Gas Chromatograph - kinetics.com.t · Gas Chromatograph . Features. Detection to 1 ppb (application...

Post on 28-Jul-2020

20 views 0 download

Transcript of Gas Chromatograph - kinetics.com.t · Gas Chromatograph . Features. Detection to 1 ppb (application...

Gas Chromatograph

www.agc-instruments.com

Features Detectionto1ppb(applicationdependent)

LargeColour6.5”LCDTouchScreen

Compact19”RackDesign

FullyAutomatedUse

IntegratedConfigurableAlarmsSystem

ElectronicPressureControlofCarrierGas

Multi-ColumnOvenswithindividualTemperature Controlusingdifferentcolumnswitchingtechnologies suchasBackflush,HeartcutandPrecut.

IntegratedDiagnosticsSystem

DataHandlingControlbyTrendVisionPLUS SoftwareofboththeGCanditsancillary componentse.g.asasamplemultiplexer

IncreasedConnectivityviaRS-232,RS-485 andFieldBUScommunications

DropDownFrontPanelforeasyaccessto electronics

CustomisedChromatographySolutions

Suitedforspacesavinginstallationsassingle modulesorminisystems

Designedwithindustrialinterfacesforrack integrationasnewcabinetsorasreplacementunits

Designedforbothbatch-typeanalysisand continuousmonitoring.

IdealforProcessenvironmentswithStatusSignal, Alarmcontacts,remoteoperationrequirements

FollowingonfromthesuccessoftheAGCSeries100GCrange,AGCInstruments introducesthenewNovaCHROMGC.TheNovaCHROMGCisaculminationofyearsofexperienceinhighsensitivityGasChromatographyspecificfortheAnalysisof impuritiesinawiderangeofgasapplications.Itutilisesthelatestadvancedtechnologiestoprovideourcustomerswiththepreciseresultstheyrequirewiththeeaseofuseandsupportfeaturestheyexpect.

TheNovaCHROMusesindustrydrivenandprovenmethodsofanalysis forthequalitycontrolofgasesusingdifferentdetectortechnologiesadaptedtotherequiredapplications.Minimaltrainingisnecessaryasthelargecolourinteractivetouchscreenprovidesaneasy-to-useuserinterfaceforguidedfunctionality.Itoffersexcellentcontrolofthemanyfeatureswhichenabletheprecisemonitoringofapplications.ThisallowstheoperatortoperformchosenapplicationswitheaseandensuresthattheNovaCHROMGCprovidesatopclassservicetoyouatalltimes.

EachNovaCHROMGCisequippedwithspecificchromatographycomponentsdependingontheapplication. Inordertoguaranteeacontaminationfree,precisionorUHPqualitychromatographicseparation,“highpurity”rotaryvalvesinapurgedbox(forADDandDIDdetectors)areusedtopreventleakages.1/8”StainlessSteelcolumnsarefittedeitherwithSwagelok®orVCRcompressionfittingsandcombinedwith1/16“stainlesssteeltubingandplumbingaccessoriesthroughout(electropolishedifrequired).OthermaterialssuchasTeflonorHastelloymaybeused,asrequired,toeliminateinterferencefromthematrixgasortomitigatetheeffectsofcorrosiveelements.Moreover,thepackedcolumnswiththeirmultiplecolumnovensandindividualtemperaturecontrollersalsomaintainexceptionalstability,sensitivity,accuracyandrepeatability.

Withaquickstartuptime,fastdetectorresponseandsuperiorattributessuchastheElectronicPressureControl(EPC)Systemforthecarriergas,operationoftheNovaCHROMisswift,preciseandstraightforward.TheoptimisedconsumptionofcarrierandsupplygasesbytheNovaCHROMprovidesaneconomicalplatformwithalowcostofownershipandlonglifespan.Servicingandmaintenanceistrouble-freewithadrop-downfrontpanelforeasyaccesstotheelectroniccomponentsandtheuniquecolumninfrastructure,whichcanberegeneratedin-situ,providestheuserwithseamlessoperations.

TheIntegratedDiagnosticsandConfigurableAlarmsSystemspinpointanyareaswhichrequireattentiontoallowswiftidentificationandresolutionofanyprocessissues.Withthesefeatures,theNovaCHROMcanoperateunattendedforlongperiodsoftime.ThismakesthisGCPlatformveryversatileandrobusttomeettheexactingneedsoftheoperation.

Online Gas Analysis at %, ppm and ppb levels

1

2

Detectors Available

NovaCHROM 3000

Discharge Ionisation Detector (DID) NovaCHROM 1000TheAGCNovaCHROM1000GasChromatographequippedwiththeDischargeIonisationDetector(DID)haslong-termstabilityandoutstandinganalyticalperformance,providingdetectionlimitsdowntolowppbmeasurementsforawiderangeofgases.Basedonusinganonradioactive,universalandconcentrationdependentdesign,thisdetectorgenerateshighenergyphotonsthroughanelectricaldischargeinHighPurityHelium.ThemetastableHeliumthenionisesallcomponentsexceptHelium.TheGCdesignistotallyapplicationdependentcomprisingofauniquenumberofgassamplingandcolumnswitchingvalvestypicallylinkedtotwoormorecolumnovenmodules.Ifrequired,specialisedgasmatrixscrubbersarefittedintothechromatographypathe.g.HydrogenRemovalModuleorDe-OxTrap.

Linearity >106Sensitivity <1ppbofCH4(ApplicationDependent)Response time <0.5seconds

Gases Required:Detector Supply Gas UltraPureHeN6.0(astheCarrier/ Purge/DischargeGas) Actuator Gas CleanDryAir@3bar (forValveSwitchingandActuation)

Typical Applications: • ImpuritiesinPure/HighPurityGases≥N5 • CustomisedSolutionsforO2Analysis(N4-N6) • SingleGCsolutionsformultipleN5Matrices (e.g.He/H2/Ar/N2) • Corrosive&ElectronicGasApplications

Argon Discharge Detector (ADD) NovaCHROM 2000TheAGCNovaCHROM2000GasChromatographusesanArgonDischargeDetectorforthecontinuousanalysisofimpuritiesinanArgonMatrixGastoppblevels.Ahighenergyelectromagneticfield,throughwhichthecarriergaspasses,producesanionisingeffect.Thisprocesstransformsthegastoaplasmastateandaby-productofthisistheemissionofphotonsoflight.Asthesamplecomponentelutesfromthecolumn,thelightintensityisalteredandthislightemissioncanbemonitoredbyasensitive,tunedphoto-diode.Theoutputfromthephotodiodeisconvertedtoamillivoltsignalwhichcanbemeasuredonadatacapturesystem,suchastheAGCTrendVisionPLUSsoftware.ThetypicalGCdesigncomprisesofeitherasingleordual-columnchromatographyandtheNovaCHROM2000canspecificallydetectO2tracesinArgoninparallelwithotherimpuritieswithoutusinganadditionalO2meter.SinceArgonhasanunlimitedsupplyatreasonablecosts,theNovaCHROM2000isaneconomictraceanalyserforanumberofpopularindustrialapplications.Furthermore,precisequantitativeresultsaresupportedbythelinearisationfunctionprovidedbyTrendVisionPLUS.

Linearity >103

Sensitivity <1ppb(ApplicationDependent)Response time <0.5seconds(90%)

Gases Required:Detector Supply Gas UltraPureArN6.0 (astheCarrier&PurgeGases)Actuator Gas CleanDryAir@4bar (forValveSwitchingandActuation)

Typical Applications: • ImpuritiesinPure/HighPurityAr • CustomisedSolutionsforCO2Analysis (SoftDrinksapplication)

Flame Ionisation Detector (FID) TheAGCNovaCHROM3000,usingtheFlameIonisationDetector(FID),isusedtomeasureconcentrationsofhydrocarbonswithinasampledgas.Thepresenceofhydrocarbonsisdetectablebyburningthesampledgasinanair-hydrogenflame.Burningjustpurehydrogenwithairproducesonlysmallamountsofionisation.Thepresenceofhydrocarbonsinthesam-pledgas,whenburntwithanair-hydrogenmixcausesincreasedlevelsofionisation.Theionisationoccursasaresultofthecarbonatomspresentinthesampledgas.Thelevelofionisationisproportionaltothenumberofcarbonatomswithinthesample.ThetypicalGCdesigncomprisesofoneordual-column(packedorwide-bore)chromatographywithbackflushorheartcutswitchingtechnology.AGCInstrumentsalsoproducesitsownmethanisermoduletechnologywhichisfittedup-streamtothedetectorforCOandCO2detection.

3

Linearity >106Sensitivity <10ppbofCH4

Response time <0.5 seconds

Gases Required:Carrier Gas Applicationdependent:N2,He,H2orArDetector Supply Gas 1 H2N5.0orN6.0(Applicationdependent)Detector Supply Gas 2 SyntheticAirorPurifiedAir(“THCfree”) Actuator Gas CleanDryAir@3bar(forValveActuation)

Typical Applications: • C1-C6hydrocarbonsatppmorppblevels • CustomisedSolutionsforO2Analysis • Methane/TotalNon-Methaneanalysis • AnalysisoftracelevelCOandCO2usingamethaniser • PharmacopeiaApplications

Thermal Conductivity Detector (TCD) NovaCHROM 4000TheAGCNovaCHROM4000,usingtheThermalConductivityDetector(TCD),istypicallyusedtomeasurepermanentgasesorgasmixturecomponentsatpercentageandppmlevels.TheTCDhasfoursensingelementswhichareconnectedtoformanelectricalWheatstonebridgecircuit.Theseelementsaretypicallyminiaturerhenium-tungstenfilaments,whicharemountedinametalliccellblock.Aflowthroughtypethermalconductivitycellisnormallyusedinthisanalyser.Thiscellcontainsasampleandreferencegasflowgeometryandtwoelementsareinstalledineachflowsystem.Anelectricalcurrentfromaregulatedpowersourceheatstheelements.Changesinthermalconductivityofthesamplegasresultinanoutputvoltagechangewhichcanbemeasuredonadatacapturesystem,suchastheAGCTrendVisionPLUSChromatographySoftware.

Linearity >104

Sensitivity <5ppmResponse time <1second

Gases Required:Detector Supply Gas He,Ar,N2orH2 (astheCarrier&ReferenceGases: Purityisapplicationdependent) Actuator Gas CleanDryAir@3bar (forValveSwitchingandActuation)

Typical Applications: • PurityofGases • Preciseanalysisofthecomponentsin binaryormultiplegasmixtures:%,ppm • CustomisedSolutionsforCorrosiveGasAnalysis • PharmacopeiaApplications(Medical,Food,Diving,Laser,Excimer) • NaturalGasAnalysis

Flame Photometric Detector (FPD) NovaCHROM 5000TheAGCNovaCHROM5000GasChromatographusesadoubleFlamePhotometricDetector(FPD)whichisdesignedtogiveaselectiveresponsetosulphurorphosphorouscompounds.Whenanexcitationenergyisappliedtotheatomsofanelement,aphotometricemissionspectrumisobtainedwhosewavelengthischaracteristicoftheelement.Theintensityoftheemittedlight isproportionaltothenumberofatomsexcited.Withintheflamephotometricdetector,theexcitationenergyisderivedfromthedual-heatzonecombustionofthesampleinahydrogen-richflame.Thisdoubleflametechnologyeliminatesthewell-knowncross-interferencecausedbythematrixgas.Furthermore,precisequantitativeresultsaresupportedbythelinearisationfunctionprovidedbyTrendVisionPLUS.

Linearity 103(SulphurMode)Sensitivity 20pgS/secforThiophene(SulphurMode)

Gases Required:Carrier Gas N2N5.0orN6.0(Othersavailableuponrequest)Detector Supply Gas 1 H2N5.0orN6.0(Applicationdependent)Detector Supply Gas 2 SyntheticAirorPurifiedAir(“THCfree”) Actuator Gas CleanDryAir@3bar(forValveSwitchingandActuation)

Typical Applications: • Analysisofvolatilesulphurspeciesinpuregasesorambientair • NaturalGasAnalysis(H2S,COS,MercaptansandSulphides • CustomisedSolutionsforCO2Analysis(SoftDrinksapplication) • CustomisedApplicationsforSulphurinLightHydrocarbons

AGC HeadquartersUnit 2, Shannon Free Zone West, Shannon, Co. Clare, IrelandT: +353 61 471632 F: +353 61 471042 E: sales@agc-instruments.com

www.agc-instruments.com

Aftersales CareAGCInstrumentsarecommittedtoprovidingandmaintainingqualitysystemsfromcustomerliaisontotechnicalknowledgethroughtoSystemDesignandDelivery.WebelievethatourAfterSalesSupporttothecustomerisoneofthemostimportantserviceswecanoffer.EachDistributorhasbeencarefullyselectedandtrainedtoensureourcustomersreceivethebestpossibleservice.Furthermore,onlinecustomersupportanddirectsupportareavailabletodeliveracomprehensivesupportpackage.

For further information please contact:

Company ProfileAGC InstrumentsAGCInstrumentsisaleadingmanufacturerofGasAnalysisSolutions to all users requiring aQualityControl oridentificationoftheirgasstream.Wehaveover48yearsexperienceinprovidingourcustomerswiththeir“TotalGasAnalysisSolutions”.Weworkcloselywithallcustomerstoensuretheyobtaintheanalyticalsolutionthatmeetstheirneedsandasystemthatiseasytouseandunderstand.AllAGCdistributorsareextremelyexperiencedandfactorytrainedtothehigheststandards,offeringyouacompleteaftersalessupportservice.

ThewiderangeofDetectorsavailablecanbecustomisedtomeasureuniquegasstreamsandweplaceanemphasisonthecontinuousdevelopmentofouranalyticalsolutions.Ourworldwidereachwithstrategicpartnersensuresthatyouhavepeaceofmindandaftersalescarethatareimportanttoyouroperations.

Precision

ProvenTechnology

Flexible&VersatileSolutions

HighSensitivityAnalysis

GuaranteedApplications

4

TrendVision PLUS Software TrendVisionPLUSisthemostrecentreleaseofthewellrecognisedChromatographyDataCaptureSoftwarefromAGCInstruments.Specificallydesignedforthismarket, ithasbeendevelopedfollowingcarefulconsultationwithourcustomerssothatitiseasytouseandsetup.

Ruggedindustrial levelmodularandscalablehardwareisusedwithanEmbeddedWindowsOperatingSystem.Onceyoursystemis installed,usageinthedailyenvironmentisveryeasywithminimaltrainingrequired.Itencompassesallthe importantfunctionsrequiredinthisdemandinggasanalysisenvironment,enablingmanystandardfeaturestobe easily appliedwith the endproducts of excellentchromatographyresultsandstraightforwardreporting.Furthermore,theabilitytointegrateoutputsfromthirdpartygasanalysersisastrongfeatureandoffersalotofflexibilityforreporting.

TrendVisionPLUSprovidesaunifiedchromatographymethodwherebyallsettingsarecontainedinasinglemethod,includingeventtables,calibrationtablesandintegrationsettings.Inaddition,thissoftwareenablestheGCsystemstoruninafullyunattendedmode.ItcanalsotakecontroloftheGCsystemsandautomaticallyperformtherequiredanalysisusingthepre-programmedmethods.ThisiscoupledwiththeabilitytosendresultsbacktoaDCSorcontrolroomusingfieldbusprotocolsortraditional4-20mAsignalling.IfOn-LineoperationisnotrequiredthenthesoftwarerunsequallywellinitsStand-Alonemodewiththesamefunctionalityandeaseofuse.

PleaseconsultwithourspecificbrochureforthisSoftware.