Cryogenic Insulation Standard Data and … Extending some recent developments in the area of...

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ABSTRACT

Extendingsomerecentdevelopmentsintheareaoftechnicalconsensusstandardsforcryogenicthermalinsulationsystems,apreliminaryInter-LaboratoryStudyoffoaminsulationmaterialswasperformedbyNASAKennedySpaceCenterandLeTourneauUniversity.TheinitialfocuswasambientpressurecryogenicboilofftestingusingtheCryostat-400flat-plateinstrument.CompletionofatestfacilityatLETUhasenableddirect,comparativetesting,usingidenticalcryostatinstrumentsandmethods,andtheproductionofstandardthermaldatasetsforanumberofmaterialsundersub-ambientconditions.Thetwosetsofmeasurementswereanalyzedandindicatethereisreasonableagreementbetweenthetwolaboratories.Basedoncryogenicboiloffcalorimetry,newequipmentandmethodsfortestingthermalinsulationsystemshavebeensuccessfullydeveloped.Theseboiloffinstruments(orcryostats)includebothflatplateandcylindricalmodelsandareapplicabletoawiderangeofdifferentmaterialsunderawiderangeoftestconditions.Testmeasurementsaregenerallymadeatlargetemperaturedifference(boundarytemperaturesof293Kand78Karetypical)andincludethefullvacuumpressurerange.Resultsaregenerallyreportedineffectivethermalconductivity(ke)andmeanheatflux(q)throughtheinsulationsystem.Thenewcryostatinstrumentsprovideaneffectiveandreliablewaytocharacterizethethermalperformanceofmaterialsundersub-ambientconditions.Proveninthroughthousandsoftestsofhundredsofmaterialsystems,theyhavesupportedawiderangeofaerospace,industry,andresearchprojects.Boilofftestingtechnologyisnotjustforcryogenictestingbutisacost-effective,field-representativemethodologytotestanymaterialorsystemforapplicationsatsub-ambienttemperatures.Thistechnology,whenadequatelycoupledwithatechnicalstandardsbasis,canprovideacost-effective,field-representative

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AppliedResearch

Develop-ment

Demo&Test

TableofContents

AbstractTechnologyMaturityAnticipatedBenefitsRealizedBenefitsManagementTeamTechnologyAreasDetailedDescriptionU.S.LocationsWorkingonthisProjectDetailsforTechnology1

TechnologyMaturity

CompletedProject(2013-2014)

CryogenicInsulationStandardDataandMethodologiesProjectCenterIndependentResearch&Developments:KSCIRADProgram|MissionSupportDirectorate(MSD)

1 2 3 4 5 6 7 8 9

Formoreinformationvisittechport.nasa.govSomeNASAtechnologyprojectsaresmaller(forexampleSBIR/STTR,NIACandCenter

InnovationFund),andwillhavelesscontentthanother,largerprojects.Newlycreatedprojectsmaynotyethavedetailedprojectinformation. Printed7/27/2015

Page1

1122236

810

https://ntrs.nasa.gov/search.jsp?R=20150016085 2018-06-11T08:48:57+00:00Z

methodologytotestanymaterialorsystemforapplicationsatsub-ambienttocryogenictemperatures.Agrowingneedforenergyefficiencyandcryogenicapplicationsiscreatingaworldwidedemandforimprovedthermalinsulationsystemsforlowtemperatures.Theneedforthermalcharacterizationofthesesystemsandmaterialsraisesacorrespondingneedforinsulationteststandardsandthermaldatatargetedforcryogenic-vacuumapplications.Suchstandardshaveastrongcorrelationtoenergy,transportation,andenvironmentandtheadvancementofnewmaterialstechnologiesintheseareas.Inconjunctionwiththisproject,twonewstandardsoncryogenicinsulationwererecentlypublishedbyASTMInternational:C1774andC740.FollowingtherequirementsofNPR7120.10,TechnicalStandardsforNASAProgramsandProjects,theappropriateinformationinthisreportcanbeprovidedtotheNASAChiefEngineerasinputforNASA'sannualreporttoNIST,asrequiredbyOMBCircularNo.A-119,describingNASA'suseofvoluntaryconsensusstandardsandparticipationinthedevelopmentofvoluntaryconsensusstandardsandbodies.

ANTICIPATEDBENEFITS

ToNASAfundedmissions:

Tomakecryogensmorepracticaltostoreandtransfer,whetheronEarthorinspaceorotherdestinations,benchmarkthermalperformancedataareneeded.Toobtainsuchdata,standardapproaches,methodologies,andapparatusesarealsoneeded.Thisprojectaddressestheprobleminathreeprongedapproach:materialsscienceanddevelopment;testingmethodolgiesandequipment.Programsandprojectssupportedinclude,forexample:SLSvehicle,GameChangingTechnology-CryogenicCompositeTanks,AdvancedExplorationSystems-LiquidHydrogenandLiquidOxygenGroundOperationsDemonstrations,SBIR-materialsresearchprojects

2ConferencePapers2PeerReviewedPapers

2Publications

ManagementTeam

ProgramDirector:BurtonSummerfield

ProgramExecutive:KarenThompson

ProgramManager:NancyZeitlin

ProjectManager:PamelaMullenix

PrincipalInvestigator:JamesFesmire

Co-Investigator:AdamSwanger

CompletedProject(2013-2014)

CryogenicInsulationStandardDataandMethodologiesProjectCenterIndependentResearch&Developments:KSCIRADProgram|MissionSupportDirectorate(MSD)

Formoreinformationvisittechport.nasa.govSomeNASAtechnologyprojectsaresmaller(forexampleSBIR/STTR,NIACandCenter

InnovationFund),andwillhavelesscontentthanother,largerprojects.Newlycreatedprojectsmaynotyethavedetailedprojectinformation. Printed7/27/2015

Page2

(collaborationwithcompanies),CryogenicSpillProtectionforLNGCryofuelSystems,CIF-MultifunctionalStructuralThermalComposites,NIAC-LunarRegolithRegolith-DerivedHeatShield,etc.

ThisprojectisonepartofalargereffortthathasensuedsincethecompletionoftheNASAInternalResearchandDevelopment(IR&D)projectTechnologiestoIncreaseReliabilityofThermalInsulationSystemsfundedbytheSpaceOperationsMissionDirectorate(SOMD)in2004.

Thestandardreferencedatasetsproducedareavailableforcryogenicsystemsdesign,analysis,anddevelopment.Futuretechnicalconsensusstandardsareenvisionedforbothtestmethodsandmaterialspractices.Specifictestmethodswouldbeformulatedforcylindricalandflatplategeometriescoveringabsoluteandcomparativeapproaches,asrequiredbymutualindustryneeds.Standarddatasetsforspecificmaterialswouldthenbeproducedthrougharoundrobinofcryogenictestingamonglaboratories,thusenablingnewstandardmaterialpractices.

ToNASAunfunded&plannedmissions:

ExistinginformationcombinedwiththelatestresearchtestdatahasbeenorganizedtohelpsolvetheproblemspresentedbythethermalenvironmentsoftheEarth,launchascent,Moon,andMars.TheCryogenicsTestLaboratoryatNASAKennedySpaceCenterhasproducedmuchnewinformationoncryogenicandvacuumenvironmentsincludinghighvacuum(MoonorEarthorbit),softvacuum(Marsorlaunchascent),andnovacuum(Earthatmospherewithorwithouthumidity).Thematerialsincludemultilayerinsulation,aerogelblankets,aerogelbulk-fill,foams,composites,andmanyotherconstructions.

TechnologyAreas

Ground&LaunchSystemsProcessing(TA13)

LaunchPropulsionSystems(TA1)In-SpacePropulsionTechnologies(TA2)SpacePower&EnergyStorage(TA3)HumanHealth,LifeSupport&HabitationSystems(TA6)HumanExplorationDestinationSystems(TA7)Nanotechnology(TA10)Materials,Structures,MechanicalSystems&Manufacturing(TA12)ThermalManagementSystems(TA14)

CompletedProject(2013-2014)

CryogenicInsulationStandardDataandMethodologiesProjectCenterIndependentResearch&Developments:KSCIRADProgram|MissionSupportDirectorate(MSD)

Formoreinformationvisittechport.nasa.govSomeNASAtechnologyprojectsaresmaller(forexampleSBIR/STTR,NIACandCenter

InnovationFund),andwillhavelesscontentthanother,largerprojects.Newlycreatedprojectsmaynotyethavedetailedprojectinformation. Printed7/27/2015

Page3

Toothergovernmentagencies:

Energyuse,efficiency,conservation,andalternativesarecriticaltothefutureonEarthandinspace,only10%oftotalusagehastodowithelectricalenergywhile90%isthermalenergy!Tohavebasicinformationonlow-temperaturethermalinsulationisanenablingandcross-cuttingbenefitforNASAandindustrialneedsnationwideandonaglobalscale.Cryogenicinsulationrequirementsarespreadthroughoutpropulsion,airframe,architecture,andlaunchsystems.Historically,programshaveassumedotherswouldcoverthisworkorthattheworkwouldbecoveredbyanotherrelatedsystemarea.Theworkisdisciplineadvancingandthedevelopmentofstandardshasthepotentialtobenefitmanyprogramsandprojects.Theworkaddressesissuescommontopropulsion,lifesupport,power,andscience(refrigeration)systems,includingflight,in-space,andsurfacesystems.ProjectadvancesbothNASA-widerequirementsandNationaldirectivesbydevelopingstandarddataandtestingforcryogenicinsulationmaterials.StrategicpartnershipsensuremaximumbenefittoNASAobjectivesfortechnologyadvancement,engineeringinformation,andtechnicalcapabilities.

Tothecommercialspaceindustry:

Whatisthepoint?Newthermalmaterialsandthermalmanagementsystemsareneededforfuturespacelaunchvehiclesandthespaceexplorationenterprise.Thiscriticalareaofnewtechnologyisnowinacompetitivegloballaunchmarket.Thermalinsulationmustbeconsideredasanintegratedsystem,notmerelyanadd-onelement.Theendofinsulationasabolt-onelementistheunderlyingthemeofthisR&Dproject.Developmentofthermalinsulationsystemstechnologyshouldproceedfrombasicunderstandingofbothhightemperatureandlowtemperaturerequirements(hotside+coldside)aswellasstructuralandthermalrequirements.Toaddressthetotalenergyefficiencypictureofanycomplexspacehardwaresystemthedevelopmentmustalsoconsiderbothactivesystemssuchascryocoolersandpassivesystemssuchasfoammaterials.Multifunctionalthermalinsulationsystemsareakeytotechnologicaladvancementsthatcanbeachievedbyconsideringmaterials,testing,andengineeredapplications.

Tothenation:

Theneedforpracticalthermalconductivitydataforcryogenicapplicationscontinuestogrowinareassuchasoil&gas,electricalpower,refrigeratedtransport,aerospace,aircraft,groundtransportation,industrialprocesses,semi-conductormanufacturing,andmanyothers.Newmaterials,forexample,aerogelblankets,aerogelbulk-fill,glassbubbles,polyimidefoams,arenowcommerciallyavailableandarebeingappliedforlow-temperatureinsulationsolutionsandbroad

CompletedProject(2013-2014)

CryogenicInsulationStandardDataandMethodologiesProjectCenterIndependentResearch&Developments:KSCIRADProgram|MissionSupportDirectorate(MSD)

Formoreinformationvisittechport.nasa.govSomeNASAtechnologyprojectsaresmaller(forexampleSBIR/STTR,NIACandCenter

InnovationFund),andwillhavelesscontentthanother,largerprojects.Newlycreatedprojectsmaynotyethavedetailedprojectinformation. Printed7/27/2015

Page4

industrialapplication.Newmultilayerandcompositeinsulationmaterialshavealsobeendevelopedforhighlevelsofthermalperformancetomeetthegrowingdemandsforenergyefficiencyandenvironmentalresponsibilityintoday’seconomy.

Respondingtohighlevelobjectivesinbothenergyefficiencystandardsandtechnicalconsensusstandards,thisprojectadvancesbothNASA-widerequirementsandNationaldirectivesbydevelopingstandarddataandtestingforcryogenicinsulationmaterials.StrategicpartnershipsensuremaximumbenefittoNASAobjectivesfortechnologyadvancement,engineeringinformation,andtechnicalcapabilities.TherelevantAgencyandFederaldirectivesandinitiativesarelistedasfollows:

1.OMBCircularNo.A-119,FederalParticipationinDevelopment&UseofVoluntaryConsensusStandards&inConformityAssessmentActivities

2.MemorandumfortheHeadsofExecutiveDepartmentsandAgencies(2012)

3.TechnicalStandardsforNASAProgramsandProjects,NPR7120.10(2011)

4.TheU.S.MaterialsGenomeInitiative(2011)

Thisprojecthasenabledthedevelopmentandpublicationoftwonewinternationalstandardsonthesubjectofbelow-ambient(andcryogenic)thermalinsulationsystems,materials,andtesting.

Thermalinsulationplaysasignificantandsometimesenablingroleincryogenicsystems.TheemergingcryofuelsenterprisesincludingLNGandLH2areaparticularchallengeduetothetransienttypeoperationalprocessestobeaddressesandthecompetitiveeconomictargetstobemet.Thenewtechnicalconsensusstandardsarebutonesteptowardprovidingstandardthermalperformancedatatosupportthedesignpracticesforcryogenicsystems.Benchmarkthermalperformancedataprovidedbythenewpatentedtestinstruments,includingeffectivethermalconductivityandheatflux,canultimatelybeusedtocalibratecomparativetypeinstrumentsandsupportdetailedstudiesofinsulationsystemdesignsforspecificapplications.Atleast10futuretechnicalconsensusstandardsareplannedforbothtestmethodsandmaterialspracticestosupportthecryogenicindustryandfurthertheproliferationofnewindustrialopportunitiesintheareasoftransportationandenergy.

CompletedProject(2013-2014)

CryogenicInsulationStandardDataandMethodologiesProjectCenterIndependentResearch&Developments:KSCIRADProgram|MissionSupportDirectorate(MSD)

Formoreinformationvisittechport.nasa.govSomeNASAtechnologyprojectsaresmaller(forexampleSBIR/STTR,NIACandCenter

InnovationFund),andwillhavelesscontentthanother,largerprojects.Newlycreatedprojectsmaynotyethavedetailedprojectinformation. Printed7/27/2015

Page5

DETAILEDDESCRIPTION

Althoughsomestandardsexistforthermalinsulation,fewaddressthesub-ambienttemperaturerangeandcold-sidetemperaturesbelow100K.Standardsforcryogenicinsulationsystemsrequirecryostattestinganddataanalysisthatwillallowthedevelopmentofthetoolsneededbydesignengineersandthermalanalystsforthedesignofpracticalcryogenicsystems.Thus,thiscriticallyimportantinformationcanprovidereliabledataandmethodologiesforindustrialefficiencyandenergyconservation.

TheneedsfortechnicalstandardsforthermalinsulationsystemsaregrowingintheUSandworldwide.Energyefficiencyandconservationneeds--ofwhichthermalinsulationsystemsareakeypart--areatoppriorityforeconomic,nationalsecurity,andtechnologicalconcerns.Theemphasisontechnicalconsensusstandardsisacleardirectivefrombothgovernmentpolicyandmarketeconomicdrivers.

Summarizedherearethemostrecentandrelevantgovernmentpolicydirectivestoencouragetechnicalstandardsdevelopmentandenergyefficiencytechnologyimplementation.ThereferencefederalagencyisNASAandthetargetsubjectareaisthermalinsulationsystemsforlow-temperatureapplications.Hereisalistoftherelevantdocuments:

1. OMBCircularNo.A-119,FederalParticipationintheDevelopmentandUseofVoluntaryConsensusStandardsandinConformityAssessmentActivities.

2. MemorandumfortheHeadsofExecutiveDepartmentsandAgencies,documentM-12-08datedJanuary17,2012.

3. NPR7120.10,TechnicalStandardsforNASAProgramsandProjects,EffectiveDate:April22,2011.

OnFebruary4,2011,thePresidentreleasedAStrategyforAmericanInnovation:SecuringOurEconomicGrowthandProsperityanddirectedFederalagenciestoincreasetheireffortstocatalyzetechnologybreakthroughstoadvancenationalpriorities.PursuanttotheStrategyforAmericanInnovation,theOfficeofScienceandTechnologyPolicy(OSTP),theOfficeofManagementandBudget(OMB),andtheOfficeoftheUnitedStatesTradeRepresentative(USTR)aretheMemorandumfortheHeadsofExecutiveDepartmentsandAgencieswasissuedtoclarifyprinciplesguidingFederalGovernmentengagementinstandardsactivitiesthatcanhelpaddressnationalpriorities.

ThisR&Dprojectwasformulatedinresponsetotheseagencyandnationalobjectivesfortechnical

CompletedProject(2013-2014)

CryogenicInsulationStandardDataandMethodologiesProjectCenterIndependentResearch&Developments:KSCIRADProgram|MissionSupportDirectorate(MSD)

Formoreinformationvisittechport.nasa.govSomeNASAtechnologyprojectsaresmaller(forexampleSBIR/STTR,NIACandCenter

InnovationFund),andwillhavelesscontentthanother,largerprojects.Newlycreatedprojectsmaynotyethavedetailedprojectinformation. Printed7/27/2015

Page6

standards.ApreliminaryInter-LaboratoryStudyoffoaminsulationmaterialswasconductedbyNASAKennedySpaceCenter(KSC)andLeTourneauUniversity(LETU).Theinitialfocuswasambientpressure(novacuum)cryogenicboilofftestingusingtwoidenticalCryostat-400flat-plateinstruments.CompletionofanewtestfacilityatLETUhasenabledcomparativetesting,usingsimilarmethods,andtheproductionofstandardthermaldatasetsforcellularglassinsulationmaterialundercryogenicconditions.TestmeasurementsweremadeatbothKSCandLETUforcomparativeanalysis.Theresultsshowreasonableagreementbetweenthetwolaboratories.Theseinitialmeasurementsweremadeattheapproximateboundarytemperaturesof293Kand78K,theresultsofwhicharereportedincomparativeeffectivethermalconductivity(comparativeke)andmeanheatflux(q).

Themainchallengeistheproductionofstandardizedthermaldatasetsforcryogenicinsulationmaterialsandsystems.Thisprojecttookupthechallengeandmadeprogressinthreeways.Thefirstwastoproduceacatalogedsetofreferencetestspecimensofcellularglassmaterial.Othermaterialshavebeenidentifiedforfuturereferencetestspecimens.Secondwastoconductapreliminaryinterlaboratorystudyofthecellularglassmaterialusingthesameequipmentandmethods(Cryostat-400instrument).Thethirdwaywastoshowthepracticalityofusingboiloffcalorimetrytoobtainthermaldataforstack-upsofdifferentmaterials(compositepanelsandinsulationmaterialsalike).Theboiloffmethod,beingadirectmeasureofheatenergy,provideseffectivetestsolutionswhereotherexistingcommercialmethodsfallshortorarenotpossible.

Inconjunctionwiththisproject,twonewstandardsoncryogenicinsulationwererecentlypublishedbyASTMInternational:C1774andC740.FollowingtherequirementsofNPR7120.10,TechnicalStandardsforNASAProgramsandProjects,theappropriateinformationinthisreportcanbeprovidedtotheNASAChiefEngineerasinputforNASA'sannualreporttoNIST,asrequiredbyOMBCircularNo.A-119,describingNASA'suseofvoluntaryconsensusstandardsandparticipationinthedevelopmentofvoluntaryconsensusstandardsandbodies.Furtherstandardsintheareaofcryogenicinsulationsystemshavebeentargetedforfuturedevelopment.

ThisprojectinvolvedanumberoftasksthatweresynergeticwithotherprojectsunderAdvancedExplorationSystems,CenterInnovationFund,GameChangingTechnology,andothers.ComplianceissuesassociatedwithPVSsystemsrequirementswasamajorhitonresourcesin2013thusmakingthisleveragingamongprojectscrucialforthiswork.ThreeNewTechnologyReports,threepeer-reviewedpublications,andonefullpatentapplicationwerealsoproducedinconjunctionwiththisproject.Additonalpublicationsandpatentsarepending.

CompletedProject(2013-2014)

CryogenicInsulationStandardDataandMethodologiesProjectCenterIndependentResearch&Developments:KSCIRADProgram|MissionSupportDirectorate(MSD)

Formoreinformationvisittechport.nasa.govSomeNASAtechnologyprojectsaresmaller(forexampleSBIR/STTR,NIACandCenter

InnovationFund),andwillhavelesscontentthanother,largerprojects.Newlycreatedprojectsmaynotyethavedetailedprojectinformation. Printed7/27/2015

Page7

U.S.StatesWithWork LeadCenter:KennedySpaceCenter

U.S.LOCATIONSWORKINGONTHISPROJECT

SupportingCenters:

AmesResearchCenterGlennResearchCenterMarshallSpaceFlightCenter

OtherOrganizationsPerformingWork:

LetourneauUniversity(Longview,TX)

CompletedProject(2013-2014)

CryogenicInsulationStandardDataandMethodologiesProjectCenterIndependentResearch&Developments:KSCIRADProgram|MissionSupportDirectorate(MSD)

Formoreinformationvisittechport.nasa.govSomeNASAtechnologyprojectsaresmaller(forexampleSBIR/STTR,NIACandCenter

InnovationFund),andwillhavelesscontentthanother,largerprojects.Newlycreatedprojectsmaynotyethavedetailedprojectinformation. Printed7/27/2015

Page8

PROJECTLIBRARY

ConferencePapers

Cylindricalboiloffcalorimetersfortestingofthermalinsulations(https://techport.nasa.gov:443/file/16549)

Flatplateboiloffcalorimetersfortestingofthermalinsulationsystems(https://techport.nasa.gov:443/file/16550)

PeerReviewedPapers

Cryogenicinsulationstandarddataandmethodologies(https://techport.nasa.gov:443/file/16551)

StandardizationinCryogenicInsulationSystemsTestingandPerformanceData(https://techport.nasa.gov:443/file/16552)

Publications

ASTMC1774-StandardGuideforThermalPerformanceTestingofCryogenicInsulationSystems

(http://www.astm.org/Standards/C1774.htm)

ASTMC740-StandardGuideforEvacuatedReflectiveInsulationInCryogenicService(http://www.astm.org/Standards/C740.htm)

ContributingPartners:

NISTLetourneauUniversityUniversityofCentralFlorida(UCF)ASTMInternational

CompletedProject(2013-2014)

CryogenicInsulationStandardDataandMethodologiesProjectCenterIndependentResearch&Developments:KSCIRADProgram|MissionSupportDirectorate(MSD)

Formoreinformationvisittechport.nasa.govSomeNASAtechnologyprojectsaresmaller(forexampleSBIR/STTR,NIACandCenter

InnovationFund),andwillhavelesscontentthanother,largerprojects.Newlycreatedprojectsmaynotyethavedetailedprojectinformation. Printed7/27/2015

Page9

DETAILSFORTECHNOLOGY1

TechnologyTitle

Cryogenicthermalinsulationsystems

TechnologyDescription

Thistechnologyiscategorizedasahardwaresystemforgroundscientificresearchoranalysis

Thecloserelationshipbetweenindustrialenergyuseandcryogenicsdrivestheneedforoptimizedthermalinsulationsystems.Emergingcryofuelsusageisenabledbyadequateisolationoftheliquidhydrogenorliquefiednaturalgasfromtheambientenvironment.Thermalperformancedataforthetotalinsulationsystem,asrendered,areessentialforbothengineeringdesignsandcost-benefitdecisionsinvolvingcomparisonsamongalternatives.Thesedataareobtainedthroughrigoroustestingwithsuitableapparatusandrepeatablemethods.Properlydefinedterminology,analysis,andreportingarealsovital.AdvancesincryogenicinsulationtestapparatusandmethodshaveledtotherecentadditionoftwonewtechnicalstandardsofASTMInternational:C1774-StandardGuideforThermalPerformanceTestingofCryogenicInsulationSystemsandC740-StandardGuideforEvacuatedReflectiveCryogenicInsulation.Amongthedifferenttechniquesdescribedinthenewstandardsisthecylindricalboiloffcalorimeterforabsoluteheatmeasurementoverthefullrangeofvacuumpressureconditions.Thedetailsofthisapparatus,testmethod,anddataanalysisaregiven.Benchmarkthermalperformancedata,includingeffectivethermalconductivity(ke)andheatflux(q)fortheboundarytemperaturesof293Kand77K,aregivenforanumberofdifferentmultilayerinsulation(MLI)systemsincomparisonwithdataforothercommonly-usedinsulationsystemsincludingperlitepowder,fiberglass,polyurethanefoam,andaerogels.

CapabilitiesProvided

ThroughASTMInternational,CommitteeC16onThermalInsulation,twonewstandardswererecentlypublished:ASTMC1774-StandardGuideforThermalPerformanceTestingofCryogenicInsulationSystems(2013)andASTMC740-StandardGuideforEvacuatedReflectiveCryogenicInsulation(2014).Bothstandardsarecomprehensiveguidesthatprovidethenecessaryterminology,analyticalapproaches,andreportingrequirementsforthetechnologyareaofcryogenicinsulationsystems.Advancesintestapparatus,methods,andmaterialshaveprovidedafoundationforthesenewstandards.

CompletedProject(2013-2014)

CryogenicInsulationStandardDataandMethodologiesProjectCenterIndependentResearch&Developments:KSCIRADProgram|MissionSupportDirectorate(MSD)

Formoreinformationvisittechport.nasa.govSomeNASAtechnologyprojectsaresmaller(forexampleSBIR/STTR,NIACandCenter

InnovationFund),andwillhavelesscontentthanother,largerprojects.Newlycreatedprojectsmaynotyethavedetailedprojectinformation. Printed7/27/2015

Page10

TheC1774Guidecoversdifferentapproachestobothboiloffcalorimetryandelectricalpowermethodsofforthermalperformancemeasurementinsub-ambienttemperatureenvironments.Thetestapparatuses(apparatus)designedforthesepurposesaredividedintotwocategories:boiloffcalorimetryandelectricalpower.Bothabsoluteandcomparativeapparatusesmethodsareincluded.Thesetestingapproachesmethodsareapplicabletothemeasurementofawidevarietyofspecimens,rangingfromopaquesolidstoporousortransparentmaterials,andawiderangeofenvironmentalconditionsincludingmeasurementsconductedatextremesoftemperatureandwithvariousgasesandoverarangeofpressures.Ofparticularimportanceistheabilitytotesthighlyanisotropicmaterialsandsystemssuchasmultilayerinsulation(MLI)systems.Theguideprovidesinformationforthelaboratorymeasurementofthesteady-statethermaltransmissionpropertiesandheatfluxofthermalinsulationsystemsundercryogenicconditions.Thermalinsulationsystemsmaybecomposedofoneormorematerialsthatmaybehomogeneousornon-homogeneous;flat,cylindrical,orspherical;atboundaryconditionsfrom4to400K;andinenvironmentsfromhighvacuumtoanambientpressureofairorresidualgas.Akeyaspectofthisguideisthenotionofaninsulationsystem,notaninsulationmaterial.Underthepracticaluseenvironmentofmostcryogenicapplicationsevenasingle-materialsystemcanstillbeacomplexinsulationsystem.

TheC740guidecoversthebaselineheatfluxorthermalconductivitydata,performanceconsiderations,typicalapplications,manufacturingmethods,materialspecification,andsafetyconsiderationsintheuseofMLIsystemsincryogenicservice.Thetechnologyofevacuatedreflectiveinsulation,orMLI,firstcameaboutinthe1950sand1960sprimarilydrivenbytheneedtoliquefy,store,andtransportlargequantitiesofliquidhydrogenandliquidhelium.MLIsystemsofteninvolvewarmboundarytemperaturesintherangeof300Korhigherandcoldboundarytemperaturesrangingfrom4Kto111K,butanytemperaturebelowambientisapplicable.Insulationsystemsofthisconstructionareusedwhenheatfluxvalueswellbelow10W/m2areneededforanevacuateddesign.Heatfluxvaluesapproaching0.1W/m2arealsoachievable.Forcomparisonamongdifferentsystems,aswellasforspaceandweightconsiderations,theeffectivethermalconductivityofthesystemcanbecalculatedforaspecifictotalthickness.Effectivethermalconductivitiesoflessthan1mW/m-K[R-value143]aretypicalandvaluesontheorderof0.01mW/m-Khavebeenachieved[R-value14,300].Thermalperformancecanalsobedescribedintermsoftheeffectiveemittanceofthesystem,orΕe.Thesesystemsaretypicallyusedinahighvacuumenvironment(evacuated),butsoftvacuumornovacuumenvironmentsarealsoapplicable.Aweldedmetal,vacuum-jacketed(VJ)enclosureisoftenusedtoprovidethevacuumenvironment.MLIsystemsaregenerallyusedwhenlowerheatleakageratesthanthoseobtainedwithotherevacuatedinsulationsarerequired.Otherevacuatedinsulationsinclude,forexample,

CompletedProject(2013-2014)

CryogenicInsulationStandardDataandMethodologiesProjectCenterIndependentResearch&Developments:KSCIRADProgram|MissionSupportDirectorate(MSD)

Formoreinformationvisittechport.nasa.govSomeNASAtechnologyprojectsaresmaller(forexampleSBIR/STTR,NIACandCenter

InnovationFund),andwillhavelesscontentthanother,largerprojects.Newlycreatedprojectsmaynotyethavedetailedprojectinformation. Printed7/27/2015

Page11

perlitepowder,glassbubbles,oraerogelbulk-fill,whichcanprovideheatfluxvaluesintherangeof5to20W/m2.ThechoiceforanMLIsystemmaybedictatedbythevalueofthecryogenicfluidbeingisolatedorbyweightorthicknesslimitationsimposedbytheparticularapplication.Applicationsgenerallyfallintothefollowingcategories:storage,transfer,thermalprotection,andlow-temperatureprocesses.Verylowtemperature(4Kandbelow)refrigerationforlarge-scalesuperconductingmagnets,RFcavities,andotherdevicesisamajortechnicalcapabilityforbasicphysicsresearchworld-wide.

PotentialApplications

Potentialapplicationsinlcudebroadusageintheareasoftransportation,energy,coldchainshippingoffoodsandpharmaceuticals,buildingconstruction,thermalmanagementsystems,andgeneralmaterialsscienceresearch.Futuretechnicalconsensusstandardsareenvisionedforbothtestmethodsandmaterialspractices.Specifictestmethodswouldbeformulatedforcylindricalandflatplategeometriescoveringabsoluteandcomparativeapproaches,asrequiredbymutualindustryneeds.Standarddatasetsforspecificmaterialswouldthenbeproducedthrougharoundrobinofcryogenictestingamonglaboratories,thusenablingnewstandardmaterialpractices.Energyefficiency,systemcontrol,andoperationalsafetyareinter-relatedaspectsofdecidingthebestthermalinsulationsystemforaparticularapplication.TheemergingcryofuelsenterprisesincludingLNGandLH2areaparticularchallengeduetothetransienttypeoperationalprocessestobeaddressesandthecompetitiveeconomictargetstobemet.

PerformanceMetrics

Metric Unit Quantity

HeatFlux W/m2 1

ThermalConductivity mW/m-K 0.1

CompletedProject(2013-2014)

CryogenicInsulationStandardDataandMethodologiesProjectCenterIndependentResearch&Developments:KSCIRADProgram|MissionSupportDirectorate(MSD)

Formoreinformationvisittechport.nasa.govSomeNASAtechnologyprojectsaresmaller(forexampleSBIR/STTR,NIACandCenter

InnovationFund),andwillhavelesscontentthanother,largerprojects.Newlycreatedprojectsmaynotyethavedetailedprojectinformation. Printed7/27/2015

Page12