ INTERNAL QTANDARD)
7 BENZENE, I, 3-DKI1ETHYL-
NO M/B BCAN TIME REF RRT METH ARBA(HQHT) AHOUNT HOT1 RIC 886 7,38 1 1.000 ADD 313987, 300 000 «« 11,018 RIC 149 4:90 I 0,648 ADD 144096. -Wr-TOT" 4. U3 RIC 800 7:80 14 RIC 401 16:08 49 RIC 601 80:08 96 RIC 7QO 86:10 97 RIC 083 87.86 9
S37 A DD 338334. 144/061 6,000 ADD 360840. 800,000** 11,00000 ADD 177837, 800,000** 11,011'306 A DD 037B30. «-M«irrW—' 08, 38367 A 00 60660. BO. 063 3, 77
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(B 19D 8N OT)
31331 BPBCTRA IN LIDRARYNO SEARCHED FOR MAXIMUM PURITY69 MATCHED AT LEAST 7 OF THE 18 LARGEST PBAKB IN THE UNKNOWN
RANK IN NAME1 837 ETHANE, 1, 1 '-OXYD1B-8 8360 ETHANE, 1,8-D I GTHOXY-3 986 1-PROPENE, 1-METHOXY-S-METHYL-
HANK FORMULA M, HT P PK PURITY FIT RFITI C4 H10, 0 74 97 760 760 7778 C6. H14.08 HO 97 709- 709 7603 C9, H10. 0 06 49 719 788 760
RANK RET TIME B. P INT. UB. PAR, 1 UB, PAR, 8 C.A, B, HI __ __ 60-87-72 ™ H __ __ 687-14-13 ~ ~ __ _ l"7074-B4-4
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(B I9D 8N OT)
31331 SPECTRA IN LIORARYND SEARCHED FOR MAXIMUM PURITY839 MATCHED AT LBABT 6 OF THE 14 LARGEST PBAKB IN THE UNKNOWN
RANK IN NAMEI 1439 DBNZENB, 1, 8-DIMETHYL-2 1437 DENZBNB, 1, 4-DIMBTHYL-13 H3B DBNZENB, 1, 3-DIMETHYL-
RANK FORMULA M, WT D. PK PUKITY FIT RFIT1 CO. H10 106 71 747 790 7742 CB. HIO 106 71 741 748 7663 CB. HIO 106 91 736 743 769
RANK RET. TIME D, P 1NT, UB, PAR, 1 UB, PAR, 8 C,A. B, «I 70-47-68 — — —— 106-48-33 ~ ~ HI __ " 10B-3B-3
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A: IFD02Q Tl06/01/04 17:37:00BAMPLE: KPA/IFD CABE 2640 IIC9056 DNA (BA1 HOD-02Q)BUDM1TTED HY' IFD ANALYST EFP
AMOUNT-AREA • REF APINT/(REF AREA) • REBP.FACT)HEBP FAC FROM LIBRARY ENTR!
NO NAMKI DO-1,0-DICHLORODENZENE (IB 1-1/30/01 VERSION)2 DO-NAPMTHALENE IC2 1 8.-1/20/UO VEROION)3 D10-ACENAPHTHBNB (C3 1.S.-1/80/84 VERSION)4 D12-CHRY6ENE (C4 l.B -1/20/04 VERSION)9 DIO-PHBNANTHRBNB iC6 i B -1/20/04 VERSION)6 DO-PHENOL (ACID BURROOATE)7 2-FLUOROPHENOL (ACID SURROGATE)B D9-NITROIICNZENE (D/N SURROGATE)7 2-FLUORODIPHENYL (D/N BURROOATE)10 D14-P-TER PHENYL (B. B )II D10-PYRBNE ID.B, )18 8,4,6-TRlPROMOPHENOL (0.0 )13 DlBtS-CHLOROETMYDETHKR14 8-CMLOROPHENQL19 PHENOL16 1,3-DlCHLORODCNZEME
1,0-DlCHLORODGNZBNEB-METHYLPHENOL
17 DENZYL ALCOHOL (HDD80 IBOPHORONG81 814-D1MBTHYLPHENOL88 NAPHTHALENE23 DIB(8-BTHVLHEXYLIPHTMALATB8-1 Dl-N-UUTYL PHTHALATE
NO M/E SCAN TIME HEF RFIT METH AREA(HOHT> AMOUNT '/,TOT1 192 O'tB 1 00 11 000 A OD 66667, '10,000 •• 7 722 136 731 12.11 8 1000 A PD 848698. 00 OOP •• 7783 162 1001 Id 44 3 I 000 A DD 120160. 40.000 »• 7.784 840 I6B6 20 06 4 1,000 A?OD 77181. 40.000 M 7.739 100 1236 20:36 9 1000 ADD 898741, '10 000 *« 7786 97 900 0:20 1 0 723 A?DV 01799, 24 091 «• 4,017 112 374 6:34 1 0717 ADD 71790, 36099** 6,760 02 687 10:87 8 0060 ADD 70607, 00004 »« 7,749 172 676 14:90 8 1,280 ADD 70110, 86.346** 0,0710 240 1071 20 91 0 0 064 A DD 131707, 26,936 *« 0,80II 211"! 1464 SO 84 0 0, 06Q ADD 186019, 20,394 •« 4,0012 330 1186 1000 9 0913 ADD 80078, 07. 977 »» 7,0713 ?3 017 0,37 1 0,903 ADD 9300, 8, 977 »» 0,0710 130 939 0 05 1 0990 ADD 74769, 33,408 *« 6,4019 94 907 0:87 1 0920 ADD 80036, 9736** 1 , 1116 146 901 711 I 1.009 ADD 80676, 0,170** 1,0017 146 091 7:11 1 1000 ADD 30676, 0,800** , 1,07JH> 100 909 'MD I 1060 ADD 0280, 3. 7,'. 4 »» 0,73\1 10D 000 7,00 I 1.06B ATDII BSSO, 7. 300 «« 1,4180 08 660 11:04 8 0,70B A?VD It I SO, 1,000 »« 0,80
023517
NO M/E OfAN TIME HEP IIRT METH AREA(HOHT) AMOUNT '/.TOTfasi 122 602 11:22 2 0933 A7DV 19967. 7 760 •• 1,90
22 120 734 18:14 2 I 004 A DD 31909 4 604 »• 0,7023 107 1679 20:19 0 1009 ADD 13762. 2. 74B ** 0.9324 149 1334 2S: 14 9 1.077 ADD 24193, 2.949** 0.97
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M 95 704 B6.00 3 1300 ADD 11B737, 817,010*1 18,61vf , 04 198 0:04 1 0,671 ADD 7034. 18,03B «« 0,70Q 43 300 10> 10 1 1306 ADD 16DQ7. 100,4B3 *« 6.131 68 277 794 1 1,300 ADD 44603, 04. 106 »« •!. B7
NO RETIU RATIO RRT(L) RATIO APINT APINT(L) R, PAC R. FAC(L) RATIOi 7£ 163 SO'1 79 81* S67 40 109 7
IB000046000696OSOS
00000000000003 C01.00
.000000.000330.097,309676.374,308
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800,800,800,8B7,868,817,18,
100,04
000000104001B446IV
890890890,890,890,890,890,390,890
000000000000000000
1.0001.0001.0001. 1971.B761. 1460, 1710,8600,776
1.0001,0001.0001,0001,8341.3803,3840. 60S8 303
1,001,001.001, 161.000, 970,000.480. 34
31
•OUANTJTATION RBPORT F1LC VOUNHD
DATA: IPD03QVA Tl09/10/B4 16:17:00
: IFD VOA SAMPLE SAID B9-B3Q, BMOIt CV497, CABEK 3640 (RE-RUN)JPIlTTBD BY: BPA ANALYST: RJM
AMOUNT-AREA * REF,AMNT/(REF. AREA)* REBP,FACT)REBP, FAC. PROM LIDRARY ENTRY
NO NAME1 DROMOCHLOROMETHANEtVO LIDRARY IB)8 S-DROMO-1-CHLOROPROPANE (UY INTERNAL BTANDARD)3 li4-DlCHLORODUTANE (U2 INTERNAL BTANDARD)4 PENTANE,3,3,4-TRIMGTHYL-
NO M/E BCAN TIME REF RRT MGTH ARBA(HOHT) AMOUNT XTOT1 RIC 880 7:80 1 1.000 ADD 330163 890000** 16,788 RIC 408 16:04 8 1000 ADD 34Q738, 890,000** 16.733 RIC 603 80:06 3 1,000 A DV 130017. 800,000** 16,734 RIC 616 8033 3 1088 A VD 347370. 737.040 47,34
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iMTA IPDB30, TI06/09/84 14:27:00BAMPLE. EPA/If'D CASE 2640 HC7497 DNA (BA1 HB9-03Q)BUOMITTCD DY: EPA/1FO ANALYDT EFP
AMOUNT-AREA • REF AMNT/UIEF AREA)* REBP FACT)REBP PAC, FROM L1URARY ENTRY
NO NAMEI 1)4-1,4-D1CHLORODENZENE <! 0 1-1/30/04 VIIRQIONI2 DU-NAPHTHALENII (C2 1 S -1/20/04 VBRBION)3 1)10-ACENAI>MTHENB <C3 IB -1/20/84 VERSION)4 D13-CHRYUCNE (C4 l.B -l.'80/04 VERSION)9 DIO-PHENANTHRENE IC6 ! S -1/20/04 VERSION)6 D9-NlTrtODEN2ENC (0/N SURROGATE!7 2-FLUOR001HHENYL (0/N SUMROOATE)B D14-P-TBR PHENYL (B S )7 010-PYRENG (B B '
11 i,4-DICHLORODENi!GNE12 NAPHTHALENE13 OIB(2-ETHYLHEXYL)PHTHALATB14 Dl-N-DUTYL PMTHALA1E
NO M.'B SCAN TIME RC" I1RT MKTH AREA(HOMT) AMOUNT '/JOT£ I 192 946 * 00 1 t 000 A DO 64340 40 000 •« 10 74~S 136 727 1207 2 I 000 ADO 239344 40000 •» 10.74
3 162 1003 16 42 31 000 A 00 111317 40 000 «* 10.744 240 1609 2Q.09 14 1 000 A'DD 00003 40. 000 «• 10.749 100 1239 2039 9 1000 ADO 331670. 40 000 «« 10.746 02 627 10 27 20 060 A 00 77342. 311. 7B4 •• 10. 487 1"2 076 14 96 2 1 227 A OD 129494 36 070 *« 7.70Q 244 1470 24 90 4 0 QB4 ADD 214074. 39 137 »• 10,917 813 1463 24 23 40 06Q A DD 310306 n 744 «« 10. 1410 14s, 94" " 0" 11 003 A DD -f#*M—————1-19\-*» 2 2111 |A6 94» i 0" 1 1 002 A 00 l'»409 f ''63 t« B 1412 li'fl 732 12 12 2 1 004 A DO 3039 0 439 «• 0, 18ID 147 1644 1Q 14 4 1009 ADO 10061 2,!|e>«« 06914 14w |333 2B.13 9 1 077 ADD 6068 9 "»9 •• 031
NO RET(L) RATIO RRT(L) RATIO AMNT AMNT(L) « I'-\C H PACIL) RATIO1 709 1,01 1,000 1,00 40,00 4000 I 000 1 000 1,002 1800 1,00 1.000 1,00 40,00 4000 I 000 1 000 1.003 16 42 1 00 I 000 1 00 40,00 40.00 1 000 1.000 1,004 SB 09 1 00 1.000 I 00 40 00 40.00 1 000 1 000 1,00I) 3039 1,00 1 000 1 00 40,00 40.00 1 000 1 000 1,00b 1087 1 00 0060 1 00 30,70 90,00 0267 0347 0,7.17 14 97 1.00 1.330 1 00 P6, 07 90 00 0 436 0 570 0,740 2491 1 00 00134 I 00 37 14 90,00 S II" 2700 0, 7B7 2429 I 00 0,06'' 1 00 3774 90.00 B 0(18 2 790 0,7910 7 01 I 01 0773 1 01 0,23 9000 0 »48 1 46Q 0,16.11 7 OP 1.00 1.006 1 00 7,76 9000 0 RIB 1 917 0,16
P1B 1 8 1 1 100 1004 1,00 0,43 90.00 0010 1 103 0,0113 20 14 I 00 1 000 100 2,48 90,00 0100 8061 0, Q!)14 88 13 I 00 1.077 1 00 0,77 90,00 0 031 1 393) '
3,
OUANT1TAT10N REPORT FILE UNKQ
A IFD03Q. Tl06/09/04 14:37: 00BAMPLE: BPA/1FO CABB 8640 NC7497 ONA (OA1 H09-Q3QIBUDM1TTED DY; EPft/IFO ANALYST' EFP
AMOUNT-AREA • REF, AMNT/IREF AREA)* REBI'.FACTIREBP, FAC, FROM LIDRARY ENTRY
NO NAME1 D4-1,4-DICMLORODEN2CNE (IS 1-U30/B4 VERSION)8 METHANE, DICHLOHO- -s «./„,,,_ r3 ETHENB,TETHACHLORO- '4 l-PROPBNE,3,3'-OXY01B-9 DB-NAPHTHALENE (C3 1 S -1/30/B4 VERB ION I6 FURAN.3. D-DIBTHYLTBTRAMVOnO"7 DiO-ACENAPHTHENE <C3 1 S -1/30/Q4 VERSION)0 DI8-CHRYBGNB (C4 IB -1/30/B4 VERSION)7 DIO-'PHI'INANTHRBNE (C6 1 B -1/30/04 VERSION) ' . •
NO M/B BCAN TIME REP RRT METH ARBA(HOHT) AMOUNT XTOT1 RIC 940 7.OB 1 1000 ADD 461904, 40,000** 6,368 RIC 209 3:39 1 0374 ADD 3707110, 24! 700 W fJa, 443 RIC 383 933 1 0907 ADO 970672. 91 106' B, 144 RIC 377 617 1 0 6BQ ADD 177904 19,307 8,499 RIC 737 18 07 9 1 000 A DO 967824 40 000 «« 6,366 RIC 790 12:30 9 1'040 ADD 1707000 130.917 17,17
• 7 RIC 1002 16:48 7 1 000 A DD 977670. 40 000 »• 6,360 RIC 1606 8B 06 n 1 000 A VV 617160 40 000 *« 6,367 RIC 1839 20:39 7 1000 ADD 977840 00. 000 «« 6,36
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MA- ."*Yi——lj>>ltl< '"""'——————— —————"L-'T- CONCJNTRAriONi 10* MIDIUM IIIQM (CllcilDnil
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CONC./DIIUUCN PACTOKl
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PERCENT MOIiTUHti i
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INTITAT10N REPORT FILE:
DATA: 1FD04QV, TI09/10/84 17:00:00SAMPLE: IFD VOA BAMPLG SAIN B9-B4Q, SMOH C949B, CASED 26403UOM1TTED DY: EPA ANALYST: RJtl
AMOUNT-ARBA * REF. AMNT/IREF. AREA)* REBP. FACT)RCBP, FAC, FROM LIDRAHY ENTRY
NO NAME1 DROItOCHLORQMBTHilNBIVO LIDRARY 10)8 8-DROI10-1-CMLQROPROPANE (UY INTERNAL BTANDARD)3 1,4-DICHLOROOUTANB (UZ INTERNAL STANDARD)4 D4-I.8-DICHLORQETHANE (BURROOATE)9 DB-TOLUENE (BURROOATE)6 P-DROnOFLUORODBNZBNE (MB CHECK)7 DlCHLOROnSTHANE
MO n/B BCAN TIME RBF RRT METH ARBA(HOHT) AMOUNT XTOT1 186 880 7:80 1 1,000 ADO 94691, 390.000 «« 16,40.8 77 47B 19:96 8 1,000 A DD 130769, 890,000 *» 16.403 99 996 19:96 3 1.000 ADD 109687, 890.000 •« 16.404 69 894 9:46 1 1 336 A DD 60961, 876,701 ** IB, Bf9 100 631 81:08 3 1.099 ADD 136769, 8.8,817** 17.306 99 760 86:00 3 1,304 ADD 131430, 817,709 t« M, 80? 04 190 9:00 > 1 0. 6B8 ADD 11433, 19,734 ** 1,03
Tffl RBT(L) RATIO RRT(L) RATIO AMNT AMNT(L) R FAC R, PA.CIL) RATIO1 7:168 16:003 80:004 9:469 81:066 86:06•I 4'96
000000000000
000000000330097309
, 01 0. 676
00 890.00 890,0000 890,00 890,0000 890.00 890.0000 87Q, 7B 890,0000 868,88 200,0000 817,71 890.00
000 1.000 1,00000 1,000 1,00000 1.000 1,00119 1,000 1,18899 1,834 1,091DO 1,380 0. B7
01 10,73 890.00 0.809 3,334 0,06
i .1 023606
hiUANTITATlON RIIPORT PILE VOUNKB
1FDB4QV T!10/Q4 17 00 00\E IFD VOA BAMPLE 8A!» 00-040, BtlOH C9490, CASE* 2640
ISUOMITTED DY: EPA ANALYST: RJM"MOUNT«AREA * REF, AMNT/IREF. AREA)* REBP. FACT)
FAC. FROM LIDRARY ENTRYuo NAME
1 DKOMQCHLOROnETHANEiVO LIDRARY IB)2 2-OROMO-l-CHLOROPROPANE (UY INTERNAL STANDARD)3 1,4-DICHLORODUTANE <UZ INTERNAL BTANDARD)
NO M/E SCAN TIME REF RRT METH AREA(HOHT) AMOUNT XTOT1 RC 281 788 1 1,000 ADD 386097, 290,000*. 33,332 RG 4^6 10-06 2 1000 ADD 394013. "0.000.. 33333 RIC 99B 19:96 3 1.000 ADD 178979, 200,000 «» 33.33
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A 1PD040. Tl09/31/B4 6 91:00BAMPLE: IFD 0/N/A SAMPLE BAIH 09-040, BMO« C9490, CABEK 8640BUDM1TTGD DY: IFD ANALYST: RJM
AMOUNT-AREA * RBF. AMNT/(REF. AREA). REBP,FACT)REOP, FAC. FROM LIBRARY ENTRY
NO NAME1 D4-1.4-DICHLORODENZENE (1 B. 1-1/30/04 VERSION)2 DB-NAPHTMALENE (C2 I B,-1/20/04 VERSION)3 D10-ACBNAPHTHENG (C3 1 B -1/80/84 VERSION)4 D18-CMRYBENE (C4 l.B, -l/BO/04 VERSION)9 D10-PHENANTHRENE IC6 1.S.-1/20/04 VERSION)6 D9-PHBNOL (ACID BURROOATE)7 8-FLUOROPHBNOL (ACID BURROOATE)6 DO-NITRODENZENE (D/N BURROOATE)9 8-FLUOROD1PHENYL (0/N BURROOATE) " • •10 014-P-TER PMENYL (B, B, )11 D10-PYRENE (8 B, I18 8, 4,6-TRIDRQMOPHBNOL IB S I13 8-CHLOROPHBNOL14 DIBia-ETHYLHBXYDPHTHALATE19 Dl-N-DUTYL PHTHALATG
NO M/E 8CAN TIME REF RRT METH , ARGAIHOMTI AMOUNT KTQTMl 198 040 <7,04 1 1,000 A?DV 39176 40.000** 7.30
3 136 786 18:06 8 1000 ADD M47B9, 40.000** 7,363 168 1003 1643 3 1,000 ADD 61930. 40000** 7.364 840 16B6 8606 4 1.000 ADD 26611. 40.000*. 7.309 160 1839 80:39 9 1.000 ADD 116633 40,000** 7,306 99 497 B:17 i 0.914 ADD 90149. 4M. «?46 *» 7,937 118 364 6:84 1 0706 ADO 98809. 44996*. 6,300 68 686 10:86 8 0,060 ADD 97303, 43, 498 #* B, 039 178 B96 14:96 2 1,231 ADD 74496, 33,397** 6,1610 844 1491 84:91 4 0.064 ADD 6313B. 41.036** 79711 218 1464 84:84 4 0. 06B ADD 71490, 42 007 *» 7,0418 330 1127 IB: 47 D 0,913 ADD 7016 44.470** 6,8113 18B 019 037 1 0,904 ADD 96413, 44, 714 *t 6,8914 149 1696 86:16 ,4 1,006 ADD 8723. 1 378 «« 0,8619 149 1334 88:14 9 1000 ADD 11064 8.936** 0,04
NO RBTIL) RATIO RRTIU RATIO AMNT AMNT(U) R, FAC R, FAC(L> RATIO1 9,09 0,99 1,0008 18:18 0,99 1,0003 16:404 86: Of0 80:37
6 10:KB9 14:96
JO 84:00Jl 84:8418 16:47
00 1,00000 1,00000 1.000
6 6:81 0.99 0,9147 6:8? 0,99 0,710
00 0, 66100 1 88900 0, 00000 0, 06900 0,913
,00 40.00 40,00,00 40,00 40,00, 00 40. 00 40, 00, 00 40, 00 40, 00. 00 40. 00 40. 00. 00 48, 99 90. 00, 99 44. 96 90, 00
000 1.000 1,00000 1,000 1,00000 1,000 1,00000 1,000 1,00000 1,000 1,00141 1,386 0,66107 1,381 0,90
00 43,49 00,00 0,317 0,360 0,67,00 33 40 90,00 0. 412 0,616 0 67,00 41,04 9000 1 070 8,313 0,08,00 48, 01 90 00 8, 14Q 8,087 0, DO.00 44.47 00,00 0.040 0,004 0,09
023410.
_NO RCT(L) RATIO RRT(L) RATIO AMNT AMNT(L) II FAC fl.FAC(L) RATIOfall B 44 0.99 0.994 100 4471 90.00 1203 1.439 0.09
14 20 IB 1.00 1009 1,00 137 90,00 0002 8,941 0,0319 22:16 1.00 1060 1.00 2,74 90.00 0076 1298 0.06
3 i 0236U
OUANTITATION REPORT IMLC: UNKQ
fa f\\ IFD04Q, TI09/31/64 B:I>1:00SAMPLE: IFD 0/N/A OAMPLG BAIN 09-040, BMOK C9496, CAOEN 8640BUDMITTED DY: IFD ANALYST: RJM
AMOUNT-AREA » RBF, AMNT/I REF. AREA). REBP FACT)RGBP. FAC, FROM LIDRARY ENTRY
NO NAME '1 D4-1,4-DICHLORODBNZGNR 1 1 8.. 1-1/30/04 VERSION)8
9 DB-NAPMTHALENE (C8 1 B, -1/20/04 VERSION)6 D10-ACENAPHTHBNE (C3 1.8. -1/80/B4 VERSION)7 D12-CHRYBENE (C4 I, B -1/80/84 VBRB10N)B D10-PHENANTHRENE (C6 IB -1/20/64 VERSION)
NO M/E BCAN TIME REF RRT MRTH AREA(HOHT) AMOUNT '/.TOT1 RIC 944 7:04 I 1000 ADO 160464. 40.000** 0,678 RIC 193 2:33 1 0 281 ADD 9796670. *ttrtt--70' 37,913 RIC 163 8:43 1 0300 A VO 4176B70, im-M*-* 16.064 RIC ISO 3:00 1 0331 A VD 11179900 .a W-fOO —— 48.769 RIC 78B 12: OB 9 1,000 ADD 263432. 10, 000 "• 0.696 RIC 1003 16:43 6 1.000 ADD 274994. 40,000*. 0,697 RIC 16B7 80:07 7 1,000 ADD 106696 40,000*. 0,69Q RIC 1236 20:36 B 1,000 ADD 262631 40000** 0.69
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NO NAME1 DROMQCHLQROMETMANEIVO LIDRARY IB)8 8-DROflO-l-CHLORQPROPANE <UY INTERNAL BTANDARD)3 li4-DICHLORODUTANE <UZ INTERNAL BTANDARD)4 D4-U8-DICHLORQRTHANB (BURROOATE)9 OB-TOLUENE (BURROOATC)6 P-DRQMOFLUOROOBNZBNB (MB CHECK)7 DICHLOROM6THANBB M-DICHLQRQETHANB9 TRICHUOROGTHYLGNe10 TETRACMLQRQETHINC
NO fl/R BCAN TIME RBF RRT METH ARBAIHOHT) AMOUNT XTOT1 IBS 886 7' 38 18 77 408 16:043 9D 608 80:04 3.A 69 897 9:98 1If 100 630 81:10 36 99 709 86: 10 3
000 ADD 41094. 890. 000 «» 19,90000 ADD 10110S. 890,000 M 19,9000.0 ADD 06083, 890 000 «» 19,90383 A 00 47334. ' 8Q8. 647 «« 17.98ODD ADO 104967. 847. 109 M 19,38304 A7DD 9487B, 813.678 «» 13,89
7 B4 19B 9:16 1 0.699 ADO 10000. 86.491 «» 1,77Q 63 849 B: IB 1 1,108 ADO 6917, 10.934 «« 0,609 130 48B 14:16 8 0, OilD ADD 7B89, 36.169** 3,4fl10 164 999 19:90 3 0,9flQ ADD 13499, 84,118** 149
NO RRTIL) RATIO RRT(L) RATIO AMNT AMNT(L) R PAC R.FAC(L) RATIO1 7: IS8 16,00a 80: oo4 9:469 81: OB6 S6:067 4:96ft 0 069 14'0610 19 49
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BPLB: EPA/1FD VOA SAMPLE BA1 (169-000. CABE 8640 MC9499 (9.OML)11TTED DY: EPA ANALYST: RJM
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NO NAMBI DROMOCHLOROMETHANBtVO LIDRARY IB)8 METHANE,DICMLOROFLUQRO-3 8-OROMO-l-CHLQROPROPANB (UY INTERNAL BTANDARD)4 1,4-DICHLORODUTANB (UZ INTERNAL BTANDARD)
NO n/B SCAN TIME RRF RRT METH AREA(HOHT) AMOUNT XTOT1 RIC 886 7; 38 1 1.000 ADO 849039, 890.000** 89,638 RIC 144 400 I 0.637 ADD 884640, 889,910 83,133 RIC 488 16:04 3 1,000 ADD 87070D. 890 000 «« 39.634 RIC 60S 80:04 4 1,000 A HI) 806899. 890.000 • • 89.63
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NO NAME1 D4-1,4-DICHLORODENZENE <1 0, 1-1/30/04 VERSION)8 DB-NAPHTHALENE IC8 I. S -1/20/04 VERSION)3 D10-ACGNAPHTHGNE IC3 13 -1/80/04 VERSION)4 DI8-CHRY.8ENE (04 IB -1/80/04 VERSION)9 DIO-PHRNANTHRENE IC6 IB -1/80/B4 VERSION)6 D9-PHENOL (ACID QURROOATG)7 8-FLUOROPHENOL (ACID 6UIIROOATE)B D9-NITROOENZENE (0/N BURROOATE) " • >9 B-FLUORODIPH8NYL (0/N SURROGATE)
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• NO M/E BCAN TIME REF RRT METH AREA(HOHT) AMOUNT '/.TOT1 198 940 9 00 18 136 730 18:10 53 168 1003 16:43 34 840 16B7 SO 07 49 ISO 1836 20:36 9
000 A 00 698B3 40,000 «* B.41000 A DD 893811. 40,000 »* 8,41000 A?DD ,127007 40,000** B, 41000 A?DD 79404. 40.000** 8,41000 ADD 846379 40.000** B, 41
6 99 90S 0 88 1 0 "16 A 00 76783 39,909 »« 7,467 118 390 6 30 1 0.718 A 00 73069, 39 714 «* 7.91B 02 68B 10 SB 8 0 QfaO ADD 10940*; 44601 ** 9,399 178 B97 14 97 SI 28? A 00 10898Q, 86,308 «« 0.9410 844 1498 84:98 0 0 004 ADD 130990. 8B, OOB «« 9. B?II 818 1469 8489 4 0 060 ADD 138980, 87, Q60 ** 0. B618 330 1I8Q 1040 S 0^13 ADD 16486, 40.019** 0,4113 I8B 983 (1:43 1 0 V94 ADD 00193. 34.3B3 »" 7.8314 94 003 B:83 1 0 910 ADD 9377, 1.494** 0,3119 149 1339 88:19 9 1 000 A 00 14893, 1.709 ** 0.30
NO HBTILI RATIO RRTIU RATIO AMNT AMNT(L) R, FAC R.FAC(U) RATIO1 9 098 18; II3 16:444 86:099 80:3Bt» 0:837 6; 38B 10.8V| 9 14:97F10 84:9811 84:8918 IB: 49
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RET(L) RATIO RRT(L) RATIO AMNT AMNT(L) R FAC R.FAC<L) RATIO8:44 1.00 0. ?94 1.00 34.3D 90.00 0,926 1,347 0,69
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OAT,A: JFD090. TI06/01/B4 11:20:00SAMPLE: IFD 0/N/A BAMPLE SA1H CJS-QOQ, UMOII C9409, CABGK 8640 * IS8UOM1TTED DY: IFD ANALYST RJT
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NO NAME1 D4-1, 4-DlCHLOriOOENZENE (1 S, 1-1/30/04 VERSION)
4 METHANE,TETRACHLORD-9 I-PROPBNE, 3, S'-OXYBIS-6 DB-NAPHTHALENE (C8 IB -1/20/04 VERBIONI7 DIO-ACBNAPHTHENE (C3 1. B -1/80/04 VERSION)S D18-CHRYBENE (C4 I. B -1/80/04 VERSION)9 D10-PHENANTHRENE (C6 1 S -1/80/04 VERSION)
NO M/E SCAN TIME REF RUT METH ARKA(HOHT) AMOUNT '/.TOT1 RIC 94B 90S8 RIC 120 80S3 RIC 146 8864 RIC 179 8:999 RIC 377 6.17 . _._6 NIC 730 18 10 6 I 000 A IID 904084 40 000 *« 1.44
| 7 RIC 1003 16:43 7 1,000 A 00 614860. 40.000 »« 1,44Q RIC 16QB afl'OB S 1.000 ADD 907960. 40000** 1.449 RIC 1837 80:37 9 1,000 ADD 903040, 40, 000 *« 1,44
1 000 A IIU 379064, 40 000 ** 1,440.234 ADD 14703400. •ttTOreOO «"""' 96. 980 866 A VD 7B31940 -S38-44.-Ui(- 89,940387 ADD 1990330. krtrWT «<««f 9, V30 60Q A DO 118944. 11. 977 0; 43
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LE IFD D/N/A SAMPLE OAI« 09-090, BMON C9499, CASE* 8640 » IBJONDB. : 40DO, FOR 3 HIM, THEN S79DO. « 10DO, /M1N. THEN HOLDENHANCED (B 190 2N OT)
31331 SPECTRA IN LIDRARYND SEARCHED FOR MAXIMUM PURITY09 MATCHED AT LEAST 0 OF THE 16 LAROEBT PGAKB IN THE UNKNOWN
RANK IN NAME1 BB3 l-PROPENE,3,3'-OXYDIB-3 918 4-PENTENAL,2-METHYL-3 BB9 l-PENTYN-3-OL,4-METHYL-
RANK FORMULA M. HT D, PK PURITY FIT RFIT1 Cft, HIO. 0 9B 41 744 837 7718 Cft, HIO. 0 9Q 41 789 898 7893 C6.H10 0 9B B3 714 7B8 789
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DATA: IPD860V, TI09/10/B4 18:88:00BAMPLE: EPA/1FD VOA 8AM?LE BAI HB9-B60, CASE 3640 *C7460 (9. OML)8UDMITTED DY: ERA ANALYBT. RJM
AMOUNT-AREA « REF. AMNT/(REP, AREA)* RESP.FACT)REBP, FAC, FROM LIDRAHY ENTRY
NO NAME1 BRQMOCHLQROMETHANGIVQ LIDRARY IB)8 8-DROMQ-l-CHLOROPROPANE (UY INTERNAL STANDARD)3 1,4-D1CMLQROOUTANE <U2 INTERNAL BTANDARD)4 D4-1,8-D1CHLORO-THANB (DURROQATB)9 DB-TQLUENE (BURROOATE)6 P-BROMOFLUDRODBNZENE (MB CHECK)7 D1CHLOROMBTHANBB TETRACHLOROETHENE
NO n/R 8CAN TIME REF RRT METM AREA(HOHT) AMOUNT XTOT1 188 884 7.86 1 .000 ADD 60372, 890 000 «• 19, 778 77 OBI 16:08 8 ,000 ADD 148014. 890 000 •• 19. 7*3 99 608 80,04 3 ,000 ADD 119674, 890000** 19. 7?4 69 8<?B 7:96 1 ,330 ADD 66070 879 974 «« 17.639 100 639 81:10 3 ,099 A OD 146890 847 448 »« 19.03
79 7B9 86:10 3 ,304 ADD 130947. 818.641 «• 13.6004 199 9:10 1 0.678 ADD 84307 30 874 «• 1,74164 979 17:90 3 0,70S ADD 36789. 47.870** 3.03
NO RET(L) RATIO RRT(L) RATIO AMNT AMNTtL) R. FAC R. PAUL) RATIO1 7:16 1,08 1,000 1.00 890.00 890,00 1.000 1.000 1,008 16:003 80:00A 7:469 81:OB0 86:067 4.96B 17:4B
00 1.000 1,00 890.00 890.00 1,000 1.000 1,0000 1 000 1 00 890.00 890,00 1,000 1.000 1.0008 13-0 077 879.97 800.00 1.103 1.000 1,1000 1 097 1.00 847.44 890.00 1,888 1,834 0,7900 1,309 1 00 818.64 890.00 1.071 1,293 0,6909 0676 1.08 30.87 890,00 0.403 3,384 0.1800 0770 100 47.30 890,00 0.307 1.688 0.17
0236813|
OUANTJTATION RBPORT FILE, VQUNKD
DATA. IPDB60V TIQVIO/B4 IB: 88: 00r>PLE EPA/IFD VOA SAMPLE BA1 NB9-06Q, CASE S640 NC7460 19. OML)SUBMITTED DY: EPA ANALYST: RJM
AMOUNT"AREA f REF.AMNT/IREF. AREA)* RESP.FACT)REBP. FAC. FROM LIDRARY ENTRY
NO NAME1 DROMOCHLOROMETHANEIVO LIDRARY IB)8 8-DROMO-l-CHLOROPROPANE (UY INTERNAL BTANDARD)
NO M/B BCAN TIME REF RRT METH AREA(HOHT) AMOUNT XTOTI RIC 884 728 1 1.000 ADD 3640BB. 890,000** 90,008 RIC 488 16 04 8 1.000 A DD 383781. 890,000 •« 90,00
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JATA IFD06Q, TI06/09/B4 IS: 17:00BAMPLE: IFD D/N/A BAMPLE BA1H B9-06Q, 6MOH C7460, CASED 2640BUDMITTED OY: EPA/IFD ANALYST RJM
AMOUNT-AREA • HKF.AMNT/IREF AREA)* HEBP.FACTIRKBP FAC FROM LIDRARY ENTRY
NO NAME1 D4-l,4-DICHLORODENZGNi: I I 1} 1-1/30/01 VERSION)8 OS-NAPHTHALENE <C2 1 B -I/20/B4 VERSION)3 D10-ACBNAPMTHENB (CD I S -1/80/B4 VERSION)4 D18-CMHYBBNE (C4 1 3 -1/80/84 VERSION)9 D10-PHBNANTHRENB (C6 ! S -1/80/B4 VERSION)6 D9-PHENOL (ACID SURROGATE)7 8-FLUOROPMENOL (ACID BURROOATE)B D9-NITRODBNZENB (D/N BURROOATE)7 8-FLUORODIPMBNYL (D/N OUHROOATEI10 D14-P-TKM PHENYL IB 8 I11 DlO-PYRENE (88 )18 2,4,6-TRlDROMOPHENOl. <0 S I13 8-CMLOROPHENOL14 PHENOL19 DIBtS-ETHYLHEXYDPHTHALft'E16 Dl-N-DUTYL PHTHALATE
M/B SCAN TIME REF RRT METH AREA(HOHT) AMOUNT '/JOT1 198 940 '? OB It 000 A DD 93B71 40 000 *• 7,388 136 730 12 10 S 1 000 A DD 808080 -10 000 »• 7.383 168 1003 1643 3 1000 ADD 77180 .JO. 000 •• V. JS4 840 1606 80:06 4 1 000 A?DD 61317 -10 000 •« 7,389 1UB 1836 8036 D 1.000 ADD B037B7 40 000 i>« 7.38o 79 902 B'BB I 0716 ADD 7923V iO 060 •» 6.767 US .170 6,30 I 0718 ADD 6734? -M loo "' B. 000 S8 68B 10 SB SO S60 A DD 77402 ?'• t>34 •• 10. 167 172 877 14 97 S 1 88V A DD 67463 ;.J "01 *« 4,3910 S4'l 1471 24:.1 4 0 004 A DD 140Q86 :,J "'56 ** 6,8111 818 1464 S4 84 4 0,860 A DO 1373B4 ;; 474 • « 9.7418 3aO lU'Q 1848 S 0 "13 ADD 17290 cr 'HO M 11,0713 120 984 0:44 1 0796 ADD 76077 ,| I "31 •• 7.6714 74 904 0:84 1 0780 ADD 190"'l !MI76 •• 1.0819 147 1679 88:19 4 t 009 A DD 27070 t) .23 «• 1 6116 147 1334 88:14 9 I 077 A DO 10877 I 440 >« 0,87
NO HE11L) RATIO RRTiL) RA110 AMNT AMNT(L) P FAC R I'ACIL) RATIO1 7 09 1 01 1 000 I 00 40. 00 40 008 18:00 1,00 1 000 1 00 40,00 40,003 Iti, 48 1,00 I 000 1.00 40,00 40.004 80:09 1.00 1 000 I 00 40,00 40,009 80:39 I 00 1,000 1 00 4000 40006 Q: 17 I 01 0 716 1 00 38,06 40,007 6:86 1,01 0,700 1,00 44,17 90,00
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IB 10:87 1,00 0.860 100 99.93 90.00 0 306 0347 1 , 1 17 14:97 1,00 1,830 100 83,70 9000 0 2?9 0,978 0,4B10 8491 1.00 0 Hfl4 100 3373 00.00 1037 R 70Q 060
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00 0, 06700 0,71300 0. 79800 0, 78100 1.00900 1.077
00 38 47 90 00 1 772 B 798 0 6900 6091 9000 0.076 0. 06B 1.8100 41.73 90.00 1. 1B7 1.347 0.0400 9. 88 90, 00 0. 836 B. 007 0. 1800 Q. 82 90 00 0 364 8 061 0. IB00 I 47 90.00 0.040 1 393 0.03
023672
QUANT I TAT I ON REPORT FILE UNKO
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NO NAME1 D4-l,4-DICHLORODENZGNE (1 S 1-1/30/04 VERSION)B METHANE, DICHLORO-3 l-PROPENE, 3i3'-OXYDlB-4 B-CYCLOHfiXEN-l-ONE9 D8-NAPMTHALENG (C2 IS -l/SO/04 VERSION)6 DIO-ACBNAPMTMKNE (C3 1 S -1/80/04 VERSION)7 D18-CMRYBENE (C4 1 S -1(80/04 VERSION)B 1-DECENG,3, 4-DIMETHYL-7 D10-PMBNANTHRENE (C6 1 3 -1/80/04 VERSION) , , ,
NO M/E BCAN TIME RBF HRT METH AREiMHOMT) AMOUNT XTOTI RIC 94B 7 08 II 000 A DD 309790 40 000 •* 7 972 RIC 809 3:B9 1 0374 A DV 1300200 171.041 40,773 RIC 377 617 1 0608 ADO 181798. 19.717 3, Bl4 RIC 461 7 41 10 341 A DD 01062 10 708 8,975 RIC 730 18,10 5 1 000 A 1)1) 406886 40 000 •» 7.976 RIC 1003 16 43 6 1 000 A DD 406084 40i 000 «« 7,97V RIC 1687 20 07 7 I 000 A II V A6Q077 40.000 »« 7 97S RIC 1983 86 B3 7 0 738 A DO 2B71BQ 17 91)0 4.671 RIC 1236 20 36 7 1 000 A DD 909060 40 000 •« 7.97
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NO NAME1 DROrtOCMLORONKTHANEIVU LIBRARY 10)B 2-DROMO-l-CHLQROPROPANE IUY INTERNAL STANDARD)3 1,4-DICMl.QRODUTANE (UZ INTERNAL BTANDAHD)4 D4-1.8-DICHLOROETMANE (DURROBATEl. DO-TOLUENE <SURROGATE)6 P-DROnOPLUORODENZENE tnS CHECK)7 DICMLORQMBTHANE0 TRANB-1.B-DICHLOROETHENE9 TETRACHLORQETHENE
HO tVE SCAN TIME REF RRT METH AREAIHOHT) AMOUNT XTOT1 ISO 834 7: SO 1 1.000 ADO 49004, 890,000** 16,17S 77 401 16: OS 8 1,000 ADD 181404, 800,000** 16,173 99 60S 80' 04 3 1 000 ADD 100604. 890000** 16,174 69 896 9.96 1 1.330 ADD 99411, 879. 746 »« IB. 09
.5 100 639 21 10 3 1.099 ADD 189933 898,693** 16,34ft 99 764 86: OB 3 1,308 ADD 110000. 889,799** 14,66
7 04 199 9:10 1 0698 ADD 7009 10,764** 0,700 96 867 0:94 11 198 ADD 1391, 3307** 0.819 164 999 19:90 3 0900 ADD 13199, 80.163** 1,30
NO RGTIL) RATIO RRT(L) RATIO AMNT AMNT(L) R. PAC It PAC(L) RATIO1 7 108 16003 SO 004 9.46$ 81:00it 86067 4:96B U 469 19:40
08 1, 00000 1 00000 1.000
00 1 09700 1 30909 0.676
00 890.00 890,00 1,000 1.000 1.0000 890,00 890.00 1,000 1,000 1,0000 890,00 800.00 1.000 1.000 1,00
08 1.330 0.99 879.70 890.00 1.119 1,000 1.1800 898.69 590.00 1.840 1,834 1.0100 889.00 890.00 1.179 1.868 0.9808 10.76 890.00 0 143 3,394 0,04
01 1,809 0,99 3,31 890.00 0,080 8.184 0.0100 0,990 1.00 80.16 890.00 0.131 1,688 0, OB
023695
lOUANTJTATlON REPORT FILE VOUNNU
DATA: IF007QV. TI09/10/64 19:04:00(IH'LE: IPD VOA BAMPLE BAIIt 09-070, OnOtt C9461, CAHEK 2640SU-MITTED DY EPA ANALYST: RJT
AMOUNTKAREA « REP, AMNT/(REP, AREA)* REBP.FACT)HEBP. FAC. FROM L1DRARY ENTRY
NO NAME1 DRQMOCHLOROMETHANflVO LIDRARY IB)8 8-DROMO-l-CHLOROPROPANE (UY INTERNAL STANDARD)3 1,4-D1CMLORODUTANE (UZ INTERNAL STANDARD)4 CYCLQTRIBILOXANE, HEXAMETHYL- **-&———
NO M/E 8CAN TIME REF RRT METH AREA(HOHT) AMOUNT XTOT1 RIC 884 7 SB 1 1.000 ADO 899966. 890 000 «« IB, 808 RIC 4BI 1608 8 1.000 ADD 383740. 890.000** 10,803 RIC 601 8008 3 1000 ADO 831403. 590000** 19,804 RIC 769 86:10 3 I 306 ABO 077630. -480.016 49,4!
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ATA IPD070A TI06/04/04 16; 9(1 00OAMPLK GPA/IF'O CABEB640 ItC^l DNA (BA1 M09-07Q)SUBMITTED DY: KPA/1FD ANALYST: EFP
AMOUNTnAHfiA • IIEF AMNT/IREF AREA)* REBP, FACT)REBP. FAC FROM LIDRARY ENTRY
NO NAMEI D4-I,4-D1CMLOHOOBNZGNE II 0 1-1/30/04 VERSION)S DO-NAPHTHALENE (C8 IB -l/SO/04 VERBION)3 D10-ACBNAPHTHENE IC3 1 Q -l/SO/04 VERBION)4 DIB-CHRYBliNE IC4 1 B -1/80/04 VERSION)9 D10-PMENANTHRENE IC6 1 B.-1/80/B4 VERBION)6 D9-PHUNQL (ACID BURROOATE)7 8-PLUOROPHENOL (ACID BURRQOATE)0 PS-NITROBENZENE (D/N BURROOATE)9 B-FLUOROOIPHENYL (0/N BURROOATE) "10 D14-P-TBR PHENYL (8 Q )II D10-PYRENE I B S . )18 8,4,6-TfUDROMOPHSNQL (6 B )13 8-CHLOROPHENOL14 PHENOL19 ANILINE (HBL)16 DIOIB-BTHYLHGXYDPHTHALAin17 DI-N-DUTYL PHT.IIALATE
MO M/E BCAN TIME REF RRT METH AREA(HOHT) AMOUNT XTOT1 198 940 900 1£ 136 730 18 10 S:i 168 1003 16:43 34 840 1606 80:06 49 100 1836 80:36 3
000 A DO 94000 40 000 »* 0, 10000 A DO 317860 40 000 *• 0, 1Q000 A DO 169671 40 000 »» 6, IB000 AI'DD 113879 40000** 6,10
. 000 A DD 349397 40 000 •• 0. 166 99 908 0:88 1 0. <Ht> ADD 97307 26 V86 »« 9.017 118 391 6 31 10 714 A DD 00014 31 417 *» 6.48Q 68 686 1080 8 0 060 ADD 180073 49 40. ** 9,809 178 097 14'97 2 1889 ADD 1808111 84977** 0,1110 844 1418 8498 4 0009 ADO 844400. 39989** 7.8611 818 14e>4 S4 24 4 0060 ADO 848V04 39 196 *« 7,8018 330 1120 10 40 90 "13 A DD 86796. 40 11Q »• 10,0813 180 084 0 44 10 996 A DD 99809, 30 669 •• 6.8714 94 909 B 29 1 0.''28 A"UV 6309. 1,UOS*« 0,8719 93 910 030 1 0931 ADD 3804 I 983 M 0.3116 149 1699 80:19 4 1009 A Oil 0609 1. 106 •« 0,8317 149 1334 8814 9 1079 A 1)0 60003, b, 003 «« 1,«3
NO RETILi RATIO RRT (I.) RATIO' AflNT AMNT(L) R, FAC H.FAC(L) RATIOI 9:09 1 01 1.000 I 00 40.00 40.00 1.0008 18:09 I 00 1.000 I 00 40 00 40 00 1.0003 16:43 100 1,000 100 4000 40,00 1.0004 86.07 I 00 1.000 1 00 40.00 4000 1.0009 80:36 1.00 1.000 I 00 , 40 00 40.00 1.0006 6:81 1,00 0 916 1 00 86,93 40 00 1.0877 6:30 1 00 0 713 1 00 31 4? 00.00 0, T43
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FAC303727714061030093017061190
R. FAC(L)0.607S. '1308. 4390.0631 3668.0430.9022 7901.314
RATIO0.900.710 700,960,610.030,080,080. 18
31023706
OUANT1TAT10N IMPORT F1LB UNKB
A: IFD07QA. TI06/04/04 16:90:00BAMPLE: EPA/IPD CASE8640 HC946I DNA (BA1 KQ9-07Q)OUDMITTED DY: EPA/1PD ANALYST: EFP
AMOUNT»AHBA * REF. AMNT/(REF AREA)* REBP. PACT)REBP FAC. PROM LIDRARY ENTRY
NO NAMEI D4-l,4-DICHLORODGNZGNF (I 0 1-1/30/04 VERSION)2 METHANE. DICHLORO-';3 METHANE, DICHLORO"/4 1-PROPENE,3,3--OXYDIB-9 DO-NAPHTHALENE (C8 I, B -1/30/04 VERSION)6 DiO-ACENAPHTHENB (C3 IS -1/80/D4 VERBION)7 D18-CHRYBENE (C4 1C -1/80/04 VERBION)Q DIO-PHENAimiRENE (C6 1 B -1/80/04 VERBION)
NO M/E SCAN TIME REP RRT METH AREA(HOHT) AMOUNT '/JOT1 MIC 540 9 OB 11 000 A DD 960380, 40.000 ** 6,702 RIC 809 3,89 I 0,374 A DV 1966800 140363 83,983 RIC 816 3:36 1 0394 A VD 3488070. 244899 40,944 RIC 376 6:16 I 0690 ADO 169696 1 8 114 8,039 RIC 730 18:10 9 1 000 A DD 703734 40,000 ** 6,706 RIC 1003 16:43 6 I 000 A DD 909790 40 000 «* 6,70
__ 7 RIC 1607 20,07 7 I 000 A DV 90163?' 40 000 «* 6,70P) 0 RIC 1836 80.36 0 I 000 A DD 008094. 40.000 «« 6,70
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