newtowncreek.infonewtowncreek.info/docs2/2 Remedial Investigation/Phase 1...

ANALYTICAL REPORT

Job Number: 180-15932-1

Job Description: 120782-01.01 Newtown Creek

For:Anchor QEA LLC

720 Olive WaySuite 1900

Seattle, WA 98101

Attention: Delaney Peterson

_____________________________________________

Approved for release.Carrie L GamberCustomer Service Manager12/4/2012 9:14 AM

Carrie L GamberCustomer Service Manager

[email protected]/04/2012Revision: 1

The test results in this report meet all NELAP requirements for parameters for which accreditation is required oravailable. Any exceptions to the NELAP requirements are noted in this report. Pursuant to NELAP, this report may notbe reproduced, except in full, without the written approval of the laboratory. This report is confidential and is intendedfor the sole use of TestAmerica and its client. All questions regarding this report should be directed to the TestAmericaProject Manager or designee who has signed this report.

TestAmerica Laboratories, Inc.

TestAmerica Pittsburgh 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238

Tel (412) 963-7058 Fax (412) 963-2468 www.testamericainc.com

Page 1 of 334

mailto:[email protected]://www.testamericainc.comhttp://

Table of ContentsCover Title Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Data Summaries . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

Report Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

Manual Integration Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

Executive Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10

Method / Analyst Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11

Sample Datasheets . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12

Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16

QC Data Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17

Data Qualifiers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24

QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25

Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26

Reagent Traceability . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27

COAs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 85

Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 117

Organic Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 118

GC/MS Semi VOA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 118

Method 8270C . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 118Method 8270C QC Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 119Method 8270C Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 131Standards Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 181

Method 8270C ICAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 181Method 8270C CCAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 243

Raw QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 267

Page 2 of 334

Table of ContentsMethod 8270C Tune Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 267Method 8270C Blank Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 279Method 8270C LCS/LCSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 288

Method 8270C Run Logs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 306Method 8270C Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 308

Inorganic Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 325

General Chemistry Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 325

Gen Chem Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 326

Gen Chem MDL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 327

Gen Chem Analysis Run Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 329

Gen Chem Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 330

Shipping and Receiving Documents . . . . . . . . . . . . . . . . . . . . . . . . . . . 331

Client Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 332

Sample Receipt Checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 334

Page 3 of 334

CASE NARRATIVE

Client: Anchor QEA LLC

Project: 120782-01.01 Newtown Creek

Report Number: 180-15932-1 Revised

NOTE: This report has been revised to include the corrected dilution factor for the semivolatile sample.

With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no

problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control

limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of

the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,

the reporting limits are adjusted relative to the dilution required.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the

individual sections below.

RECEIPT

The sample was received on 10/31/2012; the samples arrived in good condition, properly preserved and on ice. The temperature of the

cooler at receipt was 19.8º C.

SEMIVOLATILE ORGANIC COMPOUNDS (GC-MS)

As per client request, sample SED-20121017-1 was extracted and analyzed outside of holding time for 8270C semivolatile organic

compounds. The data are qualified and reported with this narrative.

Surrogate compounds were inadvertently omitted during the extraction process for sample SED-20121017-1 (180-15932-1). There was

insufficient sample remaining to perform re-extraction and/or re-analysis; therefore, the data have been reported and qualified. All QC

surrogate compounds recovered within acceptable limits.

GENERAL CHEMISTRY

Sample SED-20121017-1 (180-15932-1) was analyzed for percent solids in accordance with EPA SW846 3550C. The sample was

analyzed on 10/30/2012 and originally reported in job 180-15569-1.

Page 4 of 334

Lab Name: Job No.:

SDG No.:

GC/MS SEMI VOA MANUAL INTEGRATION SUMMARY

TestAmerica Pittsburgh 180-15932-1

Instrument ID: Analysis Batch Number:722 54021

Lab Sample ID: Client Sample ID:

Date Analyzed: Lab File ID:

COMPOUND NAME RETENTION

TIME

MANUAL INTEGRATION

DATEANALYSTREASON

ICIS 180-54021/21

F11010C1.D11/01/12 09:09 GC Column: Rxi-5SilMS ID: 0.32(mm)

1,4-Dioxane Poor Chromatography PGH_BNA 11/02/12 08:510.98

Benzoic acid Poor Chromatography PGH_BNA 11/02/12 08:525.03




TIME

MANUAL INTEGRATION

DATEANALYSTREASON

IC 180-54021/22


Pyridine Poor Chromatography PGH_BNA 11/02/12 08:571.43

Methyl methanesulfonate Peak Not Found PGH_BNA 11/02/12 08:573.02

Isophorone Poor Chromatography PGH_BNA 11/02/12 08:574.87

Dimethyl phthalate Peak Integrated Incorrectly bungardf 11/01/12 23:516.38

2-Naphthylamine Peak Integrated Incorrectly bungardf 11/01/12 23:516.86

2,4,6-Tribromophenol Peak Integrated Incorrectly bungardf 11/01/12 23:527.19

Atrazine Peak Integrated Incorrectly bungardf 11/01/12 23:527.51

Benzidine Peak Integrated Incorrectly bungardf 11/01/12 23:518.81

3,3'-Dichlorobenzidine Peak Integrated Incorrectly bungardf 11/01/12 23:519.91

Bis(2-ethylhexyl) phthalate Peak Integrated Incorrectly bungardf 11/01/12 23:529.97

Di-n-octyl phthalate Peak Integrated Incorrectly bungardf 11/01/12 23:5210.59

Indeno[1,2,3-cd]pyrene Peak Integrated Incorrectly bungardf 11/01/12 23:5212.76




TIME

MANUAL INTEGRATION

DATEANALYSTREASON

IC 180-54021/24


Benzoic acid Poor Chromatography PGH_BNA 11/02/12 09:015.05

8270C LL

Page 5 of 334

Lab Name: Job No.:

SDG No.:







TIME

MANUAL INTEGRATION

DATEANALYSTREASON

IC 180-54021/25


Benzoic acid Peak Integrated Incorrectly bungardf 11/01/12 23:585.07




TIME

MANUAL INTEGRATION

DATEANALYSTREASON

IC 180-54021/26






TIME

MANUAL INTEGRATION

DATEANALYSTREASON

IC 180-54021/27






TIME

MANUAL INTEGRATION

DATEANALYSTREASON

IC 180-54021/28



Benzo[b]fluoranthene Peak Integrated Incorrectly bungardf 11/02/12 00:0810.91




TIME

MANUAL INTEGRATION

DATEANALYSTREASON

ICV 180-54021/29

F11010V1.D11/01/12 12:22 GC Column: Rxi-5SilMS ID: 0.32(mm)


8270C LL

Page 6 of 334

Lab Name: Job No.:

SDG No.:







TIME

MANUAL INTEGRATION

DATEANALYSTREASON

CCVIS 180-54476/2


1,4-Dioxane Peak Integrated Incorrectly bachas 11/07/12 08:240.93

Pyridine Peak Integrated Incorrectly bungardf 11/07/12 06:561.34

Benzyl alcohol Peak Integrated Incorrectly bungardf 11/07/12 06:564.33


Pentachlorophenol Peak Integrated Incorrectly bungardf 11/07/12 06:577.53

Benzidine Peak Integrated Incorrectly bungardf 11/07/12 06:578.73




TIME

MANUAL INTEGRATION

DATEANALYSTREASON

LCS 180-54209/2-B

F1107003.D11/07/12 08:43 GC Column: Rxi-5SilMS ID: 0.32(mm)

1,4-Dioxane Peak Integrated Incorrectly bungardf 11/08/12 09:000.93

Pentachlorophenol Peak Integrated Incorrectly bachas 11/08/12 10:467.54




TIME

MANUAL INTEGRATION

DATEANALYSTREASON

LCSD 180-54209/3-B

F1107004.D11/07/12 09:04 GC Column: Rxi-5SilMS ID: 0.32(mm)

1,4-Dioxane Peak Integrated Incorrectly bungardf 11/08/12 09:020.93

Pentachlorophenol Peak Integrated Incorrectly bachas 11/08/12 10:477.55

8270C LL

Page 7 of 334

SAMPLE SUMMARY

Client: Anchor QEA LLC Job Number: 180-15932-1

Client Sample IDLab Sample ID Client Matrix Sampled Received

Date/Time Date/Time

180-15932-1 SED-20121017-1 Sediment 10/17/2012 1510 10/31/2012 0900

TestAmerica Pittsburgh Page 8 of 334

EXECUTIVE SUMMARY - Detections


Analyte Result

Reporting

Limit Units Method

Lab Sample ID Client Sample ID

Qualifier

180-15932-1 SED-20121017-1

260 ug/Kg 8270C LL74 J H1,1'-Biphenyl

260 ug/Kg 8270C LL170 J HAcetophenone

260 ug/Kg 8270C LL330 HBenzaldehyde

53 ug/Kg 8270C LL110 HAcenaphthene

53 ug/Kg 8270C LL490 HAcenaphthylene

53 ug/Kg 8270C LL490 HAnthracene

53 ug/Kg 8270C LL2500 HBenzo[a]anthracene

53 ug/Kg 8270C LL1900 HBenzo[a]pyrene

53 ug/Kg 8270C LL2900 HBenzo[b]fluoranthene

53 ug/Kg 8270C LL1500 HBenzo[g,h,i]perylene

530 ug/Kg 8270C LL10000 HBis(2-ethylhexyl) phthalate

260 ug/Kg 8270C LL280 HButyl benzyl phthalate

53 ug/Kg 8270C LL100 HCarbazole

260 ug/Kg 8270C LL170 J H4-Chloroaniline

53 ug/Kg 8270C LL2700 HChrysene

53 ug/Kg 8270C LL470 HDibenz(a,h)anthracene

260 ug/Kg 8270C LL150 J HDibenzofuran

260 ug/Kg 8270C LL220 J HDi-n-butyl phthalate

260 ug/Kg 8270C LL74 J HDiethyl phthalate

260 ug/Kg 8270C LL120 J HDi-n-octyl phthalate

53 ug/Kg 8270C LL4700 HFluoranthene

53 ug/Kg 8270C LL180 HFluorene

53 ug/Kg 8270C LL1400 HIndeno[1,2,3-cd]pyrene

260 ug/Kg 8270C LL26 J HIsophorone

53 ug/Kg 8270C LL230 H2-Methylnaphthalene

53 ug/Kg 8270C LL370 HNaphthalene

53 ug/Kg 8270C LL2300 HPhenanthrene

53 ug/Kg 8270C LL3400 HPyrene

260 ug/Kg 8270C LL46 J HMethylphenol, 3 & 4

53 ug/Kg 8270C LL73 HPhenol

0.10 % Moisture1.1Percent Moisture


METHOD SUMMARY


Preparation MethodMethodLab LocationDescription

Matrix: Sediment

Semivolatile Organic Compounds by GCMS - Low Levels TAL PIT SW846 8270C LL

Automated Soxhlet Extraction (Low Level) TAL PIT SW846 3541

Gel-Permeation Cleanup TAL PIT SW846 3640A

Percent Moisture TAL PIT EPA Moisture

Lab References:

TAL PIT = TestAmerica Pittsburgh

Method References:

EPA = US Environmental Protection Agency

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.


METHOD / ANALYST SUMMARY


Method Analyst Analyst ID

Bacha, Sharon A SABSW846 8270C LL

Kunkle, Sarah SKEPA Moisture

TestAmerica Pittsburgh

Page 11 of 334

Analytical Data


Client Sample ID:

Lab Sample ID:

SED-20121017-1

Client Matrix: % Moisture: 1.1

180-15932-1

Sediment

Date Sampled: 10/17/2012 1510

Date Received: 10/31/2012 0900

8270C LL Semivolatile Organic Compounds by GCMS - Low Levels

Dilution:

11/05/2012 0739

11/07/2012 0925

5.0

8270C LL

Injection Volume:

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID:

F1107005.D

19.2 g

10.0 mL

2 uL

3541

722

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

180-54476

180-54209

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL

74 J H 260241,1'-Biphenyl

170 J H 26022Acetophenone

260 U H 26026Atrazine

330 H 26040Benzaldehyde

1300 U H 1300200Caprolactam

110 H 535.1Acenaphthene

490 H 536.0Acenaphthylene

490 H 535.2Anthracene

2500 H 536.6Benzo[a]anthracene

1900 H 535.3Benzo[a]pyrene

2900 H 538.3Benzo[b]fluoranthene

1500 H 535.2Benzo[g,h,i]perylene

53 U H 5311Benzo[k]fluoranthene

53 U H 537.1Bis(2-chloroethyl)ether

260 U H 26017Bis(2-chloroethoxy)methane

10000 H 53043Bis(2-ethylhexyl) phthalate

260 U H 260234-Bromophenyl phenyl ether

280 H 26036Butyl benzyl phthalate

100 H 534.9Carbazole

170 J H 260214-Chloroaniline

53 U H 535.52-Chloronaphthalene

260 U H 260294-Chlorophenyl phenyl ether

2700 H 536.3Chrysene

470 H 535.9Dibenz(a,h)anthracene

150 J H 26026Dibenzofuran

220 J H 26033Di-n-butyl phthalate

260 U H 260283,3'-Dichlorobenzidine

74 J H 26029Diethyl phthalate

260 U H 26029Dimethyl phthalate

260 U H 260212,4-Dinitrotoluene

260 U H 260272,6-Dinitrotoluene

120 J H 26028Di-n-octyl phthalate

4700 H 535.6Fluoranthene

180 H 536.9Fluorene

53 U H 535.6Hexachlorobenzene

53 U H 535.9Hexachlorobutadiene

260 U H 26028Hexachlorocyclopentadiene

260 U H 26019Hexachloroethane

1400 H 535.4Indeno[1,2,3-cd]pyrene

26 J H 26020Isophorone

230 H 534.72-Methylnaphthalene

370 H 534.5Naphthalene

1300 U H 13001202-Nitroaniline



530 U H 53022Nitrobenzene


Analytical Data


Client Sample ID:

Lab Sample ID:

SED-20121017-1


180-15932-1

Sediment

Date Sampled: 10/17/2012 1510



Dilution:

11/05/2012 0739

11/07/2012 0925

5.0

8270C LL

Injection Volume:



Lab File ID:

Instrument ID:

F1107005.D

19.2 g

10.0 mL

2 uL

3541

722

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

180-54476

180-54209

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL

53 U H 536.2N-Nitrosodi-n-propylamine

260 U H 26024N-Nitrosodiphenylamine

2300 H 538.4Phenanthrene

3400 H 535.3Pyrene

260 U H 260244-Chloro-3-methylphenol

260 U H 260222-Chlorophenol

260 U H 260182-Methylphenol

46 J H 26026Methylphenol, 3 & 4

53 U H 535.32,4-Dichlorophenol

260 U H 260412,4-Dimethylphenol

1300 U H 13003102,4-Dinitrophenol

1300 U H 13001104,6-Dinitro-2-methylphenol

1300 U H 1300964-Nitrophenol

260 U H 260292-Nitrophenol

260 U H 26024Pentachlorophenol

73 H 536.2Phenol

260 U H 260282,4,5-Trichlorophenol

260 U H 260392,4,6-Trichlorophenol

53 U H 535.72,2'-oxybis[1-chloropropane]

260 U H 260172,3,4,6-Tetrachlorophenol

260 U H 260201,2,4,5-Tetrachlorobenzene

530 U H 530301,4-Dioxane

Surrogate %Rec Acceptance LimitsQualifier

0 21 - 116X2,4,6-Tribromophenol

0 28 - 108X2-Fluorobiphenyl

0 28 - 107X2-Fluorophenol

0 27 - 110XNitrobenzene-d5

0 30 - 112XPhenol-d5

0 21 - 130XTerphenyl-d14


Analytical Data


Client Sample ID:

Lab Sample ID:

SED-20121017-1


180-15932-1

Sediment

Date Sampled: 10/17/2012 1510



Dilution:

11/05/2012 0739

11/07/2012 0925

5.0

8270C LL

Injection Volume:



Lab File ID:

Instrument ID:

F1107005.D

19.2 g

10.0 mL

2 uL

3541

722

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

180-54476

180-54209

Analysis Method:

Prep Method:

Tentatively Identified Compounds

QualifierEst. Result (ug/Kg)RTAnalyteCas Number

10Number TIC's Found:

2.29 2900 H JUnknown


106-46-7 4.23 51 J H1,4-Dichlorobenzene

120-82-1 5.15 27 J H1,2,4-Trichlorobenzene

949-41-7 8.08 1600 H J N1H-Cyclopropa[l]phenanthrene,1a,9b-dihyd


10.19 150 H JUnknown Hydrocarbon





Analytical Data


General Chemistry

Client Sample ID:

Lab Sample ID:

SED-20121017-1

Client Matrix:

180-15932-1

Sediment

Date Sampled: 10/17/2012 1510


Analyte Result Qual Units MDL RL Dil Method

Percent Moisture 1.1 % 0.10 0.10 1.0 Moisture

DryWt Corrected: NAnalysis Date: 10/30/2012 1538Analysis Batch: 180-54503


Quality Control Results

Job Number: 180-15932-1Client: Anchor QEA LLC

Surrogate Recovery Report


Client Matrix: Sediment

Lab Sample ID Client Sample ID

2FP PHL NBZ FBP TBP TPH

%Rec %Rec %Rec %Rec %Rec %Rec

180-15932-1 SED-20121017-1 0X 0X 0X 0X 0X 0X

MB 180-54209/1-B 84 84 74 68 78 83

LCS 180-54209/2-B 87 83 80 74 84 78

LCSD 180-54209/3-B 88 88 78 73 83 79

Surrogate Acceptance Limits

2FP = 2-Fluorophenol 28-107

PHL = Phenol-d5 30-112

NBZ = Nitrobenzene-d5 27-110

FBP = 2-Fluorobiphenyl 28-108

TBP = 2,4,6-Tribromophenol 21-116

TPH = Terphenyl-d14 21-130


Page 16 of 334



SedimentClient Matrix:

1.0Dilution:

Lab Sample ID:

Method Blank - Batch: 180-54209

Instrument ID:

Lab File ID:



F1107001.D

30.0 g

10.0 mLUnits: ug/Kg

Method: 8270C LL

Preparation: 3541

722MB 180-54209/1-B

Analysis Date: 11/07/2012 0634

Analysis Batch:

Prep Batch:

Leach Batch: N/A

180-54476

180-54209

Prep Date: Injection Volume: 2 uL

Leach Date:

11/05/2012 0739

N/A

Analyte RLMDLQualResult

33 U 333.01,1'-Biphenyl

33 U 332.7Acetophenone

33 U 333.2Atrazine

33 U 335.0Benzaldehyde

170 U 17025Caprolactam

6.7 U 6.70.64Acenaphthene

6.7 U 6.70.76Acenaphthylene

6.7 U 6.70.65Anthracene

6.7 U 6.70.84Benzo[a]anthracene

6.7 U 6.70.67Benzo[a]pyrene

6.7 U 6.71.0Benzo[b]fluoranthene

6.7 U 6.70.66Benzo[g,h,i]perylene

6.7 U 6.71.3Benzo[k]fluoranthene

6.7 U 6.70.90Bis(2-chloroethyl)ether

33 U 332.2Bis(2-chloroethoxy)methane

67 U 675.4Bis(2-ethylhexyl) phthalate

33 U 332.94-Bromophenyl phenyl ether

33 U 334.6Butyl benzyl phthalate

6.7 U 6.70.61Carbazole

33 U 332.74-Chloroaniline

6.7 U 6.70.702-Chloronaphthalene

33 U 333.74-Chlorophenyl phenyl ether

6.7 U 6.70.79Chrysene

6.7 U 6.70.74Dibenz(a,h)anthracene

33 U 333.3Dibenzofuran

33 U 334.2Di-n-butyl phthalate

33 U 333.53,3'-Dichlorobenzidine

33 U 333.6Diethyl phthalate

33 U 333.6Dimethyl phthalate

33 U 332.72,4-Dinitrotoluene

33 U 333.42,6-Dinitrotoluene

33 U 333.5Di-n-octyl phthalate

6.7 U 6.70.71Fluoranthene

6.7 U 6.70.88Fluorene

6.7 U 6.70.71Hexachlorobenzene

6.7 U 6.70.75Hexachlorobutadiene

33 U 333.6Hexachlorocyclopentadiene

33 U 332.4Hexachloroethane

6.7 U 6.70.69Indeno[1,2,3-cd]pyrene

33 U 332.5Isophorone

6.7 U 6.70.602-Methylnaphthalene

6.7 U 6.70.58Naphthalene

170 U 170152-Nitroaniline






SedimentClient Matrix:

1.0Dilution:

Lab Sample ID:

Method Blank - Batch: 180-54209

Instrument ID:

Lab File ID:



F1107001.D

30.0 g

10.0 mLUnits: ug/Kg

Method: 8270C LL

Preparation: 3541

722MB 180-54209/1-B

Analysis Date: 11/07/2012 0634

Analysis Batch:

Prep Batch:

Leach Batch: N/A

180-54476

180-54209

Prep Date: Injection Volume: 2 uL

Leach Date:

11/05/2012 0739

N/A

Analyte RLMDLQualResult

67 U 672.8Nitrobenzene

6.7 U 6.70.78N-Nitrosodi-n-propylamine

33 U 333.1N-Nitrosodiphenylamine

6.7 U 6.71.1Phenanthrene

6.7 U 6.70.67Pyrene

33 U 333.14-Chloro-3-methylphenol

33 U 332.72-Chlorophenol

33 U 332.32-Methylphenol

33 U 333.3Methylphenol, 3 & 4

6.7 U 6.70.672,4-Dichlorophenol

33 U 335.22,4-Dimethylphenol

170 U 170402,4-Dinitrophenol

170 U 170134,6-Dinitro-2-methylphenol

170 U 170124-Nitrophenol

33 U 333.72-Nitrophenol

33 U 333.0Pentachlorophenol

6.7 U 6.70.79Phenol

33 U 333.62,4,5-Trichlorophenol

33 U 335.02,4,6-Trichlorophenol

6.7 U 6.70.722,2'-oxybis[1-chloropropane]

33 U 332.12,3,4,6-Tetrachlorophenol

33 U 332.51,2,4,5-Tetrachlorobenzene

67 U 673.81,4-Dioxane

Surrogate % Rec Acceptance Limits

2,4,6-Tribromophenol 78 21 - 116

2-Fluorobiphenyl 68 28 - 108

2-Fluorophenol 84 28 - 107

Nitrobenzene-d5 74 27 - 110

Phenol-d5 84 30 - 112

Terphenyl-d14 83 21 - 130

Method Blank TICs- Batch: 180-54209

Cas Number Analyte RT Est. Result Qual

Tentatively Identified Compound None




Dilution:

Dilution:

Lab Control Sample/

Lab Control Sample Duplicate Recovery Report - Batch: 180-54209

1.0

1.0

Sediment

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Units:

Instrument ID:

Lab File ID:



Injection Volume:


Units:

Instrument ID:

Lab File ID:



Injection Volume:

ug/Kg

F1107003.D

30.0 g

10.0 mL

2 uL

F1107004.D

30.0 g

10.0 mL

2 uL

ug/Kg

Method: 8270C LL

Preparation: 3541

722

722

LCS 180-54209/2-B

LCSD 180-54209/3-B

Analysis Date:

Prep Date:

Leach Date:

11/07/2012 0843

11/05/2012 0739

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

180-54476

180-54209

N/A

Analysis Date:

Prep Date:

Leach Date:

11/07/2012 0904

11/05/2012 0739

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

180-54476

180-54209

N/A

Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS

% Rec.

7474 30 - 150 0 401,1'-Biphenyl

7973 30 - 150 8 40Acetophenone

112115 30 - 150 3 40Atrazine

3735 30 - 150 6 40Benzaldehyde

9395 30 - 150 2 40Caprolactam

7475 42 - 104 2 34Acenaphthene

7980 43 - 117 0 36Acenaphthylene

7774 43 - 111 3 35Anthracene

7876 45 - 110 3 31Benzo[a]anthracene

7676 42 - 114 0 31Benzo[a]pyrene

6766 37 - 108 2 28Benzo[b]fluoranthene

7474 35 - 127 1 21Benzo[g,h,i]perylene

6971 39 - 115 3 42Benzo[k]fluoranthene

7975 40 - 100 5 33Bis(2-chloroethyl)ether

7575 42 - 103 0 35Bis(2-chloroethoxy)methane

7773 41 - 121 5 31Bis(2-ethylhexyl) phthalate

7172 43 - 111 1 204-Bromophenyl phenyl ether

7473 40 - 117 1 34Butyl benzyl phthalate

8383 42 - 114 0 35Carbazole

7979 33 - 102 0 284-Chloroaniline

7069 40 - 104 2 342-Chloronaphthalene

8273 42 - 111 12 374-Chlorophenyl phenyl ether

7979 44 - 108 0 31Chrysene

6868 34 - 131 0 32Dibenz(a,h)anthracene

7371 42 - 106 2 33Dibenzofuran

8281 44 - 120 2 34Di-n-butyl phthalate

8886 24 - 113 2 303,3'-Dichlorobenzidine

8876 44 - 113 14 32Diethyl phthalate

7373 44 - 111 0 34Dimethyl phthalate

8380 48 - 118 3 332,4-Dinitrotoluene

8079 47 - 119 2 302,6-Dinitrotoluene

7067 35 - 129 4 33Di-n-octyl phthalate

8784 40 - 118 3 23Fluoranthene

8476 43 - 110 10 37Fluorene

7169 42 - 110 3 29Hexachlorobenzene

7275 40 - 114 4 25Hexachlorobutadiene




Dilution:

Dilution:

Lab Control Sample/

Lab Control Sample Duplicate Recovery Report - Batch: 180-54209

1.0

1.0

Sediment

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Units:

Instrument ID:

Lab File ID:



Injection Volume:


Units:

Instrument ID:

Lab File ID:



Injection Volume:

ug/Kg

F1107003.D

30.0 g

10.0 mL

2 uL

F1107004.D

30.0 g

10.0 mL

2 uL

ug/Kg

Method: 8270C LL

Preparation: 3541

722

722

LCS 180-54209/2-B

LCSD 180-54209/3-B

Analysis Date:

Prep Date:

Leach Date:

11/07/2012 0843

11/05/2012 0739

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

180-54476

180-54209

N/A

Analysis Date:

Prep Date:

Leach Date:

11/07/2012 0904

11/05/2012 0739

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

180-54476

180-54209

N/A

Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS

% Rec.

8181 10 - 150 0 33Hexachlorocyclopentadiene

8076 40 - 102 5 34Hexachloroethane

6970 34 - 130 1 30Indeno[1,2,3-cd]pyrene

7677 39 - 114 1 33Isophorone

7779 43 - 105 2 342-Methylnaphthalene

7979 42 - 104 0 25Naphthalene

7471 41 - 118 3 332-Nitroaniline

8281 38 - 116 2 273-Nitroaniline

9687 37 - 120 10 314-Nitroaniline

7273 40 - 109 2 31Nitrobenzene

7872 42 - 108 8 32N-Nitrosodi-n-propylamine

7676 41 - 110 1 32N-Nitrosodiphenylamine

7471 41 - 107 4 20Phenanthrene

7067 39 - 113 3 28Pyrene

8283 43 - 110 2 314-Chloro-3-methylphenol

8076 40 - 105 5 372-Chlorophenol

8077 41 - 104 4 372-Methylphenol

8581 43 - 107 5 36Methylphenol, 3 & 4

7779 44 - 110 2 272,4-Dichlorophenol

7072 39 - 106 3 422,4-Dimethylphenol

7180 19 - 140 12 432,4-Dinitrophenol

7880 28 - 130 2 354,6-Dinitro-2-methylphenol

8279 27 - 131 4 334-Nitrophenol

7980 45 - 112 1 302-Nitrophenol

8283 18 - 125 1 34Pentachlorophenol

7874 39 - 105 5 40Phenol

7474 42 - 110 0 352,4,5-Trichlorophenol

7168 43 - 111 4 362,4,6-Trichlorophenol

7670 37 - 105 8 312,2'-oxybis[1-chloropropane]

8186 43 - 108 7 362,3,4,6-Tetrachlorophenol

7371 30 - 125 2 251,2,4,5-Tetrachlorobenzene

6562 41 - 102 5 351,4-Dioxane

Surrogate LCS % Rec LCSD % Rec Acceptance Limits

2,4,6-Tribromophenol 84 83 21 - 116

2-Fluorobiphenyl 74 73 28 - 108




Surrogate LCS % Rec LCSD % Rec Acceptance Limits

2-Fluorophenol 87 88 28 - 107

Nitrobenzene-d5 80 78 27 - 110

Phenol-d5 83 88 30 - 112

Terphenyl-d14 78 79 21 - 130




Sediment

11/07/2012 0843

Dilution: Dilution:1.0 1.0

Client Matrix:

LCSD Lab Sample ID:


Laboratory Control/

Laboratory Duplicate Data Report - Batch: 180-54209

Method: 8270C LL

Preparation: 3541

Units: ug/KgLCS 180-54209/2-B LCSD 180-54209/3-BLCS Lab Sample ID:

Analysis Date:

Prep Date:

Leach Date:

11/05/2012 0739

Analysis Date:

Prep Date:

Leach Date:

11/07/2012 0904

11/05/2012 0739

N/AN/A

LCSD

Result/Qual

LCS

Result/Qual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

246247333 3331,1'-Biphenyl

264243333 333Acetophenone

373383333 333Atrazine

124116333 333Benzaldehyde

308316333 333Caprolactam

246250333 333Acenaphthene

265266333 333Acenaphthylene

255248333 333Anthracene

259252333 333Benzo[a]anthracene

254254333 333Benzo[a]pyrene

223220333 333Benzo[b]fluoranthene

245247333 333Benzo[g,h,i]perylene

231238333 333Benzo[k]fluoranthene

262248333 333Bis(2-chloroethyl)ether

249250333 333Bis(2-chloroethoxy)methane

258245333 333Bis(2-ethylhexyl) phthalate

237239333 3334-Bromophenyl phenyl ether

246243333 333Butyl benzyl phthalate

277276333 333Carbazole

263263333 3334-Chloroaniline

235230333 3332-Chloronaphthalene

273244333 3334-Chlorophenyl phenyl ether

262263333 333Chrysene

227228333 333Dibenz(a,h)anthracene

242238333 333Dibenzofuran

273269333 333Di-n-butyl phthalate

293287333 3333,3'-Dichlorobenzidine

292253333 333Diethyl phthalate

243242333 333Dimethyl phthalate

276268333 3332,4-Dinitrotoluene

268262333 3332,6-Dinitrotoluene

232224333 333Di-n-octyl phthalate

290280333 333Fluoranthene

281253333 333Fluorene

237229333 333Hexachlorobenzene

239249333 333Hexachlorobutadiene

271271333 333Hexachlorocyclopentadiene

267253333 333Hexachloroethane

229232333 333Indeno[1,2,3-cd]pyrene




Sediment

11/07/2012 0843

Dilution: Dilution:1.0 1.0

Client Matrix:

LCSD Lab Sample ID:


Laboratory Control/

Laboratory Duplicate Data Report - Batch: 180-54209

Method: 8270C LL

Preparation: 3541

Units: ug/KgLCS 180-54209/2-B LCSD 180-54209/3-BLCS Lab Sample ID:

Analysis Date:

Prep Date:

Leach Date:

11/05/2012 0739

Analysis Date:

Prep Date:

Leach Date:

11/07/2012 0904

11/05/2012 0739

N/AN/A

LCSD

Result/Qual

LCS

Result/Qual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

255258333 333Isophorone

258263333 3332-Methylnaphthalene

262263333 333Naphthalene

245237333 3332-Nitroaniline



240244333 333Nitrobenzene

259240333 333N-Nitrosodi-n-propylamine

252254333 333N-Nitrosodiphenylamine

246235333 333Phenanthrene

232225333 333Pyrene

273277333 3334-Chloro-3-methylphenol

265253333 3332-Chlorophenol

267256333 3332-Methylphenol

568540667 667Methylphenol, 3 & 4

257262333 3332,4-Dichlorophenol

233239333 3332,4-Dimethylphenol

237267333 3332,4-Dinitrophenol

261266333 3334,6-Dinitro-2-methylphenol

274264333 3334-Nitrophenol

264266333 3332-Nitrophenol

274277333 333Pentachlorophenol

259247333 333Phenol

246247333 3332,4,5-Trichlorophenol

237228333 3332,4,6-Trichlorophenol

253234333 3332,2'-oxybis[1-chloropropane]

269287333 3332,3,4,6-Tetrachlorophenol

242238333 3331,2,4,5-Tetrachlorobenzene

217207333 3331,4-Dioxane


DATA REPORTING QUALIFIERS


Lab Section Qualifier Description

GC/MS Semi VOA

Indicates an Estimated Value for TICsJ

Indicates the analyte was analyzed for but not detected.U

Result is less than the RL but greater than or equal to the MDL and the

concentration is an approximate value.

J

Sample was prepped or analyzed beyond the specified holding timeH

Surrogate is outside control limitsX

This flag indicates the presumptive evidence of a compound.N




QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

GC/MS Semi VOA

Prep Batch: 180-54209

Lab Control Sample Sediment 3541LCS 180-54209/2-B T

Lab Control Sample Duplicate Sediment 3541LCSD 180-54209/3-B T

Method Blank Sediment 3541MB 180-54209/1-B T

SedimentSED-20121017-1 3541180-15932-1 T

Analysis Batch:180-54476

Lab Control Sample Sediment 180-542098270C LLLCS 180-54209/2-B T

Lab Control Sample Duplicate Sediment 180-542098270C LLLCSD 180-54209/3-B T

Method Blank Sediment 180-542098270C LLMB 180-54209/1-B T

Sediment 180-54209SED-20121017-1 8270C LL180-15932-1 T

Report Basis

T = Total

General Chemistry

Analysis Batch:180-54503

SedimentSED-20121017-1 Moisture180-15932-1 T

Report Basis

T = Total


Page 25 of 334



Laboratory Chronicle

10/31/2012 09:00

Lab ID:

Method Bottle ID Run

Analysis

Batch Prep Batch

Date Prepared /

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: Received Date/Time:10/17/2012 15:10

180-15932-1 SED-20121017-1

P:3541 180-15932-A-1-B 180-54476 180-54209 11/05/2012 07:39 KGTAL PIT5

A:8270C LL 180-15932-A-1-B 180-54476 180-54209 11/07/2012 09:25 SABTAL PIT5

A:Moisture 180-15932-A-1 180-54503 10/30/2012 15:38 SKTAL PIT1

Lab ID:


Analysis

Batch Prep Batch

Date Prepared /


Client ID:

Sample Date/Time: N/A Received Date/Time: N/A

MB N/A

P:3541 MB 180-54209/1-B 180-54476 180-54209 11/05/2012 07:39 KGTAL PIT1

A:8270C LL MB 180-54209/1-B 180-54476 180-54209 11/07/2012 06:34 SABTAL PIT1

Lab ID:


Analysis

Batch Prep Batch

Date Prepared /


Client ID:


LCS N/A

P:3541 LCS 180-54209/2-B 180-54476 180-54209 11/05/2012 07:39 KGTAL PIT1

A:8270C LL LCS 180-54209/2-B 180-54476 180-54209 11/07/2012 08:43 SABTAL PIT1

Lab ID:


Analysis

Batch Prep Batch

Date Prepared /


Client ID:


LCSD N/A

P:3541 LCSD 180-54209/3-B 180-54476 180-54209 11/05/2012 07:39 KGTAL PIT1

A:8270C LL LCSD 180-54209/3-B 180-54476 180-54209 11/07/2012 09:04 SABTAL PIT1

Lab References:TAL PIT = TestAmerica Pittsburgh

A = Analytical Method P = Prep Method TestAmerica Pittsburgh

Page 26 of 334

REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

Job No.: 180-15932-1TestAmerica Pittsburgh

Reagent IDExpDate Date

Prep DilutantUsed

ReagentFinalVolume

Parent Reagent

Reagent IDVolumeAdded ConcentrationAnalyte

03/31/13 (Purchased Reagent) 1,1'-Biphenyl 200 ug/mLRestek, Lot A090885OPDODADNLSPKs_000041,2,4,5-Tetrachlorobenzene 200 ug/mL1,4-Dioxane 200 ug/mL2,6-Dichlorophenol 200 ug/mL2-Naphthylamine 200 ug/mL7,12-Dimethylbenz(a)anthracene 200 ug/mLAcetophenone 200 ug/mLBenzaldehyde 200 ug/mLBenzidine 200 ug/mLCaprolactam 200 ug/mLIndene 200 ug/mLMethyl methanesulfonate 200 ug/mLN-Nitrosopyrrolidine 200 ug/mL

07/31/13 (Purchased Reagent) 1,2,4-Trichlorobenzene 200 ug/mLSupelco, Lot LB93750OPHC8270SPKs_000271,2-Dichlorobenzene 200 ug/mL1,2-Dinitrobenzene 200 ug/mL1,2-Diphenylhydrazine 200 ug/mL1,3-Dichlorobenzene 200 ug/mL1,4-Dichlorobenzene 200 ug/mL1,4-Dinitrobenzene 200 ug/mL1-Methylnaphthalene 200 ug/mL2,2'-oxybis[1-chloropropane] 200 ug/mL2,3,4,6-Tetrachlorophenol 200 ug/mL2,3,5,6-Tetrachlorophenol 200 ug/mL2,4,5-Trichlorophenol 200 ug/mL2,4,6-Trichlorophenol 200 ug/mL2,4-Dichlorophenol 200 ug/mL2,4-Dimethylphenol 200 ug/mL2,4-Dinitrophenol 200 ug/mL2,4-Dinitrotoluene 200 ug/mL2,6-Dinitrotoluene 200 ug/mL2-Chloronaphthalene 200 ug/mL2-Chlorophenol 200 ug/mL2-Methylnaphthalene 200 ug/mL2-Methylphenol 200 ug/mL2-Nitroaniline 200 ug/mL2-Nitrophenol 200 ug/mL3 & 4 Methylphenol 400 ug/mL3,3'-Dichlorobenzidine 200 ug/mL3-Methylphenol 200 ug/mL3-Nitroaniline 200 ug/mL4,6-Dinitro-2-methylphenol 200 ug/mL4-Bromophenyl phenyl ether 200 ug/mL4-Chloro-3-methylphenol 200 ug/mL4-Chloroaniline 200 ug/mL4-Chlorophenyl phenyl ether 200 ug/mL4-Nitroaniline 200 ug/mL

Page 27 of 334


Lab Name:

SDG No.:



Prep DilutantUsed

ReagentFinalVolume

Parent Reagent


4-Nitrophenol 200 ug/mLAcenaphthene 200 ug/mLAcenaphthylene 200 ug/mLAniline 200 ug/mLAnthracene 200 ug/mLBenzo[a]anthracene 200 ug/mLBenzo[a]pyrene 200 ug/mLBenzo[b]fluoranthene 200 ug/mLBenzo[g,h,i]perylene 200 ug/mLBenzo[k]fluoranthene 200 ug/mLBenzoic acid 200 ug/mLBenzyl alcohol 200 ug/mLBis(2-chloroethoxy)methane 200 ug/mLBis(2-chloroethyl)ether 200 ug/mLBis(2-ethylhexyl) phthalate 200 ug/mLBis-2-ethylhexyl adipate 200 ug/mLButyl benzyl phthalate 200 ug/mLCarbazole 200 ug/mLChrysene 200 ug/mLDi-n-butyl phthalate 200 ug/mLDi-n-octyl phthalate 200 ug/mLDibenz(a,h)anthracene 200 ug/mLDibenzofuran 200 ug/mLDiethyl phthalate 200 ug/mLDimethyl phthalate 200 ug/mLFluoranthene 200 ug/mLFluorene 200 ug/mLHexachlorobenzene 200 ug/mLHexachlorobutadiene 200 ug/mLHexachlorocyclopentadiene 200 ug/mLHexachloroethane 200 ug/mLIndeno[1,2,3-cd]pyrene 200 ug/mLIsophorone 200 ug/mLMethyl Phenols,Total 600 ug/mLMethylphenol, 3 & 4 400 ug/mLN-Nitrosodi-n-propylamine 200 ug/mLN-Nitrosodimethylamine 200 ug/mLN-Nitrosodiphenylamine 200 ug/mLNaphthalene 200 ug/mLNitrobenzene 200 ug/mLPentachlorophenol 200 ug/mLPhenanthrene 200 ug/mLPhenol 200 ug/mLPyrene 200 ug/mLPyridine 200 ug/mLTotal Cresols 600 ug/mL

OPABSURRSPKs_00013 1,2-Dichlorobenzene-d4 200 ug/mL500 mL 100 mL06/19/13 10/19/12OPQL-8270SURi_00040 Methanol, Lot DG596

Page 28 of 334


Lab Name:

SDG No.:



Prep DilutantUsed

ReagentFinalVolume

Parent Reagent


2,4,6-Tribromophenol 300 ug/mL2-Chlorophenol-d4 300 ug/mL2-Fluorobiphenyl 200 ug/mL2-Fluorophenol 300 ug/mLNitrobenzene-d5 200 ug/mLPhenol-d5 300 ug/mLTerphenyl-d14 200 ug/mL

05/31/15 (Purchased Reagent) 1,2-Dichlorobenzene-d4 1000 ug/mLSupelco, Lot LB92759.OPABSURRSPKs_000132,4,6-Tribromophenol 1500 ug/mL2-Chlorophenol-d4 1500 ug/mL2-Fluorobiphenyl 1000 ug/mL2-Fluorophenol 1500 ug/mLNitrobenzene-d5 1000 ug/mLPhenol-d5 1500 ug/mLTerphenyl-d14 1000 ug/mL

SVSS1245TCBs_00003 1,2,4,5-Tetrachlorobenzene 10 ug/mL1 mL 0.01 mL10/31/12 09/07/12SV2NDSOURCEi_00009 mecl2, Lot 4954471,4-Dioxane 10 ug/mLSVSS14DIOXANs_00001 0.01 mL2,6-Dichlorophenol 10 ug/mLSVSS26DCPs_00003 0.01 mL1-Methylnaphthalene 10 ug/mLSVSSADDONs_00001 0.005 mL2,3,4,6-Tetrachlorophenol 10 ug/mL2,3,5,6-Tetrachlorophenol 10 ug/mLMethyl methanesulfonate 10 ug/mL3,3'-Dichlorobenzidine 10 ug/mLSVSSBENZIDNs_00002 0.005 mL1,2,4-Trichlorobenzene 10 ug/mLSVSSCALIBMX1s_00003 0.01 mL1,2-Diphenylhydrazine 10 ug/mL2,2'-oxybis[1-chloropropane] 10 ug/mL2,4,5-Trichlorophenol 10 ug/mL2,4,6-Trichlorophenol 10 ug/mL2,4-Dichlorophenol 10 ug/mL2,4-Dimethylphenol 10 ug/mL2,4-Dinitrophenol 10 ug/mL2,4-Dinitrotoluene 10 ug/mL2,6-Dinitrotoluene 10 ug/mL2-Chloronaphthalene 10 ug/mL2-Chlorophenol 10 ug/mL2-Methylnaphthalene 10 ug/mL2-Methylphenol 10 ug/mL2-Nitroaniline 10 ug/mL2-Nitrophenol 10 ug/mL3-Nitroaniline 10 ug/mL4,6-Dinitro-2-methylphenol 10 ug/mL4-Bromophenyl phenyl ether 10 ug/mL4-Chloro-3-methylphenol 10 ug/mL4-Chloroaniline 10 ug/mL4-Chlorophenyl phenyl ether 10 ug/mL4-Nitroaniline 10 ug/mL4-Nitrophenol 10 ug/mL

Page 29 of 334


Lab Name:

SDG No.:



Prep DilutantUsed

ReagentFinalVolume

Parent Reagent


Acenaphthene 10 ug/mLAcenaphthylene 10 ug/mLAnthracene 10 ug/mLBenzo[a]anthracene 10 ug/mLBenzo[a]pyrene 10 ug/mLBenzo[b]fluoranthene 10 ug/mLBenzo[g,h,i]perylene 10 ug/mLBenzo[k]fluoranthene 10 ug/mLBis(2-chloroethoxy)methane 10 ug/mLBis(2-chloroethyl)ether 10 ug/mLBis(2-ethylhexyl) phthalate 10 ug/mLButyl benzyl phthalate 10 ug/mLCarbazole 10 ug/mLChrysene 10 ug/mLDi-n-butyl phthalate 10 ug/mLDi-n-octyl phthalate 10 ug/mLDibenz(a,h)anthracene 10 ug/mLDibenzofuran 10 ug/mLDiethyl phthalate 10 ug/mLDimethyl phthalate 10 ug/mLFluoranthene 10 ug/mLFluorene 10 ug/mLHexachlorobenzene 10 ug/mLHexachlorobutadiene 10 ug/mLHexachlorocyclopentadiene 10 ug/mLHexachloroethane 10 ug/mLIndeno[1,2,3-cd]pyrene 10 ug/mLIsophorone 10 ug/mLMethylphenol, 3 & 4 10 ug/mLN-Nitrosodi-n-propylamine 10 ug/mLN-Nitrosodimethylamine 10 ug/mLNaphthalene 10 ug/mLNitrobenzene 10 ug/mLPentachlorophenol 10 ug/mLPhenanthrene 10 ug/mLPhenol 10 ug/mLPyrene 10 ug/mLAniline 10 ug/mLSVSSCALIBMX4s_00003 0.005 mLBenzyl alcohol 10 ug/mLPyridine 10 ug/mLN-Nitrosodiphenylamine 10 ug/mLSVSSNNITRDPAs_00007 0.002 mL1,1'-Biphenyl 10 ug/mLSVSSOLMO42s_00003 0.005 mLAcetophenone 10 ug/mLCaprolactam 10 ug/mL

02/22/15 (Purchased Reagent) 1,2,4,5-Tetrachlorobenzene 1000 ug/mLSpex Certiprep, Lot T1090123013.SVSS1245TCBs_0000308/09/15 (Purchased Reagent) 1,4-Dioxane 1000 ug/mLAbsolute, Lot 080910.SVSS14DIOXANs_0000106/04/13 (Purchased Reagent) 2,6-Dichlorophenol 1000 ug/mLSpex Certiprep, Lot N1060606003.SVSS26DCPs_0000309/30/14 (Purchased Reagent) 1-Methylnaphthalene 2000 ug/mLSupelco, Lot LB66202.SVSSADDONs_00001

Page 30 of 334


Lab Name:

SDG No.:



Prep DilutantUsed

ReagentFinalVolume

Parent Reagent


2,3,4,6-Tetrachlorophenol 2000 ug/mL2,3,5,6-Tetrachlorophenol 2000 ug/mLMethyl methanesulfonate 2000 ug/mL

06/30/14 (Purchased Reagent) 3,3'-Dichlorobenzidine 2000 ug/mLSupelco, Lot LB85259.SVSSBENZIDNs_0000204/30/13 (Purchased Reagent) 1,2,4-Trichlorobenzene 1000 ug/mLSupelco, Lot LB75037.SVSSCALIBMX1s_00003

1,2-Diphenylhydrazine 1000 ug/mL2,2'-oxybis[1-chloropropane] 1000 ug/mL2,4,5-Trichlorophenol 1000 ug/mL2,4,6-Trichlorophenol 1000 ug/mL2,4-Dichlorophenol 1000 ug/mL2,4-Dimethylphenol 1000 ug/mL2,4-Dinitrophenol 1000 ug/mL2,4-Dinitrotoluene 1000 ug/mL2,6-Dinitrotoluene 1000 ug/mL2-Chloronaphthalene 1000 ug/mL2-Chlorophenol 1000 ug/mL2-Methylnaphthalene 1000 ug/mL2-Methylphenol 1000 ug/mL2-Nitroaniline 1000 ug/mL2-Nitrophenol 1000 ug/mL3-Nitroaniline 1000 ug/mL4,6-Dinitro-2-methylphenol 1000 ug/mL4-Bromophenyl phenyl ether 1000 ug/mL4-Chloro-3-methylphenol 1000 ug/mL4-Chloroaniline 1000 ug/mL4-Chlorophenyl phenyl ether 1000 ug/mL4-Nitroaniline 1000 ug/mL4-Nitrophenol 1000 ug/mLAcenaphthene 1000 ug/mLAcenaphthylene 1000 ug/mLAnthracene 1000 ug/mLBenzo[a]anthracene 1000 ug/mLBenzo[a]pyrene 1000 ug/mLBenzo[b]fluoranthene 1000 ug/mLBenzo[g,h,i]perylene 1000 ug/mLBenzo[k]fluoranthene 1000 ug/mLBis(2-chloroethoxy)methane 1000 ug/mLBis(2-chloroethyl)ether 1000 ug/mLBis(2-ethylhexyl) phthalate 1000 ug/mLButyl benzyl phthalate 1000 ug/mLCarbazole 1000 ug/mLChrysene 1000 ug/mLDi-n-butyl phthalate 1000 ug/mLDi-n-octyl phthalate 1000 ug/mLDibenz(a,h)anthracene 1000 ug/mLDibenzofuran 1000 ug/mLDiethyl phthalate 1000 ug/mLDimethyl phthalate 1000 ug/mL

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ReagentFinalVolume

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Fluoranthene 1000 ug/mLFluorene 1000 ug/mLHexachlorobenzene 1000 ug/mLHexachlorobutadiene 1000 ug/mLHexachlorocyclopentadiene 1000 ug/mLHexachloroethane 1000 ug/mLIndeno[1,2,3-cd]pyrene 1000 ug/mLIsophorone 1000 ug/mLMethylphenol, 3 & 4 1000 ug/mLN-Nitrosodi-n-propylamine 1000 ug/mLN-Nitrosodimethylamine 1000 ug/mLNaphthalene 1000 ug/mLNitrobenzene 1000 ug/mLPentachlorophenol 1000 ug/mLPhenanthrene 1000 ug/mLPhenol 1000 ug/mLPyrene 1000 ug/mL

05/31/14 (Purchased Reagent) Aniline 2000 ug/mLSupelco, Lot LB86775.SVSSCALIBMX4s_00003Benzyl alcohol 2000 ug/mLPyridine 2000 ug/mL

02/28/14 (Purchased Reagent) N-Nitrosodiphenylamine 5000 ug/mLSupelco, Lot LB82298.SVSSNNITRDPAs_0000710/31/12 (Purchased Reagent) 1,1'-Biphenyl 2000 ug/mLSupelco, Lot LB70627.SVSSOLMO42s_00003

Acetophenone 2000 ug/mLCaprolactam 2000 ug/mL

09/30/14 (Purchased Reagent) Atrazine 200 ug/mLRestek, Lot A030933SVATRAZINEs_00034

SV2NAPAMINEs_00001 2-Naphthylamine 10 ug/mL1 mL 0.01 mL10/31/12 09/07/12SVDOD2NDSORi_00004 MeCl2, Lot 495447Benzidine 10 ug/mLSVBENZIDINEDs_00001 0.01 mLAtrazine 10 ug/mLSVSSOLMO42s_00002 0.005 mLBenzaldehyde 10 ug/mL

04/30/14 (Purchased Reagent) 2-Naphthylamine 1000 ug/mLUltra Scientific, Lot CG-1087.SV2NAPAMINEs_0000110/11/13 (Purchased Reagent) Benzidine 1000 ug/mLAbsolute, Lot 101110.SVBENZIDINEDs_0000110/31/12 (Purchased Reagent) Atrazine 2000 ug/mLSupelco, Lot LB70627.SVSSOLMO42s_00002

Benzaldehyde 2000 ug/mL

SV24DINITPOHi_00004 2,4-Dinitrophenol 1 ug/mL1 mL 0.008 mL12/12/12 07/30/12SVLLSSTD0.4i_00010 MeCl2, Lot 4800194,6-Dinitro-2-methylphenol 1 ug/mLSV46DN2MPHOHi_00004 0.008 mL4-Nitrophenol 1 ug/mLSV4NITPHOHi_00004 0.008 mLBenzoic acid 1 ug/mLSVBENZOICACi_00005 0.008 mL1-Methylnaphthalene 0.2 ug/mLSVLLSTOCKi_00008 0.005 mL2,3,4,6-Tetrachlorophenol 0.2 ug/mL2,3,5,6-Tetrachlorophenol 0.2 ug/mL2-Naphthylamine 0.2 ug/mL7,12-Dimethylbenz(a)anthracene 0.2 ug/mLMethyl methanesulfonate 0.2 ug/mL1,2,4,5-Tetrachlorobenzene 0.2 ug/mL1,4-Dioxane 0.2 ug/mL2,6-Dichlorophenol 0.2 ug/mL2,4,6-Tribromophenol 0.2 ug/mL

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2-Fluorophenol 0.2 ug/mLPhenol-d5 0.2 ug/mL3,3'-Dichlorobenzidine 0.2 ug/mLBenzidine 0.2 ug/mL2-Fluorobiphenyl 0.2 ug/mLNitrobenzene-d5 0.2 ug/mLTerphenyl-d14 0.2 ug/mLAniline 0.2 ug/mLBenzoic acid 1 ug/mLBenzyl alcohol 0.2 ug/mLPyridine 0.2 ug/mL1,1'-Biphenyl 0.2 ug/mLAcetophenone 0.2 ug/mLAtrazine 0.2 ug/mLBenzaldehyde 0.2 ug/mLCaprolactam 0.2 ug/mL1,2,4-Trichlorobenzene 0.2 ug/mL1,2-Dichlorobenzene 0.2 ug/mL1,2-Diphenylhydrazine 0.2 ug/mL1,3-Dichlorobenzene 0.2 ug/mL1,4-Dichlorobenzene 0.2 ug/mL2,2'-oxybis[1-chloropropane] 0.2 ug/mL2,4,5-Trichlorophenol 0.2 ug/mL2,4,6-Trichlorophenol 0.2 ug/mL2,4-Dichlorophenol 0.2 ug/mL2,4-Dimethylphenol 0.2 ug/mL2,4-Dinitrophenol 1 ug/mL2,4-Dinitrotoluene 0.2 ug/mL2,6-Dinitrotoluene 0.2 ug/mL2-Chloronaphthalene 0.2 ug/mL2-Chlorophenol 0.2 ug/mL2-Methylnaphthalene 0.2 ug/mL2-Methylphenol 0.2 ug/mL2-Nitroaniline 0.2 ug/mL2-Nitrophenol 0.2 ug/mL3-Nitroaniline 0.2 ug/mL4,6-Dinitro-2-methylphenol 1 ug/mL4-Bromophenyl phenyl ether 0.2 ug/mL4-Chloro-3-methylphenol 0.2 ug/mL4-Chloroaniline 0.2 ug/mL4-Chlorophenyl phenyl ether 0.2 ug/mL4-Nitroaniline 0.2 ug/mL4-Nitrophenol 1 ug/mLAcenaphthene 0.2 ug/mLAcenaphthylene 0.2 ug/mLAnthracene 0.2 ug/mLBenzo[a]anthracene 0.2 ug/mLBenzo[a]pyrene 0.2 ug/mL

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ReagentFinalVolume

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Benzo[b]fluoranthene 0.2 ug/mLBenzo[g,h,i]perylene 0.2 ug/mLBenzo[k]fluoranthene 0.2 ug/mLBis(2-chloroethoxy)methane 0.2 ug/mLBis(2-chloroethyl)ether 0.2 ug/mLBis(2-ethylhexyl) phthalate 0.2 ug/mLButyl benzyl phthalate 0.2 ug/mLCarbazole 0.2 ug/mLChrysene 0.2 ug/mLDi-n-butyl phthalate 0.2 ug/mLDi-n-octyl phthalate 0.2 ug/mLDibenz(a,h)anthracene 0.2 ug/mLDibenzofuran 0.2 ug/mLDiethyl phthalate 0.2 ug/mLDimethyl phthalate 0.2 ug/mLFluoranthene 0.2 ug/mLFluorene 0.2 ug/mLHexachlorobenzene 0.2 ug/mLHexachlorobutadiene 0.2 ug/mLHexachlorocyclopentadiene 0.2 ug/mLHexachloroethane 0.2 ug/mLIndeno[1,2,3-cd]pyrene 0.2 ug/mLIsophorone 0.2 ug/mLMethylphenol, 3 & 4 0.2 ug/mLN-Nitrosodi-n-propylamine 0.2 ug/mLN-Nitrosodimethylamine 0.2 ug/mLNaphthalene 0.2 ug/mLNitrobenzene 0.2 ug/mLPentachlorophenol 1 ug/mLPhenanthrene 0.2 ug/mLPhenol 0.2 ug/mLPyrene 0.2 ug/mLIndene 0.2 ug/mLN-Nitrosodiphenylamine 0.2 ug/mLN-Nitrosopyrrolidine 0.2 ug/mLPentachlorophenol 1 ug/mLSVPENTACHLPHi_00005 0.008 mL1,4-Dichlorobenzene-d4 4 ug/mLSVSIMINTERNi_00009 0.01 mLAcenaphthene-d10 4 ug/mLChrysene-d12 4 ug/mLNaphthalene-d8 4 ug/mLPerylene-d12 4 ug/mLPhenanthrene-d10 4 ug/mL

12/12/12 07/30/12 1 mL SV24DINITPHNs_00001 0.1 mL 2,4-Dinitrophenol 100 ug/mL.SV24DINITPOHi_00004 MeCl2, Lot 48001912/12/12 (Purchased Reagent) 2,4-Dinitrophenol 1000 ug/mLAbsolute Standards, Lot 121207..SV24DINITPHNs_0000101/30/13 07/30/12 1 mL SV46DN2MPHOHs_00001 0.1 mL 4,6-Dinitro-2-methylphenol 100 ug/mL.SV46DN2MPHOHi_00004 MeCl2, Lot 48001901/27/15 (Purchased Reagent) 4,6-Dinitro-2-methylphenol 1000 ug/mLAbsolute Standards, Lot 012710..SV46DN2MPHOHs_0000101/31/13 07/30/12 1 mL SV4NITROPHOHs_00001 0.1 mL 4-Nitrophenol 100 ug/mL.SV4NITPHOHi_00004 MeCl2, Lot 48001903/08/15 (Purchased Reagent) 4-Nitrophenol 1000 ug/mLAbsolute Standards, Lot 030810..SV4NITROPHOHs_00001

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01/31/13 07/30/12 1 mL SVBENZOICACDs_00001 0.1 mL Benzoic acid 100 ug/mL.SVBENZOICACi_00005 MeCl2, Lot 48001910/21/14 (Purchased Reagent) Benzoic acid 1000 ug/mLAbsolute Standards, Lot 102109..SVBENZOICACDs_00001

SV ADDON MIXs_00003 1-Methylnaphthalene 40 ug/mL10 mL 0.2 mL01/27/13 07/30/12.SVLLSTOCKi_00008 MeCl2, Lot 2997512,3,4,6-Tetrachlorophenol 40 ug/mL2,3,5,6-Tetrachlorophenol 40 ug/mL2-Naphthylamine 40 ug/mL7,12-Dimethylbenz(a)anthracene 40 ug/mLMethyl methanesulfonate 40 ug/mL1,2,4,5-Tetrachlorobenzene 40 ug/mLSV1245TCBENZs_00001 0.4 mL1,4-Dioxane 40 ug/mLSV14DIOXANEs_00002 0.2 mL2,6-Dichlorophenol 40 ug/mLSV26DCPHENOLs_00001 0.08 mL2,4,6-Tribromophenol 40 ug/mLSVACIDSURMIXs_00001 0.2 mL2-Fluorophenol 40 ug/mLPhenol-d5 40 ug/mL3,3'-Dichlorobenzidine 40 ug/mLSVBENZIDINEs_00008 0.2 mLBenzidine 40 ug/mL2-Fluorobiphenyl 40 ug/mLSVBNSURMIXs_00003 0.4 mLNitrobenzene-d5 40 ug/mLTerphenyl-d14 40 ug/mLAniline 40 ug/mLSVCALIBMIX4s_00002 0.2 mLBenzoic acid 40 ug/mLBenzyl alcohol 40 ug/mLPyridine 40 ug/mL1,1'-Biphenyl 40 ug/mLSVCLPOLM4MIXs_00003 0.2 mLAcetophenone 40 ug/mLAtrazine 40 ug/mLBenzaldehyde 40 ug/mLCaprolactam 40 ug/mL1,2,4-Trichlorobenzene 40 ug/mLSVCLPSVMIXs_00005 0.4 mL1,2-Dichlorobenzene 40 ug/mL1,2-Diphenylhydrazine 40 ug/mL1,3-Dichlorobenzene 40 ug/mL1,4-Dichlorobenzene 40 ug/mL2,2'-oxybis[1-chloropropane] 40 ug/mL2,4,5-Trichlorophenol 40 ug/mL2,4,6-Trichlorophenol 40 ug/mL2,4-Dichlorophenol 40 ug/mL2,4-Dimethylphenol 40 ug/mL2,4-Dinitrophenol 40 ug/mL2,4-Dinitrotoluene 40 ug/mL2,6-Dinitrotoluene 40 ug/mL2-Chloronaphthalene 40 ug/mL2-Chlorophenol 40 ug/mL2-Methylnaphthalene 40 ug/mL2-Methylphenol 40 ug/mL2-Nitroaniline 40 ug/mL2-Nitrophenol 40 ug/mL3-Nitroaniline 40 ug/mL

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ReagentFinalVolume

Parent Reagent


4,6-Dinitro-2-methylphenol 40 ug/mL4-Bromophenyl phenyl ether 40 ug/mL4-Chloro-3-methylphenol 40 ug/mL4-Chloroaniline 40 ug/mL4-Chlorophenyl phenyl ether 40 ug/mL4-Nitroaniline 40 ug/mL4-Nitrophenol 40 ug/mLAcenaphthene 40 ug/mLAcenaphthylene 40 ug/mLAnthracene 40 ug/mLBenzo[a]anthracene 40 ug/mLBenzo[a]pyrene 40 ug/mLBenzo[b]fluoranthene 40 ug/mLBenzo[g,h,i]perylene 40 ug/mLBenzo[k]fluoranthene 40 ug/mLBis(2-chloroethoxy)methane 40 ug/mLBis(2-chloroethyl)ether 40 ug/mLBis(2-ethylhexyl) phthalate 40 ug/mLButyl benzyl phthalate 40 ug/mLCarbazole 40 ug/mLChrysene 40 ug/mLDi-n-butyl phthalate 40 ug/mLDi-n-octyl phthalate 40 ug/mLDibenz(a,h)anthracene 40 ug/mLDibenzofuran 40 ug/mLDiethyl phthalate 40 ug/mLDimethyl phthalate 40 ug/mLFluoranthene 40 ug/mLFluorene 40 ug/mLHexachlorobenzene 40 ug/mLHexachlorobutadiene 40 ug/mLHexachlorocyclopentadiene 40 ug/mLHexachloroethane 40 ug/mLIndeno[1,2,3-cd]pyrene 40 ug/mLIsophorone 40 ug/mLMethylphenol, 3 & 4 40 ug/mLN-Nitrosodi-n-propylamine 40 ug/mLN-Nitrosodimethylamine 40 ug/mLNaphthalene 40 ug/mLNitrobenzene 40 ug/mLPentachlorophenol 40 ug/mLPhenanthrene 40 ug/mLPhenol 40 ug/mLPyrene 40 ug/mLIndene 40 ug/mLSVINDENEs_00010 0.4 mLN-Nitrosodiphenylamine 40 ug/mLSVNNDIPHENAMs_00002 0.08 mL

SVNNITROPYROs_00001 0.4 mL N-Nitrosopyrrolidine 40 ug/mL01/31/13 (Purchased Reagent) 1-Methylnaphthalene 2000 ug/mLSupelco, Lot LB 879735..SV ADDON MIXs_00003

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ReagentFinalVolume

Parent Reagent


2,3,4,6-Tetrachlorophenol 2000 ug/mL2,3,5,6-Tetrachlorophenol 2000 ug/mL2-Naphthylamine 2000 ug/mL7,12-Dimethylbenz(a)anthracene 2000 ug/mLMethyl methanesulfonate 2000 ug/mL

09/09/13 (Purchased Reagent) 1,2,4,5-Tetrachlorobenzene 1000 ug/mLAbsolute Standards, Lot 090908..SV1245TCBENZs_0000110/31/16 (Purchased Reagent) 1,4-Dioxane 2000 ug/mLRestek, Lot A077490..SV14DIOXANEs_0000208/31/13 (Purchased Reagent) 2,6-Dichlorophenol 5000 ug/mLSupelco, Lot LB78166..SV26DCPHENOLs_0000101/31/13 (Purchased Reagent) 2,4,6-Tribromophenol 2000 ug/mLUltra Scientific, Lot CF-5141..SVACIDSURMIXs_00001

2-Fluorophenol 2000 ug/mLPhenol-d5 2000 ug/mL

01/27/13 (Purchased Reagent) 3,3'-Dichlorobenzidine 2000 ug/mLSupelco, Lot LB79050..SVBENZIDINEs_00008Benzidine 2000 ug/mL

08/30/13 (Purchased Reagent) 2-Fluorobiphenyl 1000 ug/mLUltra Scientific, Lot CG-2463..SVBNSURMIXs_00003Nitrobenzene-d5 1000 ug/mLTerphenyl-d14 1000 ug/mL

11/30/14 (Purchased Reagent) Aniline 2000 ug/mLSupelco, Lot LB88725..SVCALIBMIX4s_00002Benzoic acid 2000 ug/mLBenzyl alcohol 2000 ug/mLPyridine 2000 ug/mL

04/30/13 (Purchased Reagent) 1,1'-Biphenyl 2000 ug/mLSupelco, Lot LB73726..SVCLPOLM4MIXs_00003Acetophenone 2000 ug/mLAtrazine 2000 ug/mLBenzaldehyde 2000 ug/mLCaprolactam 2000 ug/mL

09/30/13 (Purchased Reagent) 1,2,4-Trichlorobenzene 1000 ug/mLSupelco, Lot lb78428..SVCLPSVMIXs_000051,2-Dichlorobenzene 1000 ug/mL1,2-Diphenylhydrazine 1000 ug/mL1,3-Dichlorobenzene 1000 ug/mL1,4-Dichlorobenzene 1000 ug/mL2,2'-oxybis[1-chloropropane] 1000 ug/mL2,4,5-Trichlorophenol 1000 ug/mL2,4,6-Trichlorophenol 1000 ug/mL2,4-Dichlorophenol 1000 ug/mL2,4-Dimethylphenol 1000 ug/mL2,4-Dinitrophenol 1000 ug/mL2,4-Dinitrotoluene 1000 ug/mL2,6-Dinitrotoluene 1000 ug/mL2-Chloronaphthalene 1000 ug/mL2-Chlorophenol 1000 ug/mL2-Methylnaphthalene 1000 ug/mL2-Methylphenol 1000 ug/mL2-Nitroaniline 1000 ug/mL2-Nitrophenol 1000 ug/mL3-Nitroaniline 1000 ug/mL4,6-Dinitro-2-methylphenol 1000 ug/mL4-Bromophenyl phenyl ether 1000 ug/mL4-Chloro-3-methylphenol 1000 ug/mL

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ReagentFinalVolume

Parent Reagent


4-Chloroaniline 1000 ug/mL4-Chlorophenyl phenyl ether 1000 ug/mL4-Nitroaniline 1000 ug/mL4-Nitrophenol 1000 ug/mLAcenaphthene 1000 ug/mLAcenaphthylene 1000 ug/mLAnthracene 1000 ug/mLBenzo[a]anthracene 1000 ug/mLBenzo[a]pyrene 1000 ug/mLBenzo[b]fluoranthene 1000 ug/mLBenzo[g,h,i]perylene 1000 ug/mLBenzo[k]fluoranthene 1000 ug/mLBis(2-chloroethoxy)methane 1000 ug/mLBis(2-chloroethyl)ether 1000 ug/mLBis(2-ethylhexyl) phthalate 1000 ug/mLButyl benzyl phthalate 1000 ug/mLCarbazole 1000 ug/mLChrysene 1000 ug/mLDi-n-butyl phthalate 1000 ug/mLDi-n-octyl phthalate 1000 ug/mLDibenz(a,h)anthracene 1000 ug/mLDibenzofuran 1000 ug/mLDiethyl phthalate 1000 ug/mLDimethyl phthalate 1000 ug/mLFluoranthene 1000 ug/mLFluorene 1000 ug/mLHexachlorobenzene 1000 ug/mLHexachlorobutadiene 1000 ug/mLHexachlorocyclopentadiene 1000 ug/mLHexachloroethane 1000 ug/mLIndeno[1,2,3-cd]pyrene 1000 ug/mLIsophorone 1000 ug/mLMethylphenol, 3 & 4 1000 ug/mLN-Nitrosodi-n-propylamine 1000 ug/mLN-Nitrosodimethylamine 1000 ug/mLNaphthalene 1000 ug/mLNitrobenzene 1000 ug/mLPentachlorophenol 1000 ug/mLPhenanthrene 1000 ug/mLPhenol 1000 ug/mLPyrene 1000 ug/mL

10/10/13 (Purchased Reagent) Indene 1000 ug/mLAbsolute Standards, Lot 101011..SVINDENEs_0001006/30/13 (Purchased Reagent) N-Nitrosodiphenylamine 5000 ug/mLSupelco, Lot LB76738..SVNNDIPHENAMs_0000212/09/14 (Purchased Reagent) N-Nitrosopyrrolidine 1000 ug/mLAbsolute Standards, Lot 120909..SVNNITROPYROs_0000101/31/13 07/30/12 1 mL SVPENTCLPHENs_00001 0.1 mL Pentachlorophenol 100 ug/mL.SVPENTACHLPHi_00005 MeCl2, Lot 48001909/17/14 (Purchased Reagent) Pentachlorophenol 1000 ug/mLAbsolute Standards, Lot 091709..SVPENTCLPHENs_00001

SVINTSTDMIXs_00002 1,4-Dichlorobenzene-d4 400 ug/mL10 mL 2 mL12/17/12 12/17/11.SVSIMINTERNi_00009 MeCl2, Lot 222635Acenaphthene-d10 400 ug/mL

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Chrysene-d12 400 ug/mLNaphthalene-d8 400 ug/mLPerylene-d12 400 ug/mLPhenanthrene-d10 400 ug/mL

07/31/13 (Purchased Reagent) 1,4-Dichlorobenzene-d4 2000 ug/mLSupelco, Lot LB77211..SVINTSTDMIXs_00002Acenaphthene-d10 2000 ug/mLChrysene-d12 2000 ug/mLNaphthalene-d8 2000 ug/mLPerylene-d12 2000 ug/mLPhenanthrene-d10 2000 ug/mL

SV24DINITPOHi_00004 2,4-Dinitrophenol 10 ug/mL1 mL 0.05 mL12/12/12 07/30/12SVLLSSTD10i_00006 MeCl2, Lot 4800194,6-Dinitro-2-methylphenol 10 ug/mLSV46DN2MPHOHi_00004 0.05 mL4-Nitrophenol 10 ug/mLSV4NITPHOHi_00004 0.05 mLBenzoic acid 10 ug/mLSVBENZOICACi_00005 0.05 mL1-Methylnaphthalene 5 ug/mLSVLLSTOCKi_00008 0.125 mL2,3,4,6-Tetrachlorophenol 5 ug/mL2,3,5,6-Tetrachlorophenol 5 ug/mL2-Naphthylamine 5 ug/mL7,12-Dimethylbenz(a)anthracene 5 ug/mLMethyl methanesulfonate 5 ug/mL1,2,4,5-Tetrachlorobenzene 5 ug/mL1,4-Dioxane 5 ug/mL2,6-Dichlorophenol 5 ug/mL2,4,6-Tribromophenol 5 ug/mL2-Fluorophenol 5 ug/mLPhenol-d5 5 ug/mL3,3'-Dichlorobenzidine 5 ug/mLBenzidine 5 ug/mL2-Fluorobiphenyl 5 ug/mLNitrobenzene-d5 5 ug/mLTerphenyl-d14 5 ug/mLAniline 5 ug/mLBenzoic acid 10 ug/mLBenzyl alcohol 5 ug/mLPyridine 5 ug/mL1,1'-Biphenyl 5 ug/mLAcetophenone 5 ug/mLAtrazine 5 ug/mLBenzaldehyde 5 ug/mLCaprolactam 5 ug/mL1,2,4-Trichlorobenzene 5 ug/mL1,2-Dichlorobenzene 5 ug/mL1,2-Diphenylhydrazine 5 ug/mL1,3-Dichlorobenzene 5 ug/mL1,4-Dichlorobenzene 5 ug/mL2,2'-oxybis[1-chloropropane] 5 ug/mL2,4,5-Trichlorophenol 5 ug/mL

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2,4,6-Trichlorophenol 5 ug/mL2,4-Dichlorophenol 5 ug/mL2,4-Dimethylphenol 5 ug/mL2,4-Dinitrophenol 10 ug/mL2,4-Dinitrotoluene 5 ug/mL2,6-Dinitrotoluene 5 ug/mL2-Chloronaphthalene 5 ug/mL2-Chlorophenol 5 ug/mL2-Methylnaphthalene 5 ug/mL2-Methylphenol 5 ug/mL2-Nitroaniline 5 ug/mL2-Nitrophenol 5 ug/mL3-Nitroaniline 5 ug/mL4,6-Dinitro-2-methylphenol 10 ug/mL4-Bromophenyl phenyl ether 5 ug/mL4-Chloro-3-methylphenol 5 ug/mL4-Chloroaniline 5 ug/mL4-Chlorophenyl phenyl ether 5 ug/mL4-Nitroaniline 5 ug/mL4-Nitrophenol 10 ug/mLAcenaphthene 5 ug/mLAcenaphthylene 5 ug/mLAnthracene 5 ug/mLBenzo[a]anthracene 5 ug/mLBenzo[a]pyrene 5 ug/mLBenzo[b]fluoranthene 5 ug/mLBenzo[g,h,i]perylene 5 ug/mLBenzo[k]fluoranthene 5 ug/mLBis(2-chloroethoxy)methane 5 ug/mLBis(2-chloroethyl)ether 5 ug/mLBis(2-ethylhexyl) phthalate 5 ug/mLButyl benzyl phthalate 5 ug/mLCarbazole 5 ug/mLChrysene 5 ug/mLDi-n-butyl phthalate 5 ug/mLDi-n-octyl phthalate 5 ug/mLDibenz(a,h)anthracene 5 ug/mLDibenzofuran 5 ug/mLDiethyl phthalate 5 ug/mLDimethyl phthalate 5 ug/mLFluoranthene 5 ug/mLFluorene 5 ug/mLHexachlorobenzene 5 ug/mLHexachlorobutadiene 5 ug/mLHexachlorocyclopentadiene 5 ug/mLHexachloroethane 5 ug/mLIndeno[1,2,3-cd]pyrene 5 ug/mLIsophorone 5 ug/mL

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Parent Reagent


Methylphenol, 3 & 4 5 ug/mLN-Nitrosodi-n-propylamine 5 ug/mLN-Nitrosodimethylamine 5 ug/mLNaphthalene 5 ug/mLNitrobenzene 5 ug/mLPentachlorophenol 10 ug/mLPhenanthrene 5 ug/mLPhenol 5 ug/mLPyrene 5 ug/mLIndene 5 ug/mLN-Nitrosodiphenylamine 5 ug/mLN-Nitrosopyrrolidine 5 ug/mLPentachlorophenol 10 ug/mLSVPENTACHLPHi_00005 0.05 mL1,4-Dichlorobenzene-d4 4 ug/mLSVSIMINTERNi_00009 0.01 mLAcenaphthene-d10 4 ug/mLChrysene-d12 4 ug/mLNaphthalene-d8 4 ug/mLPerylene-d12 4 ug/mLPhenanthrene-d10 4 ug/mL

12/12/12 07/30/12 1 mL SV24DINITPHNs_00001 0.1 mL 2,4-Dinitrophenol 100 ug/mL.SV24DINITPOHi_00004 MeCl2, Lot 48001912/12/12 (Purchased Reagent) 2,4-Dinitrophenol 1000 ug/mLAbsolute Standards, Lot 121207..SV24DINITPHNs_0000101/30/13 07/30/12 1 mL SV46DN2MPHOHs_00001 0.1 mL 4,6-Dinitro-2-methylphenol 100 ug/mL.SV46DN2MPHOHi_00004 MeCl2, Lot 48001901/27/15 (Purchased Reagent) 4,6-Dinitro-2-methylphenol 1000 ug/mLAbsolute Standards, Lot 012710..SV46DN2MPHOHs_0000101/31/13 07/30/12 1 mL SV4NITROPHOHs_00001 0.1 mL 4-Nitrophenol 100 ug/mL.SV4NITPHOHi_00004 MeCl2, Lot 48001903/08/15 (Purchased Reagent) 4-Nitrophenol 1000 ug/mLAbsolute Standards, Lot 030810..SV4NITROPHOHs_0000101/31/13 07/30/12 1 mL SVBENZOICACDs_00001 0.1 mL Benzoic acid 100 ug/mL.SVBENZOICACi_00005 MeCl2, Lot 48001910/21/14 (Purchased Reagent) Benzoic acid 1000 ug/mLAbsolute Standards, Lot 102109..SVBENZOICACDs_00001

SV ADDON MIXs_00003 1-Methylnaphthalene 40 ug/mL10 mL 0.2 mL01/27/13 07/30/12.SVLLSTOCKi_00008 MeCl2, Lot 2997512,3,4,6-Tetrachlorophenol 40 ug/mL2,3,5,6-Tetrachlorophenol 40 ug/mL2-Naphthylamine 40 ug/mL7,12-Dimethylbenz(a)anthracene 40 ug/mLMethyl methanesulfonate 40 ug/mL1,2,4,5-Tetrachlorobenzene 40 ug/mLSV1245TCBENZs_00001 0.4 mL1,4-Dioxane 40 ug/mLSV14DIOXANEs_00002 0.2 mL2,6-Dichlorophenol 40 ug/mLSV26DCPHENOLs_00001 0.08 mL2,4,6-Tribromophenol 40 ug/mLSVACIDSURMIXs_00001 0.2 mL2-Fluorophenol 40 ug/mLPhenol-d5 40 ug/mL3,3'-Dichlorobenzidine 40 ug/mLSVBENZIDINEs_00008 0.2 mLBenzidine 40 ug/mL2-Fluorobiphenyl 40 ug/mLSVBNSURMIXs_00003 0.4 mLNitrobenzene-d5 40 ug/mLTerphenyl-d14 40 ug/mLAniline 40 ug/mLSVCALIBMIX4s_00002 0.2 mLBenzoic acid 40 ug/mLBenzyl alcohol 40 ug/mLPyridine 40 ug/mL

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1,1'-Biphenyl 40 ug/mLSVCLPOLM4MIXs_00003 0.2 mLAcetophenone 40 ug/mLAtrazine 40 ug/mLBenzaldehyde 40 ug/mLCaprolactam 40 ug/mL1,2,4-Trichlorobenzene 40 ug/mLSVCLPSVMIXs_00005 0.4 mL1,2-Dichlorobenzene 40 ug/mL1,2-Diphenylhydrazine 40 ug/mL1,3-Dichlorobenzene 40 ug/mL1,4-Dichlorobenzene 40 ug/mL2,2'-oxybis[1-chloropropane] 40 ug/mL2,4,5-Trichlorophenol 40 ug/mL2,4,6-Trichlorophenol 40 ug/mL2,4-Dichlorophenol 40 ug/mL2,4-Dimethylphenol 40 ug/mL2,4-Dinitrophenol 40 ug/mL2,4-Dinitrotoluene 40 ug/mL2,6-Dinitrotoluene 40 ug/mL2-Chloronaphthalene 40 ug/mL2-Chlorophenol 40 ug/mL2-Methylnaphthalene 40 ug/mL2-Methylphenol 40 ug/mL2-Nitroaniline 40 ug/mL2-Nitrophenol 40 ug/mL3-Nitroaniline 40 ug/mL4,6-Dinitro-2-methylphenol 40 ug/mL4-Bromophenyl phenyl ether 40 ug/mL4-Chloro-3-methylphenol 40 ug/mL4-Chloroaniline 40 ug/mL4-Chlorophenyl phenyl ether 40 ug/mL4-Nitroaniline 40 ug/mL4-Nitrophenol 40 ug/mLAcenaphthene 40 ug/mLAcenaphthylene 40 ug/mLAnthracene 40 ug/mLBenzo[a]anthracene 40 ug/mLBenzo[a]pyrene 40 ug/mLBenzo[b]fluoranthene 40 ug/mLBenzo[g,h,i]perylene 40 ug/mLBenzo[k]fluoranthene 40 ug/mLBis(2-chloroethoxy)methane 40 ug/mLBis(2-chloroethyl)ether 40 ug/mLBis(2-ethylhexyl) phthalate 40 ug/mLButyl benzyl phthalate 40 ug/mLCarbazole 40 ug/mLChrysene 40 ug/mLDi-n-butyl phthalate 40 ug/mLDi-n-octyl phthalate 40 ug/mL

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Dibenz(a,h)anthracene 40 ug/mLDibenzofuran 40 ug/mLDiethyl phthalate 40 ug/mLDimethyl phthalate 40 ug/mLFluoranthene 40 ug/mLFluorene 40 ug/mLHexachlorobenzene 40 ug/mLHexachlorobutadiene 40 ug/mLHexachlorocyclopentadiene 40 ug/mLHexachloroethane 40 ug/mLIndeno[1,2,3-cd]pyrene 40 ug/mLIsophorone 40 ug/mLMethylphenol, 3 & 4 40 ug/mLN-Nitrosodi-n-propylamine 40 ug/mLN-Nitrosodimethylamine 40 ug/mLNaphthalene 40 ug/mLNitrobenzene 40 ug/mLPentachlorophenol 40 ug/mLPhenanthrene 40 ug/mLPhenol 40 ug/mLPyrene 40 ug/mLIndene 40 ug/mLSVINDENEs_00010 0.4 mLN-Nitrosodiphenylamine 40 ug/mLSVNNDIPHENAMs_00002 0.08 mL








04/30/13 (Purchased Reagent) 1,1'-Biphenyl 2000 ug/mLSupelco, Lot LB73726..SVCLPOLM4MIXs_00003Acetophenone 2000 ug/mLAtrazine 2000 ug/mL

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Benzaldehyde 2000 ug/mLCaprolactam 2000 ug/mL

09/30/13 (Purchased Reagent) 1,2,4-Trichlorobenzene 1000 ug/mLSupelco, Lot lb78428..SVCLPSVMIXs_000051,2-Dichlorobenzene 1000 ug/mL1,2-Diphenylhydrazine 1000 ug/mL1,3-Dichlorobenzene 1000 ug/mL1,4-Dichlorobenzene 1000 ug/mL2,2'-oxybis[1-chloropropane] 1000 ug/mL2,4,5-Trichlorophenol 1000 ug/mL2,4,6-Trichlorophenol 1000 ug/mL2,4-Dichlorophenol 1000 ug/mL2,4-Dimethylphenol 1000 ug/mL2,4-Dinitrophenol 1000 ug/mL2,4-Dinitrotoluene 1000 ug/mL2,6-Dinitrotoluene 1000 ug/mL2-Chloronaphthalene 1000 ug/mL2-Chlorophenol 1000 ug/mL2-Methylnaphthalene 1000 ug/mL2-Methylphenol 1000 ug/mL2-Nitroaniline 1000 ug/mL2-Nitrophenol 1000 ug/mL3-Nitroaniline 1000 ug/mL4,6-Dinitro-2-methylphenol 1000 ug/mL4-Bromophenyl phenyl ether 1000 ug/mL4-Chloro-3-methylphenol 1000 ug/mL4-Chloroaniline 1000 ug/mL4-Chlorophenyl phenyl ether 1000 ug/mL4-Nitroaniline 1000 ug/mL4-Nitrophenol 1000 ug/mLAcenaphthene 1000 ug/mLAcenaphthylene 1000 ug/mLAnthracene 1000 ug/mLBenzo[a]anthracene 1000 ug/mLBenzo[a]pyrene 1000 ug/mLBenzo[b]fluoranthene 1000 ug/mLBenzo[g,h,i]perylene 1000 ug/mLBenzo[k]fluoranthene 1000 ug/mLBis(2-chloroethoxy)methane 1000 ug/mLBis(2-chloroethyl)ether 1000 ug/mLBis(2-ethylhexyl) phthalate 1000 ug/mLButyl benzyl phthalate 1000 ug/mLCarbazole 1000 ug/mLChrysene 1000 ug/mLDi-n-butyl phthalate 1000 ug/mLDi-n-octyl phthalate 1000 ug/mLDibenz(a,h)anthracene 1000 ug/mLDibenzofuran 1000 ug/mLDiethyl phthalate 1000 ug/mL

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Dimethyl phthalate 1000 ug/mLFluoranthene 1000 ug/mLFluorene 1000 ug/mLHexachlorobenzene 1000 ug/mLHexachlorobutadiene 1000 ug/mLHexachlorocyclopentadiene 1000 ug/mLHexachloroethane 1000 ug/mLIndeno[1,2,3-cd]pyrene 1000 ug/mLIsophorone 1000 ug/mLMethylphenol, 3 & 4 1000 ug/mLN-Nitrosodi-n-propylamine 1000 ug/mLN-Nitrosodimethylamine 1000 ug/mLNaphthalene 1000 ug/mLNitrobenzene 1000 ug/mLPentachlorophenol 1000 ug/mLPhenanthrene 1000 ug/mLPhenol 1000 ug/mLPyrene 1000 ug/mL

10/10/13 (Purchased Reagent) Indene 1000 ug/mLAbsolute Standards, Lot 101011..SVINDENEs_0001006/30/13 (Purchased Reagent) N-Nitrosodiphenylamine 5000 ug/mLSupelco, Lot LB76738..SVNNDIPHENAMs_0000212/09/14 (Purchased Reagent) N-Nitrosopyrrolidine 1000 ug/mLAbsolute Standards, Lot 120909..SVNNITROPYROs_0000101/31/13 07/30/12 1 mL SVPENTCLPHENs_00001 0.1 mL Pentachlorophenol 100 ug/mL.SVPENTACHLPHi_00005 MeCl2, Lot 48001909/17/14 (Purchased Reagent) Pentachlorophenol 1000 ug/mLAbsolute Standards, Lot 091709..SVPENTCLPHENs_00001

SVINTSTDMIXs_00002 1,4-Dichlorobenzene-d4 400 ug/mL10 mL 2 mL12/17/12 12/17/11.SVSIMINTERNi_00009 MeCl2, Lot 222635Acenaphthene-d10 400 ug/mLChrysene-d12 400 ug/mLNaphthalene-d8 400 ug/mLPerylene-d12 400 ug/mLPhenanthrene-d10 400 ug/mL

07/31/13 (Purchased Reagent) 1,4-Dichlorobenzene-d4 2000 ug/mLSupelco, Lot LB77211..SVINTSTDMIXs_00002Acenaphthene-d10 2000 ug/mLChrysene-d12 2000 ug/mLNaphthalene-d8 2000 ug/mLPerylene-d12 2000 ug/mLPhenanthrene-d10 2000 ug/mL

SV24DINITPOHi_00004 2,4-Dinitrophenol 2 ug/mL1 mL 0.01 mL12/12/12 07/30/12SVLLSSTD2.0i_00006 MeCl2, Lot 4800194,6-Dinitro-2-methylphenol 2 ug/mLSV46DN2MPHOHi_00004 0.01 mL4-Nitrophenol 2 ug/mLSV4NITPHOHi_00004 0.01 mLBenzoic acid 2 ug/mLSVBENZOICACi_00005 0.01 mL1-Methylnaphthalene 1 ug/mLSVLLSTOCKi_00008 0.025 mL2,3,4,6-Tetrachlorophenol 1 ug/mL2,3,5,6-Tetrachlorophenol 1 ug/mL2-Naphthylamine 1 ug/mL7,12-Dimethylbenz(a)anthracene 1 ug/mLMethyl methanesulfonate 1 ug/mL1,2,4,5-Tetrachlorobenzene 1 ug/mL1,4-Dioxane 1 ug/mL

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2,6-Dichlorophenol 1 ug/mL2,4,6-Tribromophenol 1 ug/mL2-Fluorophenol 1 ug/mLPhenol-d5 1 ug/mL3,3'-Dichlorobenzidine 1 ug/mLBenzidine 1 ug/mL2-Fluorobiphenyl 1 ug/mLNitrobenzene-d5 1 ug/mLTerphenyl-d14 1 ug/mLAniline 1 ug/mLBenzoic acid 2 ug/mLBenzyl alcohol 1 ug/mLPyridine 1 ug/mL1,1'-Biphenyl 1 ug/mLAcetophenone 1 ug/mLAtrazine 1 ug/mLBenzaldehyde 1 ug/mLCaprolactam 1 ug/mL1,2,4-Trichlorobenzene 1 ug/mL1,2-Dichlorobenzene 1 ug/mL1,2-Diphenylhydrazine 1 ug/mL1,3-Dichlorobenzene 1 ug/mL1,4-Dichlorobenzene 1 ug/mL2,2'-oxybis[1-chloropropane] 1 ug/mL2,4,5-Trichlorophenol 1 ug/mL2,4,6-Trichlorophenol 1 ug/mL2,4-Dichlorophenol 1 ug/mL2,4-Dimethylphenol 1 ug/mL2,4-Dinitrophenol 2 ug/mL2,4-Dinitrotoluene 1 ug/mL2,6-Dinitrotoluene 1 ug/mL2-Chloronaphthalene 1 ug/mL2-Chlorophenol 1 ug/mL2-Methylnaphthalene 1 ug/mL2-Methylphenol 1 ug/mL2-Nitroaniline 1 ug/mL2-Nitrophenol 1 ug/mL3-Nitroaniline 1 ug/mL4,6-Dinitro-2-methylphenol 2 ug/mL4-Bromophenyl phenyl ether 1 ug/mL4-Chloro-3-methylphenol 1 ug/mL4-Chloroaniline 1 ug/mL4-Chlorophenyl phenyl ether 1 ug/mL4-Nitroaniline 1 ug/mL4-Nitrophenol 2 ug/mLAcenaphthene 1 ug/mLAcenaphthylene 1 ug/mLAnthracene 1 ug/mL

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ReagentFinalVolume

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Benzo[a]anthracene 1 ug/mLBenzo[a]pyrene 1 ug/mLBenzo[b]fluoranthene 1 ug/mLBenzo[g,h,i]perylene 1 ug/mLBenzo[k]fluoranthene 1 ug/mLBis(2-chloroethoxy)methane 1 ug/mLBis(2-chloroethyl)ether 1 ug/mLBis(2-ethylhexyl) phthalate 1 ug/mLButyl benzyl phthalate 1 ug/mLCarbazole 1 ug/mLChrysene 1 ug/mLDi-n-butyl phthalate 1 ug/mLDi-n-octyl phthalate 1 ug/mLDibenz(a,h)anthracene 1 ug/mLDibenzofuran 1 ug/mLDiethyl phthalate 1 ug/mLDimethyl phthalate 1 ug/mLFluoranthene 1 ug/mLFluorene 1 ug/mLHexachlorobenzene 1 ug/mLHexachlorobutadiene 1 ug/mLHexachlorocyclopentadiene 1 ug/mLHexachloroethane 1 ug/mLIndeno[1,2,3-cd]pyrene 1 ug/mLIsophorone 1 ug/mLMethylphenol, 3 & 4 1 ug/mLN-Nitrosodi-n-propylamine 1 ug/mLN-Nitrosodimethylamine 1 ug/mLNaphthalene 1 ug/mLNitrobenzene 1 ug/mLPentachlorophenol 2 ug/mLPhenanthrene 1 ug/mLPhenol 1 ug/mLPyrene 1 ug/mLIndene 1 ug/mLN-Nitrosodiphenylamine 1 ug/mLN-Nitrosopyrrolidine 1 ug/mLPentachlorophenol 2 ug/mLSVPENTACHLPHi_00005 0.01 mL1,4-Dichlorobenzene-d4 4 ug/mLSVSIMINTERNi_00009 0.01 mLAcenaphthene-d10 4 ug/mLChrysene-d12 4 ug/mLNaphthalene-d8 4 ug/mLPerylene-d12 4 ug/mLPhenanthrene-d10 4 ug/mL

12/12/12 07/30/12 1 mL SV24DINITPHNs_00001 0.1 mL 2,4-Dinitrophenol 100 ug/mL.SV24DINITPOHi_00004 MeCl2, Lot 48001912/12/12 (Purchased Reagent) 2,4-Dinitrophenol 1000 ug/mLAbsolute Standards, Lot 121207..SV24DINITPHNs_0000101/30/13 07/30/12 1 mL SV46DN2MPHOHs_00001 0.1 mL 4,6-Dinitro-2-methylphenol 100 ug/mL.SV46DN2MPHOHi_00004 MeCl2, Lot 48001901/27/15 (Purchased Reagent) 4,6-Dinitro-2-methylphenol 1000 ug/mLAbsolute Standards, Lot 012710..SV46DN2MPHOHs_00001

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01/31/13 07/30/12 1 mL SV4NITROPHOHs_00001 0.1 mL 4-Nitrophenol 100 ug/mL.SV4NITPHOHi_00004 MeCl2, Lot 48001903/08/15 (Purchased Reagent) 4-Nitrophenol 1000 ug/mLAbsolute Standards, Lot 030810..SV4NITROPHOHs_0000101/31/13 07/30/12 1 mL SVBENZOICACDs_00001 0.1 mL Benzoic acid 100 ug/mL.SVBENZOICACi_00005 MeCl2, Lot 48001910/21/14 (Purchased Reagent) Benzoic acid 1000 ug/mLAbsolute Standards, Lot 102109..SVBENZOICACDs_00001

SV ADDON MIXs_00003 1-Methylnaphthalene 40 ug/mL10 mL 0.2 mL01/27/13 07/30/12.SVLLSTOCKi_00008 MeCl2, Lot 2997512,3,4,6-Tetrachlorophenol 40 ug/mL2,3,5,6-Tetrachlorophenol 40 ug/mL2-Naphthylamine 40 ug/mL7,12-Dimethylbenz(a)anthracene 40 ug/mLMethyl methanesulfonate 40 ug/mL1,2,4,5-Tetrachlorobenzene 40 ug/mLSV1245TCBENZs_00001 0.4 mL1,4-Dioxane 40 ug/mLSV14DIOXANEs_00002 0.2 mL2,6-Dichlorophenol 40 ug/mLSV26DCPHENOLs_00001 0.08 mL2,4,6-Tribromophenol 40 ug/mLSVACIDSURMIXs_00001 0.2 mL2-Fluorophenol 40 ug/mLPhenol-d5 40 ug/mL3,3'-Dichlorobenzidine 40 ug/mLSVBENZIDINEs_00008 0.2 mLBenzidine 40 ug/mL2-Fluorobiphenyl 40 ug/mLSVBNSURMIXs_00003 0.4 mLNitrobenzene-d5 40 ug/mLTerphenyl-d14 40 ug/mLAniline 40 ug/mLSVCALIBMIX4s_00002 0.2 mLBenzoic acid 40 ug/mLBenzyl alcohol 40 ug/mLPyridine 40 ug/mL1,1'-Biphenyl 40 ug/mLSVCLPOLM4MIXs_00003 0.2 mLAcetophenone 40 ug/mLAtrazine 40 ug/mLBenzaldehyde 40 ug/mLCaprolactam 40 ug/mL1,2,4-Trichlorobenzene 40 ug/mLSVCLPSVMIXs_00005 0.4 mL1,2-Dichlorobenzene 40 ug/mL1,2-Diphenylhydrazine 40 ug/mL1,3-Dichlorobenzene 40 ug/mL1,4-Dichlorobenzene 40 ug/mL2,2'-oxybis[1-chloropropane] 40 ug/mL2,4,5-Trichlorophenol 40 ug/mL2,4,6-Trichlorophenol 40 ug/mL2,4-Dichlorophenol 40 ug/mL2,4-Dimethylphenol 40 ug/mL2,4-Dinitrophenol 40 ug/mL2,4-Dinitrotoluene 40 ug/mL2,6-Dinitrotoluene 40 ug/mL2-Chloronaphthalene 40 ug/mL2-Chlorophenol 40 ug/mL2-Methylnaphthalene 40 ug/mL2-Methylphenol 40 ug/mL2-Nitroaniline 40 ug/mL

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2-Nitrophenol 40 ug/mL3-Nitroaniline 40 ug/mL4,6-Dinitro-2-methylphenol 40 ug/mL4-Bromophenyl phenyl ether 40 ug/mL4-Chloro-3-methylphenol 40 ug/mL4-Chloroaniline 40 ug/mL4-Chlorophenyl phenyl ether 40 ug/mL4-Nitroaniline 40 ug/mL4-Nitrophenol 40 ug/mLAcenaphthene 40 ug/mLAcenaphthylene 40 ug/mLAnthracene 40 ug/mLBenzo[a]anthracene 40 ug/mLBenzo[a]pyrene 40 ug/mLBenzo[b]fluoranthene 40 ug/mLBenzo[g,h,i]perylene 40 ug/mLBenzo[k]fluoranthene 40 ug/mLBis(2-chloroethoxy)methane 40 ug/mLBis(2-chloroethyl)ether 40 ug/mLBis(2-ethylhexyl) phthalate 40 ug/mLButyl benzyl phthalate 40 ug/mLCarbazole 40 ug/mLChrysene 40 ug/mLDi-n-butyl phthalate 40 ug/mLDi-n-octyl phthalate 40 ug/mLDibenz(a,h)anthracene 40 ug/mLDibenzofuran 40 ug/mLDiethyl phthalate 40 ug/mLDimethyl phthalate 40 ug/mLFluoranthene 40 ug/mLFluorene 40 ug/mLHexachlorobenzene 40 ug/mLHexachlorobutadiene 40 ug/mLHexachlorocyclopentadiene 40 ug/mLHexachloroethane 40 ug/mLIndeno[1,2,3-cd]pyrene 40 ug/mLIsophorone 40 ug/mLMethylphenol, 3 & 4 40 ug/mLN-Nitrosodi-n-propylamine 40 ug/mLN-Nitrosodimethylamine 40 ug/mLNaphthalene 40 ug/mLNitrobenzene 40 ug/mLPentachlorophenol 40 ug/mLPhenanthrene 40 ug/mLPhenol 40 ug/mLPyrene 40 ug/mLIndene 40 ug/mLSVINDENEs_00010 0.4 mLN-Nitrosodiphenylamine 40 ug/mLSVNNDIPHENAMs_00002 0.08 mL

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04/30/13 (Purchased Reagent) 1,1'-Biphenyl 2000 ug/mLSupelco, Lot LB73726..SVCLPOLM4MIXs_00003Acetophenone 2000 ug/mLAtrazine 2000 ug/mLBenzaldehyde 2000 ug/mLCaprolactam 2000 ug/mL

09/30/13 (Purchased Reagent) 1,2,4-Trichlorobenzene 1000 ug/mLSupelco, Lot lb78428..SVCLPSVMIXs_000051,2-Dichlorobenzene 1000 ug/mL1,2-Diphenylhydrazine 1000 ug/mL1,3-Dichlorobenzene 1000 ug/mL1,4-Dichlorobenzene 1000 ug/mL2,2'-oxybis[1-chloropropane] 1000 ug/mL2,4,5-Trichlorophenol 1000 ug/mL2,4,6-Trichlorophenol 1000 ug/mL2,4-Dichlorophenol 1000 ug/mL2,4-Dimethylphenol 1000 ug/mL2,4-Dinitrophenol 1000 ug/mL2,4-Dinitrotoluene 1000 ug/mL2,6-Dinitrotoluene 1000 ug/mL2-Chloronaphthalene 1000 ug/mL2-Chlorophenol 1000 ug/mL2-Methylnaphthalene 1000 ug/mL2-Methylphenol 1000 ug/mL2-Nitroaniline 1000 ug/mL2-Nitrophenol 1000 ug/mL3-Nitroaniline 1000 ug/mL4,6-Dinitro-2-methylphenol 1000 ug/mL

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