Cannabis Report with QC...THCV-Total†

8
12423 NE Whitaker Way Portland, OR 97230 503-254-1794 Report Number: Report Date: ORELAP#: 02/11/2020 OR100028 14:00 Received: 02/04/20 Purchase Order: 20-001378/D03.R00 Product identity: #53 - 1000 Berry Tincture Client/Metrc ID: . Customer: 02/04/20 Sample Date: 20-001378-0002 Laboratory ID: Healthy Roots Summary Potency: Units Status Result Limits Analyte % CBC 0.0758 % CBC-A 0.00491 % CBD 3.53 % CBD-A 0.0164 % CBDV 0.0183 % CBG 0.0551 % ∆9-THC 0.0563 % THCV 0.00584 Units Status Result Limits Analyte per 28g 21.2 CBC per 28g mg/28g 1.37 CBC-A per 28g mg/28g 988 CBD per 28g mg/28g 4.59 CBD-A per 28g mg/28g 5.12 CBDV per 28g mg/28g 15.4 CBG per 28g mg/28g 15.8 ∆9-THC per 28g mg/28g 1.64 THCV per 28g mg/28g 992 mg/28g CBD-Total per 28g 15.8 mg/28g THC-Total per 28g (Reported in milligrams per serving) Page 1 of 8 Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unless otherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be retained for a maximum of 30 days from the receipt date unless prior arrangements have been made. Testing in accordance with: OAR 333-007-0430

Transcript of Cannabis Report with QC...THCV-Total†

Page 1: Cannabis Report with QC...THCV-Total†

12423 NE Whitaker WayPortland, OR 97230

503-254-1794

Report Number:

Report Date:

ORELAP#:

02/11/2020

OR100028

14:00Received: 02/04/20

Purchase Order:

20-001378/D03.R00

Product identity: #53 - 1000 Berry Tincture

Client/Metrc ID: .

Customer:

02/04/20Sample Date:20-001378-0002Laboratory ID:

Healthy Roots

SummaryPotency:

Units StatusResult LimitsAnalyte

%CBC† 0.0758

%CBC-A† 0.00491

%CBD 3.53

%CBD-A 0.0164

%CBDV† 0.0183

%CBG† 0.0551

%∆9-THC 0.0563

%THCV† 0.00584

Units StatusResult LimitsAnalyte per 28g

21.2CBC per 28g† mg/28g

1.37CBC-A per 28g† mg/28g

988CBD per 28g mg/28g

4.59CBD-A per 28g mg/28g

5.12CBDV per 28g† mg/28g

15.4CBG per 28g† mg/28g

15.8∆9-THC per 28g mg/28g

1.64THCV per 28g† mg/28g

992 mg/28gCBD-Total per 28g

15.8 mg/28gTHC-Total per 28g

(Reported in milligrams per serving)

Page 1 of 8Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unlessotherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be retained for a maximum of 30 days from the receipt date unlessprior arrangements have been made.

Testing in accordance with: OAR 333-007-0430

Page 2: Cannabis Report with QC...THCV-Total†

12423 NE Whitaker WayPortland, OR 97230

503-254-1794

Report Number:

Report Date:

ORELAP#:

02/11/2020

OR100028

14:00Received: 02/04/20

Purchase Order:

20-001378/D03.R00

Customer: Healthy Roots

Product identity: #53 - 1000 Berry Tincture

02/04/20Sample Date:

20-001378-0002Laboratory ID:

Client/Metrc ID: .

Jason MerrittRelinquished by:

18.7 °CTemp:

28 gServing Size #1:

Sample Results

Batch: 2001170Potency

Units LOQ Analyze NotesMethodAnalyte Result Limits

J AOAC 2015 V98-6% 02/05/20CBC† 0.0758 0.0032

J AOAC 2015 V98-6% 02/05/20CBC-A† 0.00491 0.0032

J AOAC 2015 V98-6% 02/11/20CBC-Total† 0.0801 0.0061

J AOAC 2015 V98-6% 02/06/20CBD 3.53 0.0325

J AOAC 2015 V98-6% 02/05/20CBD-A 0.0164 0.0032

J AOAC 2015 V98-6% 02/11/20CBD-Total 3.54 0.0353

J AOAC 2015 V98-6% 02/05/20CBDV† 0.0183 0.0032

J AOAC 2015 V98-6% 02/05/20CBDV-A† < LOQ 0.0032

J AOAC 2015 V98-6% 02/11/20CBDV-Total† 0.0183 0.0061

J AOAC 2015 V98-6% 02/05/20CBG† 0.0551 0.0032

J AOAC 2015 V98-6% 02/05/20CBG-A† < LOQ 0.0032

J AOAC 2015 V98-6% 02/11/20CBG-Total† 0.0551 0.0061

J AOAC 2015 V98-6% 02/05/20CBL† < LOQ 0.0032

J AOAC 2015 V98-6% 02/05/20CBN < LOQ 0.0032

J AOAC 2015 V98-6% 02/05/20∆8-THC† < LOQ 0.0032

J AOAC 2015 V98-6% 02/05/20∆9-THC 0.0563 0.0032

J AOAC 2015 V98-6% 02/05/20THC-A < LOQ 0.0032

J AOAC 2015 V98-6% 02/11/20THC-Total 0.0563 0.0061

J AOAC 2015 V98-6% 02/05/20THCV† 0.00584 0.0032

J AOAC 2015 V98-6% 02/05/20THCV-A† < LOQ 0.0032

J AOAC 2015 V98-6% 02/11/20THCV-Total† < LOQ 0.0061

Batch: 2001170Potency per 28g

Units LOQ Analyze NotesMethodAnalyte Result Limits

J AOAC 2015 V98-602/11/2021.2CBC per 28g† mg/28g 0.933

J AOAC 2015 V98-602/11/201.37CBC-A per 28g† mg/28g 0.933

J AOAC 2015 V98-602/11/2022.4CBC-Total per 28g† mg/28g 1.75

J AOAC 2015 V98-602/11/20988CBD per 28g mg/28g 0.933

J AOAC 2015 V98-602/11/204.59CBD-A per 28g mg/28g 0.933

J AOAC 2015 V98-602/11/20992CBD-Total per 28g mg/28g 1.75

J AOAC 2015 V98-602/11/205.12CBDV per 28g† mg/28g 0.933

Page 2 of 8Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unlessotherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be retained for a maximum of 30 days from the receipt date unlessprior arrangements have been made.

Testing in accordance with: OAR 333-007-0430

Page 3: Cannabis Report with QC...THCV-Total†

12423 NE Whitaker WayPortland, OR 97230

503-254-1794

Report Number:

Report Date:

ORELAP#:

02/11/2020

OR100028

14:00Received: 02/04/20

Purchase Order:

20-001378/D03.R00

Batch: 2001170Potency per 28g

Units LOQ Analyze NotesMethodAnalyte Result Limits

J AOAC 2015 V98-602/11/20< LOQCBDV-A per 28g† mg/28g 0.933

J AOAC 2015 V98-602/11/205.12CBDV-Total per 28g† mg/28g 1.74

J AOAC 2015 V98-602/11/2015.4CBG per 28g† mg/28g 0.933

J AOAC 2015 V98-602/11/20< LOQCBG-A per 28g† mg/28g 0.933

J AOAC 2015 V98-602/11/2015.4CBG-Total per 28g† mg/28g 1.75

J AOAC 2015 V98-602/11/20< LOQCBL per 28g† mg/28g 0.933

J AOAC 2015 V98-602/11/20< LOQCBN per 28g mg/28g 0.933

J AOAC 2015 V98-602/11/20< LOQ∆8-THC per 28g† mg/28g 0.933

J AOAC 2015 V98-602/11/2015.8∆9-THC per 28g mg/28g 0.933

J AOAC 2015 V98-602/11/20< LOQTHC-A per 28g mg/28g 0.933

J AOAC 2015 V98-602/11/2015.8THC-Total per 28g mg/28g 1.75

J AOAC 2015 V98-602/11/201.64THCV per 28g† mg/28g 0.933

J AOAC 2015 V98-602/11/20< LOQTHCV-A per 28g† mg/28g 0.933

J AOAC 2015 V98-602/11/20< LOQTHCV-Total per 28g† mg/28g 1.74

Page 3 of 8Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unlessotherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be retained for a maximum of 30 days from the receipt date unlessprior arrangements have been made.

Testing in accordance with: OAR 333-007-0430

Page 4: Cannabis Report with QC...THCV-Total†

12423 NE Whitaker WayPortland, OR 97230

503-254-1794

Report Number:

Report Date:

ORELAP#:

02/11/2020

OR100028

14:00Received: 02/04/20

Purchase Order:

20-001378/D03.R00

These test results are representative of the individual sample selected and submitted by the client.

AbbreviationsLimits: Action Levels per OAR-333-007-0400, OAR-333-007-0210, OAR-333-007-0220Limit(s) of Quantitation (LOQ): The minimum levels, concentrations, or quantities of a target variable (e.g., target analyte) that can be

reported with a specified degree of confidence.

† = Analyte not NELAP accredited.

Units of Measure

g = Gram

mg/28g = Milligram per 28g

% = Percentage of sample

% wt = µg/g divided by 10,000

Derrick TannerGeneral Manager

Approved Signatory

Page 4 of 8Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unlessotherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be retained for a maximum of 30 days from the receipt date unlessprior arrangements have been made.

Testing in accordance with: OAR 333-007-0430

Page 5: Cannabis Report with QC...THCV-Total†

12423 NE Whitaker WayPortland, OR 97230

503-254-1794

Report Number:

Report Date:

ORELAP#:

02/11/2020

OR100028

14:00Received: 02/04/20

Purchase Order:

20-001378/D03.R00

Page 5 of 8Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unlessotherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be retained for a maximum of 30 days from the receipt date unlessprior arrangements have been made.

Testing in accordance with: OAR 333-007-0430

Page 6: Cannabis Report with QC...THCV-Total†

12423 NE Whitaker WayPortland, OR 97230

503-254-1794

Report Number:

Report Date:

ORELAP#:

02/11/2020

OR100028

14:00Received: 02/04/20

Purchase Order:

20-001378/D03.R00

Revision #: 0.00 Control : CFL-D06

Revision Date: 05/31/2019 Effective Date: 05/31/2019

J AOAC 2015 V98-6 Batch ID:

Laboratory Control Sample

Analyte Result Spike Units % Rec Evaluation Notes

CBDV-A 0.00948 0.01 94.8 85.0 - 115 Acceptable

CBDV 0.00976 0.01 97.6 85.0 - 115 Acceptable

CBD-A 0.0101 0.01 101 85.0 - 115 Acceptable

CBG-A 0.00990 0.01 99.0 85.0 - 115 Acceptable

CBG 0.00937 0.01 93.7 85.0 - 115 Acceptable

CBD 0.0100 0.01 100 85.0 - 115 Acceptable

THCV 0.00936 0.01 93.6 85.0 - 115 Acceptable

THCVA 0.00958 0.01 95.8 85.0 - 115 Acceptable

CBN 0.00998 0.01 99.8 85.0 - 115 Acceptable

THC 0.0102 0.01 102 85.0 - 115 Acceptable

D8THC 0.00918 0.01 91.8 85.0 - 115 Acceptable

CBL 0.00935 0.01 93.5 85.0 - 115 Acceptable

CBC 0.00955 0.01 95.5 85.0 - 115 Acceptable

THCA 0.0104 0.01 104 85.0 - 115 Acceptable

CBCA 0.00956 0.01 95.6 85.0 - 115 Acceptable

Method Blank

Analyte Result LOQ Units Evaluation Notes

CBDV-A <LOQ 0.003 < Acceptable

CBDV <LOQ 0.003 < Acceptable

CBD-A <LOQ 0.003 < Acceptable

CBG-A <LOQ 0.003 < Acceptable

CBG <LOQ 0.003 < Acceptable

CBD <LOQ 0.003 < Acceptable

THCV <LOQ 0.003 < Acceptable

THCVA <LOQ 0.003 < Acceptable

CBN <LOQ 0.003 < Acceptable

THC <LOQ 0.003 < Acceptable

D8THC <LOQ 0.003 < Acceptable

CBL <LOQ 0.003 < Acceptable

CBC <LOQ 0.003 < Acceptable

THCA <LOQ 0.003 < Acceptable

CBCA <LOQ 0.003 < Acceptable

Abbreviations

ND - None Detected at or above MRL

RPD - Relative Percent Difference

LOQ - Limit of Quantitation

Units of Measure:

% - Percent

%

%

%

0.003

% 0.003

% 0.003

0.003

Laboratory Quality Control Results

2001170

Limits

%

%

%

%

%

%

%

%

%

0.003

%

Limits

%

%

%

%

%

%

0.003%

%

%

%

% 0.003

0.003

0.003

% 0.003

% 0.003

0.003

0.003

0.003

%

%

0.003

Page 6 of 8Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unlessotherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be retained for a maximum of 30 days from the receipt date unlessprior arrangements have been made.

Testing in accordance with: OAR 333-007-0430

Page 7: Cannabis Report with QC...THCV-Total†

12423 NE Whitaker WayPortland, OR 97230

503-254-1794

Report Number:

Report Date:

ORELAP#:

02/11/2020

OR100028

14:00Received: 02/04/20

Purchase Order:

20-001378/D03.R00

Revision #: 0.00 Control : CFL-D06

Revision Date: 05/31/2019 Effective Date: 05/31/2019

Laboratory Quality Control Results

J AOAC 2015 V98-6 Batch ID:

Sample Duplicate Sample ID:

Analyte Result Org. Result LOQ Units RPD Evaluation Notes

CBDV-A <LOQ <LOQ 0.003 NA < Acceptable

CBDV 0.0159 0.0154 0.003 2.80 < Acceptable

CBD-A <LOQ <LOQ 0.003 NA < Acceptable

CBG-A <LOQ <LOQ 0.003 NA < Acceptable

CBG 0.0309 0.0323 0.003 4.50 < Acceptable

CBD 2.22 2.25 0.003 1.19 < Acceptable

THCV 0.00676 0.00651 0.003 3.69 < Acceptable

THCVA <LOQ <LOQ 0.003 NA < Acceptable

CBN <LOQ <LOQ 0.003 NA < Acceptable

THC 0.0714 0.0718 0.003 0.615 < Acceptable

D8THC <LOQ <LOQ 0.003 NA < Acceptable

CBL 0.00775 0.00753 0.003 2.79 < Acceptable

CBC 0.123 0.125 0.003 1.10 < Acceptable

THCA <LOQ <LOQ 0.003 NA < Acceptable

CBCA <LOQ <LOQ 0.003 NA < Acceptable

Abbreviations

ND - None Detected at or above MRL

RPD - Relative Percent Difference

LOQ - Limit of Quantitation

NA - Calculation Not Applicable given non-numerical results

Units of Measure:

% - Percent

% 20

Limits

% 20

% 20

% 20

% 20

20

% 20

%

% 20

2001170

% 20

% 20

% 20

% 20

%

20-001090-0001

% 20

% 20

20

Page 7 of 8Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unlessotherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be retained for a maximum of 30 days from the receipt date unlessprior arrangements have been made.

Testing in accordance with: OAR 333-007-0430

Page 8: Cannabis Report with QC...THCV-Total†

12423 NE Whitaker WayPortland, OR 97230

503-254-1794

Report Number:

Report Date:

ORELAP#:

02/11/2020

OR100028

14:00Received: 02/04/20

Purchase Order:

20-001378/D03.R00

Code Explanation

Q Matrix interferences affecting spike or surrogate recoveries.

Q1 Quality control result biased high. Only non-detect samples reported.

Q2 Quality control outside QC limits. Data considered estimate.

Q3 Sample concentration greater than four times the amount spiked.

Q4 Non-homogenous sample matrix, affecting RPD result and/or % recoveries.

Q5 Spike results above calibration curve.

Q6 Quality control outside QC limits. Data acceptable based on remaining QC.

R Relative percent difference (RPD) outside control limit.

R1 RPD non-calculable, as sample or duplicate results are less than five times the LOQ.

R2 Sample replicates RPD non-calculable, as only one replicate is within the analytical range.

LOQ1 Quantitation level raised due to low sample volume and/or dilution.

LOQ2 Quantitaion level raised due to matrix interference.

B Analyte detected in method blank, but not in associated samples.

B1 The sample concentration is greater than 5 times the blank concentration.

B2 The sample concentration is less than 5 times the blank concentration.

Explanation of QC Flag Comments:

Page 8 of 8Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unlessotherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be retained for a maximum of 30 days from the receipt date unlessprior arrangements have been made.

Testing in accordance with: OAR 333-007-0430